CN1172649A - Hair regrowth liniment and its preparation method - Google Patents
Hair regrowth liniment and its preparation method Download PDFInfo
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- CN1172649A CN1172649A CN96109158A CN96109158A CN1172649A CN 1172649 A CN1172649 A CN 1172649A CN 96109158 A CN96109158 A CN 96109158A CN 96109158 A CN96109158 A CN 96109158A CN 1172649 A CN1172649 A CN 1172649A
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Abstract
A hair-growing liniment for treating alopecia areata, general baldness and tinea baldness, especially seborrheic alopecia with special effect is prepared from natural mica ore and borneol in ratio of 500g to 2.5 g. through such steps as immersing fine mica powder in alcohol, hydrochloric acid, aqueous solution of acetic acid, reflux extracting at 100-110 deg. C for 2.5-3 hr, filter, regulating pH value to 3-4 by 80% NaOH, adding a solution of 2.5 g borneol in 30 ml. Tween-80.
Description
The present invention relates to a kind of hair regrowth liniment and preparation method thereof, or rather, the present invention relates to a kind of hair regrowth liniment that contains the effective ingredient that from the natural crystal Muscovitum, extracts and preparation method thereof.
As everyone knows, alopecia is by all multifactor causing, for example, the hair follicle poor blood circulation causes the hair growth promoting desired nutritional to lack; Local sebum secretion is vigorous, causes the Secondary cases bacterial infection; Needed by human body trace element picked-up deficiency etc. all is the direct or indirect factors that cause alopecia in the diet.The sickness rate of alopecia increases just year by year, yet the medicine of treatment alopecia is very few, and cure rate is also undesirable, and especially to seborrheic alopecia, there do not have a kind of specific medicament to be used for so far to be clinical.
The object of the invention is to provide a kind of hair regrowth liniment and preparation method thereof, and this hair regrowth liniment contains the effective ingredient that extracts from the natural crystal Muscovitum, and it is all effective in cure to alopecia areata, alopecia totalis, alopecia due to tinea, person in middle and old age's alopecia, and the treatment seborrheic alopecia is had specially good effect.
A kind of hair regrowth liniment of the present invention is characterized in that it contains effective ingredient and the Borneolum Syntheticum that extracts from the natural crystal Muscovitum, and the usage ratio of Muscovitum and Borneolum Syntheticum is 500g: 2.5g.
The preparation method of a kind of hair regrowth liniment of the present invention is characterized in that this method comprises the following steps:
(1) pre-treatment of raw material: the Muscovitum Ore is washed, dries, is fired to and is popular in, pulverizes, sieves that to obtain particle diameter be 365 purpose Muscovitum fine powders;
(2) three kinds of solution of configuration:
(A) be that the ratio that 95% ethanol and distilled water by volume are 1: 1 is made into ethanol water 2000ml with concentration;
(B) add distilled water 2400ml with 36% hydrochloric acid 600ml and be made into 20% aqueous hydrochloric acid solution 3000ml;
(C) add the 800ml distilled water with 36% acetic acid 200ml and be made into 20% aqueous acetic acid;
(3) reflux, extract:
(D) get Muscovitum fine powder 500g in the step (1), add in the 2000ml ethanol water and soaked 6 hours, adding distil water 2000ml again, under 100～110 ℃ of temperature, carried out reflux, extract, 2.5～3 hours, cooling then, reclaim ethanol, the remaining effective medicinal liquid of 2000ml (being the rice khaki) is put into container behind the clarification filtration;
(E) soak above-mentioned (D) step with the aqueous hydrochloric acid solution 1500ml that is made into and filtered residue obtained 6 hours, add the 1500ml aqueous hydrochloric acid solution again, reflux, extract, is 2.5～3 hours then, cooling, clarification filtration, after yellow filtrate is put into container;
(F) soak (E) residue obtained 6 hours of step with the 1000ml aqueous acetic acid that is made into, reflux, extract, is 2.5～3 hours then, and cooling is put into container with yellow filtrate behind the clarification filtration;
(4) gained filtrate in the combining step (D), (E), (F) concentrates and removes wherein 10% moisture, is that 80% NaOH aqueous solution adjusting PH is 3～4 with concentration then;
(5) get the 2.5g Borneolum Syntheticum and put into the 30ml Tween 80, treat that Borneolum Syntheticum dissolves fully after, add the concentrated solution in the step (4), stir, packing, with the sterilization that carries out disinfection, medicinal liquid got product with ultraviolet radiation 30 minutes;
Remaining residue dries again after (6) three reflux, extract,, pulverizes, and adds new mica powder, extracts again by above step.
Used its purity of natural crystal Muscovitum of the present invention is 98%, measures by analysis and contains 23 kinds of trace element in this Muscovitum, has trichogenous effect as wherein Ca, Fe, Cu, Zn, I, F, P; Co, Mg, K, B, Mn have enhance metabolism, antidotal effect; Ti, Ge, V have effects such as endocrine regulation, adjusting nervous dysfunction.Used Borneolum Syntheticum has the effect of wind and heat dispersing, promoting flow of QI and blood among the present invention.The inventor through more than ten years study intensively, repetition test, facts have proved that hair regrowth liniment of the present invention has the expansion blood capillary, promote local blood circulation, increase the local organization cytoactive, increase the effect of hair growth.Hair regrowth liniment usage of the present invention is every day 2～3 times, and each 5ml is coated with alopecia place outward, simultaneously scalp is done slightly to massage to increase its permeability.Painless, nontoxic with the treatment of this hair regrowth liniment, have no side effect.
Successfully treat 67 routine alopecia patients with hair regrowth liniment of the present invention, wherein cure 58 examples, account for 85%; Produce effects 6 examples account for 9%; Effective 3 examples account for 4%; Invalid 1 example accounts for 2%; Total effective rate reaches 98%.
Embodiment:
Getting 500g is 365 purpose Muscovitum fine powders through the particle diameter of pre-treatment, soaked 6 hours with 2000ml ethanol water (concentration is that 95% ethanol 1000ml adds the 1000ml distilled water), add the 2000ml distilled water again, under 105 ℃, carried out reflux, extract, 3 hours, cooling, reclaim ethanol, surplus liquid is effective medicinal liquid, get rice khaki filtrate behind the clarification filtration and put into container, filtering residue soaked 6 hours with 1500ml 20% aqueous hydrochloric acid solution (the hydrochloric acid 300ml adding distil water 1200ml by 36% is made into), add 1500ml 20% aqueous hydrochloric acid solution again, 105 ℃ of following reflux, extract, 3 hours, cooling, gained yellow filtrate behind the clarification filtration is put into container, filtering residue soaked 6 hours with 1000ml 20% aqueous acetic acid (36% acetic acid 200ml adds the 800ml distilled water), reflux, extract, is 3 hours then, cooling, the yellow filtrate that obtains behind the clarification filtration is put into container, merge gained filtrate after three reflux, extract,, and then add 6000ml ethanol water (concentration is that 95% ethanol 3000ml adds the 3000ml distilled water), under 105 ℃, carried out reflux, extract, 3 hours, cooling, reclaim ethanol, surplus liquid is effectively thick medicinal liquid, filter this thick medicinal liquid, filtrate is yellowish-brown liquid, the filtering residue drying, pulverize, repeat to soak, the reflux, extract, step 3 is inferior, merges three times filtrate, concentrates, be that to regulate PH be 3～4 for 80% NaOH with concentration then, adding 2.5g Borneolum Syntheticum is dissolved in the solution of 30ml Tween 80, stirs packing, with ultraviolet radiation 30 minutes, with the sterilization that carries out disinfection, this medicinal liquid is preserved in the cool, and the shelf-life is 2 years.
Compare with like product in the market, the advantage of hair regrowth liniment of the present invention is, its active ingredient from Extract in the natural crystal mica, be rich in the multiple trace element that can promote natural on-off cycles of hair growth, use hair tonic of the present invention The hair that grows behind the liniment is sturdy, black and close, and can again not come off, good effect, and instant effect, and also former Material source is abundant, and the preparation method is simple, and is bald effective in cure to treatment alopecia areata, whole alopecia, tinea, to treatment seborrhea Alopecia has special efficacy.
Claims (2)
1, a kind of hair regrowth liniment is characterized in that it contains effective ingredient and the Borneolum Syntheticum that extracts from the natural crystal Muscovitum, and the usage ratio of Muscovitum and Borneolum Syntheticum is 500g: 2.5g.
2, the preparation method of the described a kind of hair regrowth liniment of claim 1 is characterized in that this method comprises the following steps:
(1) pre-treatment of raw material: the Muscovitum Ore is washed, dries, is fired to and is popular in, pulverizes, sieves that to obtain particle diameter be 365 purpose Muscovitum fine powders;
(2) three kinds of solution of configuration:
(A) be that the ratio that 95% ethanol and distilled water by volume are 1: 1 is made into ethanol water 2000ml with concentration;
(B) add distilled water 2400ml with 36% hydrochloric acid 600ml and be made into 20% aqueous hydrochloric acid solution 3000ml;
(C) add the 800ml distilled water with 36% acetic acid 200ml and be made into 20% aqueous acetic acid;
(3) reflux, extract;
(D) get Muscovitum fine powder 500g in the step (1), add in the 2000ml ethanol water and soaked 6 hours, adding distil water 2000ml again, under 100～110 ℃ of temperature, carried out reflux, extract, 2.5～3 hours, cooling then, reclaim ethanol, the remaining effective medicinal liquid of 2000ml (being the rice khaki) is put into container behind the clarification filtration;
(E) soak above-mentioned (D) step with the aqueous hydrochloric acid solution 1500ml that is made into and filtered residue obtained 6 hours, add the 1500ml aqueous hydrochloric acid solution again, reflux, extract, is 2.5～3 hours then, cooling, clarification filtration, after yellow filtrate is put into container;
(F) soak (E) residue obtained 6 hours of step with the 1000ml aqueous acetic acid that is made into, reflux, extract, is 2.5～3 hours then, and cooling is put into container with yellow filtrate behind the clarification filtration;
(4) gained filtrate in the combining step (D), (E), (F) concentrates and removes wherein 10% moisture, is that 80% NaOH aqueous solution adjusting PH is 3～4 with concentration then;
(5) get the 2.5g Borneolum Syntheticum and put into the 30ml Tween 80, treat that Borneolum Syntheticum dissolves fully after, add the concentrated solution in the step (4), stir, packing, with the sterilization that carries out disinfection, medicinal liquid got product with ultraviolet radiation 30 minutes;
Remaining residue dries again after (6) three reflux, extract,, pulverizes, and adds new mica powder, extracts again by above step.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN96109158A CN1066042C (en) | 1996-08-02 | 1996-08-02 | Hair regrowth liniment and its preparation method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN96109158A CN1066042C (en) | 1996-08-02 | 1996-08-02 | Hair regrowth liniment and its preparation method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1172649A true CN1172649A (en) | 1998-02-11 |
| CN1066042C CN1066042C (en) | 2001-05-23 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN96109158A Expired - Fee Related CN1066042C (en) | 1996-08-02 | 1996-08-02 | Hair regrowth liniment and its preparation method |
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| Country | Link |
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| CN (1) | CN1066042C (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2002179582A (en) * | 2000-12-08 | 2002-06-26 | Alps Yakuhin Kogyo Kk | TESTOSTERONE-5alpha-REDUCTASE INHIBITOR |
| CN102872200A (en) * | 2011-07-12 | 2013-01-16 | 郑绯丹 | Externally-applied medicine for treating alopecia areata |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1058900A (en) * | 1991-05-21 | 1992-02-26 | 焦学恩 | A kind of preparation method of HAIR REGENERATING SOLUTION |
-
1996
- 1996-08-02 CN CN96109158A patent/CN1066042C/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2002179582A (en) * | 2000-12-08 | 2002-06-26 | Alps Yakuhin Kogyo Kk | TESTOSTERONE-5alpha-REDUCTASE INHIBITOR |
| CN102872200A (en) * | 2011-07-12 | 2013-01-16 | 郑绯丹 | Externally-applied medicine for treating alopecia areata |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1066042C (en) | 2001-05-23 |
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