CN100577156C - Instant membrane for paste and preparation method thereof - Google Patents
Instant membrane for paste and preparation method thereof Download PDFInfo
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- CN100577156C CN100577156C CN200610035940A CN200610035940A CN100577156C CN 100577156 C CN100577156 C CN 100577156C CN 200610035940 A CN200610035940 A CN 200610035940A CN 200610035940 A CN200610035940 A CN 200610035940A CN 100577156 C CN100577156 C CN 100577156C
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Abstract
An instant film sheet with nutritive, flavouring and health-care function for toothpaste, candy, medicine, etc is proportionally prepared from hydroxypropyl methylcellulose, nutrients, sweetening agent, souring agent, emulsifier, essence, pigment and water. Its preparing process is also disclosed.
Description
Technical field
The present invention relates to a kind of instant membrane that is used for mastic, and the preparation method of this instant membrane.
Background technology
Along with growth in the living standard, people as toothpaste, mastic confection, mastic medicine etc., not only require it to have traditional basic function to the articles for daily use especially children life articles for use, wish that also it has good ornamental and health care etc., makes it have better result of use.
Summary of the invention
The purpose of this invention is to provide a kind of in mastic, have decoration and/or the instant membrane of health-care effect and the preparation method of this instant membrane, this instant membrane can contain nutrient substance, flavoring agent, pigment etc., can have shades of colour, and can cut into the small pieces of tool different shape, be added on that room temperature does not dissolve in toothpaste, mastic confection and the medicine, in aqueous solution, can dissolve fast.The technical scheme that adopts is as follows:
On the one hand, the invention provides a kind of instant membrane that is used for mastic, this instant membrane is made up of following components in weight percentage: hydroxypropyl emthylcellulose 50.0～99.4%; Nutrient substance 0～19.5%; Sweeting agent 0～5.0%; Acidic flavoring agent 0～5.0%; Emulsifying agent 0.1～1.0%; Essence 0～10.0%; Pigment 0～1.5%; Water 0.2～10.0%; Described nutrient substance is vitamin, mineral, docosahexenoic acid or arachidonic acid, perhaps its mixture;
The preparation method of described instant membrane may further comprise the steps: (1) is equipped with hydroxypropyl emthylcellulose, nutrient substance, sweeting agent, acidic flavoring agent, emulsifying agent, essence, color element in proportion; (2) hydroxypropyl emthylcellulose is added weight in its water of 18～40 ℃ of 9～20 times, stir, soak, be dissolved in fully in the water, become the glue that is pellucidity until hydroxypropyl emthylcellulose; (3) nutrient substance, sweeting agent, acidic flavoring agent are dissolved fully by 60 ℃～80 ℃ the water of gross weight with 10～15 times, with emulsifying agent, essence, pigment mix homogeneously, join in the glue mix homogeneously more then; (4) material that step (3) is obtained is crossed colloid mill, through the homogenizer homogenizing, outgases in vacuum degassing machine more then, enters the material cylinder afterwards; (5) will expect material in the cylinder through the molding of film-forming machine multiple abscess knifing, dry under 80～100 ℃ temperature then, obtain instant membrane.
Wherein hydroxypropyl emthylcellulose is a film former.
In the nutrient substance, vitamin can be vitamins A, vitamins B, vitamins C, vitamins D etc., and mineral can be ferrum, zinc, calcium lactate etc.The weight percentage of preferred nutrient matter is 0～1%, and its effect mainly is the health care that increases instant membrane.
Sweeting agent is a kind of or composite in sorbitol, mannitol, xylitol, maltose, hydroxyl isomaltulose, oligomeric xylose, oligomeric isomaltose alcohol, glucide, saccharin sodium, glycyrrhizin, cyclamate, aspartame, acesulfame potassium, sucralose, neotame, palatinose preferably, preferred its weight percentage is 0～1%, plays the seasoning effect.
Acidic flavoring agent is a kind of or composite in citric acid, lactic acid, phosphoric acid, succinic acid, fumaric acid, malic acid, sodium citrate, vitamin C, adipic acid, tartaric acid preferably, and preferably its weight percentage is 0～1%, plays the seasoning effect.
Emulsifying agent is preferably from monoglyceride, sucrose ester, Tweens (20,30,60,80), spans (20,30,60,80), polyethylene glycols (200,300,400,600,1000,1500,2000,4000,6000,20000), a kind of or composite in the polyvinyl alcohol, polyacrylic acid, lecithin, dehydrogenation lecithin, play emulsification, reduce the surface tension at biphase (referring to hydroxypropyl emthylcellulose and water) interface,, prevent the coalescent of emulsion particle to keep stable emulsified state.The wherein composite mixture that is preferably monoglyceride and sucrose ester by 2: 1 weight proportions, weight percentage is 0.3～0.5%; Or tween 80 and Arlacel-20 be by the mixture of 1: 2 weight proportion, and weight percentage is 0.3～0.5%; Or tween 80 and dehydrogenation lecithin is by the mixture of 2: 1 weight proportions, and weight percentage is 0.3～0.5%.
Essence is a kind of or composite in Mentholum, Oleum menthae, Herba Menthae essence, freshener, fruity essence, plant extract (as Herba Menthae Rotundifoliae), composite essential oil preferably, and preferably its weight percentage is 0.1～1%, plays the perfumery effect.
Pigment can be a natural pigment, it also can be synthetic dyestuff, as antholeucin, lemon yellow, curcumin, light blue pigment, amaranth pigment, carmine pigment etc., play the toning effect, strengthen the decorative effect of instant membrane, can be according to the odor type of product or custom toning general sanctified by usage, the weight percentage of preferred pigment is 0.1～1%.
On the other hand, the invention provides a kind of preparation method of above-mentioned instant membrane, may further comprise the steps:
(1) is equipped with hydroxypropyl emthylcellulose, nutrient substance, sweeting agent, acidic flavoring agent, emulsifying agent, essence, color element in proportion;
(2) hydroxypropyl emthylcellulose is added weight in its water of 18～40 ℃ of 9～20 times, stir, soak, be dissolved in fully in the water, become the glue that is pellucidity until hydroxypropyl emthylcellulose; Preferred mixing speed is 50～100 rev/mins;
(3) nutrient substance, sweeting agent, acidic flavoring agent are dissolved fully by 60 ℃～80 ℃ the water of gross weight with 10～15 times, then with emulsifying agent, essence, pigment mix homogeneously, join in the glue mix homogeneously (can adopt stirring method to mix, mixing time is about 10～20 minutes usually) again;
(4) material that step (3) is obtained is crossed colloid mill, through the homogenizer homogenizing, outgases in vacuum degassing machine more then, enters the material cylinder afterwards; Preferred homogenization pressure is 40MPa～60MPa, and the vacuum of vacuum degassing machine is 0.1～0.2MPa;
(5) will expect material in the cylinder through the molding of film-forming machine multiple abscess knifing, dry under 80～100 ℃ temperature then, obtain instant membrane.Can by Producer according to practical situation be voluntarily held mainly according to the difference of final products water content and slightly different drying time, is about 30～40 minutes usually.During the molding of multiple abscess knifing, regulate steam pressure, the line speed of film-forming machine, and regulate the flow of material, with the thickness of control instant membrane.
The above-mentioned instant membrane that makes is received the film rolling through film gatherer, can cut into the small pieces of required form on request through cutting machine, add to then in the mastic, in 20～25 ℃ of temperature ranges, stir, can pack, the instant membrane small pieces can increase the health care and the aesthetic of mastic product.
Instant membrane provided by the invention can contain nutrient substance, flavoring agent, pigment etc., can have a shades of colour, and can cut into the small pieces of different shape, be added on that room temperature does not dissolve in toothpaste, mastic confection and the medicine, in aqueous solution, can dissolve fast, can add in the mastic, make the mastic product have good ornamental and health care, have better result of use, satisfy the demand of user.
The specific embodiment
Embodiment 1
(1) gets hydroxypropyl emthylcellulose 993 grams, essence 1.7 grams (wherein Mentholum 0.1 gram, Herba Menthae essence 1 gram, Herba Menthae Rotundifoliae 0.5 gram, freshener 0.1 gram), emulsifying agent 1.2 grams (wherein tween 80 0.8 gram, ovum unicorn fat 0.4 gram);
(2) hydroxypropyl emthylcellulose is added weight in its water of 20 ℃ of 9.8 times, stir, soak, mixing speed is 80 rev/mins, is dissolved in fully in the water until hydroxypropyl emthylcellulose, becomes the glue that is pellucidity;
(3) with emulsifying agent, essence mix homogeneously, join again in the glue, be stirred to mix homogeneously;
(4) material that step (3) is obtained is crossed colloid mill, and then through homogenizer homogenizing (homogenization pressure is 50MPa), the degassing in vacuum degassing machine (vacuum of vacuum degassing machine is 0.15MPa) again enters the material cylinder afterwards;
(5) will expect material in the cylinder through the molding of film-forming machine multiple abscess knifing, dry under 90 ℃ temperature then, obtain 1000 gram instant membranes.During the molding of multiple abscess knifing, regulate steam pressure, the line speed of film-forming machine, and regulate the flow of material, with the thickness of control instant membrane.
Contain hydroxypropyl emthylcellulose 993 grams, essence 1.7 grams (wherein Mentholum 0.1 gram, Herba Menthae essence 1 gram, Herba Menthae Rotundifoliae 0.5 gram, freshener 0.1 gram), emulsifying agent 1.2 grams (wherein tween 80 0.8 gram, ovum unicorn fat 0.4 gram) and water 4.1 grams in the instant membrane that makes.
Above-mentioned instant membrane is cut into the shred that length and width is 1CM,, joins in 20～25 ℃ the transparent toothpaste, stir, make toothpaste have effect refrigerant, that refresh oneself as the refrigerant diaphragm carrier of toothpaste.
Embodiment 2
(1) gets hydroxypropyl emthylcellulose 600 grams, nutrient substance 190 grams (calcium lactate 5 grams, Fructus Citri sinensis extract 185 grams,), sweeting agent 50 gram (wherein maltose 30 grams, sorbitol 14.5 grams, glycyrrhizin 5.5 grams), acidic flavoring agent 5 grams (wherein citric acid 2 grams, malic acid 3 grams), emulsifying agent 4 grams (wherein sucrose ester 2 grams, polyvinyl alcohol 2 grams), fruity essence 50 grams, curcumin 1 gram;
(2) hydroxypropyl emthylcellulose is added weight in its water of 30 ℃ of 18 times, stir, soak, mixing speed is 80 rev/mins, is dissolved in fully in the water until hydroxypropyl emthylcellulose, becomes the glue that is pellucidity;
(3) nutrient substance, sweeting agent, acidic flavoring agent are dissolved fully by 65 ℃ the water of gross weight with 12 times, with emulsifying agent, fruity essence, curcumin mix homogeneously, join again in the glue then, be stirred to mix homogeneously;
(4) material that step (3) is obtained is crossed colloid mill, and then through homogenizer homogenizing (homogenization pressure is 42MPa), the degassing in vacuum degassing machine (vacuum of vacuum degassing machine is 0.18MPa) again enters the material cylinder afterwards;
(5) will expect material in the cylinder through the molding of film-forming machine multiple abscess knifing, dry under 98 ℃ temperature then, obtain 1000 gram instant membranes.During the molding of multiple abscess knifing, regulate steam pressure, the line speed of film-forming machine, and regulate the flow of material, with the thickness of control instant membrane.
Contain hydroxypropyl emthylcellulose 600 grams, nutrient substance 190 grams (calcium lactate 5 grams in the instant membrane that makes, Fructus Citri sinensis extract 185 grams,), sweeting agent 50 gram (wherein maltose 30 grams, sorbitol 14.5 grams, glycyrrhizin 5.5 grams), acidic flavoring agent 5 grams (wherein citric acid 2 grams, malic acid 3 grams), emulsifying agent 4 grams (wherein sucrose ester 2 grams, polyvinyl alcohol 2 grams), fruity essence 50 grams, curcumin 1 gram and water 100 grams.
Above-mentioned instant membrane is cut into the diaphragm with various fruit shapes,, joins in 20～25 ℃ the mastic transparent adhesive tape (moisture≤30%) as the nutrition decorative membrance of child's colloid sugar, stir equal, make child's colloid sugar have health-care effect, and the taste uniqueness, good decorative property.
Embodiment 3
(1) gets hydroxypropyl emthylcellulose 960 grams, nutrient substance 6 grams (wherein DHA 2 grams, AA 4 grams), acesulfame potassium 3 grams, emulsifying agent 3.6 grams (wherein tween 80 1.2 grams, Arlacel-20 24 grams), pigment 2.1 grams (wherein antholeucin 2 grams, lemon yellow 0.1 gram);
(2) hydroxypropyl emthylcellulose is added weight in its water of 30 ℃ of 10 times, stir, soak, mixing speed is 60 rev/mins, is dissolved in fully in the water until hydroxypropyl emthylcellulose, becomes the glue that is pellucidity;
(3) nutrient substance, acesulfame potassium (sweeting agent) are dissolved fully by 70 ℃ the water of gross weight with 12 times, with emulsifying agent, pigment mix homogeneously, join again in the glue then, be stirred to mix homogeneously;
(4) material that step (3) is obtained is crossed colloid mill, and then through homogenizer homogenizing (homogenization pressure is 45MPa), the degassing in vacuum degassing machine (vacuum of vacuum degassing machine is 0.12MPa) again enters the material cylinder afterwards;
(5) will expect material in the cylinder through the molding of film-forming machine multiple abscess knifing, dry under 100 ℃ temperature then, obtain 1000 gram instant membranes.During the molding of multiple abscess knifing, regulate steam pressure, the line speed of film-forming machine, and regulate the flow of material, with the thickness of control instant membrane.
Contain hydroxypropyl emthylcellulose 960 grams, nutrient substance 6 grams (wherein DHA 2 grams, AA 4 grams), acesulfame potassium 3 grams, emulsifying agent 3.6 grams (wherein tween 80 1.2 grams, Arlacel-20 2.4 grams), pigment 2.1 grams (wherein antholeucin 2 grams, lemon yellow 0.1 gram) and water 25.3 grams in the instant membrane that makes.
Above-mentioned instant membrane is cut into the Fructus Citri sinensis type diaphragm that diameter is 2CM, inhales the nutrition decorative membrance of sugar, join in 20～25 ℃ the mastic syrup (moisture≤30%), stir, make the child inhale sugar and have health-care effect as the child, and good decorative property.
Embodiment 4
(1) gets hydroxypropyl emthylcellulose 885.2 grams, emulsifying agent 4.8 grams (wherein monoglyceride 3.2 grams, sucrose ester 1.6 grams), pigment 10 grams (wherein antholeucin 10 grams);
(2) hydroxypropyl emthylcellulose is added weight in its water of 20 ℃ of 16 times, stir, soak, mixing speed is 70 rev/mins, is dissolved in fully in the water until hydroxypropyl emthylcellulose, becomes the glue that is pellucidity;
(3) with emulsifying agent, pigment mix homogeneously, join again in the glue, be stirred to mix homogeneously;
(4) material that step (3) is obtained is crossed colloid mill, and then through homogenizer homogenizing (homogenization pressure is 55MPa), the degassing in vacuum degassing machine (vacuum of vacuum degassing machine is 0.11MPa) again enters the material cylinder afterwards;
(5) will expect material in the cylinder through the molding of film-forming machine multiple abscess knifing, dry under 99 ℃ temperature then, obtain 1000 gram instant membranes.During the molding of multiple abscess knifing, regulate steam pressure, the line speed of film-forming machine, and regulate the flow of material, with the thickness of control instant membrane.
Contain hydroxypropyl emthylcellulose 885.2 grams, emulsifying agent 4.8 grams (wherein monoglyceride 3.2 grams, sucrose ester 1.6 grams), pigment 10 grams (wherein antholeucin 10 grams) and water 100 grams in the instant membrane that makes.
Above-mentioned instant membrane is cut into pieces, as the decorative membrance of externally used paste, joined in 20～25 ℃ the external used medicine mastic, stir, it is good ornamental that externally used paste is had.
Embodiment 5
(1) gets hydroxypropyl emthylcellulose 900 grams, nutrient substance 6 grams (wherein vitamin C 6 grams), sweeting agent 50 grams (wherein aspartame 1 gram, sorbitol 49 grams), emulsifying agent 3.5 grams (wherein monoglyceride 3.5 grams), amaranth pigment 0.5 gram;
(2) hydroxypropyl emthylcellulose is added weight in its water of 25 ℃ of 18 times, stir, soak, mixing speed is 90 rev/mins, is dissolved in fully in the water until hydroxypropyl emthylcellulose, becomes the glue that is pellucidity;
(3) nutrient substance, sweeting agent are dissolved fully by 65 ℃ the water of gross weight with 14 times, with emulsifying agent, amaranth pigment mix homogeneously, join again in the glue then, be stirred to mix homogeneously;
(4) material that step (3) is obtained is crossed colloid mill, and then through homogenizer homogenizing (homogenization pressure is 60MPa), the degassing in vacuum degassing machine (vacuum of vacuum degassing machine is 0.18MPa) again enters the material cylinder afterwards;
(5) will expect material in the cylinder through the molding of film-forming machine multiple abscess knifing, dry under 82 ℃ temperature then, obtain 1000 gram instant membranes.During the molding of multiple abscess knifing, regulate steam pressure, the line speed of film-forming machine, and regulate the flow of material, with the thickness of control instant membrane.
Contain hydroxypropyl emthylcellulose 900 grams, nutrient substance 6 grams (wherein vitamin C 6 grams), sweeting agent 50 grams (wherein aspartame 1 gram, sorbitol 49 grams), emulsifying agent 3.5 grams (wherein monoglyceride 3.5 grams), amaranth pigment 0.5 gram and water 40 grams in the instant membrane that makes.
Above-mentioned instant membrane is cut into the diaphragm with cartoon character,, joins in 20～25 ℃ the mastic transparent adhesive tape (moisture≤30%), stir, make child's colloid sugar have health-care effect as the nutrition decorative membrance of child's colloid sugar, and good decorative property.
Claims (9)
1, a kind of instant membrane that is used for mastic is characterized in that it is made up of following components in weight percentage: hydroxypropyl emthylcellulose 50.0～99.4%; Nutrient substance 0～19.5%; Sweeting agent 0～5.0%; Acidic flavoring agent 0～5.0%; Emulsifying agent 0.1～1.0%; Essence 0～10.0%; Pigment 0～1.5%; Water 0.2～10.0%; Described nutrient substance is vitamin, mineral, docosahexenoic acid or arachidonic acid, perhaps its mixture;
The preparation method of described instant membrane may further comprise the steps: (1) is equipped with hydroxypropyl emthylcellulose, nutrient substance, sweeting agent, acidic flavoring agent, emulsifying agent, essence, color element in proportion; (2) hydroxypropyl emthylcellulose is added weight in its water of 18～40 ℃ of 9～20 times, stir, soak, be dissolved in fully in the water, become the glue that is pellucidity until hydroxypropyl emthylcellulose; (3) nutrient substance, sweeting agent, acidic flavoring agent are dissolved fully by 60 ℃～80 ℃ the water of gross weight with 10～15 times, with emulsifying agent, essence, pigment mix homogeneously, join in the glue mix homogeneously more then; (4) material that step (3) is obtained is crossed colloid mill, through the homogenizer homogenizing, outgases in vacuum degassing machine more then, enters the material cylinder afterwards; (5) will expect material in the cylinder through the molding of film-forming machine multiple abscess knifing, dry under 80～100 ℃ temperature then, obtain instant membrane.
2, the instant membrane that is used for mastic according to claim 1 is characterized in that: the weight percentage of described nutrient substance is 0～1%.
3, the instant membrane that is used for mastic according to claim 1 is characterized in that: the weight percentage of described sweeting agent is 0～1%.
4, the instant membrane that is used for mastic according to claim 1 is characterized in that: the weight percentage of described acidic flavoring agent is 0～1%.
5, the instant membrane that is used for mastic according to claim 1 is characterized in that: the weight percentage of described essence is 0.1～1%.
6, the instant membrane that is used for mastic according to claim 1 is characterized in that: the weight percentage of described pigment is 0.1～1%.
7, the instant membrane that is used for mastic according to claim 1 is characterized in that: described emulsifying agent is a kind of or composite in monoglyceride, sucrose ester, Tweens, spans, polyethylene glycols, polyvinyl alcohol, polyacrylic acid, lecithin, the dehydrogenation lecithin.
8, the described preparation method that is used for the instant membrane of mastic of claim 1 is characterized in that may further comprise the steps:
(1) is equipped with hydroxypropyl emthylcellulose, nutrient substance, sweeting agent, acidic flavoring agent, emulsifying agent, essence, color element in proportion;
(2) hydroxypropyl emthylcellulose is added weight in its water of 18～40 ℃ of 9～20 times, stir, soak, be dissolved in fully in the water, become the glue that is pellucidity until hydroxypropyl emthylcellulose;
(3) nutrient substance, sweeting agent, acidic flavoring agent are dissolved fully by 60 ℃～80 ℃ the water of gross weight with 10～15 times, with emulsifying agent, essence, pigment mix homogeneously, join in the glue mix homogeneously more then;
(4) material that step (3) is obtained is crossed colloid mill, through the homogenizer homogenizing, outgases in vacuum degassing machine more then, enters the material cylinder afterwards;
(5) will expect material in the cylinder through the molding of film-forming machine multiple abscess knifing, dry under 80～100 ℃ temperature then, obtain instant membrane.
9, the preparation method that is used for the instant membrane of mastic according to claim 8 is characterized in that: mixing speed is 50～100 rev/mins in the step (2).
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| CN200610035940A CN100577156C (en) | 2006-06-14 | 2006-06-14 | Instant membrane for paste and preparation method thereof |
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| CN200610035940A CN100577156C (en) | 2006-06-14 | 2006-06-14 | Instant membrane for paste and preparation method thereof |
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| CN100577156C true CN100577156C (en) | 2010-01-06 |
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| CN103750323A (en) * | 2014-01-26 | 2014-04-30 | 宁夏医科大学 | Oral lutein instant membrane and preparation method thereof |
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Address after: 515011 M3 in 11 districts of Jinyuan Industrial City, Chaoshan Road, Shantou City, Guangdong Province Patentee after: GUANGDONG FUWEI FRUITS & NUTS MANUFACTURING CO.,LTD. Address before: 515011 M3 in 11 districts of Jinyuan Industrial City, Chaoshan Road, Shantou City, Guangdong Province Patentee before: Shantou Fuwei Fruits & Nuts Manufacturing Co.,Ltd. |
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Address after: 515000 M3 and D buildings of 13-07 and 13-08 blocks of Jinyuan Industrial City, Chaoshan Road, Shantou City, Guangdong Province Patentee after: GUANGDONG FUWEI HEALTH TECHNOLOGY Co.,Ltd. Address before: 515011 M3 in 11 districts of Jinyuan Industrial City, Chaoshan Road, Shantou City, Guangdong Province Patentee before: GUANGDONG FUWEI FRUITS & NUTS MANUFACTURING CO.,LTD. |