CN115636644B - Ceramic tile adhesive and preparation method thereof - Google Patents
Ceramic tile adhesive and preparation method thereof Download PDFInfo
- Publication number
- CN115636644B CN115636644B CN202211336630.7A CN202211336630A CN115636644B CN 115636644 B CN115636644 B CN 115636644B CN 202211336630 A CN202211336630 A CN 202211336630A CN 115636644 B CN115636644 B CN 115636644B
- Authority
- CN
- China
- Prior art keywords
- parts
- tile adhesive
- sodium formate
- water
- tile
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 239000000853 adhesive Substances 0.000 title claims abstract description 58
- 230000001070 adhesive effect Effects 0.000 title claims abstract description 58
- 239000000919 ceramic Substances 0.000 title claims description 22
- 238000002360 preparation method Methods 0.000 title abstract description 12
- 239000000835 fiber Substances 0.000 claims abstract description 46
- 239000001866 hydroxypropyl methyl cellulose Substances 0.000 claims abstract description 41
- 229920003088 hydroxypropyl methyl cellulose Polymers 0.000 claims abstract description 41
- 235000010979 hydroxypropyl methyl cellulose Nutrition 0.000 claims abstract description 41
- UFVKGYZPFZQRLF-UHFFFAOYSA-N hydroxypropyl methyl cellulose Chemical compound OC1C(O)C(OC)OC(CO)C1OC1C(O)C(O)C(OC2C(C(O)C(OC3C(C(O)C(O)C(CO)O3)O)C(CO)O2)O)C(CO)O1 UFVKGYZPFZQRLF-UHFFFAOYSA-N 0.000 claims abstract description 41
- 239000004743 Polypropylene Substances 0.000 claims abstract description 40
- -1 polypropylene Polymers 0.000 claims abstract description 40
- 229920001155 polypropylene Polymers 0.000 claims abstract description 40
- 239000004280 Sodium formate Substances 0.000 claims abstract description 34
- HLBBKKJFGFRGMU-UHFFFAOYSA-M sodium formate Chemical compound [Na+].[O-]C=O HLBBKKJFGFRGMU-UHFFFAOYSA-M 0.000 claims abstract description 34
- 235000019254 sodium formate Nutrition 0.000 claims abstract description 34
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 26
- 239000000843 powder Substances 0.000 claims abstract description 24
- 239000000945 filler Substances 0.000 claims abstract description 19
- 239000002994 raw material Substances 0.000 claims abstract description 18
- 238000002156 mixing Methods 0.000 claims abstract description 15
- 239000004568 cement Substances 0.000 claims abstract description 14
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims abstract description 8
- XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical compound CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 claims abstract description 5
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 claims abstract description 4
- 239000005977 Ethylene Substances 0.000 claims abstract description 4
- 229920002472 Starch Polymers 0.000 claims abstract description 4
- 239000008107 starch Substances 0.000 claims abstract description 4
- 235000019698 starch Nutrition 0.000 claims abstract description 4
- 239000004576 sand Substances 0.000 claims description 23
- 239000002893 slag Substances 0.000 claims description 19
- 238000000034 method Methods 0.000 claims description 7
- 239000012530 fluid Substances 0.000 claims description 6
- 238000009210 therapy by ultrasound Methods 0.000 claims description 3
- 238000004321 preservation Methods 0.000 claims description 2
- 239000000203 mixture Substances 0.000 abstract description 7
- 230000000052 comparative effect Effects 0.000 description 12
- 239000004575 stone Substances 0.000 description 10
- 239000003292 glue Substances 0.000 description 9
- 230000000694 effects Effects 0.000 description 7
- 239000000463 material Substances 0.000 description 6
- 239000000047 product Substances 0.000 description 6
- 230000032683 aging Effects 0.000 description 5
- 239000011148 porous material Substances 0.000 description 5
- 238000003756 stirring Methods 0.000 description 5
- 238000007654 immersion Methods 0.000 description 4
- 230000009286 beneficial effect Effects 0.000 description 3
- 238000001514 detection method Methods 0.000 description 3
- BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 description 2
- 229910001424 calcium ion Inorganic materials 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 230000035484 reaction time Effects 0.000 description 2
- CBOCVOKPQGJKKJ-UHFFFAOYSA-L Calcium formate Chemical compound [Ca+2].[O-]C=O.[O-]C=O CBOCVOKPQGJKKJ-UHFFFAOYSA-L 0.000 description 1
- 229920000663 Hydroxyethyl cellulose Polymers 0.000 description 1
- 239000004354 Hydroxyethyl cellulose Substances 0.000 description 1
- 239000012790 adhesive layer Substances 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 239000011449 brick Substances 0.000 description 1
- 229940044172 calcium formate Drugs 0.000 description 1
- 235000019255 calcium formate Nutrition 0.000 description 1
- 239000004281 calcium formate Substances 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000005034 decoration Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 229920001038 ethylene copolymer Polymers 0.000 description 1
- 239000011468 face brick Substances 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 235000019447 hydroxyethyl cellulose Nutrition 0.000 description 1
- 230000006698 induction Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 239000012466 permeate Substances 0.000 description 1
- 229920002239 polyacrylonitrile Polymers 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- 238000000527 sonication Methods 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/50—Reuse, recycling or recovery technologies
- Y02W30/91—Use of waste materials as fillers for mortars or concrete
Abstract
The application relates to the field of tile paving, in particular to a tile adhesive and a preparation method thereof. The tile adhesive comprises the following raw materials in parts by weight: 450-600 parts of filler, 450-550 parts of cement, 15-30 parts of vinyl acetate/ethylene copolymerized rubber powder, 1-2 parts of hydroxypropyl methyl cellulose, 0.2-0.6 part of starch ether, 5-10 parts of sodium formate, 0.8-1.5 parts of polypropylene fiber and 180-220 parts of water; the preparation method comprises the following steps: uniformly mixing the raw materials except water; then adding water to continuously and uniformly mix to obtain the finished product. The application has the advantage of improving the bonding strength of the tile adhesive.
Description
Technical Field
The application relates to the field of tile paving, in particular to a tile adhesive and a preparation method thereof.
Background
In daily construction, tile placement is usually carried out using cement, tile glue, or the like. Cement is a relatively traditional and widely applied material, and after the cement is dried and fixed, the ceramic tile and the veneers are bonded by mechanical biting force, so that the cement has the advantages of low price, easily available raw materials and simple preparation; however, the defects are obvious, the thickness of the paving is thick, and hollowness is easy to generate. Thus, another material, tile glue, was derived. The tile glue is a new material for modern decoration for sticking tile, face brick, floor tile and other decorative materials. The slurry is utilized to permeate into capillary holes on the back of the ceramic tile, and the adhesive force is formed after induction. The bonding mode of the tile adhesive ensures that phenomena such as hollowing, falling off and the like are not easy to occur between the tile and the veneers.
If the usage amount of the tile adhesive can be further reduced, the adhesive layer is thinned, so that the space and the material consumption can be saved, but the tile is easily detached due to insufficient adhesive strength when the usage amount of the tile adhesive is reduced. Therefore, there is still a need for improvement.
Disclosure of Invention
In order to improve the bonding strength of the tile adhesive, the application provides the tile adhesive and a preparation method thereof.
In a first aspect, the application provides a tile adhesive, which adopts the following technical scheme:
the tile adhesive comprises the following raw materials in parts by weight: 450-600 parts of filler, 450-550 parts of cement, 15-30 parts of vinyl acetate/ethylene copolymerized rubber powder, 1-2 parts of hydroxypropyl methyl cellulose, 0.2-0.6 part of starch ether, 5-10 parts of sodium formate, 0.8-1.5 parts of polypropylene fiber and 180-220 parts of water.
By adopting the technical scheme, under the common coordination of hydroxypropyl methylcellulose, sodium formate and polypropylene fibers, when the hydroxypropyl methylcellulose is reacted with water in a stirring way, a uniform network complex structure can be rapidly formed in the system, and the sodium formate is rapidly attached to the network structure and uniformly distributed on all parts of the system. Moreover, the speed of delaying the saturation of calcium ions can be further improved, so that the system has longer reaction time, and the strength of the adhesive is improved.
The various raw materials are connected together due to the evenly distributed network structure generated in the system. When force acts on the ceramic tile and is transferred to the ceramic tile glue, the ceramic tile glue is used as a whole to bear the force, and the force is rapidly distributed, namely, the force cannot be intensively attacked at a certain point, so that the bonding strength between the ceramic tile and the ceramic tile glue is further improved, and the ceramic tile can be firmly bonded on a veneer.
Preferably, the mass ratio of the hydroxypropyl methylcellulose to the sodium formate to the polypropylene fibers is 1: (3-5): (0.4-0.6).
By adopting the technical scheme, the mass ratio among the hydroxypropyl methylcellulose, the sodium formate and the polypropylene fibers is further limited, the hydroxypropyl methylcellulose and the polypropylene fibers can form a network structure with flexibility and toughness, and the sodium formate can be more firmly attached to the network structure, so that the adhesive strength of the adhesive is further improved.
Preferably, the polypropylene fiber has a single fiber diameter of 22-32mm and a hydroxypropyl methylcellulose viscosity of 10W.
By adopting the technical scheme, the single fiber diameter of the polypropylene fiber and the viscosity of the hydroxypropyl methylcellulose are further limited, and the matching effect between the polypropylene fiber and the hydroxypropyl methylcellulose and between the hydroxypropyl methylcellulose and sodium formate is improved, so that the network structure is more stable, and the polypropylene fiber and the hydroxypropyl methylcellulose are rapidly dispersed in a system and uniformly dispersed.
Preferably, the filler is one or more of river sand, stone tailing Dan Wei placer and slag powder.
Preferably, the filler is river sand, stone tailing Dan Wei placer and slag powder, and the mass ratio of the river sand to the stone tailing Dan Wei placer to the slag powder is 1: (0.2-0.3): (0.1-0.18).
By adopting the technical scheme, the fillers with specific types and proportions are selected to be matched with each other, and are quickly attached to the network structure together and filled in the pores, so that the pores in the system are reduced, the compactness is increased, and the strength is improved. Due to the support of the network structure, the filler is not easy to displace and sink after being dispersed, and has higher stability.
Some tiles laid on the interior walls of a household may be exposed to high intensity, prolonged exposure to sunlight for a long time due to location problems, or severe moisture on the walls during the spring (especially in the southern areas), which may increase the risk of tile falling. The technical scheme provided by the application can effectively improve the stability of the adhesive, thereby improving the applicability of the product in different scenes.
Preferably, the river sand is 80-120 meshes, the Dan Weidan tailing is 50-80 meshes, and the slag powder is 120-160 meshes.
By adopting the technical scheme, the particle size of each filler is further limited, the porosity is reduced, the system is plump, and meanwhile, the filler is matched with the vinyl acetate/ethylene copolymerized rubber powder, so that the loss of cohesive force is reduced, and the tensile bonding strength of the adhesive is improved.
In a second aspect, the application provides a preparation method of a tile adhesive, which adopts the following technical scheme:
the preparation method of the tile adhesive comprises the following steps:
uniformly mixing the raw materials except water; then adding water to continuously and uniformly mix to obtain the finished product.
The preparation method is simple and quick, has lower requirements on equipment, is beneficial to reducing the cost and is suitable for popularization in the field.
Preferably, the hydroxypropyl methylcellulose, sodium formate and polypropylene fibers are mixed, then 35-45 parts of water is taken and mixed, and 800-1000W ultrasonic treatment is carried out to obtain treatment fluid; heat preservation treatment is carried out for 1-3h at 45-60 ℃; and then uniformly mixing the raw materials except the water and the treatment fluid, then adding the treatment fluid for mixing, and then adding and mixing the rest water to obtain a finished product.
By adopting the technical scheme, the hydroxypropyl methylcellulose, the sodium formate and the polypropylene fibers are dispersed in advance, the mutual mixing of the hydroxypropyl methylcellulose, the sodium formate and the polypropylene fibers is promoted, and then the hydroxypropyl methylcellulose, the sodium formate and the polypropylene fibers are added and mixed with other raw materials, so that the matching effect among the hydroxypropyl methylcellulose, the sodium formate and the polypropylene fibers is fully exerted, and the bonding strength of the adhesive is further improved.
In summary, the application has the following beneficial effects:
1. under the common coordination of hydroxypropyl methyl cellulose, sodium formate and polypropylene fiber, when the hydroxypropyl methyl cellulose, sodium formate and polypropylene fiber react with water under stirring, a uniform network complex structure can be formed in the system rapidly, and the sodium formate is rapidly attached to the network structure and uniformly distributed at all parts of the system. Moreover, the speed of delaying the saturation of calcium ions can be further improved, so that the system has longer reaction time, and the strength of the adhesive is improved.
2. The various raw materials are connected together due to the evenly distributed network structure generated in the system. When force acts on the ceramic tile and is transferred to the ceramic tile glue, the ceramic tile glue is used as a whole to bear the force, and the force is rapidly distributed, namely, the force cannot be intensively attacked at a certain point, so that the bonding strength between the ceramic tile and the ceramic tile glue is further improved, and the ceramic tile can be firmly bonded on a veneer.
3. The filler with specific types and proportions is selected to be matched with each other, and is quickly attached to the network structure together and filled in the pores, so that the pores in the system are reduced, the compactness is increased, and the strength is improved. Due to the support of the network structure, the filler is not easy to displace and sink after being dispersed, and has higher stability.
Detailed Description
The present application will be described in further detail with reference to examples.
The raw materials used in the following examples and comparative examples are all commercially available products.
Examples
Example 1
The ceramic tile adhesive is prepared from the following raw materials: filler, cement, vinyl acetate/ethylene copolymer rubber powder, hydroxypropyl methyl cellulose, starch ether, sodium formate, polypropylene fiber and water.
Wherein, the cement is 425 cement, the viscosity of the hydroxypropyl methylcellulose is 10W, and the diameter of the polypropylene fiber single fiber is 22mm.
The mass ratio of the hydroxypropyl methylcellulose to the sodium formate to the polypropylene fiber is 1:5:0.6, i.e. the amount of hydroxypropyl methylcellulose used was 2kg, the amount of sodium formate used was 10kg, and the amount of polypropylene fibers used was 1.2kg.
The filler is river sand, stone tailing Dan Wei placer and slag powder, and the mass ratio of the river sand to the stone tailing Dan Wei placer to the slag powder is 1:0.2:0.18. that is, the amount of river sand was 434.8kg, the amount of Dan Weidan tail sand ore was 87kg, and the amount of slag powder was 78.3kg.
River sand is 80-120 meshes, dan Weidan tailing is 50-80 meshes, and slag powder is 120-160 meshes.
The specific amounts of the raw materials are shown in Table 1.
The embodiment of the application also discloses a preparation method of the tile adhesive, which comprises the following steps:
step 1): and (3) adding the hydroxypropyl methylcellulose, sodium formate and polypropylene fibers into a stirrer, and uniformly mixing. Then, 35 parts of water is taken and mixed and stirred until uniform. Taking out, and performing 800W ultrasonic treatment to obtain a treatment liquid.
Step 2): the temperature is kept at 60 ℃ for 1h.
Step 3): mixing the raw materials except the water and the treatment fluid, and stirring until uniform. Then adding the treatment liquid, mixing and stirring until uniform.
Step 4): adding the rest water into the mixture, and stirring the mixture until the mixture is uniform to obtain a finished product.
Example 2
A tile adhesive differs from example 1 in that the polypropylene fiber single fiber diameter is 32mm. The amounts of the raw materials are different, and are shown in Table 1 in detail.
A method for preparing a tile adhesive differs from example 1 in that,
step 1): 45 parts of water are taken and mixed. Sonication at 1000W was performed.
Step 2): the temperature is kept at 45 ℃ for 3 hours.
Example 3
A tile adhesive differs from example 1 in the amount of each material used, as detailed in Table 1.
Example 4
The tile adhesive is different from example 1 in that the mass ratio of hydroxypropyl methylcellulose, sodium formate and polypropylene fibers is 1:3:0.4, i.e. the amount of hydroxypropyl methylcellulose used was 2kg, the amount of sodium formate used was 6kg, and the amount of polypropylene fibers used was 0.8kg.
Example 5
The tile adhesive is different from example 1 in that the mass ratio of hydroxypropyl methylcellulose, sodium formate and polypropylene fibers is 1:2.5:0.7. namely, the amount of hydroxypropyl methylcellulose used was 2kg, the amount of sodium formate used was 5kg, and the amount of polypropylene fiber used was 1.4kg.
Example 6
The tile adhesive is different from the tile adhesive in that the filler is river sand, stone tailing Dan Wei placer and slag powder, and the mass ratio of the river sand, stone tailing Dan Wei placer to the slag powder is 1:0.3:0.1. namely 428.6kg of river sand, 128.6kg of Dan Weidan tail sand ore and 42.9kg of slag powder.
Example 7
The tile adhesive is different from the tile adhesive in that the filler is river sand, stone tailing Dan Wei placer and slag powder, and the mass ratio of the river sand, stone tailing Dan Wei placer to the slag powder is 1:0.7:0.6. namely, the usage amount of river sand is 260.9kg, the usage amount of Dan Weidan tail sand ore is 182.6kg, and the usage amount of slag powder is 156.5kg.
The amounts used in examples 4-7 are summarized in Table 1.
TABLE 1
Example 8
A tile adhesive differs from example 1 in that the polypropylene fibers have a single fiber diameter of 15mm and hydroxypropyl methylcellulose has a viscosity of 20W.
Example 9
A tile adhesive differs from example 1 in that the filler is river sand.
Example 10
A tile adhesive is different from example 1 in that river sand is 40-70 meshes, dan Weidan tailing is 80-140 meshes, and slag powder is 180-200 meshes.
Example 11
A method for preparing a tile adhesive, which is different from example 1 in that the raw materials except water are mixed and stirred until uniform. Then adding water to continuously and uniformly mix to obtain the finished product.
Comparative example
Comparative example 1
A method for preparing a tile adhesive, which is different from example 1 in that hydroxypropyl methylcellulose is replaced with equal weight of hydroxyethyl cellulose.
Comparative example 2
A method for preparing a tile adhesive, which differs from example 1 in that sodium formate is replaced with an equal weight of calcium formate.
Comparative example 3
A method for preparing a tile adhesive, which is different from example 1 in that the polypropylene fibers are replaced with the polyacrylonitrile fibers of equal weight.
Comparative example 4
A method for preparing a tile adhesive is different from example 1 in that the cement is used in an amount of 600kg.
Comparative example 5
The preparation method of the tile adhesive is different from example 1 in that the usage amount of hydroxypropyl methylcellulose is 5kg, the usage amount of sodium formate is 3.2kg, and the usage amount of polypropylene fiber is 5kg.
Performance test
Detecting an object: examples 1 to 11 and comparative examples 1 to 5.
Detection specification: the specification of the bricks is 40mm by 40mm, and the specification of the cement base plate is 70mm by 70mm.
The detection method comprises the following steps: the samples were tested according to JC/T547-2017 ceramic tile adhesive, and the tensile bonding strength (original strength), tensile bonding strength after soaking and heat aging bonding strength were calculated for 28 days.
The detection results are shown in Table 2.
TABLE 2
As can be seen from the comparison of the data in Table 2 between examples 1-3 and comparative examples 1-3, the tensile bond strength of the tile adhesives of examples 1-3 can still be maintained at a higher level after the original strength, heat aging treatment, and water immersion treatment, than the tensile bond strength of comparative examples 1-3. The ceramic tile adhesive prepared by the cooperation of hydroxypropyl methyl cellulose, sodium formate and polypropylene fibers has a tough network structure, so that the ceramic tile adhesive has good tensile bonding strength. Meanwhile, the adhesive has good flexibility, can be suitable for various different scenes, and can show good tensile bonding strength. As is clear from the comparison of the data in comparative example 4, although the increase in the cement amount can improve the tensile bond strength to some extent, it is not possible to provide a good base system for the blending of other raw materials, and the cement composition exhibits adverse effects in both heat aging treatment and water immersion treatment. It is understood from the data of comparative example 5 that the ratio of the hydroxypropyl methylcellulose, sodium formate, and polypropylene fibers is also important, and the performance of the tile adhesive cannot be sufficiently improved when the ratio of the hydroxypropyl methylcellulose, sodium formate, and polypropylene fibers is out of the range of the present application.
As can be seen from the comparison of the data of examples 1 and 4 and example 5 in table 2, the use ratio and the use amount of the hydroxypropyl methylcellulose, the sodium formate and the polypropylene fiber are further limited, and the matching relationship between the three can be more fully exerted, so that the original strength, the performance after the heat aging treatment and the performance after the water immersion treatment of the tile adhesive are improved.
As can be seen from the comparison of the data of examples 1 and 6 and example 9 in Table 2, the tensile bonding strength of the prepared tile adhesive is obviously improved when the specific river sand, stone tailing Dan Wei placer and slag powder are defined for matching. The comparison of the data in the embodiment 7 shows that when the filler is further limited to be matched in a specific proportion, the pores in the system can be better filled, and the tensile bonding strength of the ceramic tile adhesive after heat aging and water immersion treatment is improved by relying on a network structure. Meanwhile, it is understood from example 10 that the filler of a specific kind can further exert its filling effect after being blended in a specific mesh.
From a comparison of the data in Table 2 for example 1 and example 8, it is clear that the different parameters of hydroxypropyl methylcellulose and polypropylene fibers also have an effect on the performance of the tile adhesives. The hydroxypropyl methylcellulose and polypropylene fibers which are specifically selected can have better matching effect.
As can be seen from the comparison of the data of example 1 and example 11 in table 2, the pretreatment of hydroxypropyl methylcellulose, sodium formate and polypropylene fibers is beneficial to better dispersing effect in the system, and a stronger network structure is formed, so that the performance of the tile adhesive is improved.
The present embodiment is only for explanation of the present application and is not to be construed as limiting the present application, and modifications to the present embodiment, which may not creatively contribute to the present application as required by those skilled in the art after reading the present specification, are all protected by patent laws within the scope of claims of the present application.
Claims (3)
1. The ceramic tile adhesive is characterized by comprising the following raw materials in parts by weight: 450-600 parts of filler, 450-550 parts of cement, 15-30 parts of vinyl acetate/ethylene copolymerized rubber powder, 1-2 parts of hydroxypropyl methyl cellulose, 0.2-0.6 part of starch ether, 5-10 parts of sodium formate, 0.8-1.5 parts of polypropylene fiber and 180-220 parts of water;
the mass ratio of the hydroxypropyl methylcellulose to the sodium formate to the polypropylene fibers is 1: (3-5): (0.4-0.6);
the filler is river sand, dan Wei placer and slag powder, and the mass ratio of the river sand to the Dan Wei placer to the slag powder is 1: (0.2-0.3): (0.1-0.18).
2. The tile adhesive of claim 1, wherein: the river sand is 80-120 meshes, the Dan Wei placer is 50-80 meshes, and the slag powder is 120-160 meshes.
3. A method for preparing a tile adhesive based on any one of claims 1-2, characterized by: mixing the hydroxypropyl methylcellulose, sodium formate and polypropylene fibers, mixing 35-45 parts of water, and performing 800-1000W ultrasonic treatment to obtain a treatment solution; heat preservation treatment is carried out for 1-3h at 45-60 ℃; and then uniformly mixing the raw materials except the water and the treatment fluid, then adding the treatment fluid for mixing, and then adding and mixing the rest water to obtain a finished product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202211336630.7A CN115636644B (en) | 2022-10-28 | 2022-10-28 | Ceramic tile adhesive and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202211336630.7A CN115636644B (en) | 2022-10-28 | 2022-10-28 | Ceramic tile adhesive and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN115636644A CN115636644A (en) | 2023-01-24 |
| CN115636644B true CN115636644B (en) | 2023-08-22 |
Family
ID=84946646
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202211336630.7A Active CN115636644B (en) | 2022-10-28 | 2022-10-28 | Ceramic tile adhesive and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN115636644B (en) |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20080103135A (en) * | 2007-05-23 | 2008-11-27 | 최문길 | The dry mortar with soundproof and keeping warm and the noninflammable board therewith and light brick therewith |
| CN113277804A (en) * | 2021-05-27 | 2021-08-20 | 河南伯高节能科技有限公司 | Ceramic tile glue and preparation method thereof |
-
2022
- 2022-10-28 CN CN202211336630.7A patent/CN115636644B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20080103135A (en) * | 2007-05-23 | 2008-11-27 | 최문길 | The dry mortar with soundproof and keeping warm and the noninflammable board therewith and light brick therewith |
| CN113277804A (en) * | 2021-05-27 | 2021-08-20 | 河南伯高节能科技有限公司 | Ceramic tile glue and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN115636644A (en) | 2023-01-24 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JP5165371B2 (en) | Water-soluble sulfo group-containing copolymer, process for its production and use | |
| CN1075826C (en) | Redispersible dispersion powder composition | |
| CN1061637C (en) | Ready-mixed, setting type joint compound | |
| CN100577602C (en) | Dry powder ceramic tile binding agent | |
| KR100837790B1 (en) | Floor finishing material composition of self-levelling usung water soluble synthetic rubber latex | |
| US20020195025A1 (en) | Building materials employing powder compositions as rheological additives | |
| CN104402367B (en) | Without the high-strength ceramic tile adhesive of the accumulation of salt in the surface soil | |
| CN112374833B (en) | Benzene-free ceramic tile daub | |
| CN112209690A (en) | Cement-based ceramic tile binder and preparation method thereof | |
| CN112608115A (en) | Self-leveling mortar and preparation process thereof | |
| CN110317026B (en) | Ceramic tile glue | |
| CN113372083B (en) | Graphene oxide based layered material modified self-leveling mortar and preparation method thereof | |
| CN115636644B (en) | Ceramic tile adhesive and preparation method thereof | |
| CN111205031A (en) | Ceramic tile glue | |
| CN101215130B (en) | Modified facing brick binding agent and preparation method thereof | |
| JP2016505496A (en) | Additives for water curable mixtures | |
| CN112645676A (en) | Quick-drying quick-hardening water-resistant putty for interior walls and preparation method thereof | |
| KR101030375B1 (en) | 2-component epoxy resin type adhesives for ceramic tiles | |
| JP2007320786A (en) | Dispersant for gypsum and dispersant composition for gypsum | |
| CN111777393B (en) | Quick-drying elastic repair mortar with micro-expansibility and preparation method thereof | |
| CN108863222A (en) | Boundary mortar and preparation method thereof | |
| CN110922106B (en) | Building waste recycled aggregate masonry mortar and preparation method thereof | |
| CN108949072B (en) | A kind of micro- water imbibition ceramic tile bond and preparation method | |
| CN113677646A (en) | Powder composition | |
| CN111039587B (en) | Reinforcing agent suitable for cement-based tile adhesive and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A ceramic tile adhesive and its preparation method Effective date of registration: 20231124 Granted publication date: 20230822 Pledgee: Jieyang Branch of Guangdong Nanyue Bank Co.,Ltd. Pledgor: GUANGDONG LUCKERKONG BIOTECH CO.,LTD. Registration number: Y2023980067460 |
|
| PE01 | Entry into force of the registration of the contract for pledge of patent right |