CN113277804A - Ceramic tile glue and preparation method thereof - Google Patents
Ceramic tile glue and preparation method thereof Download PDFInfo
- Publication number
- CN113277804A CN113277804A CN202110587522.6A CN202110587522A CN113277804A CN 113277804 A CN113277804 A CN 113277804A CN 202110587522 A CN202110587522 A CN 202110587522A CN 113277804 A CN113277804 A CN 113277804A
- Authority
- CN
- China
- Prior art keywords
- parts
- tile glue
- glue according
- polyvinyl alcohol
- methyl cellulose
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000003292 glue Substances 0.000 title claims abstract description 20
- 239000000919 ceramic Substances 0.000 title claims abstract description 19
- 238000002360 preparation method Methods 0.000 title claims description 9
- 239000000843 powder Substances 0.000 claims abstract description 26
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 20
- 239000000835 fiber Substances 0.000 claims abstract description 15
- 239000004576 sand Substances 0.000 claims abstract description 14
- 239000004743 Polypropylene Substances 0.000 claims abstract description 13
- -1 polypropylene Polymers 0.000 claims abstract description 13
- 229920001155 polypropylene Polymers 0.000 claims abstract description 13
- 239000004372 Polyvinyl alcohol Substances 0.000 claims abstract description 12
- 239000001866 hydroxypropyl methyl cellulose Substances 0.000 claims abstract description 12
- 229920003088 hydroxypropyl methyl cellulose Polymers 0.000 claims abstract description 12
- 235000010979 hydroxypropyl methyl cellulose Nutrition 0.000 claims abstract description 12
- UFVKGYZPFZQRLF-UHFFFAOYSA-N hydroxypropyl methyl cellulose Chemical compound OC1C(O)C(OC)OC(CO)C1OC1C(O)C(O)C(OC2C(C(O)C(OC3C(C(O)C(O)C(CO)O3)O)C(CO)O2)O)C(CO)O1 UFVKGYZPFZQRLF-UHFFFAOYSA-N 0.000 claims abstract description 12
- 229920002451 polyvinyl alcohol Polymers 0.000 claims abstract description 12
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims abstract description 10
- 229910052791 calcium Inorganic materials 0.000 claims abstract description 10
- 239000011575 calcium Substances 0.000 claims abstract description 10
- 239000010881 fly ash Substances 0.000 claims abstract description 10
- 239000004568 cement Substances 0.000 claims abstract description 8
- 238000005406 washing Methods 0.000 claims abstract description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000002994 raw material Substances 0.000 claims abstract description 4
- 239000000377 silicon dioxide Substances 0.000 claims abstract description 3
- 238000003756 stirring Methods 0.000 claims description 5
- 239000011398 Portland cement Substances 0.000 claims description 4
- 239000002245 particle Substances 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 3
- 238000006136 alcoholysis reaction Methods 0.000 claims description 2
- 230000009477 glass transition Effects 0.000 claims description 2
- 238000000034 method Methods 0.000 claims description 2
- 238000006116 polymerization reaction Methods 0.000 claims description 2
- 239000000853 adhesive Substances 0.000 abstract description 6
- 230000001070 adhesive effect Effects 0.000 abstract description 6
- 238000005336 cracking Methods 0.000 abstract description 6
- 238000001035 drying Methods 0.000 abstract description 3
- 238000004519 manufacturing process Methods 0.000 description 2
- GVXIVWJIJSNCJO-UHFFFAOYSA-L aluminum;calcium;sulfate Chemical compound [Al+3].[Ca+2].[O-]S([O-])(=O)=O GVXIVWJIJSNCJO-UHFFFAOYSA-L 0.000 description 1
- 239000004566 building material Substances 0.000 description 1
- 230000009172 bursting Effects 0.000 description 1
- 230000008602 contraction Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000011895 specific detection Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/02—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
- C04B28/04—Portland cements
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/00474—Uses not provided for elsewhere in C04B2111/00
- C04B2111/00637—Uses not provided for elsewhere in C04B2111/00 as glue or binder for uniting building or structural materials
- C04B2111/00646—Masonry mortars
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/10—Mortars, concrete or artificial stone characterised by specific physical values for the viscosity
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/50—Mortars, concrete or artificial stone characterised by specific physical values for the mechanical strength
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Curing Cements, Concrete, And Artificial Stone (AREA)
- Adhesives Or Adhesive Processes (AREA)
Abstract
The invention discloses a tile glue which is prepared from the following raw materials in parts by weight: 400-500 parts of ordinary silica cement, 400-500 parts of water washing sand, 1-3 parts of polypropylene fiber, 4-10 parts of polyvinyl alcohol powder, 3-5 parts of hydroxypropyl methyl cellulose, 15-20 parts of redispersible rubber powder, 20-40 parts of calcium sulphoaluminate and 30-50 parts of fly ash. The ceramic tile adhesive produced by the invention has the advantages that the performances of the ceramic bonding layer such as drying shrinkage resistance, cracking resistance, slippage resistance, bonding strength and the like are improved to a certain extent, and the phenomena of hollowing, falling off, cracking and the like are not easy to occur after the ceramic tile is pasted.
Description
Technical Field
The invention belongs to the field of building materials, and particularly relates to a tile glue and a preparation method thereof.
Background
At present, tile glue in the market of China is widely applied, but problems such as hollowing and falling of tiles, cracking and the like are found in the application process, the problems are generally caused by the tiles, and the main reasons for the problems are that the bonding strength is not enough, and the coefficient of expansion with heat and contraction with cold is too large.
Disclosure of Invention
The invention aims to provide a ceramic tile adhesive, which is characterized in that the ceramic bonding layer has certain improved properties such as drying shrinkage resistance, cracking resistance, slip resistance, bonding strength and the like by matching and using aluminum calcium sulfate, polypropylene fiber and redispersible rubber powder, and the ceramic tile adhesive is not easy to cause phenomena such as hollowing, falling, bursting and the like after being pasted.
The second purpose of the invention is to provide a preparation method of the ceramic tile glue, which has simple steps, stable quality, high production efficiency and low production cost and can be used for large-scale industrial production.
One of the purposes of the invention is realized by the following technical scheme:
the tile glue is prepared from the following raw materials in parts by weight: 400-500 parts of ordinary silica cement, 400-500 parts of water washing sand, 1-3 parts of polypropylene fiber, 4-10 parts of polyvinyl alcohol powder, 3-5 parts of hydroxypropyl methyl cellulose, 15-20 parts of redispersible rubber powder, 20-40 parts of calcium sulphoaluminate and 30-50 parts of fly ash.
Further, 400 parts of ordinary portland cement, 500 parts of water washing sand, 1 part of polypropylene fiber, 10 parts of polyvinyl alcohol powder, 4 parts of hydroxypropyl methyl cellulose, 15 parts of redispersible rubber powder, 20 parts of calcium sulphoaluminate and 50 parts of fly ash.
Further, the strength grade of the ordinary cement is 42.5.
Furthermore, the mud content of the washed sand is less than or equal to 1.0 wt%, and the particle size of the washed sand is 40-70 meshes.
Further, the polypropylene fiber has a fiber length of 3 to 6 mm.
Further, the polymerization degree of the polyvinyl alcohol powder was 2400, and the alcoholysis degree was 88%.
Further, the hydroxypropyl methylcellulose has a viscosity grade of greater than 10 ten thousand and a particle size of less than 180 microns.
Further, the minimum film forming temperature and the glass transition temperature of the redispersible rubber powder are both less than 0 ℃.
The second purpose of the invention is realized by the following technical scheme:
accurately weighed ordinary cement, washed sand, polypropylene fiber, polyvinyl alcohol powder, hydroxypropyl methyl cellulose, redispersible rubber powder, calcium sulphoaluminate and fly ash are sequentially added into a stirring container and uniformly stirred.
Compared with the prior art, the ceramic tile glue and the preparation method thereof provided by the invention have the following advantages: the ceramic tile adhesive produced by the invention has the advantages that the performances of the ceramic bonding layer such as drying shrinkage resistance, cracking resistance, slippage resistance, bonding strength and the like are improved to a certain extent, and the phenomena of hollowing, falling off, cracking and the like are not easy to occur after the ceramic tile is pasted.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention will be described in further detail with reference to specific embodiments.
The redispersible powders used in the examples below all used FX2350 from aksu.
Example 1
The ceramic tile glue that this embodiment provided includes according to parts by weight ratio:
400 parts of ordinary portland cement, 500 parts of water washing sand, 1 part of polypropylene fiber, 10 parts of polyvinyl alcohol powder, 4 parts of hydroxypropyl methyl cellulose, 15 parts of redispersible rubber powder, 20 parts of calcium sulphoaluminate and 50 parts of fly ash.
The preparation method comprises the following steps:
the accurately weighed components are sequentially added into a stirring container and uniformly stirred.
Example 2
The ceramic tile glue that this embodiment provided includes according to parts by weight ratio:
450 parts of ordinary cement, 450 parts of water washing sand, 2 parts of polypropylene fiber, 6 parts of polyvinyl alcohol powder, 5 parts of hydroxypropyl methyl cellulose, 19 parts of redispersible rubber powder, 28 parts of calcium sulphoaluminate and 40 parts of fly ash.
The preparation method comprises the following steps:
the accurately weighed components are sequentially added into a stirring container and uniformly stirred.
Example 3
The ceramic tile glue that this embodiment provided includes according to parts by weight ratio:
500 parts of ordinary portland cement, 400 parts of water washing sand, 3 parts of polypropylene fiber, 4 parts of polyvinyl alcohol powder, 3 parts of hydroxypropyl methyl cellulose, 20 parts of redispersible rubber powder, 40 parts of calcium sulphoaluminate and 30 parts of fly ash.
The preparation method comprises the following steps:
the accurately weighed components are sequentially added into a stirring container and uniformly stirred.
The specific formulations for each example are shown in table 1 below:
in addition, the single-component ceramic tile adhesive prepared in the embodiment of the invention passes the JC/T547-2017 ceramic tile adhesive standard in performance detection. The specific detection results are shown in the following table 2:
the above embodiments are merely illustrative of the present invention and are not to be construed as limiting the invention. Although the present invention has been described in detail with reference to the embodiments, it should be understood by those skilled in the art that various combinations, modifications or equivalents may be made to the technical solution of the present invention without departing from the spirit and scope of the technical solution of the present invention, and the technical solution of the present invention is covered by the claims of the present invention.
Claims (9)
1. The ceramic tile glue is characterized in that: the composition is characterized by comprising the following raw materials in parts by weight: 400-500 parts of ordinary silica cement, 400-500 parts of water washing sand, 1-3 parts of polypropylene fiber, 4-10 parts of polyvinyl alcohol powder, 3-5 parts of hydroxypropyl methyl cellulose, 15-20 parts of redispersible rubber powder, 20-40 parts of calcium sulphoaluminate and 30-50 parts of fly ash.
2. A tile glue according to claim 1, characterized in that: the composition is characterized by comprising the following raw materials in parts by weight: 400 parts of ordinary portland cement, 500 parts of water washing sand, 1 part of polypropylene fiber, 10 parts of polyvinyl alcohol powder, 4 parts of hydroxypropyl methyl cellulose, 15 parts of redispersible rubber powder, 20 parts of calcium sulphoaluminate and 50 parts of fly ash.
3. A tile glue according to claim 1, characterized in that: the strength grade of the ordinary cement is 42.5.
4. A tile glue according to claim 1, characterized in that: the mud content of the washed sand is less than or equal to 1.0 percent by weight, and the particle size of the washed sand is 40-70 meshes.
5. A tile glue according to claim 1, characterized in that: the polypropylene fiber has a fiber length of 3 to 6 mm.
6. A tile glue according to claim 1, characterized in that: the polymerization degree of the polyvinyl alcohol powder is 2400, and the alcoholysis degree is 88%.
7. A tile glue according to claim 1, characterized in that: the viscosity grade of the hydroxypropyl methyl cellulose is more than 10 ten thousand, and the particle size is less than 180 micrometers.
8. A tile glue according to claim 1, characterized in that: the lowest film forming temperature and the glass transition temperature of the redispersible rubber powder are both less than 0 ℃.
9. A process for the preparation of a tile glue according to any one of claims 1 to 8, characterized in that it comprises the following steps:
accurately weighed ordinary cement, washed sand, polypropylene fiber, polyvinyl alcohol powder, hydroxypropyl methyl cellulose, redispersible rubber powder, calcium sulphoaluminate and fly ash are sequentially added into a stirring container and uniformly stirred.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202110587522.6A CN113277804A (en) | 2021-05-27 | 2021-05-27 | Ceramic tile glue and preparation method thereof |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
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CN202110587522.6A CN113277804A (en) | 2021-05-27 | 2021-05-27 | Ceramic tile glue and preparation method thereof |
Publications (1)
Publication Number | Publication Date |
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CN113277804A true CN113277804A (en) | 2021-08-20 |
Family
ID=77282233
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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CN202110587522.6A Pending CN113277804A (en) | 2021-05-27 | 2021-05-27 | Ceramic tile glue and preparation method thereof |
Country Status (1)
Country | Link |
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CN (1) | CN113277804A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN115636644A (en) * | 2022-10-28 | 2023-01-24 | 广东乐尔康生物科技股份有限公司 | Ceramic tile adhesive and preparation method thereof |
Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2007277017A (en) * | 2006-04-03 | 2007-10-25 | Taiheiyo Material Kk | Adhesive for tile |
CN101121583A (en) * | 2007-07-13 | 2008-02-13 | 肥城润东建材有限公司 | Dry powder ceramic tile binding agent |
CN104086137A (en) * | 2014-07-11 | 2014-10-08 | 北京博润佳科技有限公司 | Enhanced ceramic tile adhesive |
CN107500647A (en) * | 2017-08-21 | 2017-12-22 | 浙江大森建筑节能科技有限公司 | Ceramic microsphere energy-saving ceramic tile adhesive and preparation method thereof |
CN108640620A (en) * | 2018-08-02 | 2018-10-12 | 广东金意陶陶瓷集团有限公司 | Glue for tile and preparation method thereof |
CN110330286A (en) * | 2019-05-24 | 2019-10-15 | 河北晨阳工贸集团有限公司 | A kind of single polymer cement waterproofing mortar and preparation method thereof |
CN112624676A (en) * | 2020-12-30 | 2021-04-09 | 信阳市灵石科技有限公司 | Ceramic tile glue and preparation method thereof |
-
2021
- 2021-05-27 CN CN202110587522.6A patent/CN113277804A/en active Pending
Patent Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2007277017A (en) * | 2006-04-03 | 2007-10-25 | Taiheiyo Material Kk | Adhesive for tile |
CN101121583A (en) * | 2007-07-13 | 2008-02-13 | 肥城润东建材有限公司 | Dry powder ceramic tile binding agent |
CN104086137A (en) * | 2014-07-11 | 2014-10-08 | 北京博润佳科技有限公司 | Enhanced ceramic tile adhesive |
CN107500647A (en) * | 2017-08-21 | 2017-12-22 | 浙江大森建筑节能科技有限公司 | Ceramic microsphere energy-saving ceramic tile adhesive and preparation method thereof |
CN108640620A (en) * | 2018-08-02 | 2018-10-12 | 广东金意陶陶瓷集团有限公司 | Glue for tile and preparation method thereof |
CN110330286A (en) * | 2019-05-24 | 2019-10-15 | 河北晨阳工贸集团有限公司 | A kind of single polymer cement waterproofing mortar and preparation method thereof |
CN112624676A (en) * | 2020-12-30 | 2021-04-09 | 信阳市灵石科技有限公司 | Ceramic tile glue and preparation method thereof |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN115636644A (en) * | 2022-10-28 | 2023-01-24 | 广东乐尔康生物科技股份有限公司 | Ceramic tile adhesive and preparation method thereof |
CN115636644B (en) * | 2022-10-28 | 2023-08-22 | 广东乐尔康生物科技股份有限公司 | Ceramic tile adhesive and preparation method thereof |
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RJ01 | Rejection of invention patent application after publication |
Application publication date: 20210820 |
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RJ01 | Rejection of invention patent application after publication |