CN115417719A - Xinjiang cotton fulvic acid microelement foliage water-soluble fertilizer and preparation method thereof - Google Patents

Xinjiang cotton fulvic acid microelement foliage water-soluble fertilizer and preparation method thereof Download PDF

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CN115417719A
CN115417719A CN202211074057.7A CN202211074057A CN115417719A CN 115417719 A CN115417719 A CN 115417719A CN 202211074057 A CN202211074057 A CN 202211074057A CN 115417719 A CN115417719 A CN 115417719A
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parts
acid
soluble fertilizer
fulvic acid
water
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王新勇
王冰
邵华伟
周燕
唐蕾
程新瑛
郑科勇
党小龙
宋康康
何庆明
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Xinjiang Yiguo Biotechnology Co ltd
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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05CNITROGENOUS FERTILISERS
    • C05C9/00Fertilisers containing urea or urea compounds
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05FORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F17/00Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation
    • C05F17/20Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation using specific microorganisms or substances, e.g. enzymes, for activating or stimulating the treatment
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/80Soil conditioners
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G5/00Fertilisers characterised by their form
    • C05G5/10Solid or semi-solid fertilisers, e.g. powders
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P60/00Technologies relating to agriculture, livestock or agroalimentary industries
    • Y02P60/20Reduction of greenhouse gas [GHG] emissions in agriculture, e.g. CO2
    • Y02P60/21Dinitrogen oxide [N2O], e.g. using aquaponics, hydroponics or efficiency measures
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/40Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse

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Abstract

The invention discloses a Xinjiang cotton fulvic acid microelement foliage water-soluble fertilizer and a preparation method thereof, wherein the preparation method comprises the following steps: preparing raw materials; weighing the following components: weighing the using amount of each component according to the formula proportion, wherein a weighing tool is in a dry and pollution-free state; mixing treatment; adding trace elements; fermenting at constant temperature. The Xinjiang cotton fulvic acid microelement foliage water-soluble fertilizer and the preparation method thereof are characterized in that fulvic acid is added, wherein the fulvic acid is 15 parts by weight, and the fulvic acid can promote the growth of cotton, has an important effect on drought resistance, can improve the stress resistance of the cotton, and has the effects of increasing yield and improving quality, taking foliage spraying of the cotton as an example, the average air pore opening degree can be reduced by about two thirds, meanwhile, the root activity of a plant can be improved, premature senility is prevented, various enzyme activities are improved, the chlorophyll content is increased by more than 20%, and the microelement is added: the boric acid, manganese sulfate, zinc sulfate and magnesium sulfate are added, so that the growth of cotton is facilitated, the yield of the cotton is higher, and the quality of the cotton is better.

Description

Xinjiang cotton fulvic acid microelement foliage water-soluble fertilizer and preparation method thereof
Technical Field
The invention relates to the technical field of foliar water-soluble fertilizers, in particular to a foliar water-soluble fertilizer containing fulvic acid trace elements of Xinjiang cotton and a preparation method thereof.
Background
China is a big country for agricultural production, and the fertilizer is a material guarantee for the sustainable development of agriculture and is the basis for increasing the yield of crops. However, unreasonable application of chemical fertilizers for many years not only causes a great deal of economic and resource waste, but also causes a great deal of serious acid-base formation of fertile lands, soil hardening, environmental pollution and other problems. The water-soluble fertilizer is a compound fertilizer containing nitrogen, phosphorus, potassium, calcium, magnesium, trace elements, amino acid, humic acid, alginic acid and the like, which can be completely dissolved in water. The fertilizer is divided into a solid water-soluble fertilizer and a liquid water-soluble fertilizer in form. The nutrient content of the fertilizer comprises macroelement water-soluble fertilizer, secondary element water-soluble fertilizer, microelement water-soluble fertilizer, amino acid-containing water-soluble fertilizer, humic acid-containing water-soluble fertilizer, organic water-soluble fertilizer and the like. The water-soluble fertilizer has the obvious advantages of instant dissolution, high absorption rate, quick response, no residue, convenient application and the like, and is developed rapidly.
As a novel fertilizer, compared with the traditional fertilizer, the water-soluble fertilizer has various formulas and very flexible application method, can be irrigated by soil, leads the roots of plants to be in full contact with the fertilizer and breathes various nutrient elements as much as possible; the fertilizer can be sprayed on the leaf surfaces and enters the plants through leaf surface pores, so that the absorption and utilization rate of the fertilizer is improved; can also be used for drip irrigation and soilless culture, saves irrigation water and improves the labor production efficiency. In the fertilization process, in order to achieve the best effect, certain fertilization skills are mastered by combining the characteristics of the water-soluble fertilizer.
The water soluble fertilizer is a quick-acting fertilizer, has comprehensive nutrient elements, has different formulas according to the fertilizer requirement characteristics of different crops, and is sold in the market as a special water soluble fertilizer for various crops such as vegetables, fruit trees, flowers, grains, cotton, oils and the like. The water soluble fertilizer has higher price, so the water soluble fertilizer is not popularized in a large area, and general consumption areas mainly concentrate on greenhouse vegetable production bases, fruit tree production bases, some flower planting areas and the like, for example, areas such as Liaoning, hebei, shandong, xinjiang, sichuan, guangxi, yunnan, hainan and the like in China are key consumption areas of the water soluble fertilizer. Although the water-soluble fertilizer is just started in China, the water-soluble fertilizer has a good prospect, a very wide development prospect and a bright future for the industry.
However, when the existing water-soluble fertilizer is used for regulating the growth of cotton, the drought resistance is poor, and a large amount of caking is easy to occur in the storage process, so that the use of the water-soluble fertilizer is influenced, the growth rate of the cotton is reduced, insoluble substances in the water-soluble fertilizer are more, the dissolution speed is slow, and the spray head and a drip irrigation pipeline are easy to block, so that the working efficiency is reduced.
Therefore, the Xinjiang cotton fulvic acid microelement foliage water-soluble fertilizer and the preparation method are provided so as to solve the problems.
Disclosure of Invention
The invention aims to provide a Xinjiang cotton fulvic acid microelement foliage water-soluble fertilizer and a preparation method thereof, and aims to solve the problems that the existing water-soluble fertilizer has poor drought resistance and is easy to generate a large amount of caking in the storage process, so that the cotton productivity is reduced and the work efficiency is reduced.
In order to achieve the purpose, the invention provides the following technical scheme: a Xinjiang cotton fulvic acid microelement foliage water-soluble fertilizer;
the Xinjiang cotton fulvic acid microelement foliage water-soluble fertilizer comprises the following raw materials: fulvic acid, alginic acid, amino acid, boric acid, manganese sulfate, zinc sulfate, magnesium sulfate, an enzyme preparation, urea, a dispersing agent, a high-efficiency active agent and a compound microbial agent.
Preferably, the raw materials in parts by weight are as follows: 10-20 parts of fulvic acid, 5-10 parts of alginic acid, 3-6 parts of amino acid, 1-3 parts of boric acid, 0.2-0.5 part of manganese sulfate, 1-3 parts of zinc sulfate, 6-15 parts of magnesium sulfate, 1-5 parts of an enzyme preparation, 100-150 parts of urea, 3-6 parts of a dispersing agent, 3-6 parts of a high-efficiency active agent and 1-5 parts of a compound microbial agent.
By adopting the technical scheme, the raw materials are proportioned more accurately through the raw materials in parts by weight, the effect of the water-soluble fertilizer is improved, and the problem that the working efficiency is reduced due to poor drought resistance or caking phenomenon is avoided.
Preferably, the fulvic acid solids are brown and grey black in color, and the fulvic acid is readily soluble in water, ethanol, dilute acids, dilute bases and aqueous acetone.
By adopting the technical scheme, the fulvic acid is easy to dissolve in water, ethanol, dilute acid, dilute alkali and hydrous acetone, wherein the fulvic acid plays an important role in drought resistance and is convenient to quickly dissolve in water, and by taking the example of spraying cotton on leaf surfaces, the average stomatal opening degree can be reduced by about two thirds, and meanwhile, the activity of plant root systems can be improved, premature senility can be prevented, various enzyme activities can be improved, and the chlorophyll content can be increased by more than 20%.
Preferably, the alginic acid is a natural polyuronic acid existing in the cell wall of brown algae such as kelp and kelp;
the amino acid is an organic compound containing a basic amino group and an acidic carboxyl group;
the boric acid, the manganese sulfate, the zinc sulfate and the magnesium sulfate are trace elements.
By adopting the technical scheme, the method comprises the following steps of: the boric acid, manganese sulfate, zinc sulfate and magnesium sulfate are added, so that the growth of cotton is facilitated, the yield of the cotton is higher, and the quality of the cotton is better.
Preferably, the enzyme preparation is a surfactant having both lipophilic and hydrophilic properties within the molecule;
the dispersing agent is ethylene glycol, the efficient active agent is convenient to give full play to the efficacy, the compound microbial agent is prepared by mixing trichoderma harzianum powder, bacillus subtilis powder and phanerochaete chrysosporium powder according to a weight ratio, and the use amount of the accelerator is reduced or the vulcanization time is shortened by enzyme-linked use of the microbial agent.
By adopting the technical scheme, the enzyme preparation and the dispersing agent are added, wherein the enzyme preparation has the characteristics of high catalytic efficiency, high specificity, mild action condition, energy consumption reduction, chemical pollution reduction and the like, and the dispersing agent can uniformly disperse inorganic matters which are difficult to dissolve in liquid, solid and liquid particles of organic pigments, and simultaneously can prevent the particles from settling and coagulating to form an amphiphilic agent required by a stable suspension liquid, thereby avoiding the phenomenon of insolubility in water.
Preferably, the components in parts by weight are respectively 15 parts of fulvic acid, 6 parts of alginic acid, 4 parts of amino acid, 2 parts of boric acid, 0.3 part of manganese sulfate, 2 parts of zinc sulfate, 6 parts of magnesium sulfate, 3 parts of an enzyme preparation, 120 parts of urea, 4 parts of a dispersing agent, 3 parts of a high-efficiency active agent and 3 parts of a compound microbial agent.
By adopting the technical scheme, the ratio of the water-soluble fertilizer is more accurate through numerical values of various raw materials in parts by weight, so that the effect of the water-soluble fertilizer is optimal, the growth of cotton is promoted, precipitates are reduced, and the foliage water-soluble fertilizer is suitable for being sprayed by an unmanned aerial vehicle and improves the working efficiency.
A preparation method of a Xinjiang cotton fulvic acid microelement foliage water-soluble fertilizer comprises the following steps:
s1, preparing raw materials: the required raw materials are collected, so that each raw material is independently stored, the purity of each raw material is ensured, and the raw materials are not polluted by other impurities;
s2, weighing the dosage: weighing the components according to the proportion of the formula, and taking a weighing tool in a dry and pollution-free state;
s3, mixing treatment: respectively and uniformly mixing alginic acid, urea, amino acid and an enzyme preparation, then crushing the mixture, sieving the mixture by using a fine sieve, adding water, heating the mixture to 60-80 ℃, and simultaneously stirring the mixture at a constant speed for 10-15 minutes;
s4, adding trace elements: adding trace elements to the resulting mixture: adding trace elements into manganese sulfate, zinc sulfate and magnesium sulfate, and stirring at a constant speed to uniformly stir;
s5, constant-temperature fermentation: and (3) placing the mixture in an environment with the temperature of 40-50 ℃, fermenting for 3-4 days in a constant temperature environment, respectively adding fulvic acid, boric acid and a dispersing agent after the fermentation is finished, uniformly stirring, and drying to obtain the fulvic acid trace element foliage water-soluble fertilizer.
S6, drying: and heating the obtained fulvic acid trace element foliage water-soluble fertilizer to 40 ℃, continuously stirring to dry the foliage water-soluble fertilizer, and drying to obtain the powdered foliage water-soluble fertilizer.
Preferably, each component raw material is stored separately, and the storage environment avoids impurities from being mixed, and the raw materials are pure, so that the obtained fertilizer has the best effect.
Preferably, the stirring is performed at a constant speed and in the same direction during the stirring process, so that the mixture can obtain a sufficient and uniform mixing effect.
Compared with the prior art, the invention has the beneficial effects that:
1. the invention adds fulvic acid, wherein the fulvic acid is 15 parts by weight, can promote the growth of cotton, has important function on drought resistance, can improve the stress resistance of cotton, and has the functions of increasing yield and improving quality, and the fulvic acid is easy to dissolve in water, ethanol, dilute acid, dilute alkali and water-containing acetone, for example, when the cotton is sprayed on leaf surfaces, the average stomatal opening degree can be reduced by about two thirds, and simultaneously, the activity of the root system of a plant can be improved, premature senility can be prevented, various enzyme activities can be improved, the chlorophyll content can be increased by more than 20 percent, and the fulvic acid can be prepared by the following steps of: the boric acid, manganese sulfate, zinc sulfate and magnesium sulfate are added, so that the growth of cotton is facilitated, the yield of the cotton is higher, and the quality of the cotton is better.
2. According to the invention, through the addition of the enzyme preparation and the dispersing agent, the enzyme preparation has the characteristics of high catalytic efficiency, high specificity, mild action conditions, energy consumption reduction, chemical pollution reduction and the like, the decomposition speed of the water-soluble fertilizer is improved, the dispersing agent can uniformly disperse inorganic matters which are difficult to dissolve in liquid, solid and liquid particles of organic pigments, and can prevent the particles from settling and condensing to form an amphiphilic reagent required by a stable suspension, so that the phenomenon of agglomeration in the water-adding dissolving process is avoided, the phenomenon of blocking a spray head and a drip irrigation pipeline is also avoided, and the working efficiency of using the foliage water-soluble fertilizer is improved.
Drawings
FIG. 1 is a schematic diagram of a preparation process of the water soluble fertilizer.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Referring to fig. 1, an embodiment of the present invention:
example 1
A Xinjiang cotton fulvic acid microelement foliage water-soluble fertilizer;
the Xinjiang cotton fulvic acid microelement foliage water-soluble fertilizer comprises the following raw materials: fulvic acid, alginic acid, amino acid, boric acid, manganese sulfate, zinc sulfate, magnesium sulfate, an enzyme preparation, urea, a dispersing agent, a high-efficiency active agent and a compound microbial agent.
The raw material components by weight portion are as follows: 10-20 parts of fulvic acid, 5-10 parts of alginic acid, 3-6 parts of amino acid, 1-3 parts of boric acid, 0.2-0.5 part of manganese sulfate, 1-3 parts of zinc sulfate, 6-15 parts of magnesium sulfate, 1-5 parts of an enzyme preparation, 100-150 parts of urea, 3-6 parts of a dispersing agent, 3-6 parts of a high-efficiency active agent and 1-5 parts of a compound microbial agent, wherein the raw materials are calculated according to the parts by weight of the raw materials, so that the raw material proportion is more accurate, the effect of the water-soluble fertilizer is improved, and the problem that the working efficiency is reduced due to poor drought resistance or caking phenomenon is avoided;
the fulvic acid solid is brown and grey black, and is easily soluble in water, ethanol, dilute acid, dilute alkali and water-containing acetone, and the fulvic acid is easily soluble in water, ethanol, dilute acid, dilute alkali and water-containing acetone, wherein the fulvic acid plays an important role in drought resistance, so that the fulvic acid is conveniently and quickly dissolved in water, for example, cotton sprayed on leaf surfaces can reduce the average stomatal opening degree by about two thirds, and meanwhile, the activity of the root system of a plant can be improved, premature senility can be prevented, various enzyme activities can be improved, and the chlorophyll content can be increased by more than 20%;
alginic acid is a natural polyuronic acid existing in the cell wall of brown algae such as kelp and kelp, amino acid is an organic compound containing basic amino and acidic carboxyl, boric acid, manganese sulfate, zinc sulfate and magnesium sulfate are trace elements, and the content of the polyuronic acid is determined by the following formula: boric acid, manganese sulfate, zinc sulfate and magnesium sulfate are added, the growth of cotton is facilitated, the yield of cotton is higher, the quality is better, an enzyme preparation is a surfactant which has two opposite properties of lipophilicity and hydrophilicity in a molecule, a dispersing agent is ethylene glycol, an efficient active agent is convenient to give full play to the effect, and a composite microbial agent is prepared by mixing trichoderma harzianum powder, bacillus subtilis powder and phanerochaete chrysosporium powder according to a weight ratio, the consumption of an accelerant is reduced or the vulcanization time is shortened by continuous use of microbial enzymes, and the enzyme preparation and the dispersing agent are added, wherein the enzyme preparation has the characteristics of high catalytic efficiency, high specificity, mild action conditions, energy consumption reduction, chemical pollution reduction and the like, the dispersing agent can uniformly disperse inorganic substances which are difficult to dissolve in liquid, solid and liquid particles of organic pigments, and can prevent sedimentation and agglomeration of the particles to form an amphiphilic agent required by a stable suspension liquid, so that the phenomenon of insolubilization in water is avoided;
the components in parts by weight are respectively as follows:
15 parts of fulvic acid, 6 parts of alginic acid, 4 parts of amino acid, 2 parts of boric acid, 0.3 part of manganese sulfate, 2 parts of zinc sulfate, 6 parts of magnesium sulfate, 3 parts of an enzyme preparation, 120 parts of urea, 4 parts of a dispersing agent, 3 parts of a high-efficiency active agent and 3 parts of a compound microbial agent;
numerical values through all kinds of raw materials are counted according to parts by weight, the ratio of the water-soluble fertilizer is more accurate, so that the effect of the water-soluble fertilizer is optimal, the growth of cotton is promoted, precipitates are reduced, the foliage water-soluble fertilizer is suitable for being sprayed by an unmanned aerial vehicle, and the working efficiency is improved.
With reference to fig. 1, a preparation method of a fulvic acid trace element foliar water-soluble fertilizer for Xinjiang cotton comprises the following steps:
s1, preparing raw materials: the required raw materials are collected, so that each raw material is independently stored, the purity of each raw material is ensured, and the raw materials are not polluted by other impurities;
s2, weighing the dosage: weighing the using amount of each component according to the formula proportion, wherein a weighing tool is in a dry and pollution-free state;
s3, mixing treatment: respectively and uniformly mixing alginic acid, urea, amino acid and an enzyme preparation, then crushing the mixture, sieving the mixture by using a fine sieve, adding water, heating the mixture to 60-80 ℃, and simultaneously stirring the mixture at a constant speed for 10-15 minutes;
s4, adding trace elements: adding trace elements to the obtained mixture: adding trace elements into manganese sulfate, zinc sulfate and magnesium sulfate, and stirring at a constant speed to uniformly stir;
s5, constant-temperature fermentation: and (3) placing the mixture in an environment with the temperature of 40-50 ℃, fermenting for 3-4 days in a constant temperature environment, respectively adding fulvic acid, boric acid and a dispersing agent after the fermentation is finished, uniformly stirring, and drying to obtain the fulvic acid trace element foliage water-soluble fertilizer.
S6, drying treatment: and heating the obtained fulvic acid trace element foliage water-soluble fertilizer to 40 ℃, continuously stirring to dry the foliage water-soluble fertilizer, and drying to obtain the powdered foliage water-soluble fertilizer.
All component raw materials are all deposited alone, and deposit the environment and avoid impurity interfusion, the purity of raw materials for the fertilizer effect that arrives is best.
Stirring in the same direction at a constant speed in the stirring process to ensure that the mixture obtains a sufficient and uniform mixing effect.
Example 2
A Xinjiang cotton fulvic acid microelement foliage water-soluble fertilizer;
the Xinjiang cotton fulvic acid microelement foliage water-soluble fertilizer comprises the following raw materials: fulvic acid, alginic acid, amino acid, boric acid, manganese sulfate, zinc sulfate, magnesium sulfate, an enzyme preparation, urea, a dispersing agent, a high-efficiency active agent and a compound microbial agent.
The raw material components by weight portion are as follows: 10-20 parts of fulvic acid, 5-10 parts of alginic acid, 3-6 parts of amino acid, 1-3 parts of boric acid, 0.2-0.5 part of manganese sulfate, 1-3 parts of zinc sulfate, 6-15 parts of magnesium sulfate, 1-5 parts of an enzyme preparation, 100-150 parts of urea, 3-6 parts of a dispersing agent, 3-6 parts of a high-efficiency active agent and 1-5 parts of a compound microbial agent, wherein the raw materials are calculated according to the parts by weight of the raw materials, so that the raw material proportion is more accurate, the effect of the water-soluble fertilizer is improved, and the problem that the working efficiency is reduced due to poor drought resistance or caking phenomenon is avoided;
the fulvic acid solid is brown and grey black, and is easily soluble in water, ethanol, dilute acid, dilute alkali and water-containing acetone, and the fulvic acid is easily soluble in water, ethanol, dilute acid, dilute alkali and water-containing acetone, wherein the fulvic acid plays an important role in drought resistance, so that the fulvic acid is conveniently and quickly dissolved in water, for example, cotton sprayed on leaf surfaces can reduce the average stomatal opening degree by about two thirds, and meanwhile, the activity of the root system of a plant can be improved, premature senility can be prevented, various enzyme activities can be improved, and the chlorophyll content can be increased by more than 20%;
alginic acid is a natural polyuronic acid existing in the cell wall of brown algae such as kelp and kelp, amino acid is an organic compound containing basic amino and acidic carboxyl, boric acid, manganese sulfate, zinc sulfate and magnesium sulfate are trace elements, and the content of the polyuronic acid is determined by the following formula: boric acid, manganese sulfate, zinc sulfate and magnesium sulfate are added, so that the growth of cotton is facilitated, the yield of cotton is higher, the quality is better, an enzyme preparation is a surfactant which has two opposite properties of lipophilicity and hydrophilicity in a molecule, a dispersing agent is ethylene glycol, an efficient active agent is convenient for giving full play to the effect, and a composite microbial agent is prepared by mixing trichoderma harzianum powder, bacillus subtilis powder and phanerochaete chrysosporium powder according to a weight ratio, the consumption of an accelerant is reduced or a vulcanization time is shortened by enzyme-linked use of bacteria, and through the addition of the enzyme preparation and the dispersing agent, the enzyme preparation has the characteristics of high catalytic efficiency, high specificity, mild action conditions, energy consumption reduction, chemical pollution reduction and the like, and the dispersing agent can uniformly disperse inorganic substances which are difficult to dissolve in liquid, solid and liquid particles of organic pigments, and can also prevent the sedimentation and agglomeration of the particles, so that an amphiphilic agent required by a stable suspension is formed, and the phenomenon of insolubility in water is avoided;
the components in parts by weight are respectively as follows:
18 parts of fulvic acid, 8 parts of alginic acid, 5 parts of amino acid, 2 parts of boric acid, 0.4 part of manganese sulfate, 2 parts of zinc sulfate, 8 parts of magnesium sulfate, 4 parts of an enzyme preparation, 130 parts of urea, 5 parts of a dispersing agent, 4 parts of a high-efficiency active agent and 4 parts of a compound microbial agent;
numerical values through all kinds of raw materials are counted according to parts by weight, the ratio of the water-soluble fertilizer is more accurate, so that the effect of the water-soluble fertilizer is optimal, the growth of cotton is promoted, precipitates are reduced, the foliage water-soluble fertilizer is suitable for being sprayed by an unmanned aerial vehicle, and the working efficiency is improved.
With reference to fig. 1, a preparation method of a fulvic acid trace element foliar water-soluble fertilizer for Xinjiang cotton comprises the following steps:
s1, preparing raw materials: the required raw materials are collected, so that each raw material is independently stored, the purity of each raw material is ensured, and the raw materials are not polluted by other impurities;
s2, weighing the dosage: weighing the components according to the proportion of the formula, and taking a weighing tool in a dry and pollution-free state;
s3, mixing treatment: respectively and uniformly mixing alginic acid, urea, amino acid and an enzyme preparation, then crushing the mixture, sieving the mixture by using a fine sieve, adding water, heating the mixture to 70-80 ℃, and simultaneously stirring the mixture at a constant speed for 5-10 minutes;
s4, adding trace elements: adding trace elements to the resulting mixture: manganese sulfate, zinc sulfate and magnesium sulfate are added with trace elements and stirred at a constant speed, so that the manganese sulfate, the zinc sulfate and the magnesium sulfate are uniformly stirred;
s5, constant-temperature fermentation: and (3) placing the mixture in an environment with the temperature of 40-50 ℃, fermenting for 3-4 days in a constant temperature environment, respectively adding fulvic acid, boric acid and a dispersing agent after fermentation is completed, uniformly stirring, and drying to obtain the fulvic acid trace element foliage water-soluble fertilizer.
S6, drying: heating the obtained fulvic acid trace element foliar water-soluble fertilizer to 40 ℃, continuously stirring, drying the foliar water-soluble fertilizer, and making the dried foliar water-soluble fertilizer into powder.
All component raw materials are all deposited alone, and deposit the environment and avoid impurity interfusion, the purity of raw materials for the fertilizer effect that arrives is best.
Stirring in the same direction at a constant speed in the stirring process to ensure that the mixture obtains a sufficient and uniform mixing effect.
Through the increase of the content of the fulvic acid, 1 part of the enzyme preparation and the dispersant are added, so that the mixing time of the foliar water-soluble fertilizer is reduced from 10-15 minutes to 5-10 minutes, and the dissolving speed of the foliar water-soluble fertilizer and water is not influenced.
Example 3
A Xinjiang cotton fulvic acid microelement foliage water-soluble fertilizer;
the Xinjiang cotton fulvic acid microelement foliage water-soluble fertilizer comprises the following raw materials: fulvic acid, alginic acid, amino acid, boric acid, manganese sulfate, zinc sulfate, magnesium sulfate, an enzyme preparation, urea, a dispersing agent, a high-efficiency active agent and a compound microbial agent.
The raw material components by weight portion are as follows: 10-20 parts of fulvic acid, 5-10 parts of alginic acid, 3-6 parts of amino acid, 1-3 parts of boric acid, 0.2-0.5 part of manganese sulfate, 1-3 parts of zinc sulfate, 6-15 parts of magnesium sulfate, 1-5 parts of an enzyme preparation, 100-150 parts of urea, 3-6 parts of a dispersing agent, 3-6 parts of a high-efficiency active agent and 1-5 parts of a compound microbial agent, wherein the raw materials are calculated according to the parts by weight of the raw materials, so that the raw material proportion is more accurate, the effect of the water-soluble fertilizer is improved, and the problem that the working efficiency is reduced due to poor drought resistance or caking phenomenon is avoided;
the fulvic acid solid is brown and grey black, and the fulvic acid is easy to dissolve in water, ethanol, dilute acid, dilute alkali and water-containing acetone, wherein the fulvic acid has an important function on drought resistance, so that the fulvic acid is convenient to quickly dissolve in water, for example, cotton sprayed on leaf surfaces can reduce the average pore opening degree by about two thirds, and simultaneously can also improve the root activity of plants, prevent premature senility, improve various enzyme activities and increase the chlorophyll content by more than 20%;
alginic acid is a natural polyuronic acid existing in the cell wall of brown algae such as kelp and kelp, amino acid is an organic compound containing basic amino and acidic carboxyl, boric acid, manganese sulfate, zinc sulfate and magnesium sulfate are trace elements, and the content of the polyuronic acid is determined by the following formula: boric acid, manganese sulfate, zinc sulfate and magnesium sulfate are added, so that the growth of cotton is facilitated, the yield of cotton is higher, the quality is better, an enzyme preparation is a surfactant which has two opposite properties of lipophilicity and hydrophilicity in a molecule, a dispersing agent is ethylene glycol, an efficient active agent is convenient for giving full play to the effect, and a composite microbial agent is prepared by mixing trichoderma harzianum powder, bacillus subtilis powder and phanerochaete chrysosporium powder according to a weight ratio, the consumption of an accelerant is reduced or a vulcanization time is shortened by enzyme-linked use of bacteria, and through the addition of the enzyme preparation and the dispersing agent, the enzyme preparation has the characteristics of high catalytic efficiency, high specificity, mild action conditions, energy consumption reduction, chemical pollution reduction and the like, and the dispersing agent can uniformly disperse inorganic substances which are difficult to dissolve in liquid, solid and liquid particles of organic pigments, and can also prevent the sedimentation and agglomeration of the particles, so that an amphiphilic agent required by a stable suspension is formed, and the phenomenon of insolubility in water is avoided;
the components in parts by weight are respectively as follows:
20 parts of fulvic acid, 10 parts of alginic acid, 5 parts of amino acid, 3 parts of boric acid, 0.4 part of manganese sulfate, 3 parts of zinc sulfate, 12 parts of magnesium sulfate, 5 parts of an enzyme preparation, 120 parts of urea, 6 parts of a dispersing agent, 5 parts of a high-efficiency active agent and 5 parts of a compound microbial agent;
numerical values through all kinds of raw materials are counted according to parts by weight, the ratio of the water-soluble fertilizer is more accurate, so that the effect of the water-soluble fertilizer is optimal, the growth of cotton is promoted, precipitates are reduced, the foliage water-soluble fertilizer is suitable for being sprayed by an unmanned aerial vehicle, and the working efficiency is improved.
With reference to fig. 1, a preparation method of a Xinjiang cotton fulvic acid microelement foliage water-soluble fertilizer comprises the following steps:
s1, preparing raw materials: the required raw materials are collected, so that each raw material is independently stored, the purity of each raw material is ensured, and the raw materials are not polluted by other impurities;
s2, weighing the dosage: weighing the components according to the proportion of the formula, and taking a weighing tool in a dry and pollution-free state;
s3, mixing treatment: respectively and uniformly mixing alginic acid, urea, amino acid and an enzyme preparation, then crushing the mixture, sieving the mixture by using a fine sieve, adding water, heating the mixture to 70-80 ℃, and simultaneously stirring the mixture at a constant speed for 5-10 minutes;
s4, adding trace elements: adding trace elements to the obtained mixture: adding trace elements into manganese sulfate, zinc sulfate and magnesium sulfate, and stirring at a constant speed to uniformly stir;
s5, constant-temperature fermentation: and (3) placing the mixture in an environment with the temperature of 40-50 ℃, fermenting for 3-4 days in a constant temperature environment, respectively adding fulvic acid, boric acid and a dispersing agent after fermentation is completed, uniformly stirring, and drying to obtain the fulvic acid trace element foliage water-soluble fertilizer.
S6, drying treatment: and heating the obtained fulvic acid trace element foliage water-soluble fertilizer to 40 ℃, continuously stirring to dry the foliage water-soluble fertilizer, and drying to obtain the powdered foliage water-soluble fertilizer.
All component raw materials are all deposited alone, and deposit the environment and avoid impurity interfusion, the purity of raw materials for the fertilizer effect that arrives is best.
Stirring in the same direction at a constant speed in the stirring process to ensure that the mixture obtains a sufficient and uniform mixing effect.
Through the increase of the content of fulvic acid, the amounts of trace elements of boric acid, manganese sulfate, zinc sulfate and magnesium sulfate are all increased, 1 part of dispersing agent is added, and the mixing and stirring time of the foliar water-soluble fertilizer is 10-15 minutes, so that the sedimentation and agglomeration of particles are prevented.
To thereby carry out a series of tasks, the contents of which are not described in detail in the present specification are prior art well known to those skilled in the art.
Although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that modifications may be made to the embodiments described in the foregoing embodiments, or equivalents may be substituted for elements thereof.

Claims (9)

1. A Xinjiang cotton fulvic acid microelement foliage water-soluble fertilizer is characterized in that:
the Xinjiang cotton fulvic acid microelement foliage water-soluble fertilizer comprises the following raw materials: fulvic acid, alginic acid, amino acid, boric acid, manganese sulfate, zinc sulfate, magnesium sulfate, an enzyme preparation, urea, a dispersing agent, a high-efficiency active agent and a compound microbial agent.
2. The Xinjiang cotton fulvic acid microelement foliage water-soluble fertilizer as claimed in claim 1, which is characterized in that: the raw material components by weight portion are as follows: 10-20 parts of fulvic acid, 5-10 parts of alginic acid, 3-6 parts of amino acid, 1-3 parts of boric acid, 0.2-0.5 part of manganese sulfate, 1-3 parts of zinc sulfate, 6-15 parts of magnesium sulfate, 1-5 parts of an enzyme preparation, 100-150 parts of urea, 3-6 parts of a dispersing agent, 3-6 parts of a high-efficiency active agent and 1-5 parts of a compound microbial agent.
3. The Xinjiang cotton fulvic acid microelement foliage water-soluble fertilizer according to claim 1, which is characterized in that: the fulvic acid solid is brown and grey black, and the fulvic acid is readily soluble in water, ethanol, dilute acid, dilute alkali and aqueous acetone.
4. The Xinjiang cotton fulvic acid microelement foliage water-soluble fertilizer according to claim 1, which is characterized in that: the alginic acid is a natural polyuronic acid existing in the cell wall of brown algae such as kelp and kelp;
the amino acid is an organic compound containing a basic amino group and an acidic carboxyl group;
the boric acid, manganese sulfate, zinc sulfate and magnesium sulfate are trace elements.
5. The Xinjiang cotton fulvic acid microelement foliage water-soluble fertilizer as claimed in claim 1, which is characterized in that: the enzyme preparation is a surfactant which has two opposite properties of lipophilicity and hydrophilcity in a molecule;
the dispersing agent is ethylene glycol, the efficient active agent is convenient for full performance, the composite microbial agent is prepared by mixing trichoderma harzianum powder, bacillus subtilis powder and phanerochaete chrysosporium powder according to a weight ratio, and the use amount of the accelerator is reduced or the vulcanization time is shortened by continuous use of bacterial enzymes.
6. The Xinjiang cotton fulvic acid microelement foliage water-soluble fertilizer as claimed in claim 1, which is characterized in that: the components in parts by weight are respectively 15 parts of fulvic acid, 6 parts of alginic acid, 4 parts of amino acid, 2 parts of boric acid, 0.3 part of manganese sulfate, 2 parts of zinc sulfate, 6 parts of magnesium sulfate, 3 parts of an enzyme preparation, 120 parts of urea, 4 parts of a dispersing agent, 3 parts of a high-efficiency active agent and 3 parts of a compound microbial agent.
7. The preparation method of the Xinjiang cotton fulvic acid microelement foliage water-soluble fertilizer according to claim 1, which is characterized by comprising the following steps of: the method comprises the following steps:
s1, preparing raw materials: the required raw materials are collected, so that each raw material is independently stored, the purity of each raw material is ensured, and the raw materials are not polluted by other impurities;
s2, weighing the dosage: weighing the using amount of each component according to the formula proportion, wherein a weighing tool is in a dry and pollution-free state;
s3, mixing treatment: respectively and uniformly mixing alginic acid, urea, amino acid and an enzyme preparation, then crushing the mixture, sieving the mixture by using a fine sieve, adding water, heating the mixture to 60-80 ℃, and simultaneously stirring the mixture at a constant speed for 10-15 minutes;
s4, adding trace elements: adding trace elements to the resulting mixture: adding trace elements into manganese sulfate, zinc sulfate and magnesium sulfate, and stirring at a constant speed to uniformly stir;
s5, constant-temperature fermentation: placing the mixture in an environment with the temperature of 40-50 ℃, fermenting for 3-4 days in a constant temperature environment, respectively adding fulvic acid, boric acid and a dispersing agent after fermentation is completed, uniformly stirring, and drying to obtain the fulvic acid trace element foliage water-soluble fertilizer;
s6, drying: and heating the obtained fulvic acid trace element foliage water-soluble fertilizer to 40 ℃, continuously stirring to dry the foliage water-soluble fertilizer, and drying to obtain the powdered foliage water-soluble fertilizer.
8. The preparation method of the Xinjiang cotton fulvic acid microelement foliage water-soluble fertilizer according to claim 7, which is characterized by comprising the following steps of: all deposit alone of each component raw materials, and deposit the environment and avoid impurity sneaking into, the net of raw materials for the fertilizer effect that arrives is best.
9. The preparation method of the Xinjiang cotton fulvic acid microelement foliage water-soluble fertilizer according to claim 7, which is characterized by comprising the following steps of: and stirring at a constant speed in the same direction in the stirring process to ensure that the mixture obtains a full and uniform mixing effect.
CN202211074057.7A 2022-09-02 2022-09-02 Xinjiang cotton fulvic acid microelement foliage water-soluble fertilizer and preparation method thereof Pending CN115417719A (en)

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Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101165011A (en) * 2006-10-16 2008-04-23 陕西汉唐环保农业有限公司 Organic potassium fertilizer prepared from composite organic acid and producing method thereof
CN108610183A (en) * 2018-07-11 2018-10-02 新疆农垦科学院 Prevent the fertilizer of cotton verticillium wilt

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101165011A (en) * 2006-10-16 2008-04-23 陕西汉唐环保农业有限公司 Organic potassium fertilizer prepared from composite organic acid and producing method thereof
CN108610183A (en) * 2018-07-11 2018-10-02 新疆农垦科学院 Prevent the fertilizer of cotton verticillium wilt

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Application publication date: 20221202