CN117017837A - Marine mint toothpaste essence and preparation method thereof - Google Patents
Marine mint toothpaste essence and preparation method thereof Download PDFInfo
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- CN117017837A CN117017837A CN202311019560.7A CN202311019560A CN117017837A CN 117017837 A CN117017837 A CN 117017837A CN 202311019560 A CN202311019560 A CN 202311019560A CN 117017837 A CN117017837 A CN 117017837A
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- 239000000606 toothpaste Substances 0.000 title claims abstract description 96
- 229940034610 toothpaste Drugs 0.000 title claims abstract description 96
- 235000006679 Mentha X verticillata Nutrition 0.000 title claims abstract description 94
- 235000002899 Mentha suaveolens Nutrition 0.000 title claims abstract description 94
- 235000001636 Mentha x rotundifolia Nutrition 0.000 title claims abstract description 94
- 238000002360 preparation method Methods 0.000 title abstract description 23
- 239000002994 raw material Substances 0.000 claims abstract description 40
- NOOLISFMXDJSKH-UHFFFAOYSA-N DL-menthol Natural products CC(C)C1CCC(C)CC1O NOOLISFMXDJSKH-UHFFFAOYSA-N 0.000 claims abstract description 35
- 229940041616 menthol Drugs 0.000 claims abstract description 35
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims abstract description 33
- 238000003756 stirring Methods 0.000 claims abstract description 24
- -1 WS-3 menthol amide Chemical class 0.000 claims abstract description 23
- WRMNZCZEMHIOCP-UHFFFAOYSA-N 2-phenylethanol Chemical compound OCCC1=CC=CC=C1 WRMNZCZEMHIOCP-UHFFFAOYSA-N 0.000 claims abstract description 22
- 239000010634 clove oil Substances 0.000 claims abstract description 20
- 239000010642 eucalyptus oil Substances 0.000 claims abstract description 20
- 229940044949 eucalyptus oil Drugs 0.000 claims abstract description 20
- 239000001683 mentha spicata herb oil Substances 0.000 claims abstract description 20
- 235000019721 spearmint oil Nutrition 0.000 claims abstract description 20
- 244000246386 Mentha pulegium Species 0.000 claims abstract description 15
- 235000016257 Mentha pulegium Nutrition 0.000 claims abstract description 15
- 235000004357 Mentha x piperita Nutrition 0.000 claims abstract description 15
- 235000001050 hortel pimenta Nutrition 0.000 claims abstract description 15
- NOOLISFMXDJSKH-UTLUCORTSA-N (+)-Neomenthol Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@@H]1O NOOLISFMXDJSKH-UTLUCORTSA-N 0.000 claims abstract description 13
- 238000002156 mixing Methods 0.000 claims abstract description 13
- WTEVQBCEXWBHNA-UHFFFAOYSA-N Citral Natural products CC(C)=CCCC(C)=CC=O WTEVQBCEXWBHNA-UHFFFAOYSA-N 0.000 claims abstract description 12
- 235000012828 Citrullus lanatus var citroides Nutrition 0.000 claims abstract description 12
- 150000001299 aldehydes Chemical class 0.000 claims abstract description 12
- 229940043350 citral Drugs 0.000 claims abstract description 12
- WTEVQBCEXWBHNA-JXMROGBWSA-N geranial Chemical compound CC(C)=CCC\C(C)=C\C=O WTEVQBCEXWBHNA-JXMROGBWSA-N 0.000 claims abstract description 12
- 239000001525 mentha piperita l. herb oil Substances 0.000 claims abstract description 12
- 235000019477 peppermint oil Nutrition 0.000 claims abstract description 12
- 239000000341 volatile oil Substances 0.000 claims abstract description 12
- 239000010676 star anise oil Substances 0.000 claims abstract description 3
- 244000241235 Citrullus lanatus Species 0.000 claims abstract 4
- 239000000463 material Substances 0.000 claims description 49
- 229920000881 Modified starch Polymers 0.000 claims description 39
- 239000004368 Modified starch Substances 0.000 claims description 39
- 235000019426 modified starch Nutrition 0.000 claims description 39
- 239000011248 coating agent Substances 0.000 claims description 35
- 238000000576 coating method Methods 0.000 claims description 35
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 27
- 229920002774 Maltodextrin Polymers 0.000 claims description 24
- 239000005913 Maltodextrin Substances 0.000 claims description 24
- 229940035034 maltodextrin Drugs 0.000 claims description 24
- 229920002472 Starch Polymers 0.000 claims description 23
- 235000019698 starch Nutrition 0.000 claims description 23
- 239000008107 starch Substances 0.000 claims description 23
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 21
- 240000003915 Lophatherum gracile Species 0.000 claims description 19
- 239000000203 mixture Substances 0.000 claims description 18
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 14
- 239000002002 slurry Substances 0.000 claims description 13
- 241000218645 Cedrus Species 0.000 claims description 10
- 235000010489 acacia gum Nutrition 0.000 claims description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 9
- IVOMOUWHDPKRLL-KQYNXXCUSA-N Cyclic adenosine monophosphate Chemical compound C([C@H]1O2)OP(O)(=O)O[C@H]1[C@@H](O)[C@@H]2N1C(N=CN=C2N)=C2N=C1 IVOMOUWHDPKRLL-KQYNXXCUSA-N 0.000 claims description 8
- 150000008064 anhydrides Chemical class 0.000 claims description 8
- 239000010617 anise oil Substances 0.000 claims description 8
- 235000019441 ethanol Nutrition 0.000 claims description 8
- 239000000796 flavoring agent Substances 0.000 claims description 8
- 235000019634 flavors Nutrition 0.000 claims description 8
- 238000000034 method Methods 0.000 claims description 8
- 239000003607 modifier Substances 0.000 claims description 8
- 235000017166 Bambusa arundinacea Nutrition 0.000 claims description 6
- 235000017491 Bambusa tulda Nutrition 0.000 claims description 6
- 244000082204 Phyllostachys viridis Species 0.000 claims description 6
- 235000015334 Phyllostachys viridis Nutrition 0.000 claims description 6
- 241000949456 Zanthoxylum Species 0.000 claims description 6
- 239000001785 acacia senegal l. willd gum Substances 0.000 claims description 6
- 239000011425 bamboo Substances 0.000 claims description 6
- 238000001035 drying Methods 0.000 claims description 6
- 238000001914 filtration Methods 0.000 claims description 6
- 238000005406 washing Methods 0.000 claims description 6
- 238000004108 freeze drying Methods 0.000 claims description 3
- 230000000694 effects Effects 0.000 abstract description 21
- 230000007794 irritation Effects 0.000 abstract description 17
- 206010031009 Oral pain Diseases 0.000 abstract description 2
- 235000013599 spices Nutrition 0.000 abstract description 2
- 210000000214 mouth Anatomy 0.000 description 31
- 239000003205 fragrance Substances 0.000 description 26
- 240000007472 Leucaena leucocephala Species 0.000 description 13
- 235000010643 Leucaena leucocephala Nutrition 0.000 description 13
- 240000005286 Cryptomeria japonica var. sinensis Species 0.000 description 11
- 230000000052 comparative effect Effects 0.000 description 10
- 241000219109 Citrullus Species 0.000 description 8
- 239000002304 perfume Substances 0.000 description 8
- 230000000638 stimulation Effects 0.000 description 8
- 238000012360 testing method Methods 0.000 description 7
- 210000002200 mouth mucosa Anatomy 0.000 description 5
- 240000005109 Cryptomeria japonica Species 0.000 description 4
- WFDIJRYMOXRFFG-UHFFFAOYSA-N Acetic anhydride Chemical group CC(=O)OC(C)=O WFDIJRYMOXRFFG-UHFFFAOYSA-N 0.000 description 3
- 229920000084 Gum arabic Polymers 0.000 description 3
- 239000000205 acacia gum Substances 0.000 description 3
- 230000004048 modification Effects 0.000 description 3
- 238000012986 modification Methods 0.000 description 3
- 244000215068 Acacia senegal Species 0.000 description 2
- 235000002566 Capsicum Nutrition 0.000 description 2
- 239000006002 Pepper Substances 0.000 description 2
- 235000016761 Piper aduncum Nutrition 0.000 description 2
- 240000003889 Piper guineense Species 0.000 description 2
- 235000017804 Piper guineense Nutrition 0.000 description 2
- 235000008184 Piper nigrum Nutrition 0.000 description 2
- 238000005253 cladding Methods 0.000 description 2
- 238000013329 compounding Methods 0.000 description 2
- 239000000551 dentifrice Substances 0.000 description 2
- 230000002349 favourable effect Effects 0.000 description 2
- 210000004400 mucous membrane Anatomy 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 238000010998 test method Methods 0.000 description 2
- 229920002261 Corn starch Polymers 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 230000003064 anti-oxidating effect Effects 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000000975 bioactive effect Effects 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 239000008120 corn starch Substances 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 229930003935 flavonoid Natural products 0.000 description 1
- 235000017173 flavonoids Nutrition 0.000 description 1
- 150000004676 glycans Chemical class 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 239000000543 intermediate Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 210000004379 membrane Anatomy 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 230000001575 pathological effect Effects 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 230000007180 physiological regulation Effects 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 230000004044 response Effects 0.000 description 1
- 230000008591 skin barrier function Effects 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 230000004936 stimulating effect Effects 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 230000002936 tranquilizing effect Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/11—Encapsulated compositions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/35—Ketones, e.g. benzophenone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/732—Starch; Amylose; Amylopectin; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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- Health & Medical Sciences (AREA)
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- General Health & Medical Sciences (AREA)
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- Epidemiology (AREA)
- Birds (AREA)
- Emergency Medicine (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical & Material Sciences (AREA)
- Oral & Maxillofacial Surgery (AREA)
- Cosmetics (AREA)
Abstract
The application relates to the technical field of essence and spice, and particularly discloses a marine mint toothpaste essence and a preparation method thereof. A marine mint toothpaste essence consists of the following components in parts by weight: 0.25-0.35 part of watermelon aldehyde; 0.8-1.2 parts of phenethyl alcohol; 9.5-10.5 parts of peppermint oil; 4.5-5.5 parts of spearmint oil; 42-48 parts of menthol; 0.35-0.45 parts of citral; 4.5-5.5 parts of eucalyptus oil; 4.5-5.5 parts of star anise oil; 0.45-0.55 part of clove oil; 15.2-16.4 parts of propylene glycol; 0.9-1.1 parts of WS-3 menthol amide; 0.9-1.1 parts of WS-23 menthol amide; 9-11 parts of peppermint essential oil; the preparation method comprises the following steps: and (3) uniformly stirring and mixing the raw materials, and homogenizing under high pressure to obtain the peppermint toothpaste essence. The marine mint toothpaste essence disclosed by the application not only shows excellent combination of two elements of marine and mint, but also is not easy to cause irritation to people with sensitive mouths, and has excellent and stable overall application effect.
Description
Technical Field
The application relates to the technical field of essence and spice, in particular to a marine mint toothpaste essence and a preparation method thereof.
Background
The essence for toothpaste is prepared by blending natural perfume and synthetic perfume with reference to the fragrance of natural plants, has natural flavor and various perfume raw material components, and is endowed with a certain type of fragrance and a certain type of taste of the toothpaste, so that a consumer can feel cool and refreshing in the oral cavity when using the essence, and the essence is pleasant to accept and use by the consumer.
The toothpaste essence consists of a mint fragrance base part and a protruding fragrance part which gives the fragrance characteristic of the product, wherein the protruding fragrance part of the children toothpaste essence is more and the mint fragrance base part is less; the toothpaste essence for household and adult has more mint fragrance parts and less protruding fragrance parts; different types of toothpaste essence mainly comprise different composition ratios of mint fragrance base and protruding fragrance, wherein the protruding fragrance has various compositions, and the toothpaste essence has rich diversity.
In the related art, in order to continuously optimize the flavor and taste of the toothpaste, the adopted toothpaste essence often uses a plurality of and complex perfume components for mixing, and can achieve the aim of developing new products, but the essence is easy to bring a certain oral cavity stimulation effect for people with sensitive oral cavities, so that the use experience of consumers is greatly influenced.
Therefore, there is a need to propose a solution to the above technical problems.
Disclosure of Invention
The application provides a marine mint toothpaste essence and a preparation method thereof, aiming at the problem that oral cavity stimulation is difficult to occur to people with sensitive oral cavity while improving the richness of the toothpaste essence.
In a first aspect, the application provides a marine mint toothpaste essence, which adopts the following technical scheme:
a marine mint toothpaste essence consists of the following components in parts by weight:
0.25-0.35 part of watermelon aldehyde;
0.8-1.2 parts of phenethyl alcohol;
9.5-10.5 parts of peppermint oil;
4.5-5.5 parts of spearmint oil;
42-48 parts of menthol;
0.35-0.45 parts of citral;
4.5-5.5 parts of eucalyptus oil;
4.5-5.5 parts of star anise oil;
0.45-0.55 part of clove oil;
15.2-16.4 parts of propylene glycol;
0.9-1.1 parts of WS-3 menthol amide;
0.9-1.1 parts of WS-23 menthol amide;
9-11 parts of peppermint essential oil.
By adopting the technical scheme, the excellent stable menthol fragrance can be formed by adopting the combination of the peppermint oil, menthol, WS-3 menthol amide, WS-23 menthol amide and peppermint essential oil of the purple pepper sample; the watermelon aldehyde and the citral can bring fresh and sweet fragrance, and are excellent prominent fragrance components; the phenethyl alcohol and the anise oil can enhance the fragrance and blend the components to release the fragrance; propylene glycol is used as a good solvent, so that a uniform and stable mixed state can be formed among the raw materials of all the components; the combination of the spearmint oil, the eucalyptus oil and the clove oil can ensure that the outstanding fragrance components and the mint fragrance base are stably matched, is favorable for ensuring that the essence shows excellent combination of two elements of ocean and mint, can play a role in releasing the smell aiming at the mouth-sensitive crowd, regulates the stability of the mouth environment, and further can greatly reduce the generation of the irritation; thus, the obtained marine mint toothpaste essence has excellent application effect.
Preferably, 2.8-3.6 parts of soothing composition is also added into the components of the marine mint toothpaste essence, the soothing composition consists of lophatherum gracile extract and cedar bud extract, and the weight ratio of the lophatherum gracile extract to the cedar bud extract is 1 (1.2-1.8).
By adopting the technical scheme, the main components in the lophatherum gracile extract are flavonoid compounds and bioactive polysaccharide, which can show excellent antioxidation and play a role in protecting the stable oral environment; the Cryptomeria fortunei bud extract can strengthen skin barrier ability, has tranquilizing and soothing effects, and can improve the ability of oral cavity to resist external stimulus; when the lophatherum gracile extract and the cryptomeria fortunei bud extract are combined and applied according to a specific weight ratio, the lophatherum gracile extract and the cryptomeria fortunei bud extract can play an excellent compounding synergistic effect, especially for people with sensitive oral cavity, the irritation caused by the marine mint toothpaste essence can be greatly reduced, and the consumer has better use experience.
Preferably, the weight ratio of the bamboo leaf extract to the cedar bud extract is 1:1.5.
By adopting the technical scheme, the bamboo leaf extract and the cryptomeria fortunei bud extract with the weight ratio can exert excellent matching effect, and the obtained marine mint toothpaste essence is less prone to stimulating the sensitive crowd in the mouth after being applied, and has better overall quality.
Preferably, 30-40 parts of coating wall material is also added into the components of the marine mint toothpaste essence, the coating wall material consists of maltodextrin, modified starch and acacia, and the weight ratio of the maltodextrin to the modified starch to the acacia is (0.7-0.9): (1.4-1.8): 1.
By adopting the technical scheme, the wall material is adopted to coat other component raw materials, so that the marine mint toothpaste essence can slowly release fragrance along with the rupture of the wall material after application, thus the stimulation caused by the local concentrated contact of the fragrance base component and the oral cavity can be avoided, and the application stability of the marine mint toothpaste essence is greatly improved; meanwhile, the maltodextrin, the modified starch and the Arabic gum are formed into the coating wall material according to a specific proportion, the coating wall material has excellent adhesion after rupture, a film protection structure can be formed in an oral cavity, the acting force of complex perfume components on the oral cavity of a user is greatly reduced, so that the irritation produced when the marine mint toothpaste essence is applied to the sensitive crowd of the oral cavity is greatly reduced, and the overall effect is better.
Preferably, the weight ratio of maltodextrin, modified starch and acacia is 0.8:1.6:1.
Through adopting above-mentioned technical scheme, when maltodextrin, modified starch and acacia of above-mentioned proportion are as cladding wall material, not only can make its cladding fragrant base composition can stable release, can also have comparatively excellent adhesion with the user's oral cavity, be favorable to forming more stable membrane protection structure, so, just can make ocean mint toothpaste essence be difficult for the sensitive crowd in oral cavity to produce oral cavity stimulation more.
Preferably, the modified starch is prepared by the steps of:
adding 1.5-2 times of water into the starch raw material, and uniformly stirring to obtain starch slurry; then adding cyclic adenosine monophosphate, an anhydride modifier and a sodium hydroxide solution into the starch slurry, maintaining the pH value to 8-8.5, stirring and reacting for 30-40min, and adding hydrochloric acid to adjust the pH value to 4-5; finally, filtering, washing and drying to obtain the modified starch.
By adopting the technical scheme, the modified starch prepared by the method has excellent processing performance, can be matched with maltodextrin and maltodextrin to form a stable coating wall material, has a more uniform film protection structure after rupture, and has excellent capability of resisting fragrance stimulation; meanwhile, the cyclic adenosine monophosphate is introduced in the modification process, so that the physiological regulation of the oral cavity of a user can be assisted, the irritation of the complex mixed fragrance base to the oral cavity is greatly reduced, and the use experience of the oral cavity sensitive crowd is improved.
In a second aspect, the application provides a preparation method of a marine mint toothpaste essence, which adopts the following technical scheme: a preparation method of a marine mint toothpaste essence comprises the following steps:
(1) Preparing raw materials comprising watermelon aldehyde, phenethyl alcohol, peppermint oil, spearmint oil, menthol, citral, eucalyptus oil, anise oil, clove oil, propylene glycol, WS-3 menthol amide, WS-23 menthol amide and peppermint essential oil of the zanthoxylum seed according to a proportion;
(2) And (3) uniformly stirring and mixing the raw materials in the step (1), and homogenizing under high pressure to obtain the marine mint toothpaste essence.
By adopting the technical scheme, the preparation method is simple to operate, and the marine mint toothpaste essence with excellent and stable quality can be obtained only by uniformly mixing the raw materials of all the components together, and the production applicability is excellent, so that the method is convenient for large-scale industrial production.
Preferably, the marine mint toothpaste essence comprises the following steps:
(1) Preparing raw materials comprising watermelon aldehyde, phenethyl alcohol, peppermint oil, spearmint oil, menthol, citral, eucalyptus oil, anise oil, clove oil, propylene glycol, WS-3 menthol amide, WS-23 menthol amide, peppermint essential oil of a zanthoxylum seed and a coating wall material according to a proportion;
(2) Stirring and mixing the raw materials except the coating wall material in the step (1) uniformly, homogenizing under high pressure, and dispersing in absolute ethyl alcohol to prepare an essence ethanol solution with the concentration of 4-5 mg/ml;
(3) Mixing the coating wall material with water to prepare 8-12mg/ml wall material solution; and (3) adding the essence ethanol solution in the step (2) into the wall material solution, stirring at a constant temperature of 25-35 ℃ for 5-7 hours, and freeze-drying to obtain the marine mint toothpaste essence.
By adopting the technical scheme, the method can ensure that the coating wall material stably wraps other component raw materials, has higher embedding rate, has higher effective utilization rate of the raw materials, and further can obtain the marine mint toothpaste essence with excellent quality.
In summary, the application has the following beneficial effects:
1. according to the application, peppermint oil, menthol, WS-3 menthol amide, WS-23 menthol amide and peppermint essential oil like purple pepper are used as peppermint fragrance groups, watermelon aldehyde and citral are used as prominent fragrance components, under the compounding effect of spearmint oil, eucalyptus oil and clove oil, the essence not only shows excellent combination of two elements of ocean and peppermint, but also reduces the irritation of the essence to people with sensitive oral cavity, so that the obtained ocean mint toothpaste essence has excellent application effect;
2. the soothing composition comprising the bamboo leaf extract and the cedar bud extract according to a specific weight ratio is added, so that the effects of enhancing the oral barrier and protecting the oral environment stability can be exerted for people with sensitive oral cavity, the irritation caused by the marine mint toothpaste essence can be greatly reduced, and the consumer has better use experience;
3. the application adopts the coating wall material composed of maltodextrin, modified starch and Arabic gum according to a specific weight ratio, can slowly release the perfume components, so that the perfume components are not easy to be concentrated locally to cause oral cavity stimulation, and can be attached to the oral cavity to form a film protection structure after the coating wall material is broken, thus the stimulation produced by applying the marine mint toothpaste essence to the sensitive population of the oral cavity is greatly reduced, and the overall effect is better.
Detailed Description
The present application will be described in further detail with reference to examples.
The raw materials used in the preparation examples and examples of the present application are all commercially available except for the specific descriptions:
lophatherum gracile extract is purchased from the company of Sanchikungunya biological development Co., ltd., product No. FS-ZY;
cryptomeria japonica bud extract is purchased fromRenew；
Maltodextrin was purchased from Shandong sea boat bioengineering Co., ltd, CAS number 9050-36-6;
starch raw material was purchased from wuhan poly xin company of biotechnology limited as pregelatinized corn starch;
acacia gum is purchased from Shaanxi Chenming Biotech Co., ltd., CAS number 9000-01-5;
the anhydride modifier is acetic anhydride.
Examples of preparation of starting materials and/or intermediates
Preparation example 1
A modified starch prepared by the steps of:
adding 1.75 times of water into the starch raw material, and uniformly stirring to obtain starch slurry; then adding cyclic adenosine monophosphate, an anhydride modifier and a sodium hydroxide solution into the starch slurry, maintaining the pH value at 8.5, stirring and reacting for 35min, and adding hydrochloric acid to adjust the pH value to 4.5; finally, filtering, washing and drying to obtain the modified starch.
Note that: in the preparation, the addition amount of the cyclic adenosine monophosphate is 2.5% of the weight of the starch raw material, the addition amount of the anhydride modifier is 5% of the starch slurry, the concentration of the sodium hydroxide solution is 5%, and the concentration of the hydrochloric acid solution is 5%.
Preparation example 2
Modified starch, which differs from preparation example 1 in that it is obtained by the following steps:
adding 1.5 times of water into the starch raw material, and uniformly stirring to obtain starch slurry; then adding cyclic adenosine monophosphate, an anhydride modifier and a sodium hydroxide solution into the starch slurry, maintaining the pH value at 8, stirring and reacting for 30min, and adding hydrochloric acid to adjust the pH value to 4; finally, filtering, washing and drying to obtain the modified starch.
Preparation example 3
Modified starch, which differs from preparation example 1 in that it is obtained by the following steps:
adding 2 times of water into the starch raw material, and uniformly stirring to obtain starch slurry; then adding cyclic adenosine monophosphate, an anhydride modifier and a sodium hydroxide solution into the starch slurry, maintaining the pH value at 8.5, stirring and reacting for 40min, and adding hydrochloric acid to adjust the pH value to 5; finally, filtering, washing and drying to obtain the modified starch.
Preparation example 4
Modified starch, which differs from preparation example 1 in that it is obtained by the following steps:
adding 1.75 times of water into the starch raw material, and uniformly stirring to obtain starch slurry; then adding an anhydride modifier and a sodium hydroxide solution into the starch slurry, maintaining the pH value at 8.5, stirring and reacting for 35min, and adding hydrochloric acid to adjust the pH value to 4.5; finally, filtering, washing and drying to obtain the modified starch.
Examples
Example 1
The marine mint toothpaste essence is prepared from the following raw materials in parts by weight as shown in table 1:
(1) Preparing raw materials comprising watermelon aldehyde, phenethyl alcohol, peppermint oil, spearmint oil, menthol, citral, eucalyptus oil, anise oil, clove oil, propylene glycol, WS-3 menthol amide, WS-23 menthol amide and peppermint essential oil of the zanthoxylum seed according to a proportion;
(2) And (3) uniformly stirring and mixing the raw materials in the step (1) at the stirring speed of 300r/min for 20min, homogenizing at the high pressure of 5000r/min under the homogenizing pressure of 20MPa for 35min to obtain the marine mint toothpaste essence.
Examples 2 to 3
A marine mint toothpaste essence, which differs from example 1 in that the raw materials of each component and their corresponding weights are shown in table 1.
Table 1 raw materials for each component in examples 1 to 3 and parts by weight (kg/part)
| Component (A) | Example 1 | Example 2 | Example 3 |
| Watermelon aldehyde | 0.3 | 0.25 | 0.35 |
| Phenethyl alcohol | 1 | 0.8 | 1.2 |
| Peppermint oil | 10 | 9.5 | 10.5 |
| Spearmint oil | 5 | 4.5 | 5.5 |
| Menthol crystal | 45 | 42 | 48 |
| Citral | 0.4 | 0.35 | 0.45 |
| Eucalyptus oil | 5 | 4.5 | 5.5 |
| Anise oil | 5 | 4.5 | 5.5 |
| Clove oil | 0.5 | 0.45 | 0.55 |
| Propylene glycol | 15.8 | 15.2 | 16.4 |
| WS-3 menthylamides | 1 | 0.9 | 1.1 |
| WS-23 menthylamides | 1 | 0.9 | 1.1 |
| Peppermint essential oil | 10 | 9 | 11 |
Example 4
A marine mint toothpaste essence is different from example 1 in that 3.2 parts of the component in the step (1) is added
The soothing composition consists of lophatherum gracile extract and cryptomeria fortunei bud extract according to the weight ratio of 1:1.5.
Example 5
A marine mint toothpaste essence is different from example 4 in that the soothing composition consists of lophatherum gracile extract and Cryptomeria fortunei bud extract in a weight ratio of 1:1.2.
Example 6
A marine mint toothpaste essence is different from example 4 in that the soothing composition consists of lophatherum gracile extract and Cryptomeria fortunei bud extract in a weight ratio of 1:1.8.
Example 7
A marine mint toothpaste essence differs from example 4 in that the soothing composition is added in 2.8 parts by weight.
Example 8
A marine mint toothpaste essence differs from example 4 in that the soothing composition is added in 2.8 parts by weight.
Example 9
A marine mint toothpaste essence is different from example 4 in that the soothing composition consists of lophatherum gracile extract and Cryptomeria fortunei bud extract in a weight ratio of 1:1.1.
Example 10
A marine mint toothpaste essence is different from example 4 in that the soothing composition consists of lophatherum gracile extract and Cryptomeria fortunei bud extract in a weight ratio of 1:1.9.
Example 11
A marine mint toothpaste essence is different from example 4 in that the component does not contain Lophatherum gracile extract.
Example 12
A marine mint toothpaste essence differs from example 4 in that it contains no cedar bud extract in its components.
Example 13
The difference with the embodiment 1 is that 35 parts of coating wall materials are also added into the components of the marine mint toothpaste essence, the coating wall materials consist of maltodextrin, modified starch and Arabic gum according to the weight ratio of 0.8:1.6:1, and the marine mint toothpaste essence is prepared by the following steps:
(1) Preparing raw materials comprising watermelon aldehyde, phenethyl alcohol, peppermint oil, spearmint oil, menthol, citral, eucalyptus oil, anise oil, clove oil, propylene glycol, WS-3 menthol amide, WS-23 menthol amide, peppermint essential oil of a zanthoxylum seed and a coating wall material according to a proportion;
(2) Uniformly stirring and mixing the raw materials except the coating wall material in the step (1) at the stirring speed of 300r/min for 20min, homogenizing at high pressure at the homogenizing speed of 5000r/min under the homogenizing pressure of 20MPa for 35min, and dispersing in absolute ethyl alcohol to prepare an essence ethanol solution with the concentration of 4.5 mg/ml;
(3) Mixing the coating wall material with water to prepare a wall material solution of 10 mg/ml; and (3) adding the essence ethanol solution in the step (2) into the wall material solution, stirring at a constant temperature of 30 ℃ for 6 hours, and freeze-drying to obtain the marine mint toothpaste essence.
Note that: the modified starch used was obtained in preparation example 1.
Example 14
A marine mint toothpaste essence, which differs from example 13 in that in step (2) a 4mg/ml ethanol solution of the essence is provided; in the step (3), a wall material solution of 8mg/ml was prepared, and then stirred at a constant temperature of 35℃for 5 hours.
Example 15
A marine mint toothpaste essence, which differs from example 13 in that in step (2) a 5mg/ml ethanol solution of the essence is provided; in the step (3), a wall material solution of 12mg/ml was prepared, and then stirred at a constant temperature of 25℃for 7 hours.
Example 16
The marine mint toothpaste essence is different from example 13 in that the coating wall material consists of maltodextrin, modified starch and acacia in the weight ratio of 0.7:1.4:1.
Example 17
The marine mint toothpaste essence is different from example 13 in that the coating wall material consists of maltodextrin, modified starch and acacia in the weight ratio of 0.9:1.8:1.
Example 18
The essence of the marine mint toothpaste is different from example 13 in that the coating wall material is added in 30 parts by weight.
Example 19
The essence of the marine mint toothpaste is different from example 13 in that the coating wall material is added in 40 parts by weight.
Example 20
The marine mint toothpaste essence is different from example 13 in that the coating wall material consists of maltodextrin, modified starch and acacia in the weight ratio of 0.6:1.3:1.
Example 21
The marine mint toothpaste essence is different from example 13 in that the coating wall material consists of maltodextrin, modified starch and acacia in the weight ratio of 1:1.9:1.
Example 22
A marine mint toothpaste essence differs from example 13 in that the coating wall material does not contain maltodextrin.
Example 23
A marine mint toothpaste essence, which differs from example 13 in that the coating wall material does not contain modified starch.
Example 24
A marine mint toothpaste essence differs from example 13 in that the coating wall material does not contain gum arabic.
Example 25
A marine mint toothpaste essence differs from example 13 in that the coating wall material does not contain maltodextrin and modified starch.
Example 26
A marine mint toothpaste essence differs from example 13 in that the coating wall material does not contain maltodextrin and gum arabic.
Example 27
A marine mint toothpaste essence, differing from example 13 in that the coating wall material does not contain modified starch and acacia.
Example 28
A marine mint toothpaste essence, which differs from example 13 in that modified starch was obtained in preparation example 2.
Example 29
A marine mint toothpaste essence, which differs from example 13 in that modified starch was obtained in preparation 3.
Example 30
A marine mint toothpaste essence, which differs from example 13 in that modified starch was obtained in preparation example 4.
Example 31
A marine mint toothpaste essence differs from example 13 in that the quality of the modified starch is replaced by starch material.
Comparative example
Comparative example 1
A marine mint toothpaste essence, which is different from example 1 in that the component raw materials do not contain spearmint oil.
Comparative example 2
A marine mint toothpaste essence is different from example 1 in that the component raw materials do not contain eucalyptus oil.
Comparative example 3
A marine mint toothpaste essence is different from example 1 in that the component raw materials do not contain clove oil.
Comparative example 4
A marine mint toothpaste essence is different from example 1 in that the component raw materials do not contain spearmint oil and eucalyptus oil.
Comparative example 5
The difference between the marine mint toothpaste essence and the example 1 is that the component raw materials do not contain spearmint oil and clove oil.
Comparative example 6
A marine mint toothpaste essence is different from example 1 in that the component raw materials do not contain eucalyptus oil and clove oil.
Comparative example 7
A marine mint toothpaste essence is different from example 1 in that the component raw materials do not contain spearmint oil, eucalyptus oil and clove oil.
Performance test samples: the marine mint dentifrice essence obtained in examples 1-31 was used as test samples 1-31, and the marine mint dentifrice essence obtained in comparative examples 1-7 was used as control samples 1-7.
The test method comprises the following steps: test samples 1-31 and control samples 1-7 were tested according to pharmaceutical industry standard 0279-1995 oral mucosa irritation test, oral Material biological test method, which is applicable to evaluate the irritation of oral mucosal tissue by oral materials that are in temporary or prolonged contact with oral mucosal tissue. After the test is completed, scoring is performed according to pathological response in the standard, and the scoring standard is as follows: the average of scores of each group, no 0-5 min (5 min), mild 5-9 min (9 min), moderate 9-12 min (12 min), and severe 12-16 min, was taken and the corresponding test samples 1-31 and control samples 1-7 are recorded in table 2 below.
Test results of Table test samples 1 to 31 and control samples 1 to 7
As can be seen by combining example 1 and comparative examples 1-7 and combining table 2, the combination of spearmint oil, eucalyptus oil and clove oil can greatly reduce the irritation of the marine mint toothpaste essence to the oral mucosa tissue, and thus can be more suitable for people with sensitive oral cavity; any one of spearmint oil, eucalyptus oil and clove oil is added singly, the effect of reducing the irritation is limited, or any two of spearmint oil, eucalyptus oil and clove oil are combined for use, the effect is simply overlapped, and the effect brought by the whole spearmint oil, eucalyptus oil and clove oil is more excellent when three raw materials are compounded, so that the technical effect of adding one to more than two can be brought.
As can be seen from the combination of examples 1 and 4-8 and the combination of table 2, the addition of the soothing composition comprising the lophatherum gracile extract and the cedar bud extract in a weight ratio of 1 (1.2-1.8) can further reduce the irritation of the marine mint toothpaste essence to the oral mucosa tissue, and the overall effect is excellent when the weight ratio of the lophatherum gracile extract to the cedar bud extract is 1:1.5; in combination with examples 9-10 and with Table 2, it can be seen that when the ratio of Lophatherum gracile extract to Cryptomeria japonica bud extract is outside the above range, the corresponding promotion partners are discounted; by combining examples 11-12 and combining Table 2, it can be seen that the addition of the Lophatherum gracile extract or the Cryptomeria fortunei bud extract alone brings about far less improvement effect than the excellent combination of the Lophatherum gracile extract and the Cryptomeria fortunei bud extract; in conclusion, the light bamboo leaf extract and the cryptomeria japonica bud extract are added into a soothing composition according to a specific weight ratio, so that the light bamboo leaf extract and the cryptomeria japonica bud extract have an outstanding effect of reducing the stimulation of essence to people with sensitive mouths.
As can be seen from the combination of examples 1 and examples 13 to 19 and Table 2, the addition of the coating wall material consisting of maltodextrin, modified starch and acacia in a weight ratio of (0.7-0.9): (1.4-1.8): 1 can greatly reduce the irritation influence of complex perfume components on the oral cavity of a user, and further can greatly reduce the irritation feeling generated when the oral cavity-sensitive crowd is applied, wherein the overall effect is excellent when the weight ratio of maltodextrin, modified starch and acacia is 0.8:1.6:1. It can be seen from the combination of examples 20 to 21 and Table 2 that when the ratio of the three components exceeds the above-mentioned range, the effect of the coating wall material is lost; in combination with examples 22-27 and Table 2, it can be seen that when any one or two of maltodextrin, modified starch and acacia are used, the effect is far less excellent than the combination of the three, although the irritation of the marine mint toothpaste essence to the oral mucosa tissue can be reduced to a certain extent.
As can be seen by combining examples 1, 28-29 and 31 and combining table 2, the use of modified starch, compared with the starch raw material, can exert excellent and stable effects by matching with maltodextrin and acacia, so that the irritation of the marine mint toothpaste essence to the oral mucosa tissue is greatly reduced; by combining example 30 with Table 2, it can be seen that the cyclic adenosine monophosphate is introduced in the modification process to assist the physiological adjustment of the oral cavity of the user, so that the irritation of the complex mixed fragrance base to the oral cavity is greatly reduced, and the use experience of the oral cavity sensitive crowd is improved.
The present embodiment is only for explanation of the present application and is not to be construed as limiting the present application, and modifications to the present embodiment, which may not creatively contribute to the present application as required by those skilled in the art after reading the present specification, are all protected by patent laws within the scope of claims of the present application.
Claims (8)
1. The marine mint toothpaste essence is characterized by comprising the following components in parts by weight:
0.25-0.35 part of watermelon aldehyde;
0.8-1.2 parts of phenethyl alcohol;
9.5-10.5 parts of peppermint oil;
4.5-5.5 parts of spearmint oil;
42-48 parts of menthol;
0.35-0.45 parts of citral;
4.5-5.5 parts of eucalyptus oil;
4.5-5.5 parts of star anise oil;
0.45-0.55 part of clove oil;
15.2-16.4 parts of propylene glycol;
0.9-1.1 parts of WS-3 menthol amide;
0.9-1.1 parts of WS-23 menthol amide;
9-11 parts of peppermint essential oil.
2. The marine mint toothpaste flavor of claim 1, wherein: the marine mint toothpaste essence is characterized in that 2.8-3.6 parts of relieving composition is also added into the components of the marine mint toothpaste essence, the relieving composition consists of lophatherum gracile extract and cedar bud extract, and the weight ratio of the lophatherum gracile extract to the cedar bud extract is 1 (1.2-1.8).
3. The marine mint toothpaste flavor of claim 2, wherein: the weight ratio of the bamboo leaf extract to the cedar bud extract is 1:1.5.
4. The marine mint toothpaste flavor of claim 1, wherein: the marine mint toothpaste essence comprises the following components, by weight, 30-40 parts of a coating wall material, wherein the coating wall material consists of maltodextrin, modified starch and Arabic gum, and the weight ratio of the maltodextrin to the modified starch to the Arabic gum is (0.7-0.9) (1.4-1.8) 1.
5. The marine mint toothpaste flavor of claim 4, wherein: the weight ratio of the maltodextrin to the modified starch to the Arabic gum is 0.8:1.6:1.
6. The marine mint toothpaste flavor of claim 4, wherein: the modified starch is prepared by the following steps:
adding 1.5-2 times of water into the starch raw material, and uniformly stirring to obtain starch slurry; then adding cyclic adenosine monophosphate, an anhydride modifier and a sodium hydroxide solution into the starch slurry, maintaining the pH value to 8-8.5, stirring and reacting for 30-40min, and adding hydrochloric acid to adjust the pH value to 4-5; finally, filtering, washing and drying to obtain the modified starch.
7. A method for preparing a marine mint toothpaste flavour according to any one of claims 1 to 4, characterised in that: the method comprises the following steps:
(1) Preparing raw materials comprising watermelon aldehyde, phenethyl alcohol, peppermint oil, spearmint oil, menthol, citral, eucalyptus oil, anise oil, clove oil, propylene glycol, WS-3 menthol amide, WS-23 menthol amide and peppermint essential oil of the zanthoxylum seed according to a proportion;
(2) And (3) uniformly stirring and mixing the raw materials in the step (1), and homogenizing under high pressure to obtain the marine mint toothpaste essence.
8. The marine mint toothpaste essence according to any one of claims 5-6, characterized in that: the method comprises the following steps:
(1) Preparing raw materials comprising watermelon aldehyde, phenethyl alcohol, peppermint oil, spearmint oil, menthol, citral, eucalyptus oil, anise oil, clove oil, propylene glycol, WS-3 menthol amide, WS-23 menthol amide, peppermint essential oil of a zanthoxylum seed and a coating wall material according to a proportion;
(2) Stirring and mixing the raw materials except the coating wall material in the step (1) uniformly, homogenizing under high pressure, and dispersing in absolute ethyl alcohol to prepare an essence ethanol solution with the concentration of 4-5 mg/ml;
(3) Mixing the coating wall material with water to prepare 8-12mg/ml wall material solution; and (3) adding the essence ethanol solution in the step (2) into the wall material solution, stirring at a constant temperature of 25-35 ℃ for 5-7 hours, and freeze-drying to obtain the marine mint toothpaste essence.
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