CN115536757B - Separating device and method for sea cucumber polysaccharide extraction - Google Patents
Separating device and method for sea cucumber polysaccharide extraction Download PDFInfo
- Publication number
- CN115536757B CN115536757B CN202210616126.6A CN202210616126A CN115536757B CN 115536757 B CN115536757 B CN 115536757B CN 202210616126 A CN202210616126 A CN 202210616126A CN 115536757 B CN115536757 B CN 115536757B
- Authority
- CN
- China
- Prior art keywords
- belt pulley
- separation
- separation box
- fixedly connected
- transmission
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B37/00—Preparation of polysaccharides not provided for in groups C08B1/00 - C08B35/00; Derivatives thereof
- C08B37/0003—General processes for their isolation or fractionation, e.g. purification or extraction from biomass
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D36/00—Filter circuits or combinations of filters with other separating devices
- B01D36/02—Combinations of filters of different kinds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F21/00—Dissolving
- B01F21/10—Dissolving using driven stirrers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F33/00—Other mixers; Mixing plants; Combinations of mixers
- B01F33/80—Mixing plants; Combinations of mixers
- B01F33/836—Mixing plants; Combinations of mixers combining mixing with other treatments
- B01F33/8361—Mixing plants; Combinations of mixers combining mixing with other treatments with disintegrating
- B01F33/83613—Mixing plants; Combinations of mixers combining mixing with other treatments with disintegrating by grinding or milling
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Materials Engineering (AREA)
- Sustainable Development (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
Abstract
The application discloses a separating device and a separating method for extracting sea cucumber polysaccharide, comprising a base, wherein the top of the base is fixedly connected with a separating box body, the middle position in the separating box body is fixedly connected with a separating box, separating chambers are arranged on two sides of the separating box, a convex frame filter plate is detachably arranged on the side wall of the separating chamber far away from the separating box, a bearing arc plate is arranged between the convex frame filter plate and the outer wall of the separating box, two ends of the bearing arc plate are attached to the inner wall of the separating box body, and overflow ports are formed on two sides of the surface of the separating box. The application combines the transmission component and the roller component, and is in multi-structure linkage, so that sediment can be milled while filtering, polysaccharide can be fully dissolved in clear liquid, clear liquid residues extruded by the concave roller enter the concave roller from the immersion holes and fall down after being filtered by the filtering cover and the convex frame filter plate along the impeller, raw materials are more fully mixed, substances in the clear liquid are not precipitated, the dissolution rate and the extraction rate of the polysaccharide are improved, and the production cost is greatly reduced.
Description
Technical Field
The application relates to the technical field of sea cucumber deep processing, in particular to a separation device and a separation method for sea cucumber polysaccharide extraction.
Background
Sea Cucumber (Sea Cucumber) is a traditional rare tonic in China, is rich in various bioactive substances in the body, and has higher edible and medicinal values. In China, the demands of people for sea cucumbers and sea cucumber products are increasing with the improvement of living standard. Sea cucumber polysaccharide is one of the most important bioactive substances in sea cucumber bodies, and has various activities of anticoagulation, antithrombotic, blood fat reduction, tumor inhibition and the like.
The Chinese patent of patent application publication No. CN 106117382A discloses a method for separating and refining sea cucumber polysaccharide, which comprises the steps of pulping sea cucumber raw materials to obtain sea cucumber slurry; adding water, regulating pH to 6.5-8.0, adding compound protease, and performing enzymolysis for 2-6 hr; centrifuging and collecting supernatant; repeatedly concentrating and filtering by using an ultrafiltration membrane, and collecting the final concentrated solution, namely sea cucumber polysaccharide concentrated solution; freeze-drying sea cucumber polysaccharide concentrate, filling the sea cucumber polysaccharide concentrate into a resin column, and passing through the resin column by adopting 65% alcohol and then passing through the resin column by adopting 95% alcohol; taking out sea cucumber polysaccharide in the resin column, and drying in a silica gel drying oven to obtain refined sea cucumber polysaccharide after drying. The method of the application obviously improves the purity and quality of the sea cucumber polysaccharide product, reduces the color of the sea cucumber polysaccharide, thereby expanding the application range of the sea cucumber polysaccharide, reducing the environmental pollution and reducing the consumption of fresh water resources, and can be called energy conservation and environmental protection.
However, in the method for separating and refining sea cucumber polysaccharide provided in the technical scheme, when the method is actually used, water is added for enzymolysis and supernatant liquid is collected through centrifugal separation, and a large amount of polysaccharide is still contained in the precipitate, so that the extraction amount of polysaccharide in sea cucumber slurry is low, a large amount of resource waste is caused, the extraction rate is low, and the production cost is greatly increased.
Therefore, it is necessary to invent a separating device and a separating method for extracting sea cucumber polysaccharide to solve the above problems.
Disclosure of Invention
The application aims to provide a separating device and a separating method for extracting sea cucumber polysaccharide, which are used for solving the problems that in the process of adding water for enzymolysis and centrifugally separating and collecting supernatant in the prior art, a large amount of polysaccharide is still contained in sediment, so that the extraction amount of polysaccharide in sea cucumber slurry is low, a large amount of resource is wasted, the extraction rate is low and the production cost is greatly increased.
In order to achieve the above object, the present application provides the following technical solutions: the separating device comprises a base, wherein the top of the base is fixedly connected with a separating box body, the middle position inside the separating box body is fixedly connected with a separating box, separating chambers are arranged on two sides of the separating box, a convex frame filter plate is detachably arranged on the side wall, far away from the separating box, of the separating chamber, a bearing arc plate is arranged between the convex frame filter plate and the outer wall of the separating box, and two ends of the bearing arc plate are attached to the inner wall of the separating box body;
the utility model discloses a double-shaft driving device for the double-shaft refrigerator, which comprises a separation tank, wherein overflow ports are formed in two sides of the surface of the separation tank, a cavity is formed in the separation tank, a transmission assembly is arranged in the cavity, the transmission assembly comprises a double-shaft driving motor, a poking wheel is connected with an output shaft transmission at the bottom of the double-shaft driving motor, a notch is formed in the middle of the bottom end of the separation tank, the poking wheel is matched with the notch, a first belt pulley is connected with an output shaft transmission at the top of the double-shaft driving motor, a first gear is fixedly connected with the top of the first belt pulley, two sides of the first gear are respectively connected with a second gear in a meshed manner, a shaft rod is fixedly connected with the shaft center of the second gear, a conveying dragon row is arranged at the position of the overflow ports outside the outer side of the shaft rod, the shaft rod is rotationally connected with the separation tank, a second belt pulley is rotationally connected with the inner top of the cavity, a third belt pulley is rotationally connected with the position of the inner side of the cavity which is positioned at the overflow ports, the first belt pulley, the second belt pulley and the third belt pulley are fixedly connected with a mandrel at the axle center, the mandrel penetrates through the side wall of the separation box, the joint of the mandrel and the separation box is provided with a sealing bearing, the mandrels at the two sides of the second belt pulley are fixedly connected with a fourth belt pulley, the inside of the separation chamber is rotationally connected with a roller assembly, the roller assembly consists of a concave roller, a transmission rod, an impeller and a filtering cover, the transmission rod penetrates through the separation box and extends into a cavity, the transmission rod is provided with a fifth belt pulley at the position inside the cavity outside the transmission rod, the transmission rod is fixedly connected with the axle center of the concave roller, the transmission rod is provided with the impeller outside the transmission rod, one end of the concave roller is detachably provided with the filtering cover, the impeller comprises a plurality of spiral inclined roller plates, the surface of the concave roller is provided with a dipping hole, the device is characterized in that the first belt pulley, the second belt pulley and the third belt pulley are in transmission connection through a first transmission belt, the fourth belt pulley and the fifth belt pulley are in transmission connection through a second transmission belt, mandrel end parts on two sides of the second belt pulley are in transmission connection with an adjusting rod, the middle part of the adjusting rod is fixedly connected with an eccentric torsion wheel, the outer side of the eccentric torsion wheel is rotationally connected with a push-pull rod, the bottom end of the push-pull rod is hinged with a positioning block, and the bottom end of the positioning block is fixedly connected with a piston matched with a separation chamber.
Preferably, the second belt pulley and the two third belt pulleys are located on the same section, and the second belt pulley and the two third belt pulleys are vertically distributed with the first belt pulley.
Preferably, the top of separation box both sides wall all is equipped with the inlet pipe, the bottom of separation box both sides wall all is equipped with the discharging pipe, two the inlet pipe link up with two separation rooms respectively, two the discharging pipe link up with two separation rooms respectively, inlet pipe and the inside ball valve that adjusts that all is equipped with of discharging pipe.
Preferably, both ends of the mandrel of the third belt pulley penetrate through the separate box, a sealing bearing is arranged at the joint of the mandrel and the separate box, a brush roller is arranged on the mandrel of the third belt pulley, and the brush roller is matched with the outer wall of the concave roller.
Preferably, the two eccentric torsion wheels are symmetrically distributed about the center of the second belt pulley, the number of the fifth belt pulleys is two, the two fifth belt pulleys are symmetrically distributed about one output shaft of the double-shaft driving motor, and the transmission rods on two sides are not contacted with the output shaft of the double-shaft driving motor.
Preferably, the joints of the transmission rods and the separation box body, the separation box and the convex frame filter plates are respectively provided with a sealing bearing, and the joints of the shaft rods and the separation box are respectively provided with a sealing bearing.
Preferably, the bearing arc plate is matched with the concave roller, and the two sides of the top of the bearing arc plate are fixedly connected with convex plates.
Preferably, the connecting hole has all been seted up at the flange top, equal fixedly connected with L shape connecting rod on the separate box both sides wall, and L shape connecting rod bottom surface all is equipped with the external screw thread, L shape connecting rod external screw thread connection has fixation nut, and L shape connecting rod is located connecting hole top and bottom and all is equipped with the sealing washer.
Preferably, the maintenance port is all offered to separation box openly both sides, the inside articulated closure door that has of maintenance port, and the junction of closure door and maintenance port is equipped with sealed packing, through compressing tightly hasp closure connection between closure door and the separation box.
The sea cucumber polysaccharide extraction and separation method comprises the sea cucumber polysaccharide extraction and separation device, and the separation steps are as follows:
s1: fully gelling and carrying out enzymolysis on sea cucumber powder to dissolve polysaccharide in water, carrying out enzymolysis and precipitation on protein, feeding the mixed solution into separation chambers at two sides of a separation box from a feed pipe, blocking the solution by a bearing arc plate after the solution enters, directly filtering clear liquid from a convex frame filter plate, and intercepting the enzymolysis and precipitation on the top of the bearing arc plate;
s2: starting a double-shaft driving motor, wherein an output shaft of the double-shaft driving motor is in transmission connection with a first belt pulley, the first belt pulley, a second belt pulley and a third belt pulley are in transmission connection through a first transmission belt, and under the action of a fourth belt pulley, a fifth belt pulley and a second transmission belt, two roller assemblies rotate at the top of a bearing arc plate, and precipitate is milled, so that polysaccharide can be fully dissolved in clear liquid;
s3: the first belt pulley synchronously drives the first gear and drives the two second gears to be meshed, so that the two shaft rods drive the conveying dragon to stir at the overflow port, and the two shaft rods are matched with staggered lifting adjustment of pistons at two sides to enable raw materials in the two separation chambers to be mixed more fully, and the stirring wheel at the bottom rotates to enable substances in clear liquid not to be precipitated;
s4: the two third belt pulleys drive the brush rollers to act on the surfaces of the concave rollers, after the clear liquid is discharged, the surfaces of the concave rollers are cleaned, and when the sediment is rolled, water enters the concave rollers from the immersing holes and falls down after being filtered by the filter cover and the convex frame filter plate under the guidance of the inclined wheel plate of the impeller;
s5: and opening an adjusting ball valve on the discharging pipe, and taking clear liquid containing polysaccharide out of the separation chamber for secondary fine filtration.
In the technical scheme, the application has the technical effects and advantages that:
1. through full gelatinization enzymolysis of sea cucumber powder, polysaccharide is dissolved in water and protein is subjected to enzymolysis precipitation, a transmission assembly is combined with a roller assembly, multiple structures are linked, the precipitate can be milled while filtering, so that the polysaccharide can be fully dissolved in clear liquid, clear liquid residues extruded by a concave roller enter the concave roller from a leaching hole and fall down after being filtered by a filtering cover and a convex frame filter plate along an impeller, raw materials are mixed more fully, substances in the clear liquid are not precipitated, the dissolution rate and the extraction rate of the polysaccharide are improved, and the production cost is greatly reduced;
2. through opening the compression lock catch, make the closure door can open, it is unblocked to maintain the mouth this moment, will bear the weight of the arc board and take off from L shape connecting rod, be convenient for clear up it and maintain, later seal and maintain the mouth, let in the clear water, drive at two axostylus axostyles and carry the flood dragon to arrange in overflow opening department stirring, cooperation both sides piston's crisscross lift is adjusted to and stir under the rotation of wheel, improve inside clearance effect, and this device compact structure, the linkage effect is strong, has reduced the consumption of energy and resource.
Drawings
In order to more clearly illustrate the embodiments of the present application or the technical solutions in the prior art, the drawings required for the embodiments will be briefly described below, and it is apparent that the drawings in the following description are only some embodiments described in the present application, and other drawings may be obtained according to these drawings for a person having ordinary skill in the art.
FIG. 1 is a schematic diagram of the overall structure of the present application;
FIG. 2 is a front view of the present application;
FIG. 3 is a left side view of the compartment of the present application;
FIG. 4 is a first perspective view of the transmission assembly of the present application;
FIG. 5 is a second perspective view of the transmission assembly of the present application;
FIG. 6 is a side view of the transmission assembly of the present application;
FIG. 7 is a partial perspective view of the roller assembly of the present application;
FIG. 8 is a schematic diagram of an exploded construction of the present application;
fig. 9 is a perspective view of a load bearing arc plate of the present application.
Reference numerals illustrate:
1 base, 2 separation box, 3 separation box, 4 convex frame filter plate, 5 bearing arc plate, 6 overflow port, 7 transmission component, 701 double-shaft driving motor, 702 poking wheel, 703 first belt pulley, 704 first gear, 705 second gear, 706 shaft lever, 707 conveying dragon row, 708 second belt pulley, 709 third belt pulley, 710 fourth belt pulley, 711 fifth belt pulley, 712 first transmission belt, 713 second transmission belt, 714 adjusting rod, 715 eccentric torsion wheel, 716 push-pull rod, 717 piston, 8 notch, 9 roller component, 901 concave roller, 902 transmission rod, 903 impeller, 904 filter cover, 905 immersion hole, 10 feeding pipe, 11 discharging pipe, 12 adjusting ball valve, 13 brush roller, 14 connecting hole, 15L connecting rod, 16 fixing nut, 17 closing door, 18 compressing lock catch.
Detailed Description
In order to make the technical scheme of the present application better understood by those skilled in the art, the present application will be further described in detail with reference to the accompanying drawings.
The application provides a separating device for extracting sea cucumber polysaccharide, which is shown in figures 1-9, and comprises a base 1, wherein the top of the base 1 is fixedly connected with a separating box 2, the middle position inside the separating box 2 is fixedly connected with a separating box 3, separating chambers are arranged on two sides of the separating box 3, a convex frame filter plate 4 is detachably arranged on the side wall of the separating chamber far away from the separating box 3, a bearing arc plate 5 is arranged between the convex frame filter plate 4 and the outer wall of the separating box 3, and two ends of the bearing arc plate 5 are attached to the inner wall of the separating box 2;
the two sides of the surface of the separation box 3 are provided with overflow ports 6, the inside of the separation box 3 is provided with a cavity, the inside of the cavity is provided with a transmission assembly 7, the transmission assembly 7 comprises a double-shaft driving motor 701, the bottom output shaft of the double-shaft driving motor 701 is in transmission connection with a poking wheel 702, the middle part of the bottom end of the separation box 3 is provided with a notch 8, the poking wheel 702 is matched with the notch 8, the top output shaft of the double-shaft driving motor 701 is in transmission connection with a first belt pulley 703, the top of the first belt pulley 703 is fixedly connected with a first gear 704, two sides of the first gear 704 are in meshed connection with a second gear 705, the axis of the second gear 705 is fixedly connected with a shaft lever 706, the outer side of the shaft lever 706 is provided with a conveying dragon row 707 at the overflow port 6, the shaft lever 706 is in rotary connection with the separation box 3, the top of the inner side of the cavity is in rotary connection with a second belt pulley 708, the inside of the cavity is rotationally connected with a third belt pulley 709 at the position outside the overflow port 6, the axes of the first belt pulley 703, the second belt pulley 708 and the third belt pulley 709 are fixedly connected with a mandrel, the mandrels penetrate through the side wall of the separation tank 3, the joints of the mandrels and the separation tank 3 are respectively provided with a sealing bearing, the mandrels at the two sides of the second belt pulley 708 are fixedly connected with a fourth belt pulley 710, the inside of the separation chamber is rotationally connected with a roller assembly 9, the roller assembly 9 consists of a concave roller 901, a transmission rod 902, an impeller 903 and a filtering cover 904, the transmission rod 902 penetrates through the separation tank 3 and extends into the cavity, a fifth belt pulley 711 is arranged at the position outside the transmission rod 902 and inside the cavity, the transmission rod 902 is fixedly connected with the axis of the concave roller 901, the impeller 903 is arranged outside the transmission rod 902, the filter cover 904 is detachably arranged at one end of the concave roller 901, the impeller 903 comprises a plurality of impeller plates which are spirally and obliquely arranged, the surface of the concave roller 901 is provided with a dipping hole 905, the first belt pulley 703, the second belt pulley 708 and the third belt pulley 709 are in transmission connection through a first transmission belt 712, the fourth belt pulley 710 and the fifth belt pulley 711 are in transmission connection through a second transmission belt 713, the end parts of mandrels at two sides of the second belt pulley 708 are in transmission connection with an adjusting rod 714, the middle part of the adjusting rod 714 is fixedly connected with an eccentric torsion wheel 715, the outer side of the eccentric torsion wheel 715 is rotationally connected with a push-pull rod 716, the bottom end of the push-pull rod 716 is hinged with a positioning block, and the bottom end of the positioning block is fixedly connected with a piston 717 matched with a separation chamber.
Further, in the above-mentioned technical solution, the second pulley 708 and the two third pulleys 709 are located on the same section, and the second pulley 708 and the two third pulleys 709 are vertically distributed with the first pulley 703, so as to ensure the stability of the transmission of the device.
Furthermore, in the above technical scheme, the top of separation box 2 both sides wall all is equipped with inlet pipe 10, the bottom of separation box 2 both sides wall all is equipped with discharging pipe 11, two inlet pipe 10 link up with two separation rooms respectively, two discharging pipe 11 link up with two separation rooms respectively, inlet pipe 10 and discharging pipe 11 are inside all to be equipped with regulation ball valve 12, through the whole leakproofness of regulation ball valve 12 control separation room.
Further, in the above technical solution, both ends of the mandrel of the third pulley 709 penetrate through the separate box 3, and a sealing bearing is disposed at the joint of the mandrel and the separate box 3, a brush roller 13 is disposed on the mandrel of the third pulley 709, the brush roller 13 is matched with the outer wall of the concave roller 901, and the brush roller 13 brushes on both sides of the concave roller 901, so as to sweep out impurities adhered on the surface of the concave roller 901, and facilitate improving the grinding effect of the concave roller.
Further, in the above solution, the two eccentric torsion wheels 715 are symmetrically distributed about the center of the second pulley 708, the number of the fifth pulleys 711 is two, the two fifth pulleys 711 are symmetrically distributed about one output shaft of the dual-shaft driving motor 701, and the transmission rods 902 on both sides are not in contact with the output shaft of the dual-shaft driving motor 701.
Further, in the above technical solution, the connection between the transmission rod 902 and the separation tank 2, the separation tank 3 and the flange filter plate 4 are all provided with sealing bearings, and the connection between the shaft 706 and the separation tank 3 is provided with sealing bearings, so as to improve the tightness and flexibility of the transmission of the device.
Furthermore, in the above technical scheme, bear arc board 5 and concave cylinder 901 phase-match, and bear the equal fixedly connected with flange in arc board 5 top both sides, bear arc board 5 and concave cylinder 901 cooperation and function and can grind the precipitate repeatedly, fully dissolve the polysaccharide in the precipitate.
Further, in the above technical scheme, connecting hole 14 has all been seted up at the flange top, equal fixedly connected with L shape connecting rod 15 on the separate tank 3 both sides wall, and L shape connecting rod 15 bottom surface all is equipped with the external screw thread, L shape connecting rod 15 external screw thread connection has fixation nut 16, and L shape connecting rod 15 is located connecting hole 14 top and bottom and all is equipped with the sealing washer, and L shape connecting rod 15 is used for connecting and bears arc board 5 and guarantees its stability, and the effect of sealing washer can prevent that the precipitate from leaking down from the gap simultaneously.
Furthermore, in the above technical scheme, the maintenance port is all offered on the front both sides of separation box 2, the inside articulated closure door 17 that has of maintenance port, and the junction of closure door 17 and maintenance port is equipped with sealed packing, close the connection through compressing tightly hasp 18 between closure door 17 and the separation box 2, open closure door 17 and make maintenance port department unblocked, be convenient for carry out the clearance maintenance to separation box 2 internal device, especially bear the clearance of arc board 5.
The sea cucumber polysaccharide extraction and separation method comprises the sea cucumber polysaccharide extraction and separation device, and the separation steps are as follows:
s1: fully gelling and carrying out enzymolysis on sea cucumber powder to dissolve polysaccharide in water, carrying out enzymolysis and precipitation on protein, feeding the mixed solution into separation chambers at two sides of a separation box 3 from a feed pipe 10, blocking the solution by a bearing arc plate 5 after the solution enters, directly filtering clear liquid from a convex frame filter plate 4, and intercepting protein enzymolysis precipitate at the top of the bearing arc plate 5;
s2: starting a double-shaft driving motor 701, wherein an output shaft of the double-shaft driving motor 701 is in transmission connection with a first belt pulley 703, the first belt pulley 703, a second belt pulley 708 and a third belt pulley 709 are in transmission connection through a first transmission belt 712, and under the action of a fourth belt pulley 710, a fifth belt pulley 711 and a second transmission belt 713, two roller assemblies 9 rotate at the top of a bearing arc plate 5 to grind sediment, so that polysaccharide can be fully dissolved in clear liquid;
s3: the first belt pulley 703 synchronously drives the first gear 704 and drives the two second gears 705 to mesh, so that the two shaft rods 706 drive the conveying dragon rows 707 to stir at the overflow port 6, and the two shaft rods are matched with staggered lifting adjustment of pistons 717 at two sides to ensure that the raw materials in the two separation chambers are more fully mixed, and the stirring wheel 702 at the bottom rotates to ensure that substances in clear liquid do not precipitate;
s4: the two third pulleys 709 drive the brush roller 13 to act on the surface of the concave roller 901, after the clear liquid is discharged, the surface of the concave roller 901 is cleaned, when the sediment is rolled, the water enters the concave roller 901 from the immersion holes 905, and the water is filtered by the filter cover 904 and the convex frame filter plate 4 under the guidance of the inclined wheel plate of the impeller 903 and falls down;
s5: and opening a regulating ball valve 12 on the discharge pipe 11, and taking the clear liquid containing polysaccharide out of the separation chamber for secondary fine filtration.
The working principle of the application is as follows:
referring to fig. 1-9 of the specification, when the device is used, firstly, sea cucumber powder is fully gelled and hydrolyzed, polysaccharide is dissolved in water, protein is hydrolyzed and precipitated, mixed solution is sent into separation chambers at two sides of a separation box 3 from a feed pipe 10, the solution is blocked by a bearing arc plate 5 after entering, clear solution is directly filtered from a convex frame filter plate 4, protein enzymatic precipitate is intercepted at the top of the bearing arc plate 5, a double-shaft driving motor 701 is started, an output shaft of the double-shaft driving motor 701 is in transmission connection with a first belt pulley 703, a second belt pulley 708 and a third belt pulley 709 rotate under the transmission of a first transmission belt 712, a fourth belt pulley 710 and a fifth belt pulley 711 rotate at the top of the bearing arc plate 5 under the action of a second transmission belt 713, the four brush rolls 13 are respectively acted on the surface of the concave roller 901, so that the surface of the concave roller 901 is clean, when sediment is rolled, water enters the concave roller 901 from a soaking hole 905, and falls down after being filtered by a filtering cover 904 and a convex frame filter plate 4 under the guidance of an inclined wheel plate of an impeller 903, a first belt pulley 703 synchronously drives a first gear 704 and drives two second gears 705 to be meshed, so that two shaft rods 706 drive a conveying dragon row 707 to stir at an overflow port 6, the materials in the two separation chambers are more fully mixed by matching with staggered lifting adjustment of pistons 717 at two sides, a stirring wheel 702 at the bottom rotates, so that substances in clear liquid are not precipitated, and finally clear liquid containing polysaccharide is taken out from the separation chamber to be subjected to secondary fine filtration, thereby improving the dissolution rate of polysaccharide and reducing the production cost;
referring to fig. 1-9 of the specification, when the device is cleaned, the closing door 17 can be opened by opening the compression lock catch 18, at the moment, the maintenance opening is smooth, the bearing arc plate 5 is taken down from the L-shaped connecting rod 15, cleaning and maintenance are convenient to be carried out on the bearing arc plate, then the maintenance opening is closed, clear water is introduced, the two shaft rods 706 drive the conveying dragon rows 707 to stir at the overflow port 6, and the internal cleaning effect is improved under the coordination of staggered lifting adjustment of the pistons 717 at two sides and the rotation of the poking wheel 702.
While certain exemplary embodiments of the present application have been described above by way of illustration only, it will be apparent to those of ordinary skill in the art that modifications may be made to the described embodiments in various different ways without departing from the spirit and scope of the application. Accordingly, the drawings and description are to be regarded as illustrative in nature and not as restrictive of the scope of the application, which is defined by the appended claims.
Claims (3)
1. The utility model provides a separation device that sea cucumber polysaccharide draws, includes base (1), base (1) top fixedly connected with separation box (2), its characterized in that: the middle position inside the separation box body (2) is fixedly connected with a separation box (3), separation chambers are arranged on two sides of the separation box (3), a convex frame filter plate (4) is detachably arranged on the side wall, far away from the separation box (3), of the separation chamber, a bearing arc plate (5) is arranged between the convex frame filter plate (4) and the outer wall of the separation box (3), and two ends of the bearing arc plate (5) are attached to the inner wall of the separation box body (2);
the utility model discloses a novel plastic composite material overflow port structure, which is characterized in that overflow ports (6) are formed in two sides of the surface of a separate box (3), a cavity is formed in the separate box (3), a transmission assembly (7) is arranged in the cavity, the transmission assembly (7) comprises a double-shaft driving motor (701), a stirring wheel (702) is connected to the bottom output shaft transmission of the double-shaft driving motor (701), a notch (8) is formed in the middle of the bottom end of the separate box (3), the stirring wheel (702) is matched with the notch (8), a first belt pulley (703) is connected to the top output shaft transmission of the double-shaft driving motor (701), a first gear (704) is fixedly connected to the top of the first belt pulley (703), a second gear (705) is connected to two sides of the first gear in a meshed mode, a shaft lever (706) is fixedly connected to the shaft center of the second gear (705), a conveying dragon row (707) is arranged on the outer side of the shaft lever (706) and is rotatably connected with the bottom of the separate box (3), a second belt pulley (708) is rotatably connected to the inner side of the cavity, a third belt pulley (709) is rotatably connected to the inner side of the cavity and is fixedly connected to the third belt pulley (709) at the outer side of the first belt pulley (709), the utility model discloses a centrifugal pump, including a separation box (3), a spindle, a plurality of filter covers (904) and a plurality of impeller plates, wherein the spindle penetrates through the side wall of the separation box (3), sealing bearings are arranged at the joint of the spindle and the separation box (3), a fourth belt pulley (710) is fixedly connected to the spindle on two sides of the second belt pulley (708), a roller assembly (9) is rotatably connected in the separation box, the roller assembly (9) consists of a concave roller (901), a transmission rod (902), an impeller (903) and a filter cover (904), the transmission rod (902) penetrates through the separation box (3) and extends to the inside of a cavity, a fifth belt pulley (711) is arranged at the position of the outer side of the transmission rod (902) in the cavity, the transmission rod (902) is fixedly connected to the axis of the concave roller (901), the outer side of the transmission rod (902) is provided with the impeller (903), one end of the concave roller (901) is detachably provided with the filter cover (904), the impeller (903) comprises a plurality of spiral inclined wheel plates, a dipping hole (905) is formed in the surface of the concave roller (901), a dipping hole (905) is formed between the first belt pulley (703), the second belt pulley (708) and a third belt pulley (709) through the first belt, the second belt pulley (708) is connected with the end part of the second belt pulley (714) through the transmission rod (712), the middle part of the adjusting rod (714) is fixedly connected with an eccentric torsion wheel (715), the outer side of the eccentric torsion wheel (715) is rotationally connected with a push-pull rod (716), the bottom end of the push-pull rod (716) is hinged with a positioning block, and the bottom end of the positioning block is fixedly connected with a piston (717) matched with the separation chamber;
the second belt pulley (708) and the two third belt pulleys (709) are positioned on the same section, and the second belt pulley (708) and the two third belt pulleys (709) are vertically distributed with the first belt pulley (703);
the top of the two side walls of the separation box body (2) is provided with a feed pipe (10), the bottom of the two side walls of the separation box body (2) is provided with a discharge pipe (11), two feed pipes (10) are respectively communicated with two separation chambers, two discharge pipes (11) are respectively communicated with two separation chambers, and regulating ball valves (12) are respectively arranged inside the feed pipe (10) and the discharge pipes (11);
the two ends of the mandrel of the third belt pulley (709) penetrate through the separate box (3), a sealing bearing is arranged at the joint of the mandrel and the separate box (3), a brush roller (13) is arranged on the mandrel of the third belt pulley (709), and the brush roller (13) is matched with the outer wall of the concave roller (901);
the joints of the transmission rod (902) and the separation box body (2), the separation box (3) and the convex frame filter plates (4) are respectively provided with a sealing bearing, and the joints of the shaft rods (706) and the separation box (3) are respectively provided with a sealing bearing;
the bearing arc plate (5) is matched with the concave roller (901), and convex plates are fixedly connected to two sides of the top of the bearing arc plate (5);
the top of the convex plate is provided with connecting holes (14), the two side walls of the separation box (3) are fixedly connected with L-shaped connecting rods (15), external threads are arranged on the outer surfaces of the bottoms of the L-shaped connecting rods (15), fixing nuts (16) are connected with the external threads of the L-shaped connecting rods (15), and sealing rings are arranged at the top and the bottom of the connecting holes (14) of the L-shaped connecting rods (15);
the separation box body (2) is characterized in that maintenance ports are formed in two sides of the front face of the separation box body (2), a closing door (17) is hinged in the maintenance ports, sealing packing is arranged at the joint of the closing door (17) and the maintenance ports, and the closing door (17) is in closed connection with the separation box body (2) through a compression lock catch (18).
2. The separating device for extracting sea cucumber polysaccharide according to claim 1, wherein: the two eccentric torsion wheels (715) are symmetrically distributed around the center of the second belt pulley (708), the number of the fifth belt pulleys (711) is two, the two fifth belt pulleys (711) are symmetrically distributed around one output shaft of the double-shaft driving motor (701), and the transmission rods (902) on two sides are not contacted with the output shaft of the double-shaft driving motor (701).
3. A method for separating sea cucumber polysaccharide extraction, comprising a sea cucumber polysaccharide extraction separation device as claimed in any one of claims 1-2, characterized in that: the separation steps are as follows:
s1: fully gelling and carrying out enzymolysis on sea cucumber powder to dissolve polysaccharide in water, carrying out enzymolysis and precipitation on protein, sending the mixed solution into separation chambers at two sides of a separation box (3) from a feed pipe (10), blocking the solution by a bearing arc plate (5) after the solution enters, directly filtering clear liquid from a convex frame filter plate (4), and intercepting the enzymolysis and precipitation on the top of the bearing arc plate (5);
s2: starting a double-shaft driving motor (701), wherein an output shaft of the double-shaft driving motor (701) is in transmission connection with a first belt pulley (703), the first belt pulley (703), a second belt pulley (708) and a third belt pulley (709) are in transmission connection through a first transmission belt (712), and under the action of a fourth belt pulley (710), a fifth belt pulley (711) and a second transmission belt (713), two roller assemblies (9) rotate at the top of a bearing arc plate (5), and precipitate is milled, so that polysaccharide can be fully dissolved in clear liquid;
s3: the first belt pulley (703) synchronously drives the first gear (704) and drives the two second gears (705) to be meshed, so that the two shaft rods (706) drive the conveying dragon rows (707) to stir at the overflow port (6), and the two shaft rods are matched with staggered lifting adjustment of pistons (717) at two sides to ensure that the raw materials in the two separation chambers are more fully mixed, and the stirring wheel (702) at the bottom rotates to ensure that substances in clear liquid are not precipitated;
s4: the two third pulleys (709) drive the brush rolls (13) to act on the surface of the concave rotary drum (901), after the clear liquid is discharged, the surface of the concave rotary drum (901) is cleaned, when the sediment is rolled, the water enters the concave rotary drum (901) from the immersing holes (905), and the water falls down after being filtered by the filtering cover (904) and the convex frame filter plate (4) under the guidance of the inclined wheel plate of the impeller (903);
s5: and opening an adjusting ball valve (12) on the discharging pipe (11), and taking clear liquid containing polysaccharide out of the separation chamber for secondary fine filtration.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210616126.6A CN115536757B (en) | 2022-06-01 | 2022-06-01 | Separating device and method for sea cucumber polysaccharide extraction |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210616126.6A CN115536757B (en) | 2022-06-01 | 2022-06-01 | Separating device and method for sea cucumber polysaccharide extraction |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN115536757A CN115536757A (en) | 2022-12-30 |
| CN115536757B true CN115536757B (en) | 2023-08-22 |
Family
ID=84724678
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202210616126.6A Active CN115536757B (en) | 2022-06-01 | 2022-06-01 | Separating device and method for sea cucumber polysaccharide extraction |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN115536757B (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN117535121B (en) * | 2024-01-09 | 2024-03-19 | 四川博浩达生物科技有限公司 | Industrial enzyme sample extraction equipment |
| CN117839438B (en) * | 2024-03-07 | 2024-05-03 | 山东深海生物科技股份有限公司 | Solid-liquid separation device for producing 5-aminolevulinic acid fermentation liquor by fermentation method |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN209185628U (en) * | 2018-10-30 | 2019-08-02 | 大连真久生物产业有限公司 | The device of sea cucumber oligopeptide and polysaccharide is extracted from sea cucumber deep processing byproduct |
| CN110204626A (en) * | 2019-06-17 | 2019-09-06 | 日照职业技术学院 | A kind of device and method sea cucumber polysaccharide separation and refined |
| CN212974253U (en) * | 2020-08-10 | 2021-04-16 | 青岛悦龙堂食品有限公司 | Boiling device for extracting sea cucumber polysaccharide substances |
| CN214458041U (en) * | 2020-11-24 | 2021-10-22 | 烟台和易万家生物科技有限公司 | Sea cucumber polysaccharide enzymolysis extraction element |
-
2022
- 2022-06-01 CN CN202210616126.6A patent/CN115536757B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN209185628U (en) * | 2018-10-30 | 2019-08-02 | 大连真久生物产业有限公司 | The device of sea cucumber oligopeptide and polysaccharide is extracted from sea cucumber deep processing byproduct |
| CN110204626A (en) * | 2019-06-17 | 2019-09-06 | 日照职业技术学院 | A kind of device and method sea cucumber polysaccharide separation and refined |
| CN212974253U (en) * | 2020-08-10 | 2021-04-16 | 青岛悦龙堂食品有限公司 | Boiling device for extracting sea cucumber polysaccharide substances |
| CN214458041U (en) * | 2020-11-24 | 2021-10-22 | 烟台和易万家生物科技有限公司 | Sea cucumber polysaccharide enzymolysis extraction element |
Also Published As
| Publication number | Publication date |
|---|---|
| CN115536757A (en) | 2022-12-30 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN115536757B (en) | Separating device and method for sea cucumber polysaccharide extraction | |
| CN209778487U (en) | Stirring formula sewage treatment plant | |
| CN218486207U (en) | Yak bone small molecule peptide apparatus for producing | |
| CN213492325U (en) | Food production sewage filters discharging equipment | |
| CN211536626U (en) | Active carbon adsorption device for product decoloration | |
| CN211912876U (en) | Fungus residue multi-stage filtering device for preparing edible fungus composite polysaccharide | |
| CN209068907U (en) | Screening installation is dried in rice dedusting | |
| CN216440436U (en) | Compounding device is used in processing of plant extract deodorant | |
| CN212417187U (en) | Filtering device for processing concentrated fruit juice | |
| CN112474069A (en) | Novel multi-functional seed of job's tears processing centrifugal dehydration device | |
| CN113856811A (en) | Face cream raw material extraction system and face cream raw material extraction method | |
| CN116806902B (en) | Energy-saving composite tea fermentation device with recyclable fermentation liquor | |
| CN112007733A (en) | Intelligent kitchen waste treatment equipment | |
| CN220696120U (en) | Filtering device suitable for green plum fruit processing is with filtering fruit sediment | |
| CN206318918U (en) | A kind of extraction element that astragalus polyose is extracted from the Radix Astragali | |
| CN205295201U (en) | Extraction element is glued to shaddock follicarpium | |
| CN217139595U (en) | Sweet potato starch production is with deposiing device | |
| CN217547195U (en) | Dewatering device is used in processing of schizo-alga | |
| CN211542478U (en) | Fruit ferment production that can prevent ferment and run off is with squeezing device | |
| CN213895823U (en) | Strain storage device for fermented beverage | |
| CN210448348U (en) | Ferment zymotic fluid filter equipment | |
| CN217218045U (en) | Horizontal solid state fermentation jar of ancient rhyme pu' er tea | |
| CN218001976U (en) | Dewatering device is used in spirulina production and processing | |
| CN215782119U (en) | Protein water recovery device for fish meal production | |
| CN209759420U (en) | Drying device for wine making equipment |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |