CN112645676A - Quick-drying quick-hardening water-resistant putty for interior walls and preparation method thereof - Google Patents

Quick-drying quick-hardening water-resistant putty for interior walls and preparation method thereof Download PDF

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Publication number
CN112645676A
CN112645676A CN202011580725.4A CN202011580725A CN112645676A CN 112645676 A CN112645676 A CN 112645676A CN 202011580725 A CN202011580725 A CN 202011580725A CN 112645676 A CN112645676 A CN 112645676A
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China
Prior art keywords
quick
hardening
drying
resistant putty
water
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CN202011580725.4A
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Inventor
仲崇磊
陈杰
刘月龙
李小亮
程金龙
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Shanghai Sankeshu Waterproof Technology Co ltd
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Shanghai Sankeshu Waterproof Technology Co ltd
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    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B28/00Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
    • C04B28/14Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing calcium sulfate cements
    • C04B28/16Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing calcium sulfate cements containing anhydrite, e.g. Keene's cement
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/20Resistance against chemical, physical or biological attack
    • C04B2111/27Water resistance, i.e. waterproof or water-repellent materials
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/34Non-shrinking or non-cracking materials
    • C04B2111/343Crack resistant materials
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/80Optical properties, e.g. transparency or reflexibility
    • C04B2111/82Coloured materials
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2201/00Mortars, concrete or artificial stone characterised by specific physical values
    • C04B2201/10Mortars, concrete or artificial stone characterised by specific physical values for the viscosity
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2201/00Mortars, concrete or artificial stone characterised by specific physical values
    • C04B2201/50Mortars, concrete or artificial stone characterised by specific physical values for the mechanical strength

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Organic Chemistry (AREA)
  • Curing Cements, Concrete, And Artificial Stone (AREA)

Abstract

The invention relates to quick-drying quick-hardening interior wall water-resistant putty and a preparation method thereof, wherein the quick-drying quick-hardening interior wall water-resistant putty is mainly prepared from the following components in parts by weight:

Description

Quick-drying quick-hardening water-resistant putty for interior walls and preparation method thereof
Technical Field
The invention relates to quick-drying quick-hardening interior wall water-resistant putty and a preparation method thereof, which are applied to the field of production of decoration product binders.
Background
The existing water-resistant putty for indoor buildings in the market mostly uses white portland cement as a cementing material, and has the advantages of low early strength, slow strength increasing speed, large shrinkage rate, high cracking risk and long curing time (generally requiring about 7 days), so that the construction period is greatly prolonged. And the construction period is long and the time cost is very high. Therefore, it is a need to provide a water-resistant quick-drying putty for interior walls, which has excellent properties, rapid strength development, high early strength, low shrinkage rate and short curing time, and a preparation method thereof.
Disclosure of Invention
In order to overcome the defects that the existing water-resistant putty for buildings mostly uses white portland cement as a cementing material, has low early strength, slow strength increasing speed, large shrinkage rate, high cracking risk, long curing time and the like, the invention provides the quick-drying quick-hardening interior wall water-resistant putty and the preparation method thereof.
The technical scheme of the invention is as follows:
a quick-drying quick-hardening water-resistant putty for interior walls is mainly prepared from the following components in parts by weight:
Figure BDA0002865179400000011
Figure BDA0002865179400000021
the quick-drying quick-hardening interior wall water-resistant putty is developed by using white aluminate cement, white silicate cement, anhydrite and hemihydrate gypsum as basic cementing materials to replace cementing materials of the conventional putty, namely, the white silicate cement. The white aluminate cement is special cement, has early strength, and has the situation of reverse shrinkage in later strength. The early strength of the white silicate cement is low, the later strength is slowly enhanced, the white silicate cement and the white aluminate cement are complementary, and the properly compounded cementing material of the white silicate cement and the white aluminate cement can be hydrated to accelerate the setting and hardening time. Reacting gypsum (anhydrite and semihydrate gypsum) with cement (aluminate cement and white silicate cement) to produce ettringite, wherein the ettringite has an expansion phase, so that the hardening shrinkage of the cement can be compensated, and the risk of cracking of a cementing material is reduced; the hemihydrate gypsum has a high reaction speed, so that the cementing material can be well compensated for plastic shrinkage in a plastic stage, and the anhydrite gypsum is used for compensating for volume shrinkage of the cementing material in a later hardening stage. Calcium carbonate is a filler and does not participate in the reaction of the cementitious material. The latex powder is added to sublimate the product, so that the product has better construction performance, the cohesive force of the product is increased, the tensile strength is improved, the bending strength is enhanced, the elastic modulus is reduced, the deformability is improved, and tests such as freeze-thaw cycle and thermal aging are not needed. The viscosity of the product can be adjusted by adding cellulose ether, and the constructability and the water-retaining property of the product are improved. The addition of the starch ether ensures the anti-slip performance of the product. The water reducing agent is used, so that the product has better product stirring comfort and product workability on the premise of ensuring water demand. The addition of the polyvinyl alcohol can enable the surface of the cementing material to have better film-forming strength. The early strength agent can accelerate the early strength of the cementing material, and the retarder can be used for adjusting the construction time of the product.
By taking the white aluminate cement, the white silicate cement, the anhydrite and the hemihydrate gypsum as the basic cementing materials and matching with other preferred components and dosage ratios thereof in a system, the quick-drying quick-hardening water-resistant putty for the inner wall has the characteristics of quick-drying and quick-hardening, quick strength development, high early strength, low shrinkage rate and short curing time, can be coated with emulsion paint after 6 hours after construction, greatly shortens the curing time and the construction period, is suitable for application occasions such as short project construction period, quick renovation and client driving time, can effectively save time and cost, has excellent performance, ensures the quality and is safe to use.
The preparation method of the quick-drying quick-hardening interior wall water-resistant putty is characterized by comprising the following steps: mainly comprises the following steps which are carried out in sequence:
mixing cellulose ether, starch ether, a water reducing agent, polyvinyl alcohol, an early strength agent and a retarder to obtain a master batch;
secondly, turning on a stirring blade of the mixer but not turning on a fly cutter, firstly adding calcium carbonate inwards, then sequentially adding the white aluminate cement, the master batch obtained in the step one, the white silicate cement, the anhydrous anhydrite, the semi-hydrated gypsum and the latex powder inwards, and stirring for at least 2 minutes;
thirdly, regulating the rotating speed of the stirring blades to 240 revolutions per minute, and stirring the mixture obtained in the step (II) for at least 3 minutes;
and (IV) starting a fly cutter of the mixer while keeping the rotating speed of the stirring blades at 240 revolutions per minute, wherein the rotating speed of the fly cutter is 3000 revolutions per minute, and dispersing the mixture obtained in the step (III) to be uniform to obtain the quick-drying quick-hardening inner wall water-resistant putty.
The preparation method of the quick-drying quick-hardening interior wall water-resistant putty is simple and convenient in procedure, convenient to operate and convenient to popularize.
Compared with the prior art, the method has the following advantages:
1) the quick-drying quick-hardening interior wall water-resistant putty has the characteristics of quick-drying quick-hardening and strong strength, quick development of strength, high early strength, low shrinkage rate and short curing time by matching the white aluminate cement, white silicate cement, anhydrite and hemihydrate gypsum as basic cementing materials with other preferable components and dosage ratios thereof in a system;
2) the preparation method of the quick-drying quick-hardening interior wall water-resistant putty is simple and convenient in procedure, convenient to operate and convenient to popularize.
Detailed Description
The technical solution of the present invention will be described in detail with reference to the embodiments of the specification.
Example 1
The quick-drying quick-hardening interior wall water-resistant putty is mainly prepared from the following components in parts by weight:
Figure BDA0002865179400000031
the preparation method of the quick-drying quick-hardening interior wall water-resistant putty mainly comprises the following steps of:
mixing cellulose ether, starch ether, a water reducing agent, polyvinyl alcohol, an early strength agent and a retarder to obtain a master batch;
secondly, turning on a stirring blade of the mixer but not turning on a fly cutter, firstly adding calcium carbonate inwards, then sequentially adding the white aluminate cement, the master batch obtained in the step one, the white silicate cement, the anhydrous anhydrite, the semi-hydrated gypsum and the latex powder inwards, and stirring for 2 minutes;
thirdly, regulating the rotation speed of the stirring blades to 240 revolutions per minute, and stirring the mixture obtained in the step (II) for 3 minutes;
and (IV) starting a fly cutter of the mixer while keeping the rotating speed of the stirring blades at 240 revolutions per minute, wherein the rotating speed of the fly cutter is 3000 revolutions per minute, and dispersing the mixture obtained in the step (III) to be uniform to obtain the quick-drying quick-hardening inner wall water-resistant putty.
Example 2
The quick-drying quick-hardening interior wall water-resistant putty is mainly prepared from the following components in parts by weight:
Figure BDA0002865179400000041
the preparation method of the quick-drying quick-hardening interior wall water-resistant putty mainly comprises the following steps of:
mixing cellulose ether, starch ether, a water reducing agent, polyvinyl alcohol, an early strength agent and a retarder to obtain a master batch;
secondly, turning on a stirring blade of the mixer but not turning on a fly cutter, firstly adding calcium carbonate inwards, then sequentially adding the white aluminate cement, the master batch obtained in the step one, the white silicate cement, the anhydrous anhydrite, the semi-hydrated gypsum and the latex powder inwards, and stirring for 5 minutes;
thirdly, regulating the rotating speed of the stirring blades to 260 revolutions per minute, and stirring the mixture obtained in the step (II) for 5 minutes;
and (IV) starting a fly cutter of the mixer while keeping the rotating speed of the stirring blades at 260 revolutions per minute, wherein the rotating speed of the fly cutter is 2500 revolutions per minute, and dispersing the mixture obtained in the step (III) to be uniform to obtain the quick-drying quick-hardening inner wall water-resistant putty.
Example 3
The quick-drying quick-hardening interior wall water-resistant putty is mainly prepared from the following components in parts by weight:
Figure BDA0002865179400000042
Figure BDA0002865179400000051
the preparation method of the quick-drying quick-hardening interior wall water-resistant putty mainly comprises the following steps of:
mixing cellulose ether, starch ether, a water reducing agent, polyvinyl alcohol, an early strength agent and a retarder to obtain a master batch;
secondly, turning on a stirring blade of the mixer but not turning on a fly cutter, firstly adding calcium carbonate inwards, then sequentially adding the white aluminate cement, the master batch obtained in the step one, the white silicate cement, the anhydrous anhydrite, the semi-hydrated gypsum and the latex powder inwards, and stirring for 8 minutes;
thirdly, regulating the rotating speed of the stirring blades to 220 revolutions per minute, and stirring the mixture obtained in the step (II) for 8 minutes;
and (IV) starting a fly cutter of the mixer while keeping the rotating speed of the stirring blades at 220 rpm, wherein the rotating speed of the fly cutter is 3500 rpm, and dispersing the mixture obtained in the step (III) to be uniform to obtain the quick-drying quick-hardening inner wall water-resistant putty.
Equipment and raw material sources are as follows:
a mixer: the stirring blades being arranged on a central rotating shaft and the fly-cutter being arranged on the inner wall, e.g. Mottack MR-150
Experimental data:
the test method comprises the following steps: according to JG/T298-2010
And (3) comparison: waterproof putty powder for Xian Ding Ke
Figure BDA0002865179400000052
Figure BDA0002865179400000061
As can be seen from the above table, the quick-drying quick-hardening interior wall water-resistant putty not only completely meets the JG/T298-2010 technical standard, but also has shorter drying time and higher bonding strength compared with the existing commercial products.
The quick-drying quick-hardening water-resistant putty for interior walls and the preparation method thereof according to the present invention are not limited to the above-mentioned examples, and any modification or replacement according to the principle of the present invention should be within the scope of the present invention.

Claims (2)

1. The quick-drying quick-hardening water-resistant putty for inner walls is characterized in that: the adhesive is mainly prepared from the following components in parts by weight:
Figure FDA0002865179390000011
2. the method for preparing a water resistant putty for quick-drying and quick-hardening interior walls according to claim 1, wherein: mainly comprises the following steps which are carried out in sequence:
mixing cellulose ether, starch ether, a water reducing agent, polyvinyl alcohol, an early strength agent and a retarder to obtain a master batch;
secondly, starting a stirring blade of the mixer but not starting a fly cutter, wherein the rotating speed of the stirring blade is 100-;
thirdly, the rotation speed of the stirring blade is adjusted to 220-260 rpm, and the mixture obtained in the second step is stirred for at least 3 minutes;
and (IV) keeping the rotating speed of the stirring blades at 220-.
CN202011580725.4A 2020-12-28 2020-12-28 Quick-drying quick-hardening water-resistant putty for interior walls and preparation method thereof Pending CN112645676A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113860842A (en) * 2021-10-28 2021-12-31 河北三棵树涂料有限公司 Inorganic single-component polymer tile back glue and preparation method thereof
CN115232504A (en) * 2022-07-14 2022-10-25 中建材创新科技研究院有限公司 Interior wall putty

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1260369A (en) * 1999-01-12 2000-07-19 常大勇 Putty for plastering
CN102875089A (en) * 2012-09-29 2013-01-16 北京东方雨虹防水技术股份有限公司 Low-alkali water-proof putty powder and preparation and utilization method thereof
CN104250466A (en) * 2014-09-27 2014-12-31 安徽铁创新材料科技有限公司 Water-resistant inner wall putty powder
CN108997812A (en) * 2018-09-26 2018-12-14 河北晨阳工贸集团有限公司 A kind of water-water multi-color is dedicated to exempt from priming paint black dry-powder putty and preparation method thereof
WO2020043644A1 (en) * 2018-08-29 2020-03-05 Akzo Nobel Coatings International B.V. Dry powder composition, putty composition obtainable from such composition, and substrate coated with such putty composition

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1260369A (en) * 1999-01-12 2000-07-19 常大勇 Putty for plastering
CN102875089A (en) * 2012-09-29 2013-01-16 北京东方雨虹防水技术股份有限公司 Low-alkali water-proof putty powder and preparation and utilization method thereof
CN104250466A (en) * 2014-09-27 2014-12-31 安徽铁创新材料科技有限公司 Water-resistant inner wall putty powder
WO2020043644A1 (en) * 2018-08-29 2020-03-05 Akzo Nobel Coatings International B.V. Dry powder composition, putty composition obtainable from such composition, and substrate coated with such putty composition
CN108997812A (en) * 2018-09-26 2018-12-14 河北晨阳工贸集团有限公司 A kind of water-water multi-color is dedicated to exempt from priming paint black dry-powder putty and preparation method thereof

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* Cited by examiner, † Cited by third party
Title
傅德海等: "《干粉砂浆应用指南》", 30 April 2006, 中国建材工业出版社 *
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江苏一夫科技股份有限公司: "《工业副产石膏研究报告汇编》", 31 January 2014, 中国建材工业出版社 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113860842A (en) * 2021-10-28 2021-12-31 河北三棵树涂料有限公司 Inorganic single-component polymer tile back glue and preparation method thereof
CN115232504A (en) * 2022-07-14 2022-10-25 中建材创新科技研究院有限公司 Interior wall putty

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