CN115843291A - 高纯度双-（2-羟乙基）对苯二甲酸酯的制造方法、再生聚对苯二甲酸乙二酯、脱色溶剂及双-（2-羟乙基）对苯二甲酸酯的精制方法 - Google Patents

高纯度双-（2-羟乙基）对苯二甲酸酯的制造方法、再生聚对苯二甲酸乙二酯、脱色溶剂及双-（2-羟乙基）对苯二甲酸酯的精制方法 Download PDF

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Publication number
CN115843291A
CN115843291A CN202080102342.8A CN202080102342A CN115843291A CN 115843291 A CN115843291 A CN 115843291A CN 202080102342 A CN202080102342 A CN 202080102342A CN 115843291 A CN115843291 A CN 115843291A
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China
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terephthalate
hydroxyethyl
bis
purity
bhet
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CN202080102342.8A
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English (en)
Chinese (zh)
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高尾正树
堺通
藤田博
稻田修司
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Jeplan
Cintec Co ltd
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Jeplan
Cintec Co ltd
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Priority claimed from PCT/JP2020/029418 external-priority patent/WO2022003990A1/ja
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/03—Preparation of carboxylic acid esters by reacting an ester group with a hydroxy group
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/76—Esters of carboxylic acids having a carboxyl group bound to a carbon atom of a six-membered aromatic ring
    • C07C69/80—Phthalic acid esters
    • C07C69/82—Terephthalic acid esters
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/02—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds
    • C08G63/12—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds derived from polycarboxylic acids and polyhydroxy compounds
    • C08G63/16—Dicarboxylic acids and dihydroxy compounds
    • C08G63/18—Dicarboxylic acids and dihydroxy compounds the acids or hydroxy compounds containing carbocyclic rings
    • C08G63/181—Acids containing aromatic rings
    • C08G63/183—Terephthalic acids
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J11/00—Recovery or working-up of waste materials
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J11/00—Recovery or working-up of waste materials
    • C08J11/04—Recovery or working-up of waste materials of polymers
    • C08J11/06—Recovery or working-up of waste materials of polymers without chemical reactions
    • C08J11/08—Recovery or working-up of waste materials of polymers without chemical reactions using selective solvents for polymer components
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J11/00—Recovery or working-up of waste materials
    • C08J11/04—Recovery or working-up of waste materials of polymers
    • C08J11/10—Recovery or working-up of waste materials of polymers by chemically breaking down the molecular chains of polymers or breaking of crosslinks, e.g. devulcanisation
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J11/00—Recovery or working-up of waste materials
    • C08J11/04—Recovery or working-up of waste materials of polymers
    • C08J11/10—Recovery or working-up of waste materials of polymers by chemically breaking down the molecular chains of polymers or breaking of crosslinks, e.g. devulcanisation
    • C08J11/16—Recovery or working-up of waste materials of polymers by chemically breaking down the molecular chains of polymers or breaking of crosslinks, e.g. devulcanisation by treatment with inorganic material
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J11/00—Recovery or working-up of waste materials
    • C08J11/04—Recovery or working-up of waste materials of polymers
    • C08J11/10—Recovery or working-up of waste materials of polymers by chemically breaking down the molecular chains of polymers or breaking of crosslinks, e.g. devulcanisation
    • C08J11/18—Recovery or working-up of waste materials of polymers by chemically breaking down the molecular chains of polymers or breaking of crosslinks, e.g. devulcanisation by treatment with organic material
    • C08J11/22—Recovery or working-up of waste materials of polymers by chemically breaking down the molecular chains of polymers or breaking of crosslinks, e.g. devulcanisation by treatment with organic material by treatment with organic oxygen-containing compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2367/00—Characterised by the use of polyesters obtained by reactions forming a carboxylic ester link in the main chain; Derivatives of such polymers
    • C08J2367/02—Polyesters derived from dicarboxylic acids and dihydroxy compounds
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00—Technologies for solid waste management
    • Y02W30/50—Reuse, recycling or recovery technologies
    • Y02W30/62—Plastics recycling; Rubber recycling

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Sustainable Development (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Separation, Recovery Or Treatment Of Waste Materials Containing Plastics (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
CN202080102342.8A 2020-06-29 2020-07-31 高纯度双-（2-羟乙基）对苯二甲酸酯的制造方法、再生聚对苯二甲酸乙二酯、脱色溶剂及双-（2-羟乙基）对苯二甲酸酯的精制方法 Pending CN115843291A (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP2020-111719 2020-06-29
JP2020111719 2020-06-29
PCT/JP2020/029418 WO2022003990A1 (ja) 2020-06-29 2020-07-31 高純度ビス－（２－ヒドロキシエチル）テレフタレートの製造方法、再生ポリエチレンテレフタレート、脱色溶媒およびビス－（２－ヒドロキシエチル）テレフタレートの精製方法

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CN115843291A true CN115843291A (zh) 2023-03-24

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JP (2) JP6960709B1 (enExample)
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Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR3130804B1 (fr) * 2021-12-17 2025-09-26 Ifp Energies Now Bis(2-hydroxyethyle) terephtalate ayant une teneur en azote faible
JP7708983B2 (ja) * 2022-11-29 2025-07-15 帝人フロンティア株式会社 ポリエステルの回収方法およびリサイクルポリエステルの製造方法
WO2024181689A1 (ko) 2023-02-28 2024-09-06 주식회사 엘지에너지솔루션 전기화학소자용 분리막 및 이를 포함하는 전기화학소자

Citations (8)

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US20050198742A1 (en) * 2002-02-01 2005-09-15 Berard Raymond A. Chemical compounds and methods for removing dye
JP2006232701A (ja) * 2005-02-23 2006-09-07 Is:Kk ポリエステル繊維屑からエステルモノマーを回収する方法
JP2007045874A (ja) * 2005-08-08 2007-02-22 Teijin Fibers Ltd 染着ポリエステル繊維からの有効成分回収方法
CN102241592A (zh) * 2010-05-12 2011-11-16 无棣永昕生物工程有限公司 利用聚酯废弃物生产对苯二甲酸二辛酯的方法
US20180216283A1 (en) * 2017-01-31 2018-08-02 Geo-Tech Polymers, Llc Decolorization of Post-Consumer Fibers
CN109696801A (zh) * 2017-10-20 2019-04-30 东友精细化工有限公司 着色分散液、着色感光性树脂组合物、图案层、滤色器及显示装置
CN110590551A (zh) * 2018-06-13 2019-12-20 再生聚酯研究有限公司 双(2-羟基乙基)对苯二甲酸酯的制造方法及聚对苯二甲酸乙二醇酯的制造方法
JP6659919B1 (ja) * 2019-04-15 2020-03-04 株式会社シンテック 脱色ポリエステルの製造方法、脱色ポリエステルおよび脱色剤

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US3268575A (en) * 1963-07-05 1966-08-23 Goodyear Tire & Rubber Purification of bis-beta-hydroxyethyl terephthalate
US3652649A (en) * 1967-06-05 1972-03-28 Exxon Research Engineering Co Purification of bis-beta-hydroxyethyl terephthalate
JP3715812B2 (ja) 1998-12-10 2005-11-16 株式会社アイエス ポリエチレンテレフタレート廃棄物のケミカルリサイクル方法
JP4067306B2 (ja) 1999-10-22 2008-03-26 帝人ファイバー株式会社 ポリエステル廃棄物からテレフタル酸ジメチル及びエチレングリコールを分離回収する方法
JP2005255963A (ja) * 2004-02-12 2005-09-22 Is:Kk 繊維状ポリエステルからエステルモノマーを回収する方法
AU2006277349B2 (en) * 2005-08-05 2011-08-25 Teijin Fibers Limited Method for recovery of valuable ingredient from dyed polyester fiber
JP5189266B2 (ja) 2006-09-29 2013-04-24 株式会社ニスコ ビス−（２−ヒドロキシエチル）テレフタレートの製造方法およびポリエチレンテレフタレートの製造方法
JP5134563B2 (ja) 2009-02-02 2013-01-30 帝人株式会社 ポリアルキレンテレフタレート繊維からの異素材除去方法

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US20050198742A1 (en) * 2002-02-01 2005-09-15 Berard Raymond A. Chemical compounds and methods for removing dye
JP2006232701A (ja) * 2005-02-23 2006-09-07 Is:Kk ポリエステル繊維屑からエステルモノマーを回収する方法
JP2007045874A (ja) * 2005-08-08 2007-02-22 Teijin Fibers Ltd 染着ポリエステル繊維からの有効成分回収方法
CN102241592A (zh) * 2010-05-12 2011-11-16 无棣永昕生物工程有限公司 利用聚酯废弃物生产对苯二甲酸二辛酯的方法
US20180216283A1 (en) * 2017-01-31 2018-08-02 Geo-Tech Polymers, Llc Decolorization of Post-Consumer Fibers
CN109696801A (zh) * 2017-10-20 2019-04-30 东友精细化工有限公司 着色分散液、着色感光性树脂组合物、图案层、滤色器及显示装置
CN110590551A (zh) * 2018-06-13 2019-12-20 再生聚酯研究有限公司 双(2-羟基乙基)对苯二甲酸酯的制造方法及聚对苯二甲酸乙二醇酯的制造方法
JP6659919B1 (ja) * 2019-04-15 2020-03-04 株式会社シンテック 脱色ポリエステルの製造方法、脱色ポリエステルおよび脱色剤

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KR102831944B1 (ko) 2025-07-08
JP6960709B1 (ja) 2021-11-05
JP2022013942A (ja) 2022-01-18
JPWO2022003990A1 (enExample) 2022-01-06
KR20230026495A (ko) 2023-02-24
JP7101390B2 (ja) 2022-07-15

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Address after: 9-16, Fujibetai 2-chome, Shueda City, Osaka Prefecture, Japan

Applicant after: CINTEC Co.,Ltd.

Applicant after: JEPLAN

Address before: 20 Fandi, wutiao xiacho, Takakura, Xiajing District, Kyoto City, Japan

Applicant before: CINTEC Co.,Ltd.

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