CN1161839A - Technology for extracting effective component of matsutake - Google Patents
Technology for extracting effective component of matsutake Download PDFInfo
- Publication number
- CN1161839A CN1161839A CN96100532A CN96100532A CN1161839A CN 1161839 A CN1161839 A CN 1161839A CN 96100532 A CN96100532 A CN 96100532A CN 96100532 A CN96100532 A CN 96100532A CN 1161839 A CN1161839 A CN 1161839A
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- lmai
- lto
- singer
- tricholoma matsutake
- active ingredient
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- Coloring Foods And Improving Nutritive Qualities (AREA)
- Preparation Of Fruits And Vegetables (AREA)
Abstract
The present invention provides a technological process for extracting effective components of matsutake. Said technological process includes such procedures of cleaning raw material, pulverizing, extracting, filtering, concentrating and drying so as to obtain its effective components: matsutake polysaccharose and several amino acids.
Description
The present invention relates to the extraction of mushroom active ingredient, particularly the extraction of Tricholoma matsutake (lto et lmai) Singer active ingredient.
Tricholoma matsutake (lto et lmai) Singer (Triclcolma matsutake) belongs to Basidiomycetes, Agaricales, and mouthful mill section, a mouthful mill belongs to.This mushroom body hypertrophy, fine and tender taste, aromatic flavor, other tool local flavor has very high nutritive value and special medicinal effects.But always all be bright product of Shiqi and dry product, and bright grade is perishable rotten, though dry product can be preserved inconvenient eating the long period.
The object of the present invention is to provide a kind of process of extracting the active ingredient of Tricholoma matsutake (lto et lmai) Singer, make it can become medicine, health product raw material and food flavor
The blazei polysaccharide that Tricholoma matsutake (lto et lmai) Singer had (Tricholo-ma mat sutake polysaccharide) is the effective constituent that mainly contains of Tricholoma matsutake (lto et lmai) Singer, and blazei polysaccharide is water miscible, but at high temperature can destroy its composition, and technical process of the present invention for this reason is as follows:
Tricholoma matsutake (lto et lmai) Singer active ingredient extraction process:
A, employing Tricholoma matsutake (lto et lmai) Singer are done raw material;
B, cleaning, pulverizing;
C, the Tricholoma matsutake (lto et lmai) Singer after will pulverizing add 1-4 doubly to the water of Tricholoma matsutake (lto et lmai) Singer volume, are warmed to more than 50 ℃ below the boiling point, keep this temperature 1-5 hour, leach liquid;
D, repeat above-mentioned c point 1-4 time;
E, merging leach liquid;
F, concentrated filtrate get concentrated solution.
Because Tricholoma matsutake (lto et lmai) Singer active ingredient blazei polysaccharide is to be present in intracellular polysaccharide, claim intracellular polysaccharide again, its character is water miscible, the aqueous solvent permeate through cell membranes enters in the cell dissolves blazei polysaccharide, though material can only be flowed to the low concentration direction by high concentration, when blazei polysaccharide content in the cell during with extracellular equating, more blazei polysaccharide just can't extract, at this moment the solvent that just need more renew continues to extract, and when extracting, the temperature and time of extraction is to be mutually related, and temperature is high, and to extract the required time short, but destroy the blazei polysaccharide composition when temperature is too high easily, crossing when low one is that extraction time is long, the 2nd, cause that easily Tricholoma matsutake (lto et lmai) Singer is rotten and influence product quality that first time extraction time is the longest, below successively decrease successively several times, so above-mentioned technology will repeat the C point repeatedly.
In the concentrated solution that makes by said method, blazei polysaccharide is a main component, also contains several amino acids, and concentrated solution can directly use, and also can further pass through spray drying, and obtain powdered Tricholoma matsutake (lto et lmai) Singer crystalline substance.
Above-mentioned used aqueous solvent can be used deionized water, merges to leach behind the liquid to more purified especially filtrate, can adopt the vacuum filtration process, can adopt the cryoconcentration means that reduce pressure during concentrated solution.
The advantage of this technology is that abstract has kept whole effective ingredient of Tricholoma matsutake (lto et lmai) Singer substantially, for the deep development of Tricholoma matsutake (lto et lmai) Singer provides a kind of means, particularly makes the medicinal and health care of Tricholoma matsutake (lto et lmai) Singer that the high concentration raw material is provided.
Below by embodiment the present invention is described further.
Example one, a pulverizes Tricholoma matsutake (lto et lmai) Singer in the extraction pot of packing into, the deionized water that adds 2 times of Tricholoma matsutake (lto et lmai) Singer raw material volumes, be warmed to 80 ℃ and kept temperature 3 hours, extract and filter, collect filtrate, in extraction pot, add deionized water again with the equal volume first time, be warmed to 80 ℃ and kept temperature 2 hours, extract and filter, collect filtrate, in extraction pot, add deionized water again with the equal volume first time, be warmed to 80 ℃, and kept temperature 1 hour, extract and filter, collect filtrate, the impurity that the merging of the filtrate of three collections is eliminated in the filtrate with vacuum filtration has good dissolubility to guarantee finished product.
Filtrate behind b, the sucking filtration is put into jacketed pan and is concentrated, and temperature can not be higher than 80 ℃, and (decompression) reduction boiling point of also jacketed pan can being found time is crossed to seethe with excitement in the time of 60 ℃ and carried out spissated purpose, and 10-20/one who is concentrated to the filtrate original volume gets final product.
Example two, carry out example one step after, with tower spray dryer on the concentrated solution, be spray dried to powdery.
Claims (5)
1, Tricholoma matsutake (lto et lmai) Singer active ingredient extraction process is characterized in that:
A, employing Tricholoma matsutake (lto et lmai) Singer are done raw material;
B, cleaning, pulverizing;
C, the Tricholoma matsutake (lto et lmai) Singer after will pulverizing add 1-4 doubly to the water of Tricholoma matsutake (lto et lmai) Singer volume, are warmed to that boiling point is following more than 50 ℃ kept temperature 1-5 hour, leach liquid;
D, repeat above-mentioned c point 1-4 time;
E, merging leach liquid;
F, the liquid filtrate of contracting gets concentrated solution.
2, Tricholoma matsutake (lto et lmai) Singer active ingredient extraction process according to claim 1 is characterized in that the gained concentrated solution can further obtain powder by spray drying.
3, Tricholoma matsutake (lto et lmai) Singer active ingredient extraction process according to claim 1, the water that it is characterized in that adding in the Tricholoma matsutake (lto et lmai) Singer after the pulverizing is meant from Yu Shui
4, Tricholoma matsutake (lto et lmai) Singer active ingredient extraction process according to claim 1 is characterized in that concentrated filtrate is to adopt decompression cryoconcentration mode.
5, Tricholoma matsutake (lto et lmai) Singer active ingredient extraction process according to claim 1 is characterized in that also adopting vacuum filtration to remove non-solubility impurity after merging leaches liquid.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN96100532A CN1161839A (en) | 1996-04-08 | 1996-04-08 | Technology for extracting effective component of matsutake |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN96100532A CN1161839A (en) | 1996-04-08 | 1996-04-08 | Technology for extracting effective component of matsutake |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1161839A true CN1161839A (en) | 1997-10-15 |
Family
ID=5116642
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN96100532A Pending CN1161839A (en) | 1996-04-08 | 1996-04-08 | Technology for extracting effective component of matsutake |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1161839A (en) |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102334707A (en) * | 2010-07-21 | 2012-02-01 | 张荣连 | Tricholoma matsutake beverage and preparation method thereof |
| CN101748153B (en) * | 2010-01-26 | 2012-06-06 | 四川大学 | Utilizing high-yield selenium-rich function hybridization red rice bran self-fermentation broth for producing tricholoma matsutake polysaccharose |
| CN103070388A (en) * | 2013-02-04 | 2013-05-01 | 云南茂昽生物科技有限公司 | Delicate tricholoma matsutake active extract and preparation method and application thereof |
| CN103461572A (en) * | 2013-09-18 | 2013-12-25 | 么宏伟 | Tricholoma matsutake instant drink and processing method thereof |
| CN104824632A (en) * | 2015-05-15 | 2015-08-12 | 四川食为天农业有限公司 | Preparation method of tricholoma matsutake extracting solution freeze-dried powder |
| CN105454815A (en) * | 2014-10-20 | 2016-04-06 | 大连三肽生物科技有限公司 | Freeze-dried tricholoma matsutake powder preparation method |
| CN107149139A (en) * | 2016-03-04 | 2017-09-12 | 北京圣伦食品有限公司 | A kind of preparation method for clarifying instant matsutake powder |
| CN109875106A (en) * | 2019-03-20 | 2019-06-14 | 福建绿色黄金生物科技有限公司 | Composition, preparation method and applications |
-
1996
- 1996-04-08 CN CN96100532A patent/CN1161839A/en active Pending
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101748153B (en) * | 2010-01-26 | 2012-06-06 | 四川大学 | Utilizing high-yield selenium-rich function hybridization red rice bran self-fermentation broth for producing tricholoma matsutake polysaccharose |
| CN102334707A (en) * | 2010-07-21 | 2012-02-01 | 张荣连 | Tricholoma matsutake beverage and preparation method thereof |
| CN103070388A (en) * | 2013-02-04 | 2013-05-01 | 云南茂昽生物科技有限公司 | Delicate tricholoma matsutake active extract and preparation method and application thereof |
| CN103070388B (en) * | 2013-02-04 | 2014-06-04 | 云南茂昽生物科技有限公司 | Delicate tricholoma matsutake active extract and preparation method and application thereof |
| CN103461572A (en) * | 2013-09-18 | 2013-12-25 | 么宏伟 | Tricholoma matsutake instant drink and processing method thereof |
| CN103461572B (en) * | 2013-09-18 | 2014-10-15 | 么宏伟 | Tricholoma matsutake instant drink and processing method thereof |
| CN105454815A (en) * | 2014-10-20 | 2016-04-06 | 大连三肽生物科技有限公司 | Freeze-dried tricholoma matsutake powder preparation method |
| CN104824632A (en) * | 2015-05-15 | 2015-08-12 | 四川食为天农业有限公司 | Preparation method of tricholoma matsutake extracting solution freeze-dried powder |
| CN104824632B (en) * | 2015-05-15 | 2017-04-19 | 四川食为天农业有限公司 | Preparation method of tricholoma matsutake extracting solution freeze-dried powder |
| CN107149139A (en) * | 2016-03-04 | 2017-09-12 | 北京圣伦食品有限公司 | A kind of preparation method for clarifying instant matsutake powder |
| CN109875106A (en) * | 2019-03-20 | 2019-06-14 | 福建绿色黄金生物科技有限公司 | Composition, preparation method and applications |
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