CN116283430A - Water-soluble fertilizer - Google Patents
Water-soluble fertilizer Download PDFInfo
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- CN116283430A CN116283430A CN202310366805.7A CN202310366805A CN116283430A CN 116283430 A CN116283430 A CN 116283430A CN 202310366805 A CN202310366805 A CN 202310366805A CN 116283430 A CN116283430 A CN 116283430A
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- CN
- China
- Prior art keywords
- water
- soluble fertilizer
- zhongshengmycin
- mixing
- prepared
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 239000003337 fertilizer Substances 0.000 title claims abstract description 33
- VMFXMTJCTSYHCF-HHQUSWFZSA-N [(2r,3r,4s,5r)-5-(hexylamino)-4-hydroxy-2-(hydroxymethyl)-6-[(7-hydroxy-4-oxo-1,3a,5,6,7,7a-hexahydroimidazo[4,5-c]pyridin-2-yl)amino]oxan-3-yl] carbamate Chemical compound CCCCCCN[C@@H]1[C@H](O)[C@@H](OC(N)=O)[C@@H](CO)OC1\N=C\1NC(C(=O)NCC2O)C2N/1 VMFXMTJCTSYHCF-HHQUSWFZSA-N 0.000 claims abstract description 24
- 238000002156 mixing Methods 0.000 claims abstract description 13
- 241000131360 Pythium oligandrum Species 0.000 claims abstract description 12
- 230000001954 sterilising effect Effects 0.000 claims abstract description 10
- 238000004659 sterilization and disinfection Methods 0.000 claims abstract description 10
- PAWQVTBBRAZDMG-UHFFFAOYSA-N 2-(3-bromo-2-fluorophenyl)acetic acid Chemical compound OC(=O)CC1=CC=CC(Br)=C1F PAWQVTBBRAZDMG-UHFFFAOYSA-N 0.000 claims abstract description 4
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 claims abstract description 4
- 239000004327 boric acid Substances 0.000 claims abstract description 4
- 235000010338 boric acid Nutrition 0.000 claims abstract description 4
- RUTXIHLAWFEWGM-UHFFFAOYSA-H iron(3+) sulfate Chemical compound [Fe+3].[Fe+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O RUTXIHLAWFEWGM-UHFFFAOYSA-H 0.000 claims abstract description 4
- 229910000360 iron(III) sulfate Inorganic materials 0.000 claims abstract description 4
- 229940099596 manganese sulfate Drugs 0.000 claims abstract description 4
- 235000007079 manganese sulphate Nutrition 0.000 claims abstract description 4
- 239000011702 manganese sulphate Substances 0.000 claims abstract description 4
- SQQMAOCOWKFBNP-UHFFFAOYSA-L manganese(II) sulfate Chemical compound [Mn+2].[O-]S([O-])(=O)=O SQQMAOCOWKFBNP-UHFFFAOYSA-L 0.000 claims abstract description 4
- 229910000402 monopotassium phosphate Inorganic materials 0.000 claims abstract description 4
- 235000019796 monopotassium phosphate Nutrition 0.000 claims abstract description 4
- GNSKLFRGEWLPPA-UHFFFAOYSA-M potassium dihydrogen phosphate Chemical compound [K+].OP(O)([O-])=O GNSKLFRGEWLPPA-UHFFFAOYSA-M 0.000 claims abstract description 4
- LWIHDJKSTIGBAC-UHFFFAOYSA-K potassium phosphate Substances [K+].[K+].[K+].[O-]P([O-])([O-])=O LWIHDJKSTIGBAC-UHFFFAOYSA-K 0.000 claims abstract description 4
- OTYBMLCTZGSZBG-UHFFFAOYSA-L potassium sulfate Chemical compound [K+].[K+].[O-]S([O-])(=O)=O OTYBMLCTZGSZBG-UHFFFAOYSA-L 0.000 claims abstract description 4
- 229910052939 potassium sulfate Inorganic materials 0.000 claims abstract description 4
- 235000011151 potassium sulphates Nutrition 0.000 claims abstract description 4
- WFLYOQCSIHENTM-UHFFFAOYSA-N molybdenum(4+) tetranitrate Chemical compound [N+](=O)([O-])[O-].[Mo+4].[N+](=O)([O-])[O-].[N+](=O)([O-])[O-].[N+](=O)([O-])[O-] WFLYOQCSIHENTM-UHFFFAOYSA-N 0.000 claims abstract description 3
- 239000000843 powder Substances 0.000 claims description 4
- 239000004563 wettable powder Substances 0.000 claims description 4
- 240000008067 Cucumis sativus Species 0.000 abstract description 16
- 235000010799 Cucumis sativus var sativus Nutrition 0.000 abstract description 14
- 241000233679 Peronosporaceae Species 0.000 abstract description 12
- 201000010099 disease Diseases 0.000 abstract description 9
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 abstract description 9
- 235000015097 nutrients Nutrition 0.000 abstract description 7
- 230000000844 anti-bacterial effect Effects 0.000 abstract description 6
- 230000000694 effects Effects 0.000 abstract description 4
- 206010059866 Drug resistance Diseases 0.000 abstract description 3
- 208000031888 Mycoses Diseases 0.000 abstract description 3
- 239000004480 active ingredient Substances 0.000 abstract description 3
- 230000002195 synergetic effect Effects 0.000 abstract description 3
- 244000052616 bacterial pathogen Species 0.000 abstract description 2
- 239000013589 supplement Substances 0.000 abstract description 2
- 239000003814 drug Substances 0.000 description 7
- 241000233866 Fungi Species 0.000 description 6
- 241000196324 Embryophyta Species 0.000 description 4
- 241000223198 Humicola Species 0.000 description 4
- 239000003795 chemical substances by application Substances 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- 150000001875 compounds Chemical class 0.000 description 3
- 229940079593 drug Drugs 0.000 description 3
- 238000011835 investigation Methods 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 239000000575 pesticide Substances 0.000 description 3
- 238000005507 spraying Methods 0.000 description 3
- 239000000725 suspension Substances 0.000 description 3
- 235000009849 Cucumis sativus Nutrition 0.000 description 2
- 241000238631 Hexapoda Species 0.000 description 2
- 241000607479 Yersinia pestis Species 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 206010003883 azoospermia Diseases 0.000 description 2
- 238000011081 inoculation Methods 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 208000008634 oligospermia Diseases 0.000 description 2
- 230000036616 oligospermia Effects 0.000 description 2
- 231100000528 oligospermia Toxicity 0.000 description 2
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 description 2
- 229920000053 polysorbate 80 Polymers 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 230000001018 virulence Effects 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 1
- 241000219104 Cucurbitaceae Species 0.000 description 1
- 241000936613 Peronospora farinosa Species 0.000 description 1
- 241001281805 Pseudoperonospora cubensis Species 0.000 description 1
- 241000235547 Rhizopus microsporus var. oligosporus Species 0.000 description 1
- 235000000471 Rhizopus oligosporus Nutrition 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 238000012271 agricultural production Methods 0.000 description 1
- 238000007605 air drying Methods 0.000 description 1
- 230000008485 antagonism Effects 0.000 description 1
- 239000003899 bactericide agent Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000004166 bioassay Methods 0.000 description 1
- 238000004364 calculation method Methods 0.000 description 1
- 239000013043 chemical agent Substances 0.000 description 1
- 238000007405 data analysis Methods 0.000 description 1
- 239000000645 desinfectant Substances 0.000 description 1
- 238000007865 diluting Methods 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000003306 harvesting Methods 0.000 description 1
- 238000005286 illumination Methods 0.000 description 1
- 208000015181 infectious disease Diseases 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 238000012417 linear regression Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000007619 statistical method Methods 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/60—Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Plant Pathology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention belongs to the technical field of fertilizers, and particularly relates to a water-soluble fertilizer. The water-soluble fertilizer is prepared by mixing 80-97% of water-soluble fertilizer and the balance of sterilization components in percentage by mass; wherein the water-soluble fertilizer is selected from one or more of ammonium nitrate, molybdenum nitrate, monopotassium phosphate, boric acid, potassium sulfate, ferric sulfate and manganese sulfate; the sterilization component is prepared by mixing the pythium oligandrum and the Zhongshengmycin. The water-soluble fertilizer in the water-soluble fertilizer can provide nutrients for the growth of crops, and the bactericidal component can improve the control effect on fungal diseases such as cucumber downy mildew of crops, so that the water-soluble fertilizer can be applied once to supplement the nutrients and control the diseases. In addition, the bactericidal component is formed by mixing the hypsomyces oligospermis and the Zhongshengmycin, has a co-toxicity coefficient of more than 120 on the cucumber downy mildew, has a synergistic effect, can delay the generation of drug resistance of pathogenic bacteria, reduces the application amount of bactericidal active ingredients and reduces the cost.
Description
Technical Field
The invention belongs to the technical field of fertilizers, and particularly relates to a water-soluble fertilizer.
Background
In agricultural production, the fertilizer can provide nutrients for crops, and the pesticide can prevent and control plant diseases and insect pests; after the fertilizer and the pesticide are mixed according to a certain proportion to prepare the fertilizer, the fertilizer can provide nutrients for crops and can prevent and treat target diseases and insect pests by one-time application.
Cucumber downy mildew is one of the most serious diseases that endanger cucumbers, and is harmful to more than 40 plants of the cucurbitaceae family in addition to infecting cucumbers. Cucumber downy mildew is caused by pseudoperonospora cubensis, can generate a large amount of spores, and can spread far by means of airflow. The cucumber downy mildew mainly damages the leaves of the cucumber, irregular water-immersed spots appear on the back of the leaves at the early stage of infection, the spots are gradually enlarged, gray black mildew layers appear on the back of the leaves with high humidity, the leaf margin is curled and dried, and yield reduction and harvest failure are caused when serious. Chemical agents are the most rapid, accurate and effective control methods, however, when the agents are used for control, the agents are easy to generate drug resistance after single use for a long time. Therefore, it is necessary to study a compound or a mixture for controlling cucumber downy mildew. At present, no report on the mixing of adding the hypsomyces oligospermis and the Zhongshengmycin into the water-soluble fertilizer is seen.
The information disclosed in this background section is only for enhancement of understanding of the general background of the invention and should not be taken as an acknowledgement or any form of suggestion that this information forms the prior art already known to a person of ordinary skill in the art.
Disclosure of Invention
The invention aims to provide a water-soluble fertilizer which can not only provide nutrients for the growth of crops, but also improve the control effect on fungal diseases such as cucumber downy mildew of the crops.
In order to achieve the above purpose, the present invention provides the following technical solutions:
the water-soluble fertilizer is prepared by mixing 80-97% of water-soluble fertilizer and the balance of sterilization components in percentage by mass; wherein the water-soluble fertilizer is selected from one or more of ammonium nitrate, molybdenum nitrate, monopotassium phosphate, boric acid, potassium sulfate, ferric sulfate and manganese sulfate; the sterilization component is prepared by mixing the pythium oligandrum and the Zhongshengmycin.
Preferably, the humicola oligospermia is humicola oligospermia wettable powder of 100 megaspores/gram; the Zhongshengmycin is soluble powder with the mass fraction of 6 percent.
Preferably, the mass ratio of the hypsomyces oligospermicus to the Zhongshengmycin is 1-20:20-1.
Compared with the prior art, the invention has the following beneficial effects:
(1) The water-soluble fertilizer is formed by mixing the water-soluble fertilizer and the sterilization component, wherein the water-soluble fertilizer can provide nutrients for the growth of crops, and the sterilization component can improve the control effect on fungal diseases such as cucumber downy mildew of crops, so that the water-soluble fertilizer can be applied once to supplement the nutrients and prevent and treat the diseases.
(2) The bactericidal component is prepared by mixing the oligandrum mould and the Zhongshengmycin, has a co-toxicity coefficient of more than 120 on the cucumber downy mildew, has a synergistic effect, can delay the generation of drug resistance of pathogenic bacteria, reduces the application amount of bactericidal active ingredients and reduces the cost.
Detailed Description
The following is a clear and complete description of the technical solutions of the present patent. All other embodiments, which can be made by those skilled in the art based on the embodiments of the present invention without making any inventive effort, are intended to fall within the scope of the present invention.
Example 1: potted plant test for drug mixing
1. Test crop
The cucumber variety Jinchun No. four is cultivated in a pot until 4-6 true leaves are obtained, and each pot is provided with 2 plants for standby.
2. Test agent
100 Ten thousand spores/gram of the wettable powder of the pythium oligandrum (Czech biological preparation Co., ltd., accession number: PD 20131756)
Zhongshengmycin soluble powder with mass fraction of 6% (Fujian Kaili biological products Co., ltd., registration number: PD 20211024)
3. Test method (refer to NY/T1156.7-2006 "pesticide indoor biological assay test criterion Bactericide part 7: potted method for controlling cucumber downy mildew
3.1. Preparation of spore suspension: selecting disease source leaf, washing leaf back surface with distilled water at 4deg.C to obtain sporangium of Peronospora farinosa 1×10 6 The sporangia/mL suspension is ready for use;
3.2 preparing a medicament: 1000mg/L (the mass fraction of the pythium oligandrum is 100%) of the active ingredients of the pythium oligandrum and the Zhongshengmycin are prepared, then a plurality of groups of proportions are arranged, and each single dose and the proportion mixture are diluted into 5 mass concentration gradients by using a tween-80 aqueous solution with the mass fraction of 0.1%.
3.3 inoculation and drug treatment: spraying and inoculating fresh spore suspension to the back of the leaf of the tested crop, uniformly spraying the liquid medicine on the two sides of the leaf of the tested crop after 24 hours of inoculation until the leaf is totally wet, repeating each treatment for 5 basins and 3 times, and setting the treatment without 0.1% Tween-80 aqueous solution as a blank control; after natural air drying, the mixture is transferred to a thermostatic chamber, and cultured under the conditions that the temperature is 22 ℃ and the illumination/darkness is alternated for 12 hours and the relative humidity is 95 percent.
3.4 investigation and calculation:
and when the leaf disease rate of the blank control reaches more than 80%, carrying out grading investigation on the seed leaves, and calculating individual treatment disease indexes and control effects according to investigation results. Wherein, the grading standard is shown in Table 1.
TABLE 1 disease grade assessment criteria
4. Data analysis: performing data statistical analysis by adopting DPS software, and performing linear regression with the disinfectant concentration logarithmic value x and the corresponding control efficiency numerical value y to obtain a virulence regression equation and virulence EC of the medicament on target bacteria 50 Values and co-toxicity coefficients (CTCs) were calculated according to the grand cloud Pei method.
5. Evaluation of drug efficacy
The synergy of the agents was evaluated based on the calculated co-toxicity coefficient (CTC), CTC.ltoreq.80 being antagonism, CTC.ltoreq.120 being additive, CTC.ltoreq.120 being synergy, the results being shown in Table 2.
Table 2 indoor bioactivity of oligandrum mold and mesogenic fungi compounded on cucumber downy mildew
Medicament name and ratio | EC 50 (mg/L) | ATI | TTI | CTC |
Pythium oligandrum | 98.6527 | 100.00 | -- | -- |
Zhongshengmycin | 2.9006 | 3401.1136 | -- | -- |
Oligoandrum rot fungi 1: zhongshengmycin 20 | 1.4044 | 7024.5443 | 3243.9177 | 216.5451 |
Oligoandrum rot fungi 1: zhongshengmycin 10 | 1.3268 | 7435.3859 | 3101.0123 | 239.7729 |
Oligoandrum rot fungi 1: zhongshengmycin 5 | 2.3941 | 4120.6591 | 2850.9280 | 144.5375 |
Oligoandrum rot fungi 1: zhongshengmycin 1 | 3.4543 | 2855.9390 | 1750.5568 | 163.1446 |
Oligoandrum rot fungi 5: zhongshengmycin 1 | 8.4513 | 1167.3080 | 650.1856 | 179.5346 |
Rhizopus oligosporus 10: zhongshengmycin 1 | 18.1445 | 543.7058 | 400.1012 | 135.8921 |
Pythium oligandrum 20: zhongshengmycin 1 | 25.4500 | 387.6334 | 257.1959 | 150.7152 |
As shown in table 2, after the mixture of the hypsomyces oligospermis and the Zhongshengmycin, the mass ratio is 1-20: the co-toxicity coefficient of the compound for cucumber downy mildew in 20-1 is more than 120, and the compound shows synergistic effect.
Example 2
The water-soluble fertilizer is prepared by mixing 97% of water-soluble fertilizer and the balance of sterilization components in percentage by mass; wherein, the water-soluble fertilizer is prepared from ammonium nitrate, monopotassium phosphate, boric acid, potassium sulfate, ferric sulfate and manganese sulfate according to the proportion of 1:3:5:2:1:1, a step of; the sterilization component is prepared by mixing the pythium oligandrum and the Zhongshengmycin according to the proportion of 1:10, wherein the humicola oligospermi is 100 megaspores/gram of humicola oligospermi wettable powder; the Zhongshengmycin is Zhongshengmycin soluble powder with the mass fraction of 6 percent.
The using mode is as follows: and diluting with proper amount of clear water, and spraying on leaf surface.
The foregoing descriptions of specific exemplary embodiments of the present invention are presented for purposes of illustration and description. It is not intended to limit the invention to the precise form disclosed, and obviously many modifications and variations are possible in light of the above teaching. The exemplary embodiments were chosen and described in order to explain the specific principles of the invention and its practical application to thereby enable one skilled in the art to make and utilize the invention in various exemplary embodiments and with various modifications as are suited to the particular use contemplated. It is intended that the scope of the invention be defined by the claims and their equivalents.
Claims (3)
1. The water-soluble fertilizer is characterized by being prepared by mixing 80-97% of water-soluble fertilizer and the balance of sterilization components in percentage by mass; wherein the water-soluble fertilizer is selected from one or more of ammonium nitrate, molybdenum nitrate, monopotassium phosphate, boric acid, potassium sulfate, ferric sulfate and manganese sulfate;
the sterilization component is prepared by mixing the pythium oligandrum and the Zhongshengmycin.
2. The water-soluble fertilizer of claim 1, wherein the pythium oligandrum is 100 megaspores/gram of pythium oligandrum wettable powder; the Zhongshengmycin is Zhongshengmycin soluble powder with the mass fraction of 6 percent.
3. The water-soluble fertilizer according to claim 1, wherein the mass ratio of the pythium oligandrum to the zhongshengmycin is 1-20:20-1.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202310366805.7A CN116283430A (en) | 2023-04-07 | 2023-04-07 | Water-soluble fertilizer |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202310366805.7A CN116283430A (en) | 2023-04-07 | 2023-04-07 | Water-soluble fertilizer |
Publications (1)
Publication Number | Publication Date |
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CN116283430A true CN116283430A (en) | 2023-06-23 |
Family
ID=86797887
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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CN202310366805.7A Pending CN116283430A (en) | 2023-04-07 | 2023-04-07 | Water-soluble fertilizer |
Country Status (1)
Country | Link |
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CN (1) | CN116283430A (en) |
-
2023
- 2023-04-07 CN CN202310366805.7A patent/CN116283430A/en active Pending
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