CN117530380A - Composite beverage with intestinal tract regulating effect and preparation method thereof - Google Patents
Composite beverage with intestinal tract regulating effect and preparation method thereof Download PDFInfo
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- CN117530380A CN117530380A CN202311708792.3A CN202311708792A CN117530380A CN 117530380 A CN117530380 A CN 117530380A CN 202311708792 A CN202311708792 A CN 202311708792A CN 117530380 A CN117530380 A CN 117530380A
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- dietary fiber
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- dendrobium candidum
- gynura bicolor
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- 230000001105 regulatory effect Effects 0.000 title claims abstract description 32
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- 238000002360 preparation method Methods 0.000 title claims abstract description 21
- 239000002131 composite material Substances 0.000 title claims abstract description 12
- 235000013325 dietary fiber Nutrition 0.000 claims abstract description 85
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 57
- 241000026010 Dendrobium candidum Species 0.000 claims abstract description 50
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 43
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- 150000001875 compounds Chemical class 0.000 claims abstract description 21
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Classifications
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/02—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
- A23L2/60—Sweeteners
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
- A23L2/68—Acidifying substances
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/20—Reducing nutritive value; Dietetic products with reduced nutritive value
- A23L33/21—Addition of substantially indigestible substances, e.g. dietary fibres
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
- A23L5/30—Physical treatment, e.g. electrical or magnetic means, wave energy or irradiation
- A23L5/32—Physical treatment, e.g. electrical or magnetic means, wave energy or irradiation using phonon wave energy, e.g. sound or ultrasonic waves
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Mycology (AREA)
- Botany (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention discloses a compound beverage with an intestinal tract regulating effect and a preparation method thereof, and belongs to the technical field of beverage and food. The compound beverage comprises the following preparation raw materials in parts by weight: 1 to 5 parts of dendrobium candidum dietary fiber extract, 0.5 to 3 parts of gynura bicolor, 0.05 to 0.1 part of lactitol, 0.1 to 0.5 part of sodium carboxymethyl cellulose, 0.05 to 0.2 part of citric acid and 80 to 120 parts of water. The composite beverage provided by the invention takes the dendrobium candidum dietary fiber extract and the gynura bicolor as main effective components, and takes lactitol, sodium carboxymethyl cellulose and citric acid as auxiliary components, so that the components are simple, and the raw materials are easy to obtain; the rich carbohydrate substances contained in the dendrobium candidum and the rich saponin substances contained in the gynura bicolor can generate hydrogen bond action, and weak bonding action is generated among substances, so that the stability of the drink is improved. Dendrobium officinale provides dietary fibers, gynura bicolor is beneficial to expelling toxin from the digestive system, improving the immunity of the organism, and the interaction of the two realizes the maximization of gastrointestinal function regulation.
Description
Technical Field
The invention belongs to the technical field of beverage and food, and particularly relates to a compound beverage with an intestinal tract regulating effect and a preparation method thereof.
Background
In recent years, the living standard is improved, the living rhythm is accelerated, the living style of people is changed slightly, bad living habits such as binge eating, staying up, alcoholism and the like appear, the physical health of people is seriously affected, and especially the damage to the gastrointestinal function is more obvious, and diseases such as gastrointestinal discomfort, constipation and the like are caused.
Dietary fiber is generally a polysaccharide food ingredient which is not easily digested by digestive enzymes, mainly comes from the cell wall of plants, contains cellulose, hemicellulose, resin, pectin, lignin and the like, cannot be decomposed and absorbed in the small intestine, and mostly reaches the large intestine (cecum and colon) directly, and is fermented and utilized as a carbon source of intestinal flora. The dietary fiber is mainly divided into soluble dietary fiber and insoluble dietary fiber, and has important significance in keeping the health of digestive system, preventing coronary heart disease, apoplexy, hypertension, diabetes and the like. Regarding the intake of soluble dietary fibers and insoluble dietary fibers, there are experts recommending that 1:2 is the optimal intake ratio.
The gynura bicolor is a functional vegetable for both medicine and food, is rich in anthocyanin, polyphenol and flavonoid substances, has extremely strong antioxidation capability, can effectively remove free radicals in human bodies, and has extremely high nutritive value. Dendrobium officinale is a dendrobium herb widely distributed in Hubei, guizhou, guangxi, yunnan and other places in China; modern pharmacological researches have shown that Dendrobium officinale has the effects of resisting coagulation, resisting tumor, reducing hypertension, hyperglycemia and hyperlipidemia, resisting aging, improving immunity and the like.
With the rapid rise of functional beverages, beverages with different effects including gastrointestinal function conditioning have been developed and marketed accordingly, for example, patent document CN111955547B provides a preparation of vine tea probiotic fermented milk for conditioning the intestinal tract, but no related effect demonstration has been made; patent document CN103503990B provides a brown lactobacillus beverage, which has accurate process parameter adjustment and control and high production requirement; patent document CN104277961B provides a yacon vinegar beverage, which improves gastrointestinal functions, has a plurality of added components and complex ingredients. Regarding gynura bicolor and dendrobium candidum, there are also reports in functional beverages, such as patent document CN109259023A, CN103494283A, CN103719419a, which provides a beverage containing gynura bicolor, but not for gastrointestinal conditioning; patent document CN112972631B provides a traditional Chinese medicine composition with functions of improving stomach health and regulating intestinal flora, and uses dendrobium candidum, but the composition contains more components, and the extraction and utilization of the dendrobium candidum are only general extraction and do not distinguish dietary components; patent document CN103445190B provides a method for extracting dietary fiber from dendrobium candidum, which does not mention the utilization of the extracted dietary fiber of dendrobium candidum, and the extraction efficiency is still to be further improved.
In general, in the prior art, no report on the accurate dosage of insoluble dietary fiber and soluble dietary fiber in dietary fiber is really focused on the beverage with intestinal tract regulation, and the cooperative utilization of dendrobium candidum and gynura bicolor still needs to be further developed.
In view of this, the present invention has been proposed.
Disclosure of Invention
Aiming at the defects of the prior art, the invention aims to provide a compound beverage with intestinal tract regulating effect and a preparation method thereof, and the compound beverage has simple components and a certain gastrointestinal tract regulating function.
In order to achieve the above purpose, the present invention adopts the following technical scheme:
in a first aspect, the invention provides a compound beverage with intestinal tract regulating effect, which comprises the following preparation raw materials in parts by weight: 1 to 5 parts of dendrobium candidum dietary fiber extract, 0.5 to 3 parts of gynura bicolor, 0.05 to 0.1 part of lactitol, 0.1 to 0.5 part of sodium carboxymethyl cellulose, 0.05 to 0.2 part of citric acid and 80 to 120 parts of water.
As a preferable technical scheme of the invention, the compound beverage comprises the following preparation raw materials in parts by weight: 1.5 to 4 parts of dendrobium candidum dietary fiber extract, 0.8 to 2 parts of gynura bicolor, 0.06 to 0.09 part of lactitol, 0.15 to 0.4 part of sodium carboxymethyl cellulose, 0.08 to 0.15 part of citric acid and 90 to 110 parts of water.
As a preferable technical scheme of the invention, the compound beverage comprises the following preparation raw materials in parts by weight: 2.5 parts of dendrobium candidum dietary fiber extract, 1.2 parts of gynura bicolor, 0.08 part of lactitol, 0.2 part of sodium carboxymethyl cellulose, 0.1 part of citric acid and 100 parts of water.
As a preferable technical scheme of the invention, the preparation of the dendrobium candidum dietary fiber extract comprises the following steps:
s1, degreasing treatment: drying and crushing dendrobium candidum stem and leaf raw materials, and degreasing with petroleum ether;
s2, performing steam explosion on the degreased material in the step S1, and then rapidly releasing pressure to obtain a material a;
s3, adding the material a obtained in the step S2 into an aqueous solution containing Tween 80, treating for 5-20 min under the ultrasonic power of 100-200W, regulating the pH value to 10.5-11.5 under the stirring state, adding absolute ethyl alcohol until the mass concentration of the ethyl alcohol is 75-85%, standing, and filtering to obtain a precipitate;
s4, adding the precipitate obtained in the step S3 into deionized water, regulating the pH value to 1.8-2.2 in a stirring state, and stirring for 0.5-2 h at 70-90 ℃; filtering after stirring to obtain filtrate and filter residue;
s5, concentrating and evaporating the filtrate obtained in the step S4, and then, according to the mass ratio of 1:1, adding the concentrated and evaporated material into absolute ethyl alcohol, standing and then carrying out vacuum drying treatment to obtain water-soluble dietary fiber;
s6, adding the filter residue obtained in the step S4 into deionized water again, regulating the pH value to 1.8-2.2 in a stirring state, and standing for 0.5-2 h at 65-80 ℃; filtering and drying after standing to obtain insoluble dietary fiber;
and S7, mixing the water-soluble dietary fiber obtained in the step S5 with the insoluble dietary fiber obtained in the step S6 to obtain the dendrobium candidum dietary fiber extract.
As a preferred technical solution of the present invention, in step S2, the steam explosion conditions are as follows: the explosion pressure is 1.1MPa, the maintenance time is 45-90 s, and the water vapor explosion is carried out.
In step S3, the ratio of the amount of the material a to the amount of the aqueous solution is 1g: 10-15 mL, and the concentration of Tween 80 is 0.1-0.2 wt%.
In step S6, as a preferred technical scheme of the present invention, the mass ratio of the filter residue to deionized water is 1: 8-12.
In step S7, as a preferred technical scheme of the present invention, the mass ratio of the water-soluble dietary fiber to the insoluble dietary fiber is 1:2.
in a second aspect, the present invention provides a method for preparing the above-mentioned composite beverage, comprising the steps of:
a1, preprocessing the gynura bicolor: cleaning the gynura bicolor, scalding and cooling to obtain a material b; cutting the material b, adding the cut material b into water, and pulping; finally, filtering to obtain the gynura bicolor juice;
a2, adding the gynura bicolor juice obtained in the step A1, the dendrobium candidum dietary fiber extract, lactitol, sodium carboxymethyl cellulose and citric acid into water, homogenizing, sterilizing and packaging.
In the step A1, the mass ratio of the material b to water is 1: 15-20.
Compared with the prior art, the invention has the following beneficial effects:
the composite beverage provided by the invention takes dendrobium candidum dietary fiber extract and gynura bicolor as main effective components, and takes lactitol, sodium carboxymethyl cellulose and citric acid as auxiliary components, so that the components are simple, and the raw materials are easy to obtain.
According to the composite beverage provided by the invention, the rich carbohydrate substances contained in the dendrobium candidum and the rich saponin substances contained in the gynura bicolor can generate a hydrogen bond effect, and weak bonding effect is generated among substances, so that the stability of the beverage is improved. Dendrobium officinale provides dietary fibers, gynura bicolor is beneficial to expelling toxin from the digestive system, improving the immunity of the organism, and the interaction of the two realizes the maximization of gastrointestinal function regulation.
The composite beverage provided by the invention fully extracts dendrobium candidum around the accurate control of the use proportion of the soluble dietary fiber and the insoluble dietary fiber, and specifically: after degreasing treatment is carried out on the dendrobium candidum, steam explosion treatment is adopted to fully leach out the functional components, and then the surfactant Tween 80 is utilized to easily extract and precipitate out the efficacy Cheng Fenshui after the steam explosion, so that the treatment time is greatly shortened by using ultrasonic treatment; it is particularly emphasized that the use of the water extraction and alcohol precipitation surfactant in combination with the use of the water extraction and alcohol precipitation surfactant of the present invention can greatly improve the extraction efficiency compared with the conventional alcohol precipitation in the prior art. The method for extracting the dendrobium candidum dietary fiber provided by the invention does not involve enzymolysis treatment, so that the residues of enzyme substances can be greatly avoided, the chemical components used in the extraction process are clear and simple, and the safety of controlled foods is utilized. In the experiments, the applicant found that the treatment with an aqueous solution of tween 80 after steam explosion gave a good extraction effect with a very small amount of tween 80.
The preparation method of the compound beverage provided by the invention is simple and is convenient for large-scale production.
Detailed Description
The following description of the embodiments of the present invention will clearly and fully describe the technical aspects of the embodiments of the present invention, and it is apparent that the described embodiments are only some embodiments of the present invention, not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the present invention without making any inventive effort, are intended to fall within the scope of the present invention.
In the invention, dendrobium candidum is purchased from the biological technology development limited company of rainy days in county of holly, and a steam explosion machine can be a common machine in the market, such as QBS-80.
Example 1
A preparation method of dendrobium candidum dietary fiber extract comprises the following steps:
s1, degreasing treatment: drying and crushing dendrobium candidum stem and leaf raw materials, and degreasing with petroleum ether;
s2, performing steam explosion (steam explosion, explosion pressure is 1.1MPa, and maintenance time is 60S) on the degreased material in the step S1, and then rapidly releasing pressure to obtain a material a;
s3, according to the dosage ratio of 1g:12mL, adding the material a obtained in the step S2 into an aqueous solution containing Tween 80 (the mass concentration of Tween 80 is 0.1%), treating for 10min under the ultrasonic power of 100W, adjusting the pH value to 10.5 under the stirring state, adding absolute ethyl alcohol until the mass concentration of the ethyl alcohol is 75%, standing, and filtering to obtain a precipitate;
s4, adding the precipitate obtained in the step S3 into deionized water, regulating the pH value to 2 in a stirring state, and stirring for 1h at 70 ℃; filtering after stirring to obtain filtrate and filter residue;
s5, concentrating and evaporating the filtrate obtained in the step S4, and then, according to the mass ratio of 1:1, adding the concentrated and evaporated material into absolute ethyl alcohol, standing and then carrying out vacuum drying treatment to obtain water-soluble dietary fiber;
s6, according to the mass ratio of 1:9, adding the filter residue obtained in the step S4 into deionized water again, regulating the pH value to 1.8 in a stirring state, and standing for 0.5h at 65 ℃; filtering and drying after standing to obtain insoluble dietary fiber;
s7, according to the mass ratio of 1:2, mixing the water-soluble dietary fiber obtained in the step S5 with the insoluble dietary fiber obtained in the step S6 to obtain the dendrobium candidum dietary fiber extract.
Example 2
A preparation method of dendrobium candidum dietary fiber extract comprises the following steps:
s1, degreasing treatment: drying and crushing dendrobium candidum stem and leaf raw materials, and degreasing with petroleum ether;
s2, performing steam explosion (steam explosion, explosion pressure is 1.1MPa, and maintenance time is 60S) on the degreased material in the step S1, and then rapidly releasing pressure to obtain a material a;
s3, according to the dosage ratio of 1g:11mL, adding the material a obtained in the step S2 into an aqueous solution containing Tween 80 (the mass concentration of Tween 80 is 0.15%), treating for 8min under the ultrasonic power of 100W, adjusting the pH value to 11 under the stirring state, adding absolute ethyl alcohol until the mass concentration of the ethyl alcohol is 80%, standing, and filtering to obtain a precipitate;
s4, adding the precipitate obtained in the step S3 into deionized water, regulating the pH value to 2 in a stirring state, and stirring for 0.5h at 70 ℃; filtering after stirring to obtain filtrate and filter residue;
s5, concentrating and evaporating the filtrate obtained in the step S4, and then, according to the mass ratio of 1:1, adding the concentrated and evaporated material into absolute ethyl alcohol, standing and then carrying out vacuum drying treatment to obtain water-soluble dietary fiber;
s6, according to the mass ratio of 1:10, adding the filter residue obtained in the step S4 into deionized water again, regulating the pH value to 1.8 in a stirring state, and standing for 1h at 65 ℃; filtering and drying after standing to obtain insoluble dietary fiber;
s7, according to the mass ratio of 1:2, mixing the water-soluble dietary fiber obtained in the step S5 with the insoluble dietary fiber obtained in the step S6 to obtain the dendrobium candidum dietary fiber extract.
Example 3
A compound beverage with intestinal tract regulating effect is prepared from the following raw materials in mass: dendrobium officinale dietary fiber extract 2.5g, gynura bicolor 1.2g, lactitol 0.08g, sodium carboxymethyl cellulose 0.2g, citric acid 0.1g and water 100g.
Wherein, dendrobium candidum dietary fiber extract is prepared by the method in the example 1.
In this embodiment, a method for preparing the above compound beverage is also provided, including the following steps:
a1, preprocessing the gynura bicolor: cleaning the gynura bicolor, scalding and cooling to obtain a material b; cutting the material b, and adding the cut material b into water for pulping (the mass ratio of the material b to the water is 1:15); finally, filtering to obtain the gynura bicolor juice;
a2, adding the gynura bicolor juice obtained in the step A1, the dendrobium candidum dietary fiber extract, lactitol, sodium carboxymethyl cellulose and citric acid into water, homogenizing, sterilizing and packaging.
Example 4
A compound beverage with intestinal tract regulating effect is prepared from the following raw materials in mass: dendrobium officinale dietary fiber extract 2.5g, gynura bicolor 1.2g, lactitol 0.08g, sodium carboxymethyl cellulose 0.2g, citric acid 0.1g and water 100g.
Wherein, dendrobium candidum dietary fiber extract is prepared by the method in the example 2.
In this embodiment, a method for preparing the above compound beverage is also provided, including the following steps:
a1, preprocessing the gynura bicolor: cleaning the gynura bicolor, scalding and cooling to obtain a material b; cutting the material b, and adding the cut material b into water for pulping (the mass ratio of the material b to the water is 1:15); finally, filtering to obtain the gynura bicolor juice;
a2, adding the gynura bicolor juice obtained in the step A1, the dendrobium candidum dietary fiber extract, lactitol, sodium carboxymethyl cellulose and citric acid into water, homogenizing, sterilizing and packaging.
Example 5
A compound beverage with intestinal tract regulating effect is prepared from the following raw materials in mass: dendrobium officinale dietary fiber extract 2.8g, gynura bicolor 1g, lactitol 0.06g, sodium carboxymethyl cellulose 0.18g, citric acid 0.08g and water 100g.
Wherein, dendrobium candidum dietary fiber extract is prepared by the method in the example 1.
In this embodiment, a method for preparing the above compound beverage is also provided, including the following steps:
a1, preprocessing the gynura bicolor: cleaning the gynura bicolor, scalding and cooling to obtain a material b; cutting the material b, and adding the cut material b into water for pulping (the mass ratio of the material b to the water is 1:15); finally, filtering to obtain the gynura bicolor juice;
a2, adding the gynura bicolor juice obtained in the step A1, the dendrobium candidum dietary fiber extract, lactitol, sodium carboxymethyl cellulose and citric acid into water, homogenizing, sterilizing and packaging.
Comparative example 1
A preparation method of dendrobium candidum dietary fiber extract comprises the following steps:
s1, degreasing treatment: drying and crushing dendrobium candidum stem and leaf raw materials, and degreasing with petroleum ether;
s2, performing steam explosion (steam explosion, explosion pressure is 1.1MPa, and maintenance time is 60S) on the degreased material in the step S1, and then rapidly releasing pressure to obtain a material a;
s3, according to the dosage ratio of 1g:12mL, adding the material a obtained in the step S2 into the aqueous solution, treating for 10min under the ultrasonic power of 100W, regulating the pH value to 10.5 under the stirring state, adding absolute ethyl alcohol until the mass concentration of the ethyl alcohol is 75%, standing, and filtering to obtain a precipitate;
s4, adding the precipitate obtained in the step S3 into deionized water, regulating the pH value to 2 in a stirring state, and stirring for 1h at 70 ℃; filtering after stirring to obtain filtrate and filter residue;
s5, concentrating and evaporating the filtrate obtained in the step S4, and then, according to the mass ratio of 1:1, adding the concentrated and evaporated material into absolute ethyl alcohol, standing and then carrying out vacuum drying treatment to obtain water-soluble dietary fiber;
s6, according to the mass ratio of 1:9, adding the filter residue obtained in the step S4 into deionized water again, regulating the pH value to 1.8 in a stirring state, and standing for 0.5h at 65 ℃; filtering and drying after standing to obtain insoluble dietary fiber;
s7, according to the mass ratio of 1:2, mixing the water-soluble dietary fiber obtained in the step S5 with the insoluble dietary fiber obtained in the step S6 to obtain the dendrobium candidum dietary fiber extract.
Namely, compared with the comparative example 1 and the example 1, tween 80 is not used in the water extraction and alcohol precipitation in the step S3, and the rest steps are the same.
Comparative example 2
A preparation method of dendrobium candidum dietary fiber extract comprises the following steps:
s1, degreasing treatment: drying and crushing dendrobium candidum stem and leaf raw materials, and degreasing with petroleum ether;
s2, performing steam explosion (steam explosion, explosion pressure is 1.1MPa, and maintenance time is 60S) on the degreased material in the step S1, and then rapidly releasing pressure to obtain a material a;
s3, according to the dosage ratio of 1g:12mL, adding the material a obtained in the step S2 into absolute ethyl alcohol, regulating the pH value to 10.5 in a stirring state, standing and filtering to obtain a precipitate;
s4, adding the precipitate obtained in the step S3 into deionized water, regulating the pH value to 2 in a stirring state, and stirring for 1h at 70 ℃; filtering after stirring to obtain filtrate and filter residue;
s5, concentrating and evaporating the filtrate obtained in the step S4, and then, according to the mass ratio of 1:1, adding the concentrated and evaporated material into absolute ethyl alcohol, standing and then carrying out vacuum drying treatment to obtain water-soluble dietary fiber;
s6, according to the mass ratio of 1:9, adding the filter residue obtained in the step S4 into deionized water again, regulating the pH value to 1.8 in a stirring state, and standing for 0.5h at 65 ℃; filtering and drying after standing to obtain insoluble dietary fiber;
s7, according to the mass ratio of 1:2, mixing the water-soluble dietary fiber obtained in the step S5 with the insoluble dietary fiber obtained in the step S6 to obtain the dendrobium candidum dietary fiber extract.
Namely, in the step S3, the alcohol precipitation treatment was performed in comparison with the comparative example 2 and the example 1, and the other steps were the same.
Comparative example 3
A compound beverage with intestinal tract regulating effect is prepared from the following raw materials in mass: 2.5g of dendrobium candidum dietary fiber extract, 0.08g of lactitol, 0.2g of carboxymethyl cellulose sodium, 0.1g of citric acid and 100g of water.
Wherein, dendrobium candidum dietary fiber extract is prepared by the method in the example 1.
In this comparative example, there is also provided a method for preparing the above-mentioned composite beverage, comprising the steps of:
adding herba Dendrobii dietary fiber extract, lactitol, sodium carboxymethyl cellulose, and citric acid into water, homogenizing, sterilizing, and packaging.
That is, comparative example 3 was compared with example 3, the raw material for the preparation was free of gynura bicolor, and the rest was the same.
The water-soluble dietary fibers and insoluble dietary fibers prepared in examples 1 to 2 and comparative examples 1 to 2 were measured with reference to GB5009.88-2014, and the extraction rates of the water-soluble dietary fibers and insoluble dietary fibers were calculated according to the following formulas.
Extraction ratio= (water-soluble dietary fiber or insoluble dietary fiber)/dried dendrobium candidum stem and leaf raw material x 100%.
The measurement and calculation results are shown in Table 1.
TABLE 1 extraction effect results
Further, the beverages prepared in examples 3 to 5 and comparative example 3 were subjected to stability test. The test method is as follows: the beverages were placed in storage compartments, respectively, and left standing at room temperature for visual inspection for phase stability at 1 month, 3 months, and 6 months, respectively. The results are shown in Table 2.
TABLE 2 stability test results
| 1 month | For 3 months | 6 months of | |
| Example 3 | No precipitate and good appearanceUniform color | No precipitate and uniform color | No precipitate and uniform color |
| Example 4 | No precipitate and uniform color | No precipitate and uniform color | No precipitate and uniform color |
| Example 5 | No precipitate and uniform color | No precipitate and uniform color | No precipitate and uniform color |
| Comparative example 3 | No precipitate and uniform color | Has little precipitate, and can be dispersed after shaking | Has a small amount of sediment, is not dispersed after being cleaned, |
the technical idea of the present invention is described by the above embodiments, but the present invention is not limited to the above embodiments, that is, it does not mean that the present invention must be implemented depending on the above embodiments. It should be apparent to those skilled in the art that any modification of the present invention, equivalent substitution of individual raw materials for the product of the present invention, addition of auxiliary components, selection of specific modes, etc., falls within the scope of the present invention and the scope of disclosure.
Claims (10)
1. The compound beverage with the intestinal tract regulating effect is characterized by comprising the following preparation raw materials in parts by weight: 1 to 5 parts of dendrobium candidum dietary fiber extract, 0.5 to 3 parts of gynura bicolor, 0.05 to 0.1 part of lactitol, 0.1 to 0.5 part of sodium carboxymethyl cellulose, 0.05 to 0.2 part of citric acid and 80 to 120 parts of water.
2. The compound beverage with intestinal tract regulating effect according to claim 1, which is characterized by comprising the following preparation raw materials in parts by weight: 1.5 to 4 parts of dendrobium candidum dietary fiber extract, 0.8 to 2 parts of gynura bicolor, 0.06 to 0.09 part of lactitol, 0.15 to 0.4 part of sodium carboxymethyl cellulose, 0.08 to 0.15 part of citric acid and 90 to 110 parts of water.
3. The compound beverage with intestinal tract regulating effect according to claim 1, which is characterized by comprising the following preparation raw materials in parts by weight: 2.5 parts of dendrobium candidum dietary fiber extract, 1.2 parts of gynura bicolor, 0.08 part of lactitol, 0.2 part of sodium carboxymethyl cellulose, 0.1 part of citric acid and 100 parts of water.
4. A composite beverage with intestinal tract regulating effect according to claim 3, wherein the preparation of the dendrobium candidum dietary fiber extract comprises the following steps:
s1, degreasing treatment: drying and crushing dendrobium candidum stem and leaf raw materials, and degreasing with petroleum ether;
s2, performing steam explosion on the degreased material in the step S1, and then rapidly releasing pressure to obtain a material a;
s3, adding the material a obtained in the step S2 into an aqueous solution containing Tween 80, treating for 5-20 min under the ultrasonic power of 100-200W, regulating the pH value to 10.5-11.5 under the stirring state, adding absolute ethyl alcohol until the mass concentration of the ethyl alcohol is 75-85%, standing, and filtering to obtain a precipitate;
s4, adding the precipitate obtained in the step S3 into deionized water, regulating the pH value to 1.8-2.2 in a stirring state, and stirring for 0.5-2 h at 70-90 ℃; filtering after stirring to obtain filtrate and filter residue;
s5, concentrating and evaporating the filtrate obtained in the step S4, and then, according to the mass ratio of 1:1, adding the concentrated and evaporated material into absolute ethyl alcohol, standing and then carrying out vacuum drying treatment to obtain water-soluble dietary fiber;
s6, adding the filter residue obtained in the step S4 into deionized water again, regulating the pH value to 1.8-2.2 in a stirring state, and standing for 0.5-2 h at 65-80 ℃; filtering and drying after standing to obtain insoluble dietary fiber;
and S7, mixing the water-soluble dietary fiber obtained in the step S5 with the insoluble dietary fiber obtained in the step S6 to obtain the dendrobium candidum dietary fiber extract.
5. The composite beverage with intestinal tract adjusting effect according to claim 4, wherein in step S2, the steam explosion condition is: the explosion pressure is 1.1MPa, the maintenance time is 45-90 s, and the water vapor explosion is carried out.
6. The compound beverage with intestinal tract adjusting effect according to claim 4, wherein in the step S3, the ratio of the amount of the material a to the amount of the aqueous solution is 1g: 10-15 mL, and the concentration of Tween 80 is 0.1-0.2 wt%.
7. The compound beverage with intestinal tract adjusting effect according to claim 4, wherein in step S6, the mass ratio of filter residue to deionized water is 1: 8-12.
8. The composite beverage with intestinal tract adjusting effect according to claim 4, wherein in step S7, the mass ratio of the water-soluble dietary fiber to the insoluble dietary fiber is 1:2.
9. a method of preparing a composite beverage according to any one of claims 1 to 8, comprising the steps of:
a1, preprocessing the gynura bicolor: cleaning the gynura bicolor, scalding and cooling to obtain a material b; cutting the material b, adding the cut material b into water, and pulping; finally, filtering to obtain the gynura bicolor juice;
a2, adding the gynura bicolor juice obtained in the step A1, the dendrobium candidum dietary fiber extract, lactitol, sodium carboxymethyl cellulose and citric acid into water, homogenizing, sterilizing and packaging.
10. The method according to claim 9, wherein in step A1, the mass ratio of the material b to water is 1: 15-20.
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