CN115869239A - Transparent massage cream with high oil content and preparation method thereof - Google Patents
Transparent massage cream with high oil content and preparation method thereof Download PDFInfo
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- CN115869239A CN115869239A CN202211732287.8A CN202211732287A CN115869239A CN 115869239 A CN115869239 A CN 115869239A CN 202211732287 A CN202211732287 A CN 202211732287A CN 115869239 A CN115869239 A CN 115869239A
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- 238000002360 preparation method Methods 0.000 title abstract description 10
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- Cosmetics (AREA)
Abstract
The invention discloses a transparent massage cream with high oil content and a preparation method thereof, wherein the preparation method comprises the following steps: water, polyglycerol-10 myristate, glycerol, caprylic/capric triglyceride, polydimethylsiloxane, pentaerythritol tetra (ethyl hexanoate), hydrogenated polyisobutene, triglyceride (ethyl hexanoate), erythritol, dipotassium glycyrrhizinate, a purslane extract, a dendrobium nobile extract, p-hydroxyacetophenone, 1,2-hexanediol, a sambucus nigra flower extract. The transparent massage cream prepared by the invention has the appearance of transparent gel, high oil content and lasting massage, and the preparation method thereof. A very mild polyglycerol emulsifier was chosen. The product is stable and easy to apply by adopting the D-phase emulsification method. Promoting skin blood circulation, and relieving skin by adding herba Dendrobii. The purslane has good red-removing effect, and the extract of the Sambucus nigra flower has antioxidant, blood vessel nourishing, and soothing activities.
Description
Technical Field
The invention relates to the technical field of cosmetics, in particular to a transparent massage cream with high oil content and a preparation method thereof.
Background
The massage cream is mainly used for promoting blood circulation and metabolism of skin, and is used for massaging to prevent skin aging and relaxation. Can deeply clean skin, promote blood circulation of face and body, and help nutrition penetration and absorption; moisten skin, provide moisture and nutrition to skin.
At present, the massage cream on the market adopts the following components: the grease type massage cream is prepared from polymer, emulsifier, grease, water, polyalcohol, thickener, chelating agent, neutralizer, perfuming agent, antiseptic, and auxiliary skin conditioner as raw materials, and has uniform and glossy milky appearance due to the addition of the grease. The advantages are that: the addition of the grease can greatly increase the durability of the massage. The disadvantages are as follows: the oil content of the system is generally lower than 70%, and in order to stabilize a large amount of oil, a polymer and an emulsifier are excessively added. But also sacrifice a certain skin feel, and the sticky feeling is better when the mask is used. 2, the water-soluble massage cream adopts water-soluble thickening agent, polyhydric alcohol and modified water-soluble grease as raw materials, as well as chelating agent, neutralizing agent, aromatizing agent, preservative and auxiliary skin conditioning agent. The advantages are that: the skin feeling can be made transparent, and the skin feeling can be well adjusted to keep the appearance transparent, so that the massage time is prolonged, a large amount of polyhydric alcohol is added, the polyhydric alcohol has certain hygroscopicity, and the added amount is too high to absorb the moisture and the heat of the skin, and has certain irritation.
Disclosure of Invention
In order to realize commodity differentiation, the transparent massage cream with high oil content is prepared by adopting a D-phase emulsification method, and belongs to an oil-in-water type massage cream. The transparent skin-care massage cream is prepared by the synergistic effect of the components and a D-phase emulsification method, has a high oil content and a lasting moistening effect, is combined with the advantages of transparent appearance and efficacy additives, effectively ensures the stability of the product, and can effectively promote the efficacy characteristics of relieving and eliminating redness. The nonionic surfactant in the whole formula system prepared by the D-phase emulsification method has low content, so that the cost is saved, and the damage of the surfactant to human skin is reduced.
One of the purposes of the invention is realized by adopting the following technical scheme:
a transparent massage cream with high oil content comprises the following raw materials in parts by weight: 5-15 parts of water, 5-10 parts of polyglycerol-10 myristate, 8-15 parts of glycerol, 10-20 parts of caprylic/capric triglyceride, 15-20 parts of polydimethylsiloxane, 10-25 parts of pentaerythritol tetra (ethyl hexanoate), 10-15 parts of hydrogenated polyisobutene, 15-20 parts of glycerol tri (ethyl hexanoate), 0.5-1 part of erythritol, 0.05-0.1 part of dipotassium glycyrrhizinate, 0.5-1 part of purslane (Portulaca OLERACEA) extract, 0.5-1 part of DENDROBIUM NOBILE (Dendrobii) extract, 0.1-0.5 part of p-hydroxyacetophenone, 0.1-0.5 part of 1,2-hexanediol, and 0.1-0.5 part of SAMBUCUS NIGRA flower extract.
Preferably, the transparent massage cream comprises the following raw materials in parts by weight: 10 parts of water, 8 parts of polyglycerol-10 myristate, 10 parts of glycerol, 20 parts of caprylic/capric triglyceride, 15 parts of polydimethylsiloxane, 10 parts of pentaerythritol tetra (ethyl hexanoate), 15 parts of hydrogenated polyisobutene, 10 parts of triglyceride (ethyl hexanoate), 0.5 part of erythritol, 0.05 part of dipotassium glycyrrhizinate, 0.5 part of purslane (Portulaca OLERACEA) extract, 0.5 part of DENDROBIUM NOBILE (Dendrobium NOBILE) extract, 0.15 part of p-hydroxyacetophenone, 1,2-hexanediol, 0.1 part of SAMBUCUS NIGRA (SAMBUCUS NIGRA) flower extract.
Further, the transparent massage cream also comprises 0.01-0.05 part of an aromatizer, preferably 0.05 part of an aromatizer.
The second purpose of the invention is realized by adopting the following technical scheme:
the preparation method of the transparent massage cream with high oil content comprises the following steps:
1) Respectively dividing the raw materials into an A phase and a B phase, and respectively and uniformly mixing the two phases of the raw materials for later use; wherein, the phase A is: water, polyglycerol-10 myristate, glycerol, erythritol, p-hydroxyacetophenone, dipotassium glycyrrhizinate, herba Portulacae (Portulaca OLERACEA) extract, herba Dendrobii (Dendrobium NOBILE) extract, 1,2-hexanediol, and Sambucus NIGRA (SAMBUCUS NIGRA) flower extract. The phase B is as follows: caprylic/capric triglyceride dimethicone, pentaerythritol tetra (ethyl hexanoate), hydrogenated polyisobutene, glycerol tri (ethyl hexanoate);
2) Adding the phase A raw material into a container, heating to 42-45 ℃, and stirring;
3) And adding the B-phase raw material into the material obtained in the step 2) at a dropping speed of 20-25 drops per minute, uniformly stirring and homogenizing to obtain the transparent massage cream with high oil content.
Further, the raw materials also comprise a phase C, and the phase C is an aromatizer; and 3) adding the phase A and the phase B, uniformly stirring, adding the phase C, uniformly stirring, and homogenizing to obtain the transparent massage cream with high oil content.
Further, the homogenization is to homogenize for 3 to 5 minutes by a homogenizer at the rotating speed of 4500 to 5500 revolutions per minute.
Compared with the prior art, the invention has the beneficial effects that:
(1) The high-oil content transparent massage cream comprises the following main components: water, polyglycerol-10 myristate, glycerol, caprylic/capric triglyceride, polydimethylsiloxane, pentaerythritol tetra (ethyl hexanoate), hydrogenated polyisobutene, glycerol tri (ethyl hexanoate), erythritol, dipotassium glycyrrhizinate, herba Portulacae (Portulaca OLERACEA) extract, herba Dendrobii (Dendrobii NOBILE) extract, p-hydroxyacetophenone, 1,2-hexanediol, sambucus NIGRA (SAMBUCUS NIGRA) flower extract. The transparent massage cream with high oil content obtained by compounding the components can be stored in a packaging container in a stable state, and when the transparent massage cream is used, the skin is moistened when the transparent massage cream is smeared on the skin. The long-time massage can promote the blood circulation of face and body and prevent skin aging and relaxation. The formula adopts light ester grease, the moisturizing is not sticky, the emulsifier adopts polyglycerol-10 myristate, the property is mild, the content of the nonionic surfactant in the whole formula system is low, and the damage of the surfactant to human skin is reduced.
(2) The preparation method of the transparent massage cream with high oil content firstly divides the raw materials into the phase A and the phase B, firstly heats the phase A raw materials and adds the phase B, does not need high temperature in the whole process, and avoids the purposes of high-temperature inactivation of activity and energy conservation. Meanwhile, the D-phase emulsification process is adopted, so that the dosage of the emulsifier is reduced, the acne is not caused, and the massage cream with transparent appearance is prepared.
Detailed Description
The present invention is further described below with reference to specific embodiments, and it should be noted that, without conflict, any combination between the embodiments or technical features described below may form a new embodiment.
A transparent massage cream with high oil content comprises the following raw materials in parts by weight: 5-15 parts of water, 5-10 parts of polyglycerol-10 myristate, 8-10 parts of glycerol, 10-20 parts of caprylic/capric triglyceride, 15-20 parts of polydimethylsiloxane, 10-25 parts of pentaerythritol tetra (ethyl hexanoate), 10-15 parts of hydrogenated polyisobutene, 15-20 parts of glycerol tri (ethyl hexanoate), 0.5-1 part of erythritol, 0.05-0.1 part of dipotassium glycyrrhizinate, 0.5-1 part of purslane (Portulaca OLERACEA) extract, 0.5-1 part of DENDROBIUM NOBILE (Dendrobii NOBILE) extract, 0.1-0.5 part of p-hydroxyacetophenone, 0.1-0.5 part of 1,2-hexanediol and 0.1-0.5 part of Sambucus NIGRA (SAMBUCUS NIGRA) flower extract.
The functions and functions of the components are as follows:
polyglycerol-10 myristate, a hydrophilic emulsifier, has skin conditioning effect. The surfactant is mainly used as a surfactant to be applied to cosmetics, the raw materials of the surfactant are 100% of plant sources, do not contain EO structures, are mild and not irritate, and have good biodegradability. Can improve the sensory quality of the product and improve the use feeling 。
Glycerol, a colorless, transparent viscous liquid, odorless, sweet in taste. It is the earliest and common humectant used in cosmetics. Has obvious moistening effect on human skin and hair, and can increase the solubility of other components in the cosmetic. Glycerol is widely used in various cosmetics to supplement water to the stratum corneum of the skin, regulate the physiological action of the skin and keep the skin healthy.
Hydrogenated polyisobutene, which has the cosmetic properties of natural squalane, is thus called synthetic squalane, a colorless, odorless, non-toxic, liquid, isomeric straight-chain alkane of high purity. Can be used as oil phase component of cosmetic and medicine, has moistening, non-greasy, moisturizing, lubricating, and strong permeability, has properties similar to natural squalane, good thermal stability and storage stability, easy emulsification, and no irritation or allergy.
Polydimethylsiloxanes are widely used. The transparent liquid is volatile, colorless, tasteless and non-irritant, and can be compatible with alcohol and mineral oil; dry and smooth feeling, no contamination to clothes, no stickiness, no reactivity, easy diffusion, very good permeability to skin and good effect of increasing the softness of the skin.
Caprylic/capric triglyceride, is widely used as an emollient in oils and emulsions. It can improve skin feeling and spreadability on skin, has non-greasy texture due to its characteristic of compatibility with human skin, and can improve extensibility, and has effects of lubricating and softening skin by adding into cream or lotion. And has the function of filtering ultraviolet light.
Pentaerythritol tetra (ethyl hexanoate) is a odorless, high-safety, low-viscosity liquid oil. Has a chemical three-dimensional structure, is thermally stable, can retain moisture efficiently for a long period of time, and can maintain a smooth feeling.
The triglyceride (ethyl caproate) ester is a synthetic ester, is a smooth emollient with light touch feeling, does not generate rancidity (oxidation) in brightness, has good spreadability and low cloud point, has excellent silicone oil compatibility, and has excellent low-temperature stability.
Erythritol is a biological fermentation source, has comfortable cool feeling, and is a novel humectant.
The effects of dipotassium glycyrrhizinate are mainly represented by anti-inflammatory action, antiallergic action and immunity-regulating action. The cosmetic has wide application in cosmetics, has excellent compatibility, can be commonly used with other active agents, can improve the effect by accelerating the absorption of skin on the active agents, and can be used for sun protection, assisting whitening, relieving itching, regulating sebum, growing hair, protecting hair and the like. Can prevent dermatitis, xerosis cutis, sunburn, and erythra. Can also be added into speckle removing agent and antiallergic agent to achieve antiallergic, sunscreen, skin caring, and speckle removing effects.
The herba Portulacae (Portulaca OLERACEA) extract contains alkaloid, coumarin compounds, flavonoids, phenols, mushrooms and sterol. The herba Portulacae extract has broad-spectrum antibacterial and antiinflammatory effects, and can be used for preventing and treating dermatoses such as skin eczema, allergic dermatitis, and contact dermatitis; the product has good oxygen free radical scavenging capacity, which shows that the product has obvious antioxidation effect; has good skin moisture keeping effect.
The effective components of herba Dendrobii (Dendrobium NOBILE) extract include alkaloid, polysaccharide, microelements and amino acids, and are mainly used in cosmetic for keeping moisture and delaying aging. It can exert good moisturizing effect on skin, and herba Dendrobii polysaccharide has effects of scavenging free radicals, improving antioxidase activity and inhibiting lipid peroxidation, protecting biological membrane and delaying aging
Sambucus NIGRA (SAMBUCUS NIGRA) flower extract contains flavonoid, phenolic acid, tannic acid, terpenoid, mineral, polysaccharide and amino acids, and has antioxidant, blood vessel nourishing, soothing, skin moisturizing, and skin barrier regulating effects. Is suitable for anti-aging, sensitive skin care products, edema removing and skin activating effects.
P-hydroxyacetophenone, a natural plant extract, is used as a preservative promoter and a chelating agent in cosmetics, and has multiple effects of oxidation resistance, irritation resistance and the like.
1,2-hexanediol, a glycol, is a moisture-retaining solvent, is completely soluble in water, is used as an antibacterial agent, has a good antibacterial effect, and can also be used as a defoaming agent in the production process. Is mild to skin and has good safety.
Examples 1 to 5
A transparent massage cream with high oil content is prepared from the following raw materials in percentage by weight as shown in Table 1.
Table 1 examples 1 to 5
The preparation method of the transparent massage cream with high oil content comprises the following steps:
1) Dividing each raw material into an A phase, a B phase and a C phase respectively, and weighing each raw material of the three phases for later use; wherein, the phase A is: water, polyglycerol-10 myristate, glycerol, erythritol, p-hydroxyacetophenone, dipotassium glycyrrhizinate, herba Portulacae (Portulaca OLERACEA) extract, herba Dendrobii (Dendrobium NOBILE) extract, 1,2-hexanediol, and Sambucus NIGRA (SAMBUCUS NIGRA) flower extract. The phase B is as follows: caprylic/capric triglyceride dimethicone, pentaerythritol tetra (ethyl hexanoate), hydrogenated polyisobutene, and glycerol tri (ethyl hexanoate).
2) Adding phase A raw materials into a container, heating to 45 deg.C, stirring, and keeping the temperature for use
3) Mixing the raw materials of phase B, and stirring uniformly. Slowly adding the raw material of the phase B (the dropping speed is controlled to be 20-25 drops per minute) into the A under stirring.
4) After being stirred evenly, the mixture is homogenized for 3 to 5 minutes by a homogenizer, and the transparent massage cream with high oil content can be obtained.
Comparative example 1
A transparent massage cream is different from the massage cream of example 5 in that:
the comparative example comprises the following components in percentage by weight:
polyglycerol-10 myristate 4%, carbomer 0.4%, glycerol 10%, caprylic/capric triglyceride 10%, polydimethylsiloxane 10%, pentaerythritol tetra (ethyl hexanoate) 10%, hydrogenated polyisobutene 10%, glycerol tri (ethyl hexanoate) 10%, cetostearyl alcohol 2%, erythritol 0.5%, dipotassium glycyrrhizinate 0.05%, purslane (PORTULACA OLERACEA) extract 0.5%, DENDROBIUM NOBILE (dendrobiule) extract 0.5%, p-hydroxyacetophenone 0.15%,1,2-hexanediol 0.15%, SAMBUCUS NIGRA (SAMBUCUS NIGRA) flower extract 0.1%, triethanolamine 0.4%, and water in balance.
Comparative example 2
The difference between the comparative example and the example 5 is that: the preparation method of the embodiment comprises the following steps:
heating the phase A and the phase B to 45 ℃, and stirring uniformly. Then phase B material was added to phase A with rapid stirring of phase A material. Homogenizing for 3-5 min with homogenizer after stirring to obtain massage cream.
Performance testing
1. Stability test
Following the formulation implementation in table 1, the addition of a commercial product gave the following stability-related results.
The emulsions of examples 1 to 5 and commercial product 1 were tested for centrifugal stability, high temperature stability and low temperature stability under the following conditions: centrifuging at 2000r/min for 30min; the conditions for the high temperature stability test were: keeping the temperature at 45 +/-1 ℃ for 48 hours, and recovering the temperature to room temperature; the conditions for the low temperature stability test were: keeping at-15 + -1 deg.C for 48 hr, and recovering to room temperature. After the test is completed, it is observed whether there is demulsification or stratification, and if not, it is considered stable. The results are shown in Table 1.
TABLE 1
As shown in table 1, examples 1, 4, 5 and comparative example 1 and the commercial product passed the stability test. In examples 2 and 3, the stability is reduced due to less emulsifier, and the delamination phenomenon occurs under centrifugation and high temperature, but the stability is still good at normal temperature and low temperature. Comparative example 2 a conventional oil-in-water process was used, and the oil phase was rapidly added to the water phase, resulting in a larger emulsion particle and oil droplet aggregation, which eventually led to sample delamination. The D-phase emulsification method is proved to be more stable in emulsification.
2. Skin feel test
The skin feel of examples 1, 4, 5 and the commercial products according to the stability test formula was tested by the recruited volunteers in eight dimensions (appearance, firmness, melting feel, massage time, gloss after use, softness after use, residual film feel, sliminess). According to the grade of the like degree, the total of the single items is 10, and the like degree is larger as the grade is higher. The specific data are shown in Table 2.
Table 2 test data for skin feel of each group
| Test items | Example 1 | Example 4 | Example 5 | Commercial product 1 | Comparative example 1 |
| Appearance of the product | Transparent gel | Transparent gel | Transparent gel | Milky white paste | Milky white paste |
| Texture of | 8 | 8 | 9 | 5 | 5 |
| Feeling of melting | 8 | 8 | 8 | 4 | 5 |
| Time of massage | 9 | 9 | 8 | 6 | 4 |
| Gloss after use | 8 | 8 | 9 | 5 | 5 |
| Softness after use | 8 | 8 | 9 | 5 | 5 |
| Film feeling residue | 9 | 9 | 9 | 6 | 5 |
| Sticky feeling | 7 | 9 | 8 | 5 | 5 |
As can be seen from table 2, comparative example 1 contains a certain amount of thickening component, and experiences poor feeling in use; example 1 and examples 4-5 the skin feel was lighter without the addition of a thickening agent (carbomer, fatty alcohol); the D-phase emulsification method is adopted to emulsify more grease, so that the massage time is longer, and a proper amount of emulsifier has good soft feeling and does not stick greasy after being used. The results were combined to determine the score for each of the examples 5 to be optimal for the experiment.
The above embodiments are only preferred embodiments of the present invention, and the protection scope of the present invention is not limited thereby, and any insubstantial changes and substitutions made by those skilled in the art based on the present invention are within the protection scope of the present invention.
Claims (9)
1. The transparent massage cream with high oil content is characterized by comprising the following raw materials in parts by weight: 5-15 parts of water, 5-10 parts of polyglycerol-10 myristate, 8-15 parts of glycerol, 10-20 parts of caprylic/capric triglyceride, 15-20 parts of polydimethylsiloxane, 10-25 parts of pentaerythritol tetra (ethyl hexanoate), 10-15 parts of hydrogenated polyisobutene, 15-20 parts of glycerol tri (ethyl hexanoate), 0.5-1 part of erythritol, 0.05-0.1 part of dipotassium glycyrrhizinate, 0.5-1 part of purslane extract, 0.5-1 part of dendrobium nobile extract, 0.1-0.5 part of p-hydroxyacetophenone, 0.1-0.5 part of 1,2-hexanediol and 0.1-0.5 part of Sambucus williamsii flower extract.
2. The transparent massage cream with high oil content according to claim 1, comprising the following raw materials in parts by weight: 10 parts of water, 8 parts of polyglycerol-10 myristate, 10 parts of glycerol, 20 parts of caprylic/capric triglyceride, 15 parts of polydimethylsiloxane, 10 parts of pentaerythritol tetra (ethyl hexanoate), 15 parts of hydrogenated polyisobutene, 10 parts of glycerol tri (ethyl hexanoate), 0.5 part of erythritol, 0.05 part of dipotassium glycyrrhizinate, 0.5 part of purslane extract, 0.5 part of dendrobium nobile extract, 0.15 part of p-hydroxyacetophenone, 0.15 part of 1,2-hexanediol and 0.1 part of Sambucus nigra flower extract.
3. The transparent massage cream with high oil content according to claim 1 or 2, wherein the massage cream further comprises 0.01-0.05 parts of an aromatizer.
4. The transparent massage cream with high oil content as claimed in claim 3, wherein said massage cream further comprises 0.05 parts of an aromatizer.
5. The method for preparing a transparent massage cream having a high oil content according to any one of claims 1 to 4, comprising the steps of:
1) Respectively dividing the raw materials into an A phase and a B phase, and respectively weighing the raw materials for later use; wherein, the phase A is: water, polyglycerol-10 myristate, glycerol, erythritol, p-hydroxyacetophenone, dipotassium glycyrrhizinate, herba Portulacae extract, herba Dendrobii extract, 1,2-hexanediol, and Sambucus nigra flower extract; the phase B is as follows: caprylic/capric triglyceride dimethicone, pentaerythritol tetra (ethyl hexanoate), hydrogenated polyisobutene, glycerol tri (ethyl hexanoate);
2) Heating and stirring the phase A raw material, and preserving heat for later use;
3) Mixing the phase B raw materials, stirring uniformly, adding the phase A obtained in the step 2) under the stirring state, and homogenizing to obtain the transparent massage cream with high oil content.
6. The method for preparing a transparent massage cream with high oil content as claimed in claim 5, wherein the raw material further comprises a C phase, the C phase being an aromatizer; and 3) uniformly stirring the phase A and the phase B, adding the phase C, uniformly stirring, and homogenizing to obtain the transparent massage cream with high oil content.
7. The method for preparing a transparent massage cream having a high oil content as claimed in claim 5 or 6, wherein the homogenization in step 3) is performed for 3-5 minutes using a homogenizer.
8. The method for preparing a transparent massage cream with high oil content according to claim 5, wherein in step 2), the method specifically comprises: heating the phase A raw material to 42-45 deg.C, stirring, and maintaining the temperature for 42-45min.
9. The method for preparing a transparent massage cream having a high oil content as claimed in claim 5, wherein the addition rate of the B phase to the A phase in the step 3) is 20 to 25 drops per minute.
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