CN115606844A - Acid-flavor plant porous particles, preparation method thereof and application thereof in cigarettes - Google Patents
Acid-flavor plant porous particles, preparation method thereof and application thereof in cigarettes Download PDFInfo
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- CN115606844A CN115606844A CN202211425369.8A CN202211425369A CN115606844A CN 115606844 A CN115606844 A CN 115606844A CN 202211425369 A CN202211425369 A CN 202211425369A CN 115606844 A CN115606844 A CN 115606844A
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- pulp
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/062—Use of materials for tobacco smoke filters characterised by structural features
- A24D3/066—Use of materials for tobacco smoke filters characterised by structural features in the form of foam or having cellular structure
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/04—Tobacco smoke filters characterised by their shape or structure
- A24D3/048—Tobacco smoke filters characterised by their shape or structure containing additives
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/14—Use of materials for tobacco smoke filters of organic materials as additive
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention provides a preparation method of acid scent type plant porous particles, which comprises the following steps: a) Drying and crushing hawthorn and tamarind pulp to obtain pulp micro powder; dissolving the perfume substance by adopting small molecular cluster water to obtain a perfume solution; b) And mixing the spice solution, the pulp micro powder and the adhesive, and granulating to obtain micro powder particles. According to the invention, the hawthorn and tamarind pulp are adopted to prepare the acid-flavor plant micro-powder particles, rich organic acid is used for reducing the irritation of cigarette smoke, a certain sweet feeling characteristic is given, and in the granulation process, small molecular cluster water is used as a solvent, and a specific spice component is carried into the micro-powder particles, so that the fragrance carrying capacity of the plant porous particles is improved, and the cigarette smoking quality can be improved.
Description
Technical Field
The invention relates to the technical field of cigarette materials, in particular to acid-flavor plant porous particles, a preparation method thereof and application thereof in cigarettes.
Background
The composite porous adsorption material in the cigarette filter is one of important technical means for reducing tar and harm, and the commonly used porous material is inorganic porous nano material, such as activated carbon, nano aerogel material, noble metal nano catalytic material and the like (tobacco technology, 2019,52 (01): 45-52.). In addition, adding a porous material with the functions of quality improvement and flavor enhancement to a cigarette filter is another important way for improving the functional characteristics of the filter, for example, data report that the storage and adsorption performance of the porous carbon material or the metal organic framework material on volatile flavors is adopted to realize the flavor slow release in the filter, but the reports in this respect mostly stay in the research level and related cigarette product development is not seen yet, and one important reason is that the release capacity of the porous material after adsorbing the volatile flavors is limited, and the porous material is often used for adsorbing single flavor analysis, cannot exert the sum and cooperation among flavor components, has different adsorption and slow release performances for different flavors, and is difficult to realize the synergistic regulation and control in the application of the cigarette filter (Chinese science: chemistry, 2019,49 (04): 607-612.).
The natural plant spice micro-powder is used as a carrier of the fragrance, and the natural plant spice micro-powder is used as solid spice to be applied to the cigarette filter stick, so that special fragrance characteristics and smoking experience can be provided. For example, the invention patent with application number CN114317113A discloses a momordica grosvenori solid spice and a preparation method thereof, and the main idea is to crush and dry momordica grosvenori, spray materials such as humectant and the like, and add the materials into a filter stick in powder form; in addition, the plant micro powder of citrus peels, clove and the like is also a potential characteristic spice applied to cigarette filters as a solid spice. But the single plant micro powder spice has single aroma characteristic and lacks the harmony with the aroma characteristic of cigarette smoke. In addition, the pH value of the cigarette smoke is one of the comprehensive indexes reflecting the whole quality of the cigarette, and the pH value of the cigarette smoke is a comprehensive expression form of chemical composition and chemical balance in main stream particle phase matters of the cigarette and is directly related to the sensory quality indexes such as strength, irritation and the like when the cigarette is smoked. The noise of the cigarette smoke can be weakened by regulating and controlling the pH value of the smoke, and the transfer of organic acid in the acid-flavor plant particles into the smoke or the change of the existing form of nicotine in the smoke by using abundant organic acid is an important way for reducing the irritation.
Therefore, it is very necessary to develop a kind of acid-flavor plant micropowder to prepare filter particles, and to improve the richness and harmony of the aroma of the plant micropowder particles.
Disclosure of Invention
In view of the above, the technical problem to be solved by the present invention is to provide a porous plant granule with sour flavor, which has rich fragrance and good harmonicity.
The invention provides a preparation method of acid-flavor plant porous particles, which comprises the following steps:
a) Drying and crushing hawthorn and tamarind pulp to obtain pulp micro powder;
dissolving the perfume substance by adopting small molecular cluster water to obtain a perfume solution;
b) And mixing the spice solution, the pulp micro powder and the adhesive, and granulating to obtain micro powder particles.
Preferably, the mass ratio of the hawthorn to the tamarind pulp in the step A) is (1-5): 5.
preferably, the drying in the step A) is drying at 50-80 ℃ or freeze drying; the granularity of the crushed material is 80-120 meshes.
Preferably, the perfume material of step a) is one or more of ethyl maltol, 2-acetylpyrazine, MCP, maltol, furanone, 2-acetylpyrrole, 2, 3-dimethylpyrazine, 2, 5-dimethylpyrazine or 2,3, 5-trimethylpyrazine; the mass concentration of the perfume substance in the perfume solution is 0.1-1%.
Preferably, the preparation method of the small molecule cluster water in the step B) is a freezing and cooling method;
the adhesive is one or more of sodium carboxymethylcellulose, arabic gum or dextrin; the mass ratio of the adhesive in the micro powder particles is 2-20%.
Preferably, the mixing mass ratio of the spice solution, the pulp micropowder and the adhesive in the step B) is (2-30): (50-90): (2-20);
the particle size of the micro powder particles obtained by granulation is 20-60 meshes.
The invention provides acid scent type plant porous particles which are characterized by being prepared by the preparation method of any one of the technical schemes.
The invention provides a cigarette filter, which comprises the acid aroma type plant porous particles.
Preferably, the application amount of the acid scent plant porous particles in the filter tip is 20-80 mg, and the acid scent plant porous particles can be applied in sections or distributed in the whole filter tip section.
The invention provides a cigarette, which comprises the cigarette filter tip.
Compared with the prior art, the invention provides a preparation method of acid-flavor plant porous particles, which comprises the following steps: a) Drying and crushing hawthorn and tamarind pulp to obtain pulp micro powder; dissolving the perfume substance by adopting micromolecular cluster water to obtain a perfume solution; b) And mixing the spice solution, the pulp micro powder and the adhesive, and granulating to obtain micro powder particles. According to the invention, the hawthorn and tamarind pulp are adopted to prepare the acid-flavor plant micro-powder particles, rich organic acid is used for reducing the irritation of cigarette smoke, a certain sweet feeling characteristic is given, and in the granulation process, micromolecule cluster water is used as a solvent, a specific spice component is carried into the micro-powder particles, so that the fragrance carrying capacity of the plant porous particles is improved, and the cigarette smoking quality can be improved.
Detailed Description
The invention provides a sour-flavor plant porous particle, a preparation method thereof and application thereof in cigarettes, and a person skilled in the art can realize the purpose by properly improving process parameters by referring to the content. It is specifically noted that all such substitutions and modifications will be apparent to those skilled in the art, and are intended to be within the scope of the present invention. While the methods and applications of this invention have been described in terms of preferred embodiments, it will be apparent to those of ordinary skill in the art that variations and modifications in the methods and applications described herein, as well as other suitable variations and combinations, may be made to implement and use the techniques of this invention without departing from the spirit and scope of the invention.
The invention provides a preparation method of acid-flavor plant porous particles, which comprises the following steps:
a) Drying and crushing hawthorn and tamarind pulp to obtain pulp micropowder;
dissolving the perfume substance by adopting small molecular cluster water to obtain a perfume solution;
b) And mixing the spice solution, the pulp micro powder and the adhesive, and granulating to obtain micro powder particles.
The preparation method of the acid-flavor plant porous particles provided by the invention comprises the steps of drying and crushing hawthorn and tamarind pulp to obtain pulp micropowder.
The hawthorn is hawthorn pulp. The drying is drying at 50-80 ℃ or freeze drying; the present invention is not limited to the specific drying operation and the specific freeze-drying operation, and those skilled in the art will be familiar with the present invention.
Wherein, the crushing is preferably performed by a plant crusher; the granularity of the crushing is preferably 80-120 meshes; more preferably 85 to 115 mesh.
The mass ratio of the hawthorn to the tamarind pulp is (1-5): 5; including but not limited to 1; or a point value between any of the above.
And (3) dissolving the perfume substance by adopting the small molecular cluster water to obtain a perfume solution.
The preparation method of the small molecule cluster water is a freezing and cooling method; the present invention is not limited to a specific production method, and those skilled in the art will be familiar with the method.
According to the invention, the spice substance can be monomer spice or a mixture thereof with fruity, spicy, baking, caramel and other fragrance notes; including but not limited to one or more of ethyl maltol, 2-acetylpyrazine, MCP, maltol, furanone, 2-acetylpyrrole, 2, 3-dimethylpyrazine, 2, 5-dimethylpyrazine, or 2,3, 5-trimethylpyrazine; the mass concentration of the perfume substance in the perfume solution is preferably 0.1-1%; more preferably 0.1% to 0.9%; most preferably 0.1% to 0.8%.
Mixing the spice solution, the pulp micropowder and the adhesive.
The flavor solution is applied to the pulp micro powder in a mass ratio of 1-5%, and is mixed with the adhesive to obtain micro powder particles with the granularity of 20-60 meshes through a granulation process. And after granulation and molding, drying the mixture in an oven at the temperature of not more than 60 ℃ until the water content is 11-13%.
The adhesive is one or more of sodium carboxymethylcellulose, arabic gum or dextrin; the mass ratio of the adhesive in the micro powder particles is 2-20%.
According to the invention, the mass ratio of the mixture of the spice solution, the pulp micropowder and the adhesive is (2-30): (50-90): (2-20).
The invention takes micromolecular cluster water as a solvent of the additional spice, utilizes the fragrance-carrying permeation effect of the micromolecular cluster water to enhance the synergistic effect of the additional spice and the plant micro powder, and prepares micro powder particles by a granulation method.
The porous particles are prepared by blending plant micro powder with sour and sweet taste characteristics, and the particles are infiltrated by utilizing the fragrance-carrying effect of small molecular cluster water in the granulation process, so that the cigarette smoking quality is obviously improved.
The invention provides acid-flavor plant porous particles which are characterized by being prepared by the preparation method of any one of the technical schemes.
The preparation method of the invention is clearly described, and the description is omitted.
The invention reduces the pH value of cigarette smoke by utilizing the elution effect of rich organic acid in the acid-flavor natural plant micro powder during smoking, avoids the risk of changing the flavor formula caused by adding acid and other components into tobacco shreds, and has strong applicability in cigarette products.
The micromolecule cluster water is introduced as a solvent of the additional material fragrance in the preparation process of the porous plant micro-powder particles, so that the adsorption capacity of the additional material fragrance can be increased, the fragrance harmony of the porous plant particles is improved, the fragrance characteristics and richness of the porous particles are synergistically improved from the two aspects of the inside and the outside of the plant micro-powder, and the cigarette smoke quality improvement effect is remarkable.
The invention provides a cigarette filter, which comprises the acid scent type plant porous particles.
The application amount of the acid scent type plant porous particles in the filter tip is 20-80 mg, and the acid scent type plant porous particles can be applied in sections or distributed in the whole filter tip section.
The invention does not limit the rest components of the cigarette filter, as long as the acid scent type plant porous particles are included.
The porous particles are added into the cigarette filter, can be used for purifying the smoke and reducing the irritation, and can directionally improve the aroma and the sweet feeling characteristics of the cigarette smoke. And in the granulation process, the small molecular cluster water is used as a solvent, and the specific spice component is carried into the micro powder particles, so that the fragrance carrying capacity of the plant porous particles is improved, and the cigarette smoking quality can be improved.
The acid-flavor plant porous particles are simple and convenient in preparation process, and have an obvious effect of improving the smoking quality of cigarettes.
According to the invention, the micro powder particles are added into the cigarette filter stick, and the elution effect of the mainstream smoke on the characteristic flavor substances in the plant particles during cigarette smoking is utilized to transfer the organic acid and the flavor substances into the smoke, so that the purpose of improving and increasing the cigarette smoking quality is realized. The micro powder particles do not participate in the combustion process of cigarettes, and only release characteristic aroma during smoking.
The invention provides a cigarette, which comprises the cigarette filter tip.
The cigarette filter has been described clearly, and will not be described in detail.
The invention provides a preparation method of acid-flavor plant porous particles, which comprises the following steps: a) Drying and crushing hawthorn and tamarind pulp to obtain pulp micro powder; dissolving the perfume substance by adopting small molecular cluster water to obtain a perfume solution; b) And mixing the spice solution, the pulp micro powder and the adhesive, and granulating to obtain micro powder particles. According to the invention, the hawthorn and tamarind pulp are adopted to prepare the acid-flavor plant micro-powder particles, rich organic acid is used for reducing the irritation of cigarette smoke, a certain sweet feeling characteristic is given, and in the granulation process, small molecular cluster water is used as a solvent, and a specific spice component is carried into the micro-powder particles, so that the fragrance carrying capacity of the plant porous particles is improved, and the cigarette smoking quality can be improved.
In order to further illustrate the invention, the following detailed description of the acid-flavor plant porous particles, the preparation method thereof and the application thereof in cigarettes provided by the invention are combined with the examples.
Example 1
The embodiment provides a preparation method and application of acid-flavor plant porous particles, and the preparation method comprises the following specific steps:
1) Drying the hawthorn and the tamarind pulp in an oven at 60 ℃, respectively, crushing by using a plant crusher with the crushing granularity of 90 meshes, and uniformly mixing the hawthorn and the tamarind pulp according to the mass ratio of 2;
2) Dissolving a perfume substance with characteristic aroma characteristics by using small molecule cluster water as a solvent, wherein the small molecule cluster water is prepared by freezing and cooling, the perfume substance is a mixture of ethyl maltol, 2-acetylpyrazine and MCP, and the concentration of the perfume is 0.1%;
3) Applying the flavor solution obtained in the step 2) to the pulp micropowder obtained in the step 1) in a mass ratio of 1%, mixing with an adhesive mainly containing sodium carboxymethylcellulose and dextrin, wherein the mass ratio of the adhesive is 2%, and granulating to obtain micropowder particles with a particle size of 40 meshes.
4) 40mg of the micro powder particles obtained in the step 3) is added into a cigarette filter stick, organic acid and aroma substances are transferred into smoke by utilizing the elution effect of mainstream smoke on characteristic aroma substances in plant particles during cigarette smoking, so that the irritation of the cigarette smoke can be reduced, the baking aroma and baking sweet aroma characteristics are increased, the smoke is mellow, and the aim of improving the cigarette smoking quality is fulfilled.
Example 2
The embodiment provides a preparation method and application of acid-flavor plant porous particles, and the preparation method comprises the following specific steps:
1) Drying the hawthorn and tamarind pulp in an oven at 50 ℃, respectively, crushing by using a plant crusher to obtain a crushed particle size of 200 meshes, and uniformly mixing the hawthorn and the tamarind pulp in a mass ratio of 1;
2) Dissolving a perfume substance with characteristic aroma characteristics by using small molecule cluster water as a solvent, wherein the small molecule cluster water is prepared by freezing and cooling, the perfume substance is a mixture of ethyl maltol and 2-acetylpyrazine, the mass ratio of the perfume substance is 1;
3) Applying the flavor solution obtained in the step 2) to the pulp micropowder obtained in the step 1) in a mass ratio of 1%, mixing with an adhesive mainly containing sodium carboxymethylcellulose and dextrin, wherein the mass ratio of the adhesive is 10%, and granulating to obtain micropowder particles with a particle size of 20 meshes.
4) 80mg of the micro-powder particles obtained in the step 3) is added into a cigarette filter stick, and organic acid and flavor substances are transferred into smoke by utilizing the elution effect of mainstream smoke on characteristic flavor substances in plant particles during cigarette smoking, so that the irritation of the cigarette smoke can be reduced, the baking aroma and baking sweet aroma characteristics can be increased, the smoke is mellow, and the purpose of improving and enhancing the cigarette smoking quality can be realized.
Example 3
The embodiment provides a preparation method and application of acid scent type plant porous particles, and the specific steps are as follows:
1) Drying the hawthorn and the tamarind pulp in an oven at 80 ℃, respectively, crushing by using a plant crusher with the crushing granularity of 100 meshes, and uniformly mixing the hawthorn and the tamarind pulp according to the mass ratio of 5;
2) Dissolving a perfume substance with characteristic aroma characteristics by using small molecular cluster water as a solvent, wherein the small molecular cluster water is prepared by freezing and cooling, the perfume substance is a mixture of ethyl maltol and MCP, the mass ratio of the perfume substance to the mixture is 5;
3) Applying the flavor solution obtained in the step 2) to the pulp micropowder obtained in the step 1) in a mass ratio of 1%, mixing with an adhesive mainly containing sodium carboxymethylcellulose and dextrin, wherein the mass ratio of the adhesive is 20%, and granulating to obtain micropowder particles with a particle size of 60 meshes.
4) 20mg of the micro-powder particles obtained in the step 3) is added into a cigarette filter stick, organic acid and flavor substances are transferred into smoke by utilizing the elution effect of mainstream smoke on characteristic flavor substances in plant particles during cigarette smoking, so that the irritation of the cigarette smoke can be reduced, the baking aroma and baking sweet aroma characteristics are increased, the smoke is pure and mild, and the aim of improving the cigarette smoking quality is fulfilled.
The foregoing is only a preferred embodiment of the present invention, and it should be noted that, for those skilled in the art, various modifications and decorations can be made without departing from the principle of the present invention, and these modifications and decorations should also be regarded as the protection scope of the present invention.
Claims (10)
1. The preparation method of the acid scent type plant porous particles is characterized by comprising the following steps:
a) Drying and crushing hawthorn and tamarind pulp to obtain pulp micropowder;
dissolving the perfume substance by adopting micromolecular cluster water to obtain a perfume solution;
b) And mixing the spice solution, the pulp micro powder and the adhesive, and granulating to obtain micro powder particles.
2. The preparation method according to claim 1, wherein the mass ratio of the hawthorn and the tamarind pulp in the step A) is (1-5): 5.
3. the method according to claim 1, wherein the drying in step a) is oven drying or freeze drying at 50-80 ℃; the granularity of the crushed material is 80-200 meshes.
4. The process according to claim 1, wherein the flavor material of step a) is one or more of ethyl maltol, 2-acetylpyrazine, MCP, maltol, furanone, 2-acetylpyrrole, 2, 3-dimethylpyrazine, 2, 5-dimethylpyrazine or 2,3, 5-trimethylpyrazine; the mass concentration of the perfume substance in the perfume solution is 0.1-1%.
5. The method according to claim 1, wherein the method for producing the small molecule cluster water in step B) is a freezing and cooling method;
the adhesive is one or more of sodium carboxymethylcellulose, arabic gum or dextrin; the mass ratio of the adhesive in the micro powder particles is 2-20%.
6. The preparation method according to claim 1, wherein the flavor solution, the pulp micropowder and the adhesive in the step B) are mixed in a mass ratio of (2-30): (50 to 90): (2-20);
the particle size of the micro powder particles obtained by granulation is 20-60 meshes.
7. A porous granule of a plant with a sour flavor, which is prepared by the preparation method of any one of claims 1 to 6.
8. A cigarette filter comprising the acid-flavored plant porous particles of claim 7.
9. The cigarette filter according to claim 8, wherein the application amount of the acid-flavor plant porous particles in the filter is 20-80 mg, and the acid-flavor plant porous particles can be applied in sections or distributed in the whole filter section.
10. A cigarette comprising the cigarette filter of claim 9.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202211425369.8A CN115606844A (en) | 2022-11-15 | 2022-11-15 | Acid-flavor plant porous particles, preparation method thereof and application thereof in cigarettes |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202211425369.8A CN115606844A (en) | 2022-11-15 | 2022-11-15 | Acid-flavor plant porous particles, preparation method thereof and application thereof in cigarettes |
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| Publication Number | Publication Date |
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| CN115606844A true CN115606844A (en) | 2023-01-17 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202211425369.8A Pending CN115606844A (en) | 2022-11-15 | 2022-11-15 | Acid-flavor plant porous particles, preparation method thereof and application thereof in cigarettes |
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| Country | Link |
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| CN (1) | CN115606844A (en) |
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2022
- 2022-11-15 CN CN202211425369.8A patent/CN115606844A/en active Pending
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