CN116549340A - Preparation method of durable agilawood sandalwood perfume - Google Patents
Preparation method of durable agilawood sandalwood perfume Download PDFInfo
- Publication number
- CN116549340A CN116549340A CN202310711246.9A CN202310711246A CN116549340A CN 116549340 A CN116549340 A CN 116549340A CN 202310711246 A CN202310711246 A CN 202310711246A CN 116549340 A CN116549340 A CN 116549340A
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- China
- Prior art keywords
- sandalwood
- essential oil
- perfume
- tincture
- raw material
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 235000008632 Santalum album Nutrition 0.000 title claims abstract description 57
- 241000221035 Santalaceae Species 0.000 title claims abstract description 56
- 239000002304 perfume Substances 0.000 title claims abstract description 42
- 238000002360 preparation method Methods 0.000 title claims abstract description 19
- 239000000341 volatile oil Substances 0.000 claims abstract description 56
- 239000002994 raw material Substances 0.000 claims abstract description 45
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 29
- 229940098465 tincture Drugs 0.000 claims abstract description 28
- 241000402754 Erythranthe moschata Species 0.000 claims abstract description 23
- 238000002156 mixing Methods 0.000 claims abstract description 23
- 239000001615 FEMA 2049 Substances 0.000 claims abstract description 19
- 238000003756 stirring Methods 0.000 claims abstract description 8
- 238000000605 extraction Methods 0.000 claims description 32
- 238000000034 method Methods 0.000 claims description 23
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 20
- 239000000843 powder Substances 0.000 claims description 20
- 239000000203 mixture Substances 0.000 claims description 15
- 238000003815 supercritical carbon dioxide extraction Methods 0.000 claims description 14
- 238000001914 filtration Methods 0.000 claims description 12
- 238000000227 grinding Methods 0.000 claims description 12
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 10
- 239000001569 carbon dioxide Substances 0.000 claims description 10
- 238000000926 separation method Methods 0.000 claims description 10
- 238000002791 soaking Methods 0.000 claims description 10
- 241000271309 Aquilaria crassna Species 0.000 claims description 9
- 241000196324 Embryophyta Species 0.000 claims description 5
- 239000007787 solid Substances 0.000 claims description 5
- JEYCTXHKTXCGPB-UHFFFAOYSA-N Methaqualone Chemical compound CC1=CC=CC=C1N1C(=O)C2=CC=CC=C2N=C1C JEYCTXHKTXCGPB-UHFFFAOYSA-N 0.000 claims 1
- 239000000463 material Substances 0.000 claims 1
- 239000012254 powdered material Substances 0.000 claims 1
- 230000009286 beneficial effect Effects 0.000 abstract description 8
- 230000000711 cancerogenic effect Effects 0.000 abstract description 3
- 231100000315 carcinogenic Toxicity 0.000 abstract description 3
- 238000005507 spraying Methods 0.000 abstract description 3
- 239000000284 extract Substances 0.000 abstract description 2
- 230000002045 lasting effect Effects 0.000 abstract description 2
- 239000000419 plant extract Substances 0.000 abstract description 2
- 238000004519 manufacturing process Methods 0.000 abstract 1
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 6
- 150000001875 compounds Chemical class 0.000 description 6
- 244000153234 Hibiscus abelmoschus Species 0.000 description 4
- 239000003205 fragrance Substances 0.000 description 4
- 230000003177 cardiotonic effect Effects 0.000 description 3
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 3
- OESSQZSTPKCQOE-UHFFFAOYSA-M sodium;2,4-dinitronaphthalen-1-olate Chemical compound [Na+].C1=CC=C2C([O-])=C([N+]([O-])=O)C=C([N+]([O-])=O)C2=C1 OESSQZSTPKCQOE-UHFFFAOYSA-M 0.000 description 3
- 230000000694 effects Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 240000000513 Santalum album Species 0.000 description 1
- 230000003796 beauty Effects 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/981—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of mammals or bird
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q13/00—Formulations or additives for perfume preparations
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids
Abstract
The invention discloses a preparation method of durable agilawood sandalwood perfume, which comprises the following steps: step 1, preparing raw materials; step 2, preparing essential oil; step 3, preparing tincture; step 4, mixing and stirring; and 5, blending perfume. The beneficial effects are that: the natural plant extracts are used for obtaining the heavy essential oil, the sandalwood essential oil, the ambergris tincture and the musk tincture, and the perfume prepared by mixing the natural extracts with alcohol is healthy, harmless and free from carcinogenic risk after long-time spraying; the ambergris is fragrant, healthy, harmless and lasting in taste; the manufacturing steps are simple, the time consumption is short, and the preparation efficiency of the perfume is effectively improved.
Description
Technical Field
The invention relates to the technical field of perfume preparation, in particular to a preparation method of durable agilawood sandalwood perfume.
Background
Perfume is a beauty cosmetic made of essential oil and alcohol, which can emit strong and durable fragrance, and can enhance the aesthetic feeling and attraction of users. With the rise in the level of living and the transition in consumption concepts, perfumes have changed from a luxury to a necessity for people's daily life. Although the perfume shows unique individuality and charm of the user, perfects the cultural image of the user, the existing perfumes are all made of chemical essence, and the long-time spraying of the chemical essence has a cancerogenic risk.
Disclosure of Invention
In order to solve the problems, particularly the defects existing in the prior art, the invention provides a preparation method of durable agilawood sandalwood perfume, which can solve the problems.
In order to achieve the above purpose, the invention adopts the following technical means:
a preparation method of durable agilawood sandalwood perfume comprises the following steps:
step 1, raw material preparation:
grinding 8-12 parts of agilawood raw materials into 50-70 mesh powder;
grinding 8-12 parts of sandalwood raw materials into 50-70 mesh powder;
step 2, essential oil preparation:
extracting the powdery agilawood raw material in the step 1, wherein 0.02-0.04 part of essential oil is obtained by extraction;
extracting the powdery sandalwood raw material in the step 1, wherein 0.02-0.04 part of sandalwood essential oil is obtained by extraction;
step 3, tincture preparation:
grinding 0.8-1.2 parts of ambergris raw material into powder of 20-40 meshes, soaking ambergris powder in 0.8-1.2 parts of alcohol for 80-100 days, filtering to obtain ambergris tincture of 0.2-0.6 parts;
soaking 0.004-0.006 parts of musk raw material in 0.08-0.12 parts of alcohol for 80-100 days, filtering to prepare musk tincture, and preparing 0.1-0.3 parts of musk tincture;
step 4, mixing and stirring:
adding 0.02-0.04 part of heavy essential oil, 0.02-0.04 part of sandalwood essential oil, 0.2-0.6 part of ambergris tincture, 0.1-0.3 part of musk tincture and 1.22-1.28 parts of alcohol into a mixing bottle, and slowly stirring until the essential oil and the tincture are completely dissolved in the alcohol;
step 5, perfume blending:
standing the mixture in the mixing bottle in the step 4 for 80-100 days, shaking every 5-7 days for 3-6 minutes, placing the mixing bottle in a refrigerator after 80-100 days, setting the temperature to 3-6 ℃, standing for 10-14 hours, enabling the mixing bottle to see solid flocculent or snowflake-shaped objects, and filtering to obtain the natural plant perfume.
According to a further scheme, the agilawood raw material is a wild agilawood raw material.
The beneficial effects of the method are that the wild agilawood has good fragrance, the quality of perfume can be effectively improved, and the using effect of the perfume can be effectively improved.
According to a further scheme, the sandalwood raw material is a Sandalwood raw material of Soneler indicum.
The beneficial effects of the method are that the Inanel sandalwood has better fragrance, can effectively improve the quality of perfume and can effectively improve the using effect of perfume.
According to a further scheme, the alcohol is 96% edible alcohol.
The beneficial effects are that the edible alcohol is harmless to human body, 96% of the edible alcohol can facilitate the dissolution of the essential oil, the sandalwood essential oil, the ambergris tincture and the musk tincture.
According to a further scheme, the powdery agilawood raw material is extracted by a supercritical carbon dioxide extraction method, and the extraction conditions are as follows: the extraction column is 28-32Mpa, and the temperature is: 35-45 ℃, separation column: 6-10Mpa, the carbon dioxide flow is: 20-25L/h, the extraction time is 1.5-2.5 hours, and 0.02-0.04 part of the obtained heavy essential oil is extracted.
The supercritical carbon dioxide extraction method has the advantages that the supercritical carbon dioxide extraction method can prevent the extracted compound from decomposing at high temperature, prevent the extracted compound from being polluted, prevent the extracted compound from being oxidized, and effectively improve the quality of the heavy essential oil.
According to a further scheme, the powdery Sonnell sandalwood raw material is extracted by a supercritical carbon dioxide extraction method, and the extraction conditions are as follows: the extraction column is 28-32Mpa, and the temperature is: 35-45 ℃, separation column: 6-10Mpa, the carbon dioxide flow is: 20-25L/h, the extraction time is 1.5-2.5 hours, and 0.022-0.028 parts of the obtained sandalwood essential oil is extracted.
The supercritical carbon dioxide extraction method has the beneficial effects that the supercritical carbon dioxide extraction method can prevent the extracted compound from decomposing at high temperature, prevent the extracted compound from being polluted, prevent the extracted compound from being oxidized, and effectively improve the quality of the sandalwood essential oil.
According to a further scheme, the mass ratio of the agilawood essential oil to the santalum album essential oil in the mixing bottle is 1:1.
The beneficial effects of the above-mentioned arrangement are that this kind of setting can make perfume distribute even eaglewood and sandalwood.
In a further aspect of the invention, the mixing flask is a brown laboratory flask.
The beneficial effects of the utility model are that dark glass can absorb light, and light can not penetrate into the bottle, can effectively prevent the liquid in the laboratory bottle from taking place the decomposition phenomenon.
The invention has the beneficial effects that:
1. according to the invention, the natural plant extracts are used for obtaining the heavy essential oil, the sandalwood essential oil, the ambergris tincture and the musk tincture, and the perfume prepared by mixing the natural extracts with the alcohol is healthy, harmless and free from carcinogenic risk after long-time spraying.
2. The invention has the advantages of fragrance fixation, health, no harm and lasting taste through the natural ambergris.
3. The method has simple steps and short time consumption, and effectively improves the preparation efficiency of the perfume.
Detailed Description
The following description of the present invention will be made clearly and fully, and it is apparent that the embodiments described are some, but not all, of the embodiments of the present invention. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
Example 1
A preparation method of durable agilawood sandalwood perfume comprises the following steps:
1. preparing 10 kg of wild agilawood raw material, and grinding the 10 kg of wild agilawood raw material into 60-mesh powder;
10 kg of the Indian sonel sandalwood raw material is prepared and ground into 60 mesh powder;
preparing 1 kg of ambergris raw material, grinding into 30 meshes, soaking 1 kg of ambergris powder in 1 kg of 96% edible alcohol for 90 days, and filtering to obtain 0.4 kg of ambergris tincture;
preparing Moschus 0.005 kg, soaking with 96% edible alcohol 0.1 kg for 90 days, and filtering to obtain Moschus tincture 0.105 kg.
2. Extracting the wild agilawood raw material powder by a supercritical carbon dioxide extraction method, wherein the extraction conditions are as follows: the extraction column is 30Mpa, and the temperature is: 40 degrees celsius, separation column: the flow rate of carbon dioxide is 8 Mpa: 22L/h, the extraction time is 2 hours, and 0.02 kg of the obtained essential oil is extracted;
3. extracting the raw materials of the Inanel sandalwood by a supercritical carbon dioxide extraction method under the following extraction conditions: the extraction column is 30Mpa, and the temperature is: 40 degrees celsius, separation column: the flow rate of carbon dioxide is 8 Mpa: 22L/h, the extraction time is 2 hours, and 0.026 kg of the obtained sandalwood essential oil is extracted;
4. using the obtained 0.02 kg of the essential oil, taking 0.02 kg of the essential oil for standby: 0.026 kg of sandalwood essential oil and 0.02 kg of sandalwood essential oil are taken for standby; 0.4 kg of ambergris tincture and 0.1 kg of ambergris tincture are taken for standby; 0.105 kg of musk tincture and 0.1 kg of musk tincture are taken for standby.
5. Mixing 0.02 kg of agilawood essential oil, 0.02 kg of sandalwood essential oil, 0.1 kg of ambergris tincture, 0.1 kg of musk tincture and 1.26 kg of 96% edible alcohol, adding 1.5 kg of the mixture into a brown laboratory bottle, and slowly stirring until the essential oil and the tincture are completely dissolved in the alcohol.
6. The mixture in the brown laboratory bottle is kept still for 90 days, the mixture is rocked once every 7 days for 5 minutes, the brown laboratory bottle is placed into a refrigerator after 90 days, the temperature is set to be 4 ℃, after the mixture is placed for 12 hours, the brown laboratory bottle can see solid flocculent or snowflake-shaped objects, and then the mixture is filtered, so that pure golden yellow perfume, natural plant perfume, first-class taste and cardiotonic glycol can be obtained.
Example 2
A preparation method of durable agilawood sandalwood perfume comprises the following steps:
1. preparing 8 kg of wild agilawood raw material, and grinding the raw material into 50 mesh powder;
8 kg of the Indian sonel sandalwood raw material is prepared and ground into 50 mesh powder;
preparing 0.8 kg of ambergris raw material, grinding into 25 meshes, soaking 0.8 kg of ambergris powder in 1.2 kg of 96% edible alcohol for 80 days, and filtering to obtain 0.3 kg of ambergris tincture;
preparing musk raw material 0.004 kg, soaking musk raw material 0.004 kg in 96% edible alcohol 0.08 kg for 90 days, filtering, and preparing musk tincture 0.084 kg.
2. Extracting the wild agilawood raw material powder by a supercritical carbon dioxide extraction method, wherein the extraction conditions are as follows: the extraction column is 25Mpa, and the temperature is: 35 degrees celsius, separation column: 6Mpa, the carbon dioxide flow is: 20L/h for 1.8 hours, and 0.018 kg of the obtained essential oil is extracted;
3. extracting the raw materials of the Inanel sandalwood by a supercritical carbon dioxide extraction method under the following extraction conditions: the extraction column is 28Mpa, and the temperature is: 38 degrees celsius, separation column: 7Mpa, the carbon dioxide flow is: 21L/h, the extraction time is 2 hours, and 0.022 kg of the obtained sandalwood essential oil is extracted;
4. using the above obtained 0.018 kg of heavy essential oil, 0.018 kg g was taken for use: 0.022 kg of sandalwood essential oil and 0.018 kg of sandalwood essential oil are taken for standby; 0.3 kg of ambergris tincture and 0.1 kg of ambergris tincture are taken for standby; 0.084 kg of musk tincture and 0.08 kg of musk tincture are taken for standby.
5. Mixing 0.018 kg of lignum Aquilariae Resinatum essential oil, 0.018 kg of lignum Santali albi essential oil, 0.1 kg of ambergris tincture, 0.08 kg of Moschus tincture with 1.22 kg of 96% edible alcohol, adding 1.436 kg into brown laboratory bottle, and slowly stirring until the essential oil and tincture are completely dissolved in alcohol.
6. The mixture in the brown laboratory bottle is kept still for 80 days, the mixture is rocked once every 5 days for 8 minutes, the brown laboratory bottle is placed into a refrigerator after 80 days, the temperature is set to be 3 ℃, after the mixture is placed for 10 hours, the brown laboratory bottle can see solid flocculent or snowflake-shaped objects, and then the mixture is filtered, so that pure golden yellow perfume, natural plant perfume, first-class taste and cardiotonic glycol can be obtained.
Example 3
A preparation method of durable agilawood sandalwood perfume comprises the following steps:
1. preparing 12 kg of wild agilawood raw material, and grinding the raw material into 70-mesh powder;
12 kg of the Indian sonel sandalwood raw material is prepared and ground into 70 mesh powder;
preparing 1.2 kg of ambergris raw material, grinding into 40 meshes, soaking 1.2 kg of ambergris powder in 0.8 kg of 96% edible alcohol for 100 days, and filtering to obtain 0.5 kg of ambergris tincture;
preparing musk 0.006 kg, soaking 0.006 kg musk in 0.12 kg 96% edible alcohol for 100 days, and filtering to obtain musk tincture 0.11 kg.
2. Extracting the wild agilawood raw material powder by a supercritical carbon dioxide extraction method, wherein the extraction conditions are as follows: the extraction column is 32Mpa, and the temperature is: 42 degrees celsius, separation column: the flow rate of the carbon dioxide is 9 Mpa: 23L/h, the extraction time is 2.2 hours, and 0.025 kg of the obtained essential oil is extracted;
3. extracting the raw materials of the Inanel sandalwood by a supercritical carbon dioxide extraction method under the following extraction conditions: the extraction column is 33Mpa, and the temperature is: 45 degrees celsius, separation column: 10Mpa, the carbon dioxide flow is: 25L/h, the extraction time is 2.5 hours, and 0.035 kg of the obtained sandalwood essential oil is extracted;
4. using the above obtained 0.025 kg of essential oil, 0.025 kg of essential oil is taken for standby: 0.035 kg of sandalwood essential oil and 0.025 kg of sandalwood essential oil are taken for standby; 0.5 kg of ambergris tincture and 0.09 kg of ambergris tincture are taken for standby; 0.11 kg of musk tincture is taken out and 0.11 kg is used.
5. Mixing 0.025 kg of lignum Aquilariae Resinatum essential oil, 0.025 kg of lignum Santali albi essential oil, 0.09 kg of ambergris tincture, 0.11 kg of Moschus tincture with 1.35 kg of 96% edible alcohol, adding 1.6 kg into brown laboratory bottle, and slowly stirring until the essential oil and tincture are completely dissolved in alcohol.
6. The mixture in the brown laboratory bottle is kept still for 100 days, the mixture is rocked once every 10 days for 9 minutes, the brown laboratory bottle is placed into a refrigerator after 100 days, the temperature is set to be 5 ℃, after the mixture is placed for 16 hours, the brown laboratory bottle can see solid flocculent or snowflake-shaped objects, and then the mixture is filtered, so that pure golden yellow perfume, natural plant perfume, first-class taste and cardiotonic glycol can be obtained.
The invention is illustrated by way of example and not by way of limitation. Other variations or modifications of the above description will be apparent to those of ordinary skill in the art, and it is not necessary or exhaustive of all embodiments, and obvious variations or modifications are contemplated as falling within the scope of the invention.
Claims (8)
1. The preparation method of the durable agilawood sandalwood perfume is characterized by comprising the following steps of:
step 1, raw material preparation:
grinding 8-12 parts of agilawood raw materials into 50-70 mesh powder;
grinding 8-12 parts of sandalwood raw materials into 50-70 mesh powder;
step 2, essential oil preparation:
extracting the powdery agilawood raw material in the step 1, wherein 0.02-0.04 part of essential oil is obtained by extraction;
extracting the powdery sandalwood raw material in the step 1, wherein 0.02-0.04 part of sandalwood essential oil is obtained by extraction;
step 3, tincture preparation:
grinding 0.8-1.2 parts of ambergris raw material into powder of 20-40 meshes, soaking ambergris powder in 0.8-1.2 parts of alcohol for 80-100 days, filtering to obtain ambergris tincture of 0.2-0.6 parts;
soaking 0.004-0.006 parts of musk raw material in 0.08-0.12 parts of alcohol for 80-100 days, filtering to prepare musk tincture, and preparing 0.1-0.3 parts of musk tincture;
step 4, mixing and stirring:
adding 0.02-0.04 part of heavy essential oil, 0.02-0.04 part of sandalwood essential oil, 0.2-0.6 part of ambergris tincture, 0.1-0.3 part of musk tincture and 1.22-1.28 parts of alcohol into a mixing bottle, and slowly stirring until the essential oil and the tincture are completely dissolved in the alcohol;
step 5, perfume blending:
standing the mixture in the mixing bottle in the step 4 for 80-100 days, shaking every 5-7 days for 3-6 minutes, placing the mixing bottle in a refrigerator after 80-100 days, setting the temperature to 3-6 ℃, standing for 10-14 hours, enabling the mixing bottle to see solid flocculent or snowflake-shaped objects, and filtering to obtain the natural plant perfume.
2. The method for preparing durable eaglewood sandalwood perfume as described in claim 1, wherein said eaglewood raw material is a wild eaglewood raw material.
3. The method for preparing durable eaglewood sandalwood perfume as described in claim 1, wherein said sandalwood raw material is a material of sonal sandalwood.
4. The method for preparing durable eaglewood sandalwood perfume as described in claim 1, wherein said alcohol is 96% edible alcohol.
5. The method for preparing durable agilawood sandalwood perfume according to claim 1, wherein the powdery agilawood raw material is extracted by a supercritical carbon dioxide extraction method under the following extraction conditions: the extraction column is 28-32Mpa, and the temperature is: 35-45 ℃, separation column: 6-10Mpa, the carbon dioxide flow is: 20-25L/h, the extraction time is 1.5-2.5 hours, and 0.02-0.04 part of the obtained heavy essential oil is extracted.
6. The method for preparing durable agalloch sandalwood perfume according to claim 1, wherein the powdered material of the agalloch sandalwood is extracted by supercritical carbon dioxide extraction under the following conditions: the extraction column is 28-32Mpa, and the temperature is: 35-45 ℃, separation column: 6-10Mpa, the carbon dioxide flow is: 20-25L/h, the extraction time is 1.5-2.5 hours, and 0.022-0.028 parts of the obtained sandalwood essential oil is extracted.
7. The method for preparing durable eaglewood sandalwood perfume as described in claim 1, wherein the mass ratio of eaglewood essential oil to sandalwood essential oil in said mixing bottle is 1:1.
8. The method for preparing durable eaglewood sandalwood perfume as described in claim 1, wherein said mixing flask is a brown laboratory flask.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202310711246.9A CN116549340A (en) | 2023-06-15 | 2023-06-15 | Preparation method of durable agilawood sandalwood perfume |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202310711246.9A CN116549340A (en) | 2023-06-15 | 2023-06-15 | Preparation method of durable agilawood sandalwood perfume |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN116549340A true CN116549340A (en) | 2023-08-08 |
Family
ID=87491704
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202310711246.9A Pending CN116549340A (en) | 2023-06-15 | 2023-06-15 | Preparation method of durable agilawood sandalwood perfume |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN116549340A (en) |
-
2023
- 2023-06-15 CN CN202310711246.9A patent/CN116549340A/en active Pending
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