CN115651771A - Preparation method of tea saponin detergent - Google Patents
Preparation method of tea saponin detergent Download PDFInfo
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- CN115651771A CN115651771A CN202211172025.0A CN202211172025A CN115651771A CN 115651771 A CN115651771 A CN 115651771A CN 202211172025 A CN202211172025 A CN 202211172025A CN 115651771 A CN115651771 A CN 115651771A
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- tea saponin
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- deionized water
- xanthan gum
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Abstract
The invention belongs to the technical field of detergents, and provides a preparation method of a tea saponin detergent, which comprises the following steps: adding xanthan gum into certain deionized water to fully expand to form uniform gel; step two, adding the tea saponin into deionized water, heating and stirring until the tea saponin is completely dissolved; step three, mixing sodium bicarbonate, potassium sorbate, sodium chloride, lemon essence and sorbitol according to a certain proportion, and then completely dissolving the mixture by using deionized water; and step four, fully mixing the solution A obtained in the step two and the solution B obtained in the step three, and adding the mixture into the gel obtained in the step one while stirring to ensure that the mixture is fully and uniformly mixed, thus finally obtaining the tea saponin detergent. The detergent prepared by the preparation method of the tea saponin detergent has the advantages of strong oil stain removing capability, no harm to hands, low foam, easiness in bleaching, environmental friendliness, simple preparation process and capability of realizing industrial production.
Description
Technical Field
The invention belongs to the technical field of detergents, and particularly relates to a preparation method of a tea saponin detergent.
Background
The detergent is a daily chemical product widely applied to daily life of people, and is mainly used for washing tableware, tea sets, kitchenware and the like; it can also be used for washing fruits, vegetables and clothes with heavy oil. In the research of detergents, the current main stream is ionic detergents, chemical residues are easy to generate after the detergents are used, and the bacteriostatic effect is poor.
Disclosure of Invention
The invention aims to solve the defects of the prior art and provides the preparation method of the tea saponin detergent, which has the advantages of strong oil stain removing capability, no damage to hands, low foam, easy bleaching, environmental friendliness, simple preparation process and capability of realizing industrial production.
A preparation method of a tea saponin detergent comprises the following steps:
adding xanthan gum into certain deionized water to fully expand to form uniform gel;
step two, adding the tea saponin into deionized water, heating and stirring until the tea saponin is completely dissolved;
step three, mixing sodium bicarbonate, potassium sorbate, sodium chloride, lemon essence and sorbitol according to a certain proportion, and then completely dissolving the mixture by using deionized water;
and step four, fully mixing the solution A obtained in the step two and the solution B obtained in the step three, and adding the mixture into the gel obtained in the step one while stirring to ensure that the mixture is fully and uniformly mixed, thus finally obtaining the tea saponin detergent.
Further, the tea saponin adopted in the second step is a purified product of the tea saponin separated from the camellia seeds.
Further, the tea saponin detergent is prepared from the following raw materials in parts by weight: 12 parts of tea saponin, 0.1 part of sodium bicarbonate, 0.2 part of potassium sorbate, 0.25 part of sodium chloride, 0.5 part of lemon essence, 1 part of xanthan gum, 9 parts of sorbitol and 76.95 parts of deionized water.
Further, the tea saponin detergent is prepared from the following raw materials in parts by weight: 14 parts of tea saponin, 0.11 part of sodium bicarbonate, 0.21 part of potassium sorbate, 0.3 part of sodium chloride, 0.6 part of lemon essence, 1.1 part of xanthan gum, 10 parts of sorbitol and 77.95 parts of deionized water.
Further, the tea saponin detergent is prepared from the following raw materials in parts by weight: 16 parts of tea saponin, 0.12 part of sodium bicarbonate, 0.22 part of potassium sorbate, 0.35 part of sodium chloride, 0.7 part of lemon essence, 1.2 parts of xanthan gum, 11 parts of sorbitol and 78.95 parts of deionized water.
Further, the tea saponin detergent is prepared from the following raw materials in parts by weight: 10 parts of tea saponin, 0.09 part of sodium bicarbonate, 0.19 part of potassium sorbate, 0.20 part of sodium chloride, 0.4 part of lemon essence, 0.9 part of xanthan gum, 8 parts of sorbitol and 75.95 parts of deionized water.
Further, the tea saponin detergent is prepared from the following raw materials in parts by weight: 8 parts of tea saponin, 0.08 part of sodium bicarbonate, 0.18 part of potassium sorbate, 0.15 part of sodium chloride, 0.3 part of lemon essence, 0.8 part of xanthan gum, 7 parts of sorbitol and 74.95 parts of deionized water.
Further, the tea saponin detergent is prepared from the following raw materials in parts by weight: 8-16 parts of tea saponin, 0.08-0.12 part of sodium bicarbonate, 0.18-0.22 part of potassium sorbate, 0.15-0.35 part of sodium chloride, 0.3-0.7 part of lemon essence, 0.8-1.2 parts of xanthan gum, 7-11 parts of sorbitol and 74.95-78.95 parts of deionized water.
The detergent prepared by the preparation method of the tea saponin detergent has the advantages of strong oil stain removing capability, no harm to hands, low foam, easiness in bleaching, environmental friendliness, simple preparation process and capability of realizing industrial production.
Drawings
FIG. 1 is a comparison of the detergency of different detergents.
Detailed Description
The conception, the specific structure and the technical effects of the present invention will be clearly and completely described in conjunction with the embodiments and the accompanying drawings to fully understand the objects, the schemes and the effects of the present invention. It should be noted that the embodiments and features of the embodiments in the present application may be combined with each other without conflict. The same reference numbers will be used throughout the drawings to refer to the same or like parts.
The invention provides a preparation method of a tea saponin detergent, which comprises the following steps:
adding xanthan gum into certain deionized water to fully expand to form uniform gel;
step two, adding the tea saponin into deionized water, heating and stirring until the tea saponin is completely dissolved;
step three, adding sodium bicarbonate, potassium sorbate, sodium chloride, lemon essence and sorbitol according to a certain proportion, and then completely dissolving with deionized water;
and step four, fully mixing the step two and the step three, stirring and adding the mixture into the step one to ensure that the mixture is fully and uniformly mixed, and finally obtaining the tea saponin detergent.
The tea saponin adopted in the second step is a purified product of the tea saponin separated from the camellia seeds.
Example 1
The tea saponin detergent is prepared from the following raw materials in parts by weight: 12 parts of tea saponin, 0.1 part of sodium bicarbonate, 0.2 part of potassium sorbate, 0.25 part of sodium chloride, 0.5 part of lemon essence, 1 part of xanthan gum, 9 parts of sorbitol and 76.95 parts of deionized water.
Example 2
The tea saponin detergent is prepared from the following raw materials in parts by weight: 14 parts of tea saponin, 0.11 part of sodium bicarbonate, 0.21 part of potassium sorbate, 0.3 part of sodium chloride, 0.6 part of lemon essence, 1.1 part of xanthan gum, 10 parts of sorbitol and 77.95 parts of deionized water.
Example 3
The tea saponin detergent is prepared from the following raw materials in parts by weight: 16 parts of tea saponin, 0.12 part of sodium bicarbonate, 0.22 part of potassium sorbate, 0.35 part of sodium chloride, 0.7 part of lemon essence, 1.2 parts of xanthan gum, 11 parts of sorbitol and 78.95 parts of deionized water.
Example 4
The tea saponin detergent is prepared from the following raw materials in parts by weight: 10 parts of tea saponin, 0.09 part of sodium bicarbonate, 0.19 part of potassium sorbate, 0.20 part of sodium chloride, 0.4 part of lemon essence, 0.9 part of xanthan gum, 8 parts of sorbitol and 75.95 parts of deionized water.
Example 5
The tea saponin detergent is prepared from the following raw materials in parts by weight: 8 parts of tea saponin, 0.08 part of sodium bicarbonate, 0.18 part of potassium sorbate, 0.15 part of sodium chloride, 0.3 part of lemon essence, 0.8 part of xanthan gum, 7 parts of sorbitol and 74.95 parts of deionized water.
The tea saponin detergent is prepared from the following raw materials in parts by weight: 8-16 parts of tea saponin, 0.08-0.12 part of sodium bicarbonate, 0.18-0.22 part of potassium sorbate, 0.15-0.35 part of sodium chloride, 0.3-0.7 part of lemon essence, 0.8-1.2 parts of xanthan gum, 7-11 parts of sorbitol and 74.95-78.95 parts of deionized water.
To further verify the effect of the present invention, the following test methods were provided:
1. degreasing test
(1) Preparation of the soil
Putting 15 g of mixed oil into a beaker, heating to 50-60 ℃, and pouring 15 g of flour and 7.5 g of all-in-one
The preparation method comprises the steps of preparing milk powder, pouring 30 g of fresh egg juice, uniformly stirring, pouring 32.5g of water into a beaker, and stirring to obtain 100g of fine artificial dirt serving as a dirt remover.
(2) Preparation of soil flakes
The dirt prepared above was uniformly coated on the surface of the slide glass with a glass rod, and the thickness was controlled to be about 2 cm, and left to stand for 24 hours.
(3) Preparation of solutions
The self-made laboratory detergent and the two brands of detergents were weighed 1g into 250mL beakers, respectively, and 200mL of tap water was added thereto at room temperature.
(4) Washing process
Respectively putting the prepared and weighed dirty sheets into a beaker, soaking for 15min, then washing under the same conditions, and weighing the dirty sheets after washing and drying.
(5) Determination of decontamination efficiency
Decontamination efficiency = (mass of glass slide after smear-mass of glass slide after wash)/(mass of glass slide after smear-mass of glass slide before smear)
2. Evaluation of physical and chemical indexes
(1) Total active assay
The measurement was carried out according to method A of GB/T3173.2-2000.
(2) Determination of the pH value
The measurement was carried out according to the specification of GB/T6368.
(3) Determination of Formaldehyde content
According to the provisions of appendix E of GB 9985-2000.
(4) Determination of moisture and volatile content (oven method)
2 g of the sample (weighed to 0.001 g) was accurately weighed, placed in a constant weight weighing bottle, dried in an electric hot air drying oven at (105. + -. 2) ℃ for 4 hours, removed, cooled in a drier for 30 minutes, covered and weighed. The calculation formula is as follows:
X＝m 1 /m 0 ×100％
in the formula:
x-moisture and its volatile content;
m 1 -the mass reduced after drying of the sample in grams (g);
m 0 the mass of the sample in grams (g).
(5) Determination of fluorescent whitening Agents
Since the fluorescent whitening agent functions to make the luminescent material emit light brighter by neutralizing the yellow light with the blue light excited by the ultraviolet rays, whether or not the fluorescent whitening agent is contained can be judged by direct irradiation of the ultraviolet rays.
3. Microbiological indicator assay
The total number of bacteria in the detergent and the coliform group are respectively determined according to national standard GB4789.2-2016 and national standard GB4789.2-2016
The measurement was carried out as specified in GB/T4789.3-2008.
The test results were as follows:
1. determination of soil Release Effect
As shown in FIG. 1, this experiment compared the detergency of a laboratory home-made tea saponin detergent with that of two commercially available brands, libai and super. The results show that the detergents of the two brands have good decontamination effect, because the main components of the detergents are sodium alkyl sulfonate, sodium fatty alcohol ether sulfate and the like, the anionic surfactants have good removal effect on oil stains, but easily cause damage to the skin. The detergent prepared from the tea saponin has inferior decontamination effect to the detergent prepared from the tea saponin sold on the market, but all the surfactants used in the detergent are nonionic surfactants, so that the damage to the skin and the like is far less than that of the detergent prepared from the tea saponin sold on the market, and the decontamination rates of the three are not greatly different.
2. Measurement of physical and chemical indexes
The physical and chemical indexes of the self-made tea saponin detergent are determined according to the specification, and then the self-made tea saponin detergent is compared with two detergents (Libai and super) sold in the market. As shown in Table 1, the physicochemical indexes of the tea saponin detergent self-made in the laboratory are in accordance with the regulations, and the difference between the physicochemical indexes is not great compared with those of two detergents sold in the market.
TABLE 1
3. Microbiological indicator assay
In order to verify whether the microbial indexes of the laboratory self-made tea saponin detergent meet the specifications, the laboratory self-made detergent and the two commercially available detergents are determined by using the specifications of related national standards, and the test results are shown in table 2. The experimental result shows that the tea saponin detergent prepared by the laboratory and two commercial detergents both reach the national standard.
TABLE 2
In the description herein, references to the description of the term "one embodiment," "some embodiments," "an illustrative embodiment," "an example," "a specific example," or "some examples" or the like mean that a particular feature, structure, material, or characteristic described in connection with the embodiment or example is included in at least one embodiment or example of the invention. In this specification, the schematic representations of the terms used above do not necessarily refer to the same embodiment or example.
It is to be understood that the embodiments described are only a few embodiments of the present application and not all embodiments. Reference herein to "an embodiment" means that a particular feature, structure, or characteristic described in connection with the embodiment can be included in at least one embodiment of the present application. The appearances of the phrase in various places in the specification are not necessarily all referring to the same embodiment, nor are separate or alternative embodiments mutually exclusive of other embodiments. Those skilled in the art will explicitly and implicitly appreciate that the embodiments described herein may be combined with other embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present application.
While embodiments of the invention have been shown and described, it will be understood by those of ordinary skill in the art that: various changes, modifications, substitutions and alterations can be made to the embodiments without departing from the principles and spirit of the invention, the scope of which is defined by the claims and their equivalents.
Claims (8)
1. The preparation method of the tea saponin detergent is characterized by comprising the following steps:
adding xanthan gum into certain deionized water to fully expand to form uniform gel;
step two, adding the tea saponin into deionized water, heating and stirring until the tea saponin is completely dissolved;
step three, mixing sodium bicarbonate, potassium sorbate, sodium chloride, lemon essence and sorbitol according to a certain proportion, and then completely dissolving the mixture by using deionized water;
and step four, fully mixing the solution A obtained in the step two and the solution B obtained in the step three, stirring and adding the mixture into the gel obtained in the step one to ensure that the mixture is fully and uniformly mixed, and finally obtaining the tea saponin detergent.
2. The method for preparing tea saponin detergent as claimed in claim 1, wherein the tea saponin used in the second step is a purified product of tea saponin separated from oil tea seeds.
3. The method for preparing the tea saponin detergent as claimed in claim 1, wherein the tea saponin detergent is prepared from the following raw materials in parts by weight: 12 parts of tea saponin, 0.1 part of sodium bicarbonate, 0.2 part of potassium sorbate, 0.25 part of sodium chloride, 0.5 part of lemon essence, 1 part of xanthan gum, 9 parts of sorbitol and 76.95 parts of deionized water.
4. The method for preparing the tea saponin detergent as claimed in claim 1, wherein the tea saponin detergent is prepared from the following raw materials in parts by weight: 14 parts of tea saponin, 0.11 part of sodium bicarbonate, 0.21 part of potassium sorbate, 0.3 part of sodium chloride, 0.6 part of lemon essence, 1.1 part of xanthan gum, 10 parts of sorbitol and 77.95 parts of deionized water.
5. The method for preparing the tea saponin detergent as claimed in claim 1, wherein the tea saponin detergent is prepared from the following raw materials in parts by weight: 16 parts of tea saponin, 0.12 part of sodium bicarbonate, 0.22 part of potassium sorbate, 0.35 part of sodium chloride, 0.7 part of lemon essence, 1.2 parts of xanthan gum, 11 parts of sorbitol and 78.95 parts of deionized water.
6. The method for preparing the tea saponin detergent as claimed in claim 1, wherein the tea saponin detergent is prepared from the following raw materials in parts by weight: 10 parts of tea saponin, 0.09 part of sodium bicarbonate, 0.19 part of potassium sorbate, 0.20 part of sodium chloride, 0.4 part of lemon essence, 0.9 part of xanthan gum, 8 parts of sorbitol and 75.95 parts of deionized water.
7. The method for preparing the tea saponin detergent as claimed in claim 1, wherein the tea saponin detergent is prepared from the following raw materials in parts by weight: 8 parts of tea saponin, 0.08 part of sodium bicarbonate, 0.18 part of potassium sorbate, 0.15 part of sodium chloride, 0.3 part of lemon essence, 0.8 part of xanthan gum, 7 parts of sorbitol and 74.95 parts of deionized water.
8. The method for preparing the tea saponin detergent as claimed in claim 1, wherein the tea saponin detergent is prepared from the following raw materials in parts by weight: 8-16 parts of tea saponin, 0.08-0.12 part of sodium bicarbonate, 0.18-0.22 part of potassium sorbate, 0.15-0.35 part of sodium chloride, 0.3-0.7 part of lemon essence, 0.8-1.2 parts of xanthan gum, 7-11 parts of sorbitol and 74.95-78.95 parts of deionized water.
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| CN202211172025.0A CN115651771A (en) | 2022-09-26 | 2022-09-26 | Preparation method of tea saponin detergent |
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| CN202211172025.0A CN115651771A (en) | 2022-09-26 | 2022-09-26 | Preparation method of tea saponin detergent |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104017661A (en) * | 2014-06-16 | 2014-09-03 | 湖南农业大学 | Tea saponin dishwashing liquid and preparation method thereof |
| CN106367216A (en) * | 2016-08-26 | 2017-02-01 | 华侨大学 | Tea saponin liquid detergent |
| CN106753856A (en) * | 2016-12-19 | 2017-05-31 | 肖晴 | A kind of fruits and vegetables cleaning agent and preparation method thereof |
| CN107841389A (en) * | 2017-09-19 | 2018-03-27 | 谭志华 | A kind of vegetables and fruits cleaning agent and preparation method thereof |
| CN108148691A (en) * | 2017-08-22 | 2018-06-12 | 济宁锦祥科技发展有限公司 | A kind of preparation method of pollution-free food grade meal wash agent |
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- 2022-09-26 CN CN202211172025.0A patent/CN115651771A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104017661A (en) * | 2014-06-16 | 2014-09-03 | 湖南农业大学 | Tea saponin dishwashing liquid and preparation method thereof |
| CN106367216A (en) * | 2016-08-26 | 2017-02-01 | 华侨大学 | Tea saponin liquid detergent |
| CN106753856A (en) * | 2016-12-19 | 2017-05-31 | 肖晴 | A kind of fruits and vegetables cleaning agent and preparation method thereof |
| CN108148691A (en) * | 2017-08-22 | 2018-06-12 | 济宁锦祥科技发展有限公司 | A kind of preparation method of pollution-free food grade meal wash agent |
| CN107841389A (en) * | 2017-09-19 | 2018-03-27 | 谭志华 | A kind of vegetables and fruits cleaning agent and preparation method thereof |
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