CN113956005A - Self-leveling mortar and preparation method thereof - Google Patents

Self-leveling mortar and preparation method thereof Download PDF

Info

Publication number
CN113956005A
CN113956005A CN202111488649.9A CN202111488649A CN113956005A CN 113956005 A CN113956005 A CN 113956005A CN 202111488649 A CN202111488649 A CN 202111488649A CN 113956005 A CN113956005 A CN 113956005A
Authority
CN
China
Prior art keywords
self
leveling mortar
gypsum
powder
reducing agent
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202111488649.9A
Other languages
Chinese (zh)
Inventor
潘定邦
易嘉桢
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hunan Huacai Aia Technology Co ltd
Original Assignee
Hunan Huacai Aia Technology Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hunan Huacai Aia Technology Co ltd filed Critical Hunan Huacai Aia Technology Co ltd
Priority to CN202111488649.9A priority Critical patent/CN113956005A/en
Publication of CN113956005A publication Critical patent/CN113956005A/en
Pending legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B28/00Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
    • C04B28/02Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
    • C04B28/06Aluminous cements
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/60Flooring materials
    • C04B2111/62Self-levelling compositions
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2201/00Mortars, concrete or artificial stone characterised by specific physical values
    • C04B2201/50Mortars, concrete or artificial stone characterised by specific physical values for the mechanical strength

Abstract

The invention discloses self-leveling mortar which comprises the following materials in percentage by weight: 20-70% of high-strength gypsum powder, 0-30% of light calcium powder, 0-50% of heavy calcium powder, 0-40% of portland cement, 0-20% of high-alumina cement, 0-30% of quartz sand, 0.1-3% of cellulose ether, 0.1-3% of water reducing agent, 0.1-3% of dispersing agent, 0.1-10% of powdery adhesive and 1-5% of gypsum retarder, the invention improves the overall performance of the self-leveling mortar by the superposition of functions of the water reducing agent, the gypsum retarder, the dispersing agent, the powdery adhesive and the like, has the characteristics of water resistance, wear resistance and one-time construction thickness of 3-50mm, can be applied to various environments indoors and outdoors, obviously improves the decoration quality of buildings and saves a large amount of labor cost, and in addition, the preparation method of the self-leveling mortar is safe, environment-friendly, simple, convenient and rapid, and has low requirements on production equipment, is favorable for reducing the production cost of enterprises.

Description

Self-leveling mortar and preparation method thereof
Technical Field
The invention relates to the field of building materials, in particular to self-leveling mortar and a preparation method thereof.
Background
Recently, cement and gypsum materials are widely applied in building decoration processes, and hydration products of the cement and gypsum materials have high compressive strength and rupture strength and are good decoration and finishing materials. But the gypsum-based self-leveling mortar also has the defects of poor cement material cohesiveness, easy shrinkage, hollowing and cracking, low relative strength of gypsum materials, water intolerance, incapability of being used in a humid environment and the like, and is prepared from high-strength gypsum, cement, fine aggregate and various building chemical additives. The gypsum-based self-leveling has the advantages of high levelness and difficult hollowing and cracking. Most manufacturers adopt building gypsum for preparation, and ensure that the corresponding performance requirements are met by increasing the doping amount of a chemical additive, and the cost of the additive accounts for about two thirds of the production cost of the self-leveling gypsum, so that the application cost of the self-leveling gypsum is higher than that of cement mortar, the popularization and the application are hindered, and the development is slow.
The invention with the publication number of CN109694228B discloses gypsum-based self-leveling mortar and a preparation method thereof, wherein the gypsum-based self-leveling mortar comprises SiO2 aerogel, portland cement, desulfurized gypsum, a retarder, a water reducing agent, latex powder, a stabilizer and a filler, and the SiO2 aerogel is prepared by adopting the following method: preparing the silane coupling agent into a silane coupling agent solution by using water; adding the hydrophobic SiO2 aerogel into the silane coupling agent solution, and stirring until the hydrophobic SiO2 aerogel is completely dissolved in the silane coupling agent solution; the preparation method of the gypsum-based self-leveling mortar comprises the following steps: surface modifying hydrophobic SiO2 aerogel with silane coupling agent; mixing the modified SiO2 aerogel with portland cement, and performing ball milling; adding other components, and mixing. The present application also provides gypsum-based self-leveling slurries prepared using the above-described gypsum-based self-leveling mortars, which, however, are not water-resistant.
Disclosure of Invention
The invention aims to overcome the defects in the prior art and provide the self-leveling mortar which is waterproof and wear-resistant and can be applied to various indoor and outdoor environments.
The invention also aims to overcome the defects in the prior art and provide the preparation method of the self-leveling mortar with simple and reliable preparation process and convenient operation.
The purpose of the invention is realized by the following technical scheme:
the self-leveling mortar comprises the following materials in percentage by weight: 20-70% of high-strength gypsum powder, 0-30% of light calcium powder, 0-50% of heavy calcium powder, 0-40% of portland cement, 0-20% of high-alumina cement, 0-30% of quartz sand, 0.1-3% of cellulose ether, 0.1-3% of a water reducing agent, 0.1-3% of a dispersing agent, 0.1-10% of a powdery adhesive and 1-5% of a gypsum retarder.
Further, the cellulose ether is one or more of hydroxypropyl methyl cellulose ether, hydroxyethyl methyl cellulose ether and hydroxyethyl cellulose ether, and the viscosity of an aqueous solution of the hydroxyethyl methyl cellulose with a mass concentration of 2% at 25 ℃ is 6000mPa & s-22000mPa & s.
Further, the gypsum retarder is tartaric acid, citric acid or salts thereof.
Further, the powdery adhesive is polyvinyl alcohol.
Further, the water reducing agent is selected from one or more of an ether polycarboxylic acid water reducing agent and an ester polycarboxylic acid water reducing agent.
A preparation method of self-leveling mortar comprises the following steps:
step one, sequentially adding high-strength gypsum powder, light calcium powder, heavy calcium powder, portland cement, high-alumina cement and quartz sand into a gravity-free powder stirrer, and stirring for 10 minutes;
and step two, sequentially adding the cellulose ether, the water reducing agent, the dispersing agent, the powdery adhesive and the gypsum retarder, and continuously stirring for 30 minutes until the mixture is uniformly stirred.
Further, the rotation speed of the stirring is 200-300 r/min.
Compared with the prior art, the invention has the following advantages and beneficial effects:
the invention reasonably utilizes the grading combination to improve the workability, mechanical property and durability of the self-leveling mortar; the powder material mainly improves the working performance, the later strength and the durability of the self-leveling mortar. The self-leveling mortar also comprises functional components, the overall performance of the self-leveling mortar is improved mainly by the superposition of functions of a water reducing agent, a gypsum retarder, a dispersing agent, a powdery adhesive and the like, and the self-leveling mortar has the characteristics of water resistance, wear resistance and one-time construction thickness of 3-50mm, can be applied to various indoor and outdoor environments, remarkably improves the building decoration quality and saves a large amount of labor cost.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The self-leveling mortar comprises the following materials in percentage by weight: 20-70% of high-strength gypsum powder, 0-30% of light calcium powder, 0-50% of heavy calcium powder, 0-40% of portland cement, 0-20% of high-alumina cement, 0-30% of quartz sand, 0.1-3% of cellulose ether, 0.1-3% of a water reducing agent, 0.1-3% of a dispersing agent, 0.1-10% of a powdery adhesive and 1-5% of a gypsum retarder.
The cellulose ether is one or a mixture of more of hydroxypropyl methyl cellulose ether, hydroxyethyl methyl cellulose ether and hydroxyethyl cellulose ether, the viscosity of an aqueous solution of the hydroxyethyl methyl cellulose with the mass concentration of 2% is 6000mPa & s-22000mPa & s at 25 ℃, and the self-leveling mortar has good construction performance by utilizing the water retention, thickening and air entraining functions of the cellulose ether in the self-leveling mortar, and can reduce the phenomena of chalking and cracking of the self-leveling mortar after the self-leveling mortar is applied to a wall.
The gypsum retarder is tartaric acid, citric acid or salts thereof, and the retarder is used for prolonging the hydration hardening time of the self-leveling mortar, so that the freshly mixed self-leveling mortar can keep plasticity for a long time, and the setting time of the freshly mixed self-leveling mortar is adjusted.
The powdery adhesive is polyvinyl alcohol, and the powdery adhesive is moved to an interface or a surface of self-leveling mortar along with water by utilizing the water solubility of the polyvinyl alcohol, is gathered and formed into a film at the interface, and is used for connecting and filling gaps and pores in an interface transition area so as to greatly improve the bonding strength.
The water reducing agent is selected from one or more of an ether polycarboxylic acid water reducing agent and an ester polycarboxylic acid water reducing agent.
A preparation method of self-leveling mortar comprises the following steps:
step one, sequentially adding high-strength gypsum powder, light calcium powder, heavy calcium powder, portland cement, high-alumina cement and quartz sand into a gravity-free powder stirrer, and stirring for 10 minutes;
and step two, sequentially adding the cellulose ether, the water reducing agent, the dispersing agent, the powdery adhesive and the gypsum retarder, and continuously stirring for 30 minutes until the mixture is uniformly stirred.
The rotating speed of the stirring is 200-300 r/min.
Example one
A self-leveling mortar is prepared from 450kg of high-strength gypsum powder, 100kg of light calcium powder, 50kg of heavy calcium powder, 100kg of portland cement, 50kg of high-alumina cement, 233kg of quartz sand, 1kg of cellulose ether, 3kg of a water reducing agent, 2kg of a dispersing agent, 10kg of a powdery adhesive and 1kg of a gypsum retarder.
A preparation method of self-leveling mortar comprises the following steps:
step one, sequentially adding high-strength gypsum powder, light calcium powder, heavy calcium powder, portland cement, high-alumina cement and quartz sand into a gravity-free powder stirrer, and stirring for 10 minutes;
and step two, sequentially adding the cellulose ether, the water reducing agent, the dispersing agent, the powdery adhesive and the gypsum retarder, and continuously stirring for 30 minutes until the mixture is uniformly stirred.
The rotating speed of the stirring is 250 r/min.
Example two
A self-leveling mortar is prepared from 420kg of high-strength gypsum powder, 120kg of light calcium powder, 60kg of heavy calcium powder, 100kg of portland cement, 60kg of high-alumina cement, 223kg of quartz sand, 1kg of cellulose ether, 2.5kg of a water reducing agent, 2.5kg of a dispersing agent, 10kg of a powdery adhesive and 1kg of a gypsum retarder.
A preparation method of self-leveling mortar comprises the following steps:
step one, sequentially adding high-strength gypsum powder, light calcium powder, heavy calcium powder, portland cement, high-alumina cement and quartz sand into a gravity-free powder stirrer, and stirring for 15 minutes;
and step two, sequentially adding cellulose ether, a water reducing agent, a dispersing agent, a powdery adhesive and a gypsum retarder, and continuously stirring for 35 minutes until the mixture is uniformly stirred.
The rotating speed of the stirring is 260 r/min.
EXAMPLE III
A self-leveling mortar is prepared from 430kg of high-strength gypsum powder, 120kg of light calcium powder, 55kg of heavy calcium powder, 95kg of Portland cement, 70kg of high-alumina cement, 213kg of quartz sand, 1kg of cellulose ether, 3kg of a water reducing agent, 2.5kg of a dispersing agent, 9kg of a powdery adhesive and 1.5kg of a gypsum retarder.
A preparation method of self-leveling mortar comprises the following steps:
step one, sequentially adding high-strength gypsum powder, light calcium powder, heavy calcium powder, portland cement, high-alumina cement and quartz sand into a gravity-free powder stirrer, and stirring for 20 minutes;
and step two, sequentially adding the cellulose ether, the water reducing agent, the dispersing agent, the powdery adhesive and the gypsum retarder, and continuously stirring for 30 minutes until the mixture is uniformly stirred.
The rotating speed of the stirring is 270 r/min.
The self-leveling mortar obtained by screening and combining is further reduced in cost on the basis of contribution to stability through synergistic interaction among the components, so that the self-leveling mortar is green and environment-friendly.
TABLE 1 self-leveling mortar Properties
Figure BDA0003398326870000041
TABLE 1
Figure BDA0003398326870000051
Comparative examples 1 to 3
Comparative examples 1 to 3 provide a self-leveling mortar, which is different from the first to third examples in that: the high-strength gypsum powder, the portland cement and the high-alumina cement are different in mass ratio, and the raw materials of the high-strength gypsum powder, the portland cement and the high-alumina cement are shown in a table 2:
table 2 raw material composition of the self-leveling mortar of comparative examples 1 to 3:
Figure BDA0003398326870000052
the stirring rotation speeds of comparative examples 1 to 3 were all set to 250 r/min.
TABLE 3 Properties of self-leveling mortars of comparative examples 1 to 3
Figure BDA0003398326870000053
By combining the tables 1 and 3, it can be seen that the performances of the comparative examples 1 to 3 are all inferior to those of the examples one to three, the flowability in half an hour is not changed greatly, the breaking strength and the compressive strength are low, the tensile bonding strength is not high, even the comparative examples 1 and 2 can crack, and compared with the tensile bonding strength, the compressive strength and the breaking resistance of the examples one to three are better, and the waterproof and wear-resistant composite material has the characteristics of water resistance, wear resistance and one-time construction thickness of 3-50mm, and can be applied to various environments indoors and outdoors.
It should be understood that the above-described embodiments are merely preferred embodiments of the present invention and the technical principles applied thereto, and that any changes, modifications, substitutions, combinations and simplifications made by those skilled in the art without departing from the spirit and principle of the present invention shall be regarded as equivalent substitutions and shall be covered by the protection scope of the present invention.

Claims (7)

1. The self-leveling mortar is characterized by comprising the following materials in percentage by weight: 20-70% of high-strength gypsum powder, 0-30% of light calcium powder, 0-50% of heavy calcium powder, 0-40% of portland cement, 0-20% of high-alumina cement, 0-30% of quartz sand, 0.1-3% of cellulose ether, 0.1-3% of a water reducing agent, 0.1-3% of a dispersing agent, 0.1-10% of a powdery adhesive and 1-5% of a gypsum retarder.
2. The self-leveling mortar of claim 1, wherein: the cellulose ether is one or more of hydroxypropyl methyl cellulose ether, hydroxyethyl methyl cellulose ether and hydroxyethyl cellulose ether, and the viscosity of an aqueous solution of hydroxyethyl methyl cellulose with the mass concentration of 2% at 25 ℃ is 6000 mPa-s-22000 mPa-s.
3. The self-leveling mortar of claim 2, wherein: the gypsum retarder is tartaric acid, citric acid or its salts.
4. The self-leveling mortar of claim 3, wherein: the powdery adhesive is polyvinyl alcohol.
5. The self-leveling mortar of claim 4, wherein: the water reducing agent is selected from one or more of an ether polycarboxylic acid water reducing agent and an ester polycarboxylic acid water reducing agent.
6. A method of preparing a self-levelling mortar according to any one of claims 1 to 5, comprising:
step one, sequentially adding high-strength gypsum powder, light calcium powder, heavy calcium powder, portland cement, high-alumina cement and quartz sand into a gravity-free powder stirrer, and stirring for 10 minutes;
and step two, sequentially adding the cellulose ether, the water reducing agent, the dispersing agent, the powdery adhesive and the gypsum retarder, and continuously stirring for 30 minutes until the mixture is uniformly stirred.
7. The method for preparing a self-leveling mortar according to claim 6, characterized in that: the rotating speed of the stirring is 200-300 r/min.
CN202111488649.9A 2021-12-08 2021-12-08 Self-leveling mortar and preparation method thereof Pending CN113956005A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202111488649.9A CN113956005A (en) 2021-12-08 2021-12-08 Self-leveling mortar and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202111488649.9A CN113956005A (en) 2021-12-08 2021-12-08 Self-leveling mortar and preparation method thereof

Publications (1)

Publication Number Publication Date
CN113956005A true CN113956005A (en) 2022-01-21

Family

ID=79473176

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202111488649.9A Pending CN113956005A (en) 2021-12-08 2021-12-08 Self-leveling mortar and preparation method thereof

Country Status (1)

Country Link
CN (1) CN113956005A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115677307A (en) * 2022-10-31 2023-02-03 江苏兆佳建材科技有限公司 Gypsum-based self-leveling mortar and preparation method thereof

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2013040788A1 (en) * 2011-09-23 2013-03-28 Rohm And Haas Company Low temperature mortar for exterior insulation finish system
CN105645898A (en) * 2015-12-30 2016-06-08 上海每天节能环保科技股份有限公司 Modified gypsum-based self-leveling mortar and preparation and application thereof
CN106431146A (en) * 2016-10-09 2017-02-22 南京工业大学 Composite gypsum-based self-leveling mortar and preparation method
CN111393125A (en) * 2020-03-25 2020-07-10 河南强耐新材股份有限公司 Gypsum-based self-leveling repair mortar and preparation method thereof
CN113387662A (en) * 2021-05-24 2021-09-14 苏州金世晟建筑装饰工程有限公司 Novel gypsum surface layer self-leveling material

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2013040788A1 (en) * 2011-09-23 2013-03-28 Rohm And Haas Company Low temperature mortar for exterior insulation finish system
CN105645898A (en) * 2015-12-30 2016-06-08 上海每天节能环保科技股份有限公司 Modified gypsum-based self-leveling mortar and preparation and application thereof
CN106431146A (en) * 2016-10-09 2017-02-22 南京工业大学 Composite gypsum-based self-leveling mortar and preparation method
CN111393125A (en) * 2020-03-25 2020-07-10 河南强耐新材股份有限公司 Gypsum-based self-leveling repair mortar and preparation method thereof
CN113387662A (en) * 2021-05-24 2021-09-14 苏州金世晟建筑装饰工程有限公司 Novel gypsum surface layer self-leveling material

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115677307A (en) * 2022-10-31 2023-02-03 江苏兆佳建材科技有限公司 Gypsum-based self-leveling mortar and preparation method thereof

Similar Documents

Publication Publication Date Title
CN111606676B (en) High-water-retention gypsum self-leveling material and preparation method thereof
CN105218024A (en) A kind of ceramic tile bond
CN108546072B (en) Water-resistant machine-whitewashing gypsum material
CN112723841A (en) Anti-crack plastering mortar
CN108975755B (en) Additive special for recycled concrete
CN115108796B (en) Light plastering gypsum and preparation method thereof
KR20180060672A (en) Composition for construction materials and construction materials having the same
CN110563376B (en) Concrete reinforcing agent suitable for being prepared from machine-made sand and preparation method of mother liquor of concrete reinforcing agent
CN112159191A (en) Gypsum-based self-leveling and preparation method thereof
CN108516764A (en) A kind of crack resistance type plastering mortar
CN108585698B (en) Special joint filling mortar for light partition wall board
CN113956005A (en) Self-leveling mortar and preparation method thereof
CN111689747B (en) 3D printed color decoration mortar
EP2658821B1 (en) Hydraulic binder composition
CN110981362B (en) Plastering mortar and application thereof
CN113800861B (en) Premixed mortar with smooth surface and preparation method thereof
CN105503141A (en) Waste-residue and magnesium-phosphate cement self-leveling mortar
CN112479628B (en) Building mortar additive and plastering mortar containing same
CN109665790B (en) Cement-based self-leveling mortar and preparation method thereof
CN114477922A (en) Floor filling and leveling mortar for civil building decoration and preparation method thereof
CN113387662A (en) Novel gypsum surface layer self-leveling material
CN112679150A (en) High-strength concrete slurry with adjustable surface characteristics
CN114477923B (en) Self-leveling mortar with later-stage crack self-repairing function and preparation method thereof
CN112125601A (en) Low-cost cement self-leveling mortar, preparation method and application method thereof
CN112851219A (en) Repair mortar for concrete member and preparation method thereof

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20220121