CN116115514B - Hair-care plant protein composition and preparation method and application thereof - Google Patents

Hair-care plant protein composition and preparation method and application thereof Download PDF

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CN116115514B
CN116115514B CN202310347072.2A CN202310347072A CN116115514B CN 116115514 B CN116115514 B CN 116115514B CN 202310347072 A CN202310347072 A CN 202310347072A CN 116115514 B CN116115514 B CN 116115514B
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hair
essential oil
protein composition
vegetable protein
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CN116115514A (en
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刘伟
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Guangzhou Meisi Biotechnology Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • A61K8/645Proteins of vegetable origin; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • A61K8/65Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • A61K8/66Enzymes
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/002Preparations for repairing the hair, e.g. hair cure
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/02Preparations for cleaning the hair
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/12Preparations containing hair conditioners
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Dermatology (AREA)
  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Cosmetics (AREA)

Abstract

The invention relates to the field of washing and caring products, and in particular provides a plant protein composition for hair care, a preparation method and application thereof, wherein the plant protein composition comprises the following components in parts by weight: 1-3 parts of lauryl dimethyl ammonium hydroxypropyl hydrolyzed keratin, 1-3 parts of hydrolyzed vegetable protein PG-propylsilanetriol, 2-4 parts of hydrolyzed hair keratin, 0.5-5 parts of elastin, 6-7 parts of plant essential oil and 0.01-0.1 part of complex enzyme; according to the invention, hydrolyzed keratin is added as an active ingredient, and plant essential oil is added to promote permeation and synergistic effect, so that damaged hair can be repaired pertinently, meanwhile, hair care cores and hair scales are nourished and repaired, and complex enzyme is used for catalytic repair, so that the hair is smooth and glossy, full of elasticity and is healthier.

Description

Hair-care plant protein composition and preparation method and application thereof
Technical Field
The invention relates to the field of washing and caring, in particular to a plant protein composition for hair care and a preparation method and application thereof.
Background
The hair is damaged due to various styling designs such as ironing, dyeing, straightening and the like, such as rubbing of a disordered washing product such as a pillow towel on the hair, other factors such as environment and the like, all damage the hair structure, the hair is not an organ with a self-repairing function, nerve cells and blood vessels are not contained, after damage is received, the damage can spread, the hair damage is generally the structure of hair scales is damaged, disulfide bonds of the hair scales are damaged, curling or shedding are carried out, the structure of a fiber component substance a-keratin is damaged, the mechanical property of the hair is reduced, and the hair is easy to break.
At present, many hair care products on the market repair the hair scales on the surface of the hair through chemical substances, the repair effect is not ideal, and the hair quality is not improved fundamentally.
Disclosure of Invention
Based on the technical problems, the invention has the technical effects that: the added hydrolyzed keratin developed by adopting a bionic technology has the component peptide sequence consistent with the naturally-occurring peptide sequence of the hairline, so that the different damage degree parts of the hairline can be intelligently identified, the different damage degree parts can be directionally repaired, meanwhile, the hairline fibers can be penetrated and reinforced, the strength of the hairline scales is externally wrapped and reinforced, the damaged hairline is repaired, and the strength and the toughness of the hair are improved;
the plant essential oil extracted from fir, cedar and tea tree is added, and the plant essential oil and hydrolyzed keratin act synergistically to promote the hydrolyzed keratin to act on hair penetration;
the invention adds complex enzyme, which is composed of alanine aminotransferase and aminopeptidase, and plays a role in catalyzing and repairing the whole hair repairing process of hydrolyzed keratin.
The technical scheme provided by the invention is as follows:
the invention provides a plant protein composition for hair care, which comprises the following components in parts by weight: 1-3 parts of lauryl dimethyl ammonium hydroxypropyl hydrolyzed keratin, 1-3 parts of hydrolyzed vegetable protein PG-propyl silanetriol, 2-4 parts of hydrolyzed hair keratin, 0.5-5 parts of elastin, 6-7 parts of plant essential oil and 0.01-0.1 part of complex enzyme.
Further investigation, it comprises the following components by weight: 2 parts of lauryl dimethyl ammonium hydroxypropyl hydrolyzed keratin, 2 parts of hydrolyzed vegetable protein PG-propyl silanetriol, 3 parts of hydrolyzed hair keratin, 0.5-5 parts of elastin, 6 parts of plant essential oil and 0.05 part of complex enzyme.
Further studied, the complex enzyme is alanine aminotransferase and aminopeptidase, and the mass ratio of the alanine aminotransferase to the aminopeptidase is 1:1-1.6.
Further studied, the complex enzyme is alanine aminotransferase and aminopeptidase, and the mass ratio of the alanine aminotransferase to the aminopeptidase is 1:1.3.
further researched, the plant essential oil is fir essential oil, cedar essential oil and tea tree essential oil.
Further researched, the preparation method of the plant essential oil comprises the following steps: pulverizing branches and leaves of fir, cedar and tea tree, adding water with volume multiple of 8-10, performing heat extraction for 1-3 hr, adding sodium chloride with mass multiple of 0.2-0.3, performing secondary heat extraction for 4-6 hr, filtering, and steaming to obtain plant essential oil; the mass ratio of the fir to the cedar to the tea tree is 1-3:1:2-4.
Further, the extraction temperature of the heat extraction was 70-80 ℃.
Further, the preparation method of the hair care vegetable protein composition comprises the following steps: and (3) weighing all the components in parts by weight, adding the components into a homogenizing pot, and homogenizing and heating to obtain the vegetable protein composition.
In a further study, the heating temperature of the homogenizing heating is 50-60 ℃, and the homogenizing heating time is 1-3h.
Further, the use of a vegetable protein composition for hair care in hair care products and hair care products has been studied.
The beneficial effects are that: according to the invention, hydrolyzed keratin is added as an active ingredient, and plant essential oil is added to promote permeation and synergistic effect, so that damaged hair can be repaired pertinently, meanwhile, hair care cores and hair scales are nourished and repaired, and complex enzyme is used for catalytic repair, so that the hair is smooth and glossy, full of elasticity and is healthier.
Description of the embodiments
The invention is illustrated below by way of specific examples, which are chosen to illustrate and explain the invention only and are not intended to limit the invention.
Example 1
The embodiment provides a plant protein composition for hair care, which comprises the following components in parts by weight: 2 parts of lauryl dimethyl ammonium hydroxypropyl hydrolyzed keratin, 2 parts of hydrolyzed vegetable protein PG-propylsilanetriol, 3 parts of hydrolyzed hair keratin, 3 parts of elastin, 6 parts of plant essential oil and 0.05 part of complex enzyme.
The compound enzyme is alanine aminotransferase and aminopeptidase, and the mass ratio of the alanine aminotransferase to the aminopeptidase is 1:1.3.
the plant essential oil is fir essential oil, cedar essential oil, tea tree essential oil.
The preparation method of the plant essential oil comprises the following steps: pulverizing branches and leaves of fir, cedar and tea tree, adding water with volume multiple of 9, performing heat extraction for 2h, adding sodium chloride with mass multiple of 0.2, performing secondary heat extraction for 5h, filtering, and steaming to obtain plant essential oil; the mass ratio of the fir to the cedar to the tea tree is 2:1:3.
the extraction temperature of the heat extraction is 70-80 ℃.
The preparation method of the hair care plant protein composition comprises the following steps: and (3) weighing all the components in parts by weight, adding the components into a homogenizing pot, and homogenizing and heating to obtain the vegetable protein composition.
The heating temperature of the homogenizing heating is 55 ℃, and the homogenizing heating time is 2 hours.
Example 2
The embodiment provides a plant protein composition for hair care, which comprises the following components in parts by weight: 1 part of lauryl dimethyl ammonium hydroxypropyl hydrolyzed keratin, 1 part of hydrolyzed vegetable protein PG-propyl silanetriol, 2 parts of hydrolyzed hair keratin, 0.5 part of elastin, 6 parts of plant essential oil and 0.01 part of complex enzyme.
The compound enzyme is alanine aminotransferase and aminopeptidase, and the mass ratio of the alanine aminotransferase to the aminopeptidase is 1:1.
the plant essential oil is fir essential oil, cedar essential oil, tea tree essential oil.
The preparation method of the plant essential oil comprises the following steps: pulverizing branches and leaves of fir, cedar and tea tree, adding water with volume multiple of 8, performing heat extraction for 1 hr, adding sodium chloride with mass multiple of 0.2, performing secondary heat extraction for 4 hr, filtering, and steaming to obtain plant essential oil; the mass ratio of the fir to the cedar to the tea tree is 1:1:2.
the extraction temperature of the heat extraction is 70 ℃.
The preparation method of the hair care plant protein composition comprises the following steps: and (3) weighing all the components in parts by weight, adding the components into a homogenizing pot, and homogenizing and heating to obtain the vegetable protein composition.
The heating temperature of the homogenizing heating is 50 ℃, and the homogenizing heating time is 1h.
Example 3
The embodiment provides a plant protein composition for hair care, which comprises the following components in parts by weight: 3 parts of lauryl dimethyl ammonium hydroxypropyl hydrolyzed keratin, 3 parts of hydrolyzed vegetable protein PG-propyl silanetriol, 4 parts of hydrolyzed hair keratin, 5 parts of elastin, 7 parts of plant essential oil and 0.1 part of complex enzyme.
The compound enzyme is alanine aminotransferase and aminopeptidase, and the mass ratio of the alanine aminotransferase to the aminopeptidase is 1:6.
the plant essential oil is fir essential oil, cedar essential oil, tea tree essential oil.
The preparation method of the plant essential oil comprises the following steps: pulverizing branches and leaves of fir, cedar and tea tree, adding water with volume multiple of 10, performing heat extraction for 3 hr, adding sodium chloride with mass multiple of 0.3, performing secondary heat extraction for 6 hr, filtering, and steaming to obtain plant essential oil; the mass ratio of the fir to the cedar to the tea tree is 3:1:4.
the extraction temperature of the heat extraction is 80 ℃.
The preparation method of the hair care plant protein composition comprises the following steps: and (3) weighing all the components in parts by weight, adding the components into a homogenizing pot, and homogenizing and heating to obtain the vegetable protein composition.
The heating temperature of the homogenizing heating is 60 ℃, and the homogenizing heating time is 3 hours.
Comparative example 1
Comparative example 1 differs from example 1 in that comparative example 1 does not add hydrolyzed vegetable protein PG-propylsilanetriol.
Comparative example 2
Comparative example 2 differs from example 1 in that comparative example 2 does not add lauryl dimethyl ammonium hydroxypropyl hydrolyzed keratin.
Comparative example 3
Comparative example 3 is different from example 1 in that comparative example 3 does not add a plant essential oil.
Comparative example 4
Comparative example 4 is different from example 1 in that the preparation method of the plant essential oil of comparative example 4 is different in that: pulverizing branches and leaves of fir, cedar and tea tree, adding ethanol with volume multiple of 9 and mass fraction of 60%, heating and reflux extracting for 2 hr, filtering, and decompressing and compressing to obtain plant essential oil; the mass ratio of the fir to the cedar to the tea tree is 2:1:3.
the heating reflux extraction temperature is 70-80 ℃.
Comparative example 5
Comparative example 5 differs from example 1 in that comparative example 5 does not add alanine aminotransferase.
Comparative example 6
Comparative example 6 differs from example 1 in that comparative example 6 does not add aminopeptidase.
Several test subjects were prepared with a damaged hair strand of 25m length and 5g weight, and the compositions prepared in examples and comparative examples were mixed with a conventional hair care essential oil at a mixing ratio of 3:7 and applied to the damaged hair strand for performance testing.
1. Dry and wet combability test: the hair care essential oils prepared in examples and comparative examples were adequately applied to the damaged hair strands while the hair was dry and while the hair was wet, respectively, and were tested with a texture analyzer before and after the test.
2. Antistatic test: the potential pressures before and after the care of the hair care essential oils prepared in examples and comparative examples for damaged hair were measured using a vibrating volume potentiometer.
3. Average tensile Strength test the hair care essential oils prepared in examples and comparative examples were applied to damaged hair tresses, 10 of which were tested for tensile strength using a texture tester.
The test results are shown in Table 1.
TABLE 1
Figure SMS_1
As shown in the results of Table 1, the vegetable protein composition prepared by the invention has remarkable restoration effect, and the hair becomes flexible and tough, and the mechanical property of the hair is remarkably improved; from comparative examples 1-2, the active ingredients of the invention consist of lauryl dimethyl ammonium hydroxypropyl hydrolyzed keratin and hydrolyzed vegetable protein PG-propyl silanetriol, which can strengthen the hair core hair fibers and hair scales of damaged hair; as can be seen from comparative examples 3-4, the plant essential oil added in the invention can promote the effective active ingredients to exert the repairing effect and has synergistic effect compared with the plant essential oil prepared by other methods without adding the plant essential oil; as is clear from comparative examples 5 to 6, the invention adds two enzymes to perform composite catalysis, and can catalyze the strengthening and repairing effects of active ingredients on hairlines.
Finally, it should be noted that the above-mentioned embodiments are only for illustrating the technical solution of the present invention and not for limiting the scope of the present invention, and although the present invention has been described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that the technical solution of the present invention may be modified or substituted equally without departing from the spirit and scope of the technical solution of the present invention.

Claims (7)

1. A hair care vegetable protein composition comprising the following components by weight:
1-3 parts of lauryl dimethyl ammonium hydroxypropyl hydrolyzed keratin, 1-3 parts of hydrolyzed vegetable protein PG-propylsilanetriol, 2-4 parts of hydrolyzed hair keratin, 0.5-5 parts of elastin, 6-7 parts of plant essential oil and 0.01-0.1 part of complex enzyme;
the compound enzyme is alanine aminotransferase and aminopeptidase, and the mass ratio of the alanine aminotransferase to the aminopeptidase is 1:1 to 1.6;
the plant essential oil is fir essential oil, cedar essential oil and tea tree essential oil;
the preparation method of the plant essential oil comprises the following steps: pulverizing branches and leaves of fir, cedar and tea tree, adding water with volume multiple of 8-10, performing heat extraction for 1-3 hr, adding sodium chloride with mass multiple of 0.2-0.3, performing secondary heat extraction for 4-6 hr, filtering, and steaming to obtain plant essential oil; the mass ratio of the fir to the cedar to the tea tree is 1-3:1:2-4.
2. A hair care vegetable protein composition according to claim 1, wherein,
comprises the following components in parts by weight: 2 parts of lauryl dimethyl ammonium hydroxypropyl hydrolyzed keratin, 2 parts of hydrolyzed vegetable protein PG-propylsilanetriol, 3 parts of hydrolyzed hair keratin, 3 parts of elastin, 6 parts of plant essential oil and 0.05 part of complex enzyme.
3. The hair care plant protein composition according to claim 1, wherein the complex enzyme is alanine aminotransferase and aminopeptidase, and the mass ratio of alanine aminotransferase to aminopeptidase is 1:1.3.
4. the hair care vegetable protein composition according to claim 1, wherein the extraction temperature of the heat extraction is 70-80 ℃.
5. The hair care vegetable protein composition according to claim 1, wherein the vegetable protein composition is prepared by the following steps: and (3) weighing all the components in parts by weight, adding the components into a homogenizing pot, and homogenizing and heating to obtain the vegetable protein composition.
6. The hair care vegetable protein composition according to claim 5, wherein the heating temperature of the homogenizing heating is 50-60 ℃ and the homogenizing heating time is 1-3 hours.
7. Use of a hair care vegetable protein composition according to any one of claims 1 to 6 in hair care products and hair care products.
CN202310347072.2A 2023-04-04 2023-04-04 Hair-care plant protein composition and preparation method and application thereof Active CN116115514B (en)

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JP4370411B2 (en) * 2003-06-13 2009-11-25 ライオン株式会社 Hair growth agent, hair cosmetic for hair growth and pharmaceutical composition for hair growth
JP2009190985A (en) * 2008-02-12 2009-08-27 Soin:Kk Waving agent for human damaged hair or synthetic protein fiber, and method for waving
US20120058068A1 (en) * 2010-09-02 2012-03-08 Kelly Van Gogh Compositions for repairing and restoring keratin-containing fibers
CN108837003A (en) * 2018-06-25 2018-11-20 陈靈悦 A kind of degradable respiratory tract harmful microbe material and preparation method thereof
CN109394619A (en) * 2018-12-05 2019-03-01 肇庆迪彩日化科技有限公司 A kind of composition and its preparation method and application of anti-scalp and hair aging
CN109464294A (en) * 2018-12-26 2019-03-15 广州蜜妆生物科技有限公司 A kind of hydrolysis of keratin hair conditioner and preparation method thereof
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