CN115089501A - Air lip glaze composition and preparation method thereof - Google Patents
Air lip glaze composition and preparation method thereof Download PDFInfo
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- CN115089501A CN115089501A CN202210919276.4A CN202210919276A CN115089501A CN 115089501 A CN115089501 A CN 115089501A CN 202210919276 A CN202210919276 A CN 202210919276A CN 115089501 A CN115089501 A CN 115089501A
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- polydimethylsiloxane
- lip glaze
- glaze composition
- vinyl
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- 239000000203 mixture Substances 0.000 title claims abstract description 45
- 238000002360 preparation method Methods 0.000 title abstract description 9
- -1 polydimethylsiloxane Polymers 0.000 claims abstract description 71
- 239000004205 dimethyl polysiloxane Substances 0.000 claims abstract description 66
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims abstract description 66
- 229920006037 cross link polymer Polymers 0.000 claims abstract description 37
- 235000010290 biphenyl Nutrition 0.000 claims abstract description 24
- 239000004305 biphenyl Substances 0.000 claims abstract description 24
- ZUOUZKKEUPVFJK-UHFFFAOYSA-N phenylbenzene Natural products C1=CC=CC=C1C1=CC=CC=C1 ZUOUZKKEUPVFJK-UHFFFAOYSA-N 0.000 claims abstract description 24
- 229920002554 vinyl polymer Polymers 0.000 claims abstract description 24
- HGKOWIQVWAQWDS-UHFFFAOYSA-N bis(16-methylheptadecyl) 2-hydroxybutanedioate Chemical compound CC(C)CCCCCCCCCCCCCCCOC(=O)CC(O)C(=O)OCCCCCCCCCCCCCCCC(C)C HGKOWIQVWAQWDS-UHFFFAOYSA-N 0.000 claims abstract description 23
- TZCXTZWJZNENPQ-UHFFFAOYSA-L barium sulfate Chemical compound [Ba+2].[O-]S([O-])(=O)=O TZCXTZWJZNENPQ-UHFFFAOYSA-L 0.000 claims abstract description 22
- 125000000913 palmityl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims abstract description 17
- 239000003086 colorant Substances 0.000 claims abstract description 16
- 125000006267 biphenyl group Chemical group 0.000 claims abstract description 12
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 claims abstract description 12
- 238000003756 stirring Methods 0.000 claims description 20
- 239000000463 material Substances 0.000 claims description 12
- FGUZFFWTBWJBIL-XWVZOOPGSA-N [(1r)-1-[(2s,3r,4s)-3,4-dihydroxyoxolan-2-yl]-2-hydroxyethyl] 16-methylheptadecanoate Chemical compound CC(C)CCCCCCCCCCCCCCC(=O)O[C@H](CO)[C@H]1OC[C@H](O)[C@H]1O FGUZFFWTBWJBIL-XWVZOOPGSA-N 0.000 claims description 11
- 239000003995 emulsifying agent Substances 0.000 claims description 11
- 229940057429 sorbitan isostearate Drugs 0.000 claims description 11
- XDOFQFKRPWOURC-UHFFFAOYSA-N 16-methylheptadecanoic acid Chemical compound CC(C)CCCCCCCCCCCCCCC(O)=O XDOFQFKRPWOURC-UHFFFAOYSA-N 0.000 claims description 9
- 229920001353 Dextrin Polymers 0.000 claims description 9
- 239000004375 Dextrin Substances 0.000 claims description 9
- 229920001577 copolymer Polymers 0.000 claims description 9
- 235000019425 dextrin Nutrition 0.000 claims description 9
- GQEZCXVZFLOKMC-UHFFFAOYSA-N n-alpha-hexadecene Natural products CCCCCCCCCCCCCCC=C GQEZCXVZFLOKMC-UHFFFAOYSA-N 0.000 claims description 9
- ZAKOWWREFLAJOT-CEFNRUSXSA-N D-alpha-tocopherylacetate Chemical compound CC(=O)OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C ZAKOWWREFLAJOT-CEFNRUSXSA-N 0.000 claims description 8
- 238000002156 mixing Methods 0.000 claims description 8
- 239000002253 acid Substances 0.000 claims description 7
- 238000001816 cooling Methods 0.000 claims description 6
- 229940042585 tocopherol acetate Drugs 0.000 claims description 5
- 238000000227 grinding Methods 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 4
- 238000000034 method Methods 0.000 claims description 4
- 239000000853 adhesive Substances 0.000 claims description 3
- 230000001070 adhesive effect Effects 0.000 claims description 3
- ZAKOWWREFLAJOT-UHFFFAOYSA-N d-alpha-Tocopheryl acetate Natural products CC(=O)OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C ZAKOWWREFLAJOT-UHFFFAOYSA-N 0.000 claims description 3
- 239000012467 final product Substances 0.000 claims description 3
- FOYKKGHVWRFIBD-UHFFFAOYSA-N gamma-tocopherol acetate Natural products CC(=O)OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1 FOYKKGHVWRFIBD-UHFFFAOYSA-N 0.000 claims description 3
- 238000002844 melting Methods 0.000 claims description 3
- 230000008018 melting Effects 0.000 claims description 3
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 claims 2
- 238000004519 manufacturing process Methods 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 17
- 238000011161 development Methods 0.000 abstract description 7
- 239000002537 cosmetic Substances 0.000 abstract description 3
- 235000013870 dimethyl polysiloxane Nutrition 0.000 description 39
- 239000000049 pigment Substances 0.000 description 11
- 239000006185 dispersion Substances 0.000 description 8
- 239000003921 oil Substances 0.000 description 8
- 239000000843 powder Substances 0.000 description 7
- 229940008099 dimethicone Drugs 0.000 description 6
- 239000003795 chemical substances by application Substances 0.000 description 5
- 239000000047 product Substances 0.000 description 4
- 229920002379 silicone rubber Polymers 0.000 description 4
- 239000003974 emollient agent Substances 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 238000013112 stability test Methods 0.000 description 3
- 230000037303 wrinkles Effects 0.000 description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 239000004902 Softening Agent Substances 0.000 description 2
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 238000011049 filling Methods 0.000 description 2
- 238000009472 formulation Methods 0.000 description 2
- 238000011835 investigation Methods 0.000 description 2
- 239000007934 lip balm Substances 0.000 description 2
- 230000001050 lubricating effect Effects 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 description 2
- 229920001296 polysiloxane Polymers 0.000 description 2
- 238000004321 preservation Methods 0.000 description 2
- 229920002545 silicone oil Polymers 0.000 description 2
- 230000008719 thickening Effects 0.000 description 2
- 239000002562 thickening agent Substances 0.000 description 2
- 239000001993 wax Substances 0.000 description 2
- ULQISTXYYBZJSJ-UHFFFAOYSA-N 12-hydroxyoctadecanoic acid Chemical compound CCCCCCC(O)CCCCCCCCCCC(O)=O ULQISTXYYBZJSJ-UHFFFAOYSA-N 0.000 description 1
- KIHBGTRZFAVZRV-UHFFFAOYSA-N 2-Hydroxyoctadecanoic acid Natural products CCCCCCCCCCCCCCCCC(O)C(O)=O KIHBGTRZFAVZRV-UHFFFAOYSA-N 0.000 description 1
- PBWGCNFJKNQDGV-UHFFFAOYSA-N 6-phenylimidazo[2,1-b][1,3]thiazol-5-amine Chemical compound N1=C2SC=CN2C(N)=C1C1=CC=CC=C1 PBWGCNFJKNQDGV-UHFFFAOYSA-N 0.000 description 1
- 206010016322 Feeling abnormal Diseases 0.000 description 1
- 239000004166 Lanolin Substances 0.000 description 1
- 239000004743 Polypropylene Substances 0.000 description 1
- 235000021355 Stearic acid Nutrition 0.000 description 1
- 206010051788 Sticky skin Diseases 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 238000004220 aggregation Methods 0.000 description 1
- 229940090958 behenyl behenate Drugs 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 230000003750 conditioning effect Effects 0.000 description 1
- 239000000498 cooling water Substances 0.000 description 1
- 239000002270 dispersing agent Substances 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 238000005538 encapsulation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 239000001023 inorganic pigment Substances 0.000 description 1
- VBMVTYDPPZVILR-UHFFFAOYSA-N iron(2+);oxygen(2-) Chemical group [O-2].[Fe+2] VBMVTYDPPZVILR-UHFFFAOYSA-N 0.000 description 1
- 150000002596 lactones Chemical class 0.000 description 1
- 229940039717 lanolin Drugs 0.000 description 1
- 235000019388 lanolin Nutrition 0.000 description 1
- 230000001795 light effect Effects 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 1
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 239000004482 other powder Substances 0.000 description 1
- 239000005022 packaging material Substances 0.000 description 1
- 239000003961 penetration enhancing agent Substances 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 229920001155 polypropylene Polymers 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 230000002335 preservative effect Effects 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000009877 rendering Methods 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 229920005573 silicon-containing polymer Polymers 0.000 description 1
- 239000004945 silicone rubber Substances 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 239000008117 stearic acid Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 239000004408 titanium dioxide Substances 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 238000004078 waterproofing Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
- A61K8/894—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone modified by a polyoxyalkylene group, e.g. cetyl dimethicone copolyol
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/895—Polysiloxanes containing silicon bound to unsaturated aliphatic groups, e.g. vinyl dimethicone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/04—Preparations containing skin colorants, e.g. pigments for lips
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/001—Preparations for care of the lips
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/42—Colour properties
- A61K2800/43—Pigments; Dyes
Abstract
The invention provides an air lip glaze composition and a preparation method thereof, and relates to the field of cosmetics, wherein the air lip glaze composition comprises the following components: tribehenate, cetyl PEG/PPG-10/1 polydimethylsiloxane, bis-diglycerol polyacyladipate-2, diisostearyl malate, polydimethylsiloxane, vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane crosspolymer, diphenyl polydimethylsiloxane/vinyl diphenyl polydimethylsiloxane/silsesquioxane crosspolymer, barium sulfate, HDI/trimethylolhexyllactone crosspolymer, colorant, diisostearyl malate. The finally prepared composition has strong stability and excellent use feeling and color development effect.
Description
Technical Field
The invention relates to the field of cosmetics, and particularly relates to an air lip glaze composition and a preparation method thereof.
Background
The velvet lip glaze skin feeling is mainly provided by a large amount of silicon elastomers in a formula, and because the silicon elastomers are not easy to disperse and have poor compatibility with pigments, most velvet lip glazes on the market have two defects: the dispersibility is poor, pigment marks and granular feelings are easy to appear after the filling is carried out in a container, small air holes are easy to appear after the filling, and oil content which is easy to gather and separate at the small air holes is easy to accumulate; ② the skin feels thick, sticky and greasy. For example, patent CN113143786A discloses a velvet lip glaze with matte texture and a preparation method thereof, which is prepared from the following components: a velvet texture composition, silicone rubber, a first film former, a second film former, a first emollient, a second emollient, a third emollient, a filler, a thickener, and a colorant; the velvet texture composition consists of silica, polypropylene silsesquioxane and polydimethylsiloxane cross-linked polymer, the lip glaze has good uniform color saturation and high-grade matte sense, is good in moisture, does not have the phenomenon of skin pull-off after long-time use, is good in durability, has a light cup sticking effect, and is added with relevant raw materials such as silicone elastic gel and the like in the formula.
Patent CN114425025A discloses a frosted matte lip glaze and a preparation method thereof, and the raw materials comprise phase A, phase B, phase C, phase D and phase E; the phase A comprises 0-14 parts of a softening agent, 3-7 parts of an emulsifier, 0.5-4 parts of an adhesive, 0.05-0.25 part of a preservative and 1-5 parts of a rheological agent; the phase B comprises 30-70 parts of a silicone polymer; the phase C comprises 7-10 parts of color paste; the phase D comprises 5-15 parts of powder; the phase E comprises 5-30 parts of rheological agent and 0.2-10 parts of softening agent. The lip glaze has special cream-to-powder texture, can be used for powder transfer after makeup is applied, is dry and does not shift, and well solves the problem of uneven material body application; meanwhile, the lip balm has matte and moistening effects, and can moisten lips after the lip balm is covered by the matte surface, so that multiple requirements of consumers are met.
Compared with the prior art, the air lip glaze has the advantages of excellent moisture-preserving effect, good glossiness and strong durability, but the air lip glaze of the same type in the prior art has the following defects: uneven dispersion of pigment, smooth and sticky smearing, poor make-up effect and lip wrinkle appearance.
Aiming at the problems of poor dispersibility and thick and sticky skin feel of velvet lip glaze in the prior art, it is necessary to find an air lip glaze which is easy to disperse uniformly, has stable pigment dispersion, is not sticky and greasy in make-up air feel and has good color development effect.
Disclosure of Invention
Aiming at the problems in the prior art, the invention provides the air lip glaze composition and the preparation method thereof, and the air lip glaze composition is easy to disperse uniformly, has stable pigment dispersion, is not sticky in make-up air feel and has good color development effect.
In order to realize the purpose, the technical scheme adopted by the invention is as follows:
the invention provides an air lip glaze composition, which comprises the following components: tribehenate, cetyl PEG/PPG-10/1 dimethicone, bis-diglycerol polyacyladipate-2, diisostearyl malate, dimethicone, vinyl dimethicone/methicone silsesquioxane crosspolymer, diphenyl dimethicone/vinyl diphenyl dimethicone/silsesquioxane crosspolymer, barium sulfate, HDI/trimethylolhexyl lactone crosspolymer, colorant, diisostearyl malate.
Further, the air lip glaze composition comprises the following components in parts by weight: 1.5-3 parts of tribehenate, 1-2 parts of cetyl PEG/PPG-10/1 polydimethylsiloxane, 3-6 parts of bis-diglycerol polyacyladipate-2, 3-6 parts of diisostearyl malate, 53-70 parts of polydimethylsiloxane, 3-9 parts of vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane cross-linked polymer, 2-8 parts of diphenyl polydimethylsiloxane/vinyl diphenyl polydimethylsiloxane/silsesquioxane cross-linked polymer, 1.5-2 parts of barium sulfate, 1.5-3 parts of HDI/trihydroxymethyl hexyl lactone cross-linked polymer, 5 parts of colorant and 5 parts of diisostearyl malate.
Wherein, the Sanshan Wayasu essence is a neutral nonionic wax, and has good compatibility; higher molecular weight, effective waterproofing agent; very mild, pleasing after-use skin feel is suitable for use as an oil phase thickener and emulsion stabilizer.
The vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane cross-linked polymer is soft to touch, can absorb organic silicone oil, and has thickening property and soft light effect.
The diphenyl polydimethylsiloxane/vinyl diphenyl polydimethylsiloxane/silsesquioxane cross-linked polymer does not absorb organic silicone oil, has a matte effect, and brings a soft feeling to the skin.
The VP/hexadecene copolymer is obtained by addition of long-chain carbon olefin and VP, the VP group has high safety, and the long-chain carbon olefin has good compatibility with oil and wax, and can promote toner dispersion and provide compact moldability. Dextrin isostearate, resin with excellent adhesive force, and can form film rapidly.
The bis-diglycerol polyacyladipate-2 is excellent in water retention performance twice as high as that of lanolin and has excellent ability to prevent water evaporation.
The diisostearyl malate has excellent pigment dispersibility and plasticity, can enhance the glossiness of the product surface (lipstick and lip gloss brightener), has good skin moistening effect, and gives silk-like touch feeling.
The polydimethylsiloxane has the functions of lubricating the skin and resisting ultraviolet rays, and has good air permeability and dustproof function.
Cetyl PEG/PPG-10/1 polydimethylsiloxane is an emulsifier and penetration enhancer, as a silicone, which has lubricating and water-locking properties, makes the skin silky and silky, and, due to its good encapsulation, allows a prolonged release of active molecules, in particular pigments.
The polyhydroxy stearic acid is a high-performance dispersant for inorganic pigments, titanium dioxide and other powder in color cosmetics, and the viscosity of a dispersion system can be obviously reduced by using a small dosage, so that the addition concentration of the powder can be increased, and the stability of the dispersion system can be improved.
The HDI/trimethylolhexyllactone crosspolymer was a spherical powder having an average particle diameter: 10-15 μm, high flexibility, excellent use feeling, advanced and excellent optical characteristics, excellent effect of covering small wrinkles and hair holes, uniform coating on the surface of skin, unnoticeable small wrinkles and hair holes, high transparency and natural appearance, and soft touch.
Further, the air lip glaze composition further comprises one or more of an emulsifier, a film forming agent and a skin conditioning agent.
Further, the emulsifier comprises sorbitan isostearate and/or polyhydroxystearic acid, the film former comprises VP/hexadecene copolymer and/or dextrin isostearate, and the skin conditioner comprises tocopherol acetate.
Preferably, the air lip glaze composition further comprises, in parts by weight: 0.5-2 parts of sorbitan isostearate, 0.5-2 parts of VP/hexadecene copolymer, 0.5-1 part of tocopherol acetate, 0.5-2 parts of dextrin isostearate and 0.1-0.3 part of polyhydroxystearic acid.
In some embodiments, the air lip glaze composition comprises, in parts by weight: 3 parts of tribehenate, 1 part of sorbitan isostearate, 1 part of VP/hexadecene copolymer, 1 part of cetyl PEG/PPG-10/1 polydimethylsiloxane, 6 parts of bis-diglycerol polyacyladipate-2, 3 parts of diisostearyl malate, 0.5 part of tocopheryl acetate, 1 part of dextrin isostearate, 55.4 parts of polydimethylsiloxane, 8 parts of vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane crosspolymer, 5 parts of diphenyl polydimethylsiloxane/vinyl diphenyl polydimethylsiloxane/silsesquioxane crosspolymer, 2 parts of barium sulfate, 3 parts of HDI/HDImethyl hexyl lactone crosspolymer, 5 parts of colorant, 5 parts of diisostearyl malate, and 0.1 part of polyhydroxystearic acid.
Further, the colorant includes an iron oxide group and/or an organic toner.
Preferably, the colorant comprises one or more of CI15850, CI77492, CI19140 and CI 77491.
Further, the weight ratio of the emulsifier to the cetyl PEG/PPG-10/1 polydimethylsiloxane is 0.5-2: 1-2.
Further, the weight ratio of the sorbitan isostearate to the cetyl PEG/PPG-10/1 polydimethylsiloxane is 0.5-2: 1-2.
Further, the invention also provides a preparation method of the air lip glaze composition, which comprises the following steps:
(1) heating and stirring tribehenate, cetyl PEG/PPG-10/1 polydimethylsiloxane, di-diglycerol polyacyladipate-2, diisostearyl malate and polydimethylsiloxane, and melting to be uniform to obtain a mixture A;
(2) adding vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane cross-linked polymer, diphenyl polydimethylsiloxane/vinyl diphenyl polydimethylsiloxane/silsesquioxane cross-linked polymer, barium sulfate and HDI/trihydroxymethyl hexyl lactone cross-linked polymer into the mixture A in sequence, stirring uniformly, and preserving heat to obtain a mixture B;
(3) mixing a colorant and diisostearyl malate into color paste, and grinding the color paste until the color paste is uniform;
(4) stirring and mixing the uniform color paste obtained in the step (3) with the mixture B, preserving heat, and stirring until the material body is uniform;
(5) defoaming;
(6) cooling, stirring and cooling to obtain the final product.
In some embodiments, the method for preparing the air lip glaze composition comprises the following steps:
(1) heating and stirring tribehenate, sorbitan isostearate, VP/hexadecene copolymer, cetyl PEG/PPG-10/1 polydimethylsiloxane, di-diglycerol polyacyladipate-2, diisostearyl malate, tocopheryl acetate, dextrin isostearate and polydimethylsiloxane, and melting to be uniform to obtain a mixture A;
(2) adding vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane cross-linked polymer, diphenyl polydimethylsiloxane/vinyl diphenyl polydimethylsiloxane/silsesquioxane cross-linked polymer, barium sulfate and HDI/trihydroxymethyl hexyl lactone cross-linked polymer into the mixture A in sequence, stirring uniformly, and preserving heat to obtain a mixture B;
(3) mixing a colorant, diisostearyl malate and polyhydroxystearic acid to form color paste, and grinding the color paste until the color paste is uniform;
(4) stirring and mixing the uniform color paste obtained in the step (3) with the mixture B, preserving heat, and stirring until the material body is uniform;
(5) defoaming;
(6) cooling, stirring and cooling to obtain the final product.
Further, the heating temperature in the step (1) is 90 ℃; the temperature of the heat preservation in the step (2) is 70-75 ℃, the temperature of the heat preservation in the step (4) is 60-65 ℃, and the stirring time is 20 min; the temperature of the temperature reduction in the step (6) is 38-40 ℃.
The technical effects obtained by the invention are as follows:
1. silicon elastomer is not used, the dispersibility of the material body is good, and the material body can not agglomerate after being placed for a long time;
2. the colorant is ground and dispersed for 3 times, the compatibility of the pigment and the material body is good, and pigment aggregation can not occur;
3. the hollow powder with the soft-burnt effect is used for thickening, so that the lip glaze is soft, foggy and not sticky, and the effect of air feeling is achieved.
Detailed Description
The embodiments of the present invention are described below with reference to specific embodiments, and other advantages and effects of the present invention will be easily understood by those skilled in the art from the disclosure of the present specification. The invention is capable of other and different embodiments and of being practiced or of being carried out in various ways, and its several details are capable of modification in various respects, all without departing from the spirit and scope of the present invention.
Before the present embodiments are further described, it is to be understood that the scope of the invention is not to be limited to the specific embodiments described below; it is also to be understood that the terminology used in the examples is for the purpose of describing particular embodiments only, and is not intended to limit the scope of the present invention.
When numerical ranges are given in the examples, it is understood that both endpoints of each of the numerical ranges and any value therebetween can be selected unless the invention otherwise indicated. Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs.
It should be noted that the raw materials used in the present invention are all common commercial products, and thus the sources thereof are not particularly limited.
The stability test method of each group of products comprises the following steps: the thermostats set the temperatures respectively: at 45 degrees, 25 degrees, 0 degrees and-5 degrees, 5 samples filled in the lip glaze packaging material are respectively filled, 1 bottle of a material body is respectively filled in a 150ml bottle jar, the bottle is placed in a constant temperature box and kept for 1 month, then the material body is taken out, the state of the material body is observed after the material body is recovered to the room temperature, and the quality is evaluated according to the quality, the medium quality and the difference.
The formulations of examples 1-8 and the results of the stability tests are detailed in table 1 (the amounts in the table are parts by weight).
TABLE 1
The preparation method of the product in each embodiment comprises the following steps:
(1) behenyl behenate (sorbitan isostearate and/or VP/hexadecene copolymer are also added in examples 2-8), cetyl PEG/PPG-10/1 polydimethylsiloxane, di-diglycerol polyacyladipate-2, diisostearyl malate (tocopherol acetate and/or dextrin isostearate are also added in examples 3-8), and polydimethylsiloxane are stirred and heated to 90 ℃ to be melted to be uniform, so as to obtain a mixture A;
(2) sequentially adding vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane cross-linked polymer, diphenyl polydimethylsiloxane/vinyl diphenyl polydimethylsiloxane/silsesquioxane cross-linked polymer, barium sulfate and HDI/trihydroxymethyl hexyl lactone cross-linked polymer into the mixture A one by one, uniformly stirring, and controlling the temperature to be 70-75 ℃ to obtain a mixture B;
(3) mixing CI15850, CI77492, CI19140, CI77491, diisostearyl malate, (poly hydroxystearic acid is also added in the embodiment 3-8) to obtain color paste, and grinding for 3 times by a three-roll mill until the color paste is uniform;
(4) stirring and mixing the uniform color paste obtained in the step (3) with the mixture B, controlling the temperature to be 60-65 ℃, and stirring for 20min until the material body is uniform;
(5) defoaming;
(6) cooling water is started, and stirring is continued to cool to 38-40 ℃.
The formulations of examples 9-16 and the results of the stability tests are detailed in Table 2.
TABLE 2
Case 9 sorbitan isostearate and cetyl PEG/PPG-10/1 dimethicone colorant without the emulsifier significantly aggregated, resulting in a very non-uniform body.
In cases 10, 11, 12 and 13, the pigment dispersion was improved with the addition of either emulsifier alone, but the optimum effect was not achieved.
Cases 14, 15, 16, total emulsifier addition was 2, in ratio 1: the optimal effect is achieved when 1 hour; the addition ratio is 1:2 or 2:1, and the pigment dispersion effect is not good when the total amount is more than 2.
Examples 4, 5, 6, 7, and 8 were relatively good in stability, and each example was subjected to investigation of smoothness during use, air feeling, and color development, uniformity, graininess, and oil feeling after use.
The investigation and test method comprises the following steps: a panel of 20 female experts was used to apply the samples to the lips, and protocols 4, 5, 6, 7, 8 were scored according to the indices in table 3 for a total score of 5, and the data results were combined to give table 4.
TABLE 3
| Index (I) | Definition of |
| Degree of smoothness | The easier it is to brush the make-up with the lip glaze, the higher the score, and vice versa. |
| Air sense | The degree of stickiness and impermeability of the lip glaze when the makeup is brushed with the lip glaze is higher, the higher the score is, and vice versa. |
| Color rendering | The degree of color development was observed under standard lighting, with higher color development and higher score, and vice versa. |
| Uniformity of the film | The degree of uniformity of coverage, with or without irregularities, or lines, the higher the degree, the higher the score, and vice versa. |
| Particle size | The degree of particles was observed under standard lighting, with more powder, higher score and vice versa. |
| Feeling of oil | The degree of oil feel was observed under standard lighting, with higher oil feel and higher scores, and vice versa. |
TABLE 4
Example 4 showed relatively good results in all dimensions of stability, smoothness during use, air feel, and color development, uniformity, graininess, and oil feel after use. Comparative experiments were also performed on the plain velvet lip glaze of example 4 and example 17.
TABLE 5 common velvet lip glaze (example 17)
Comparison of example 4 and example 17 at various temperatures, such as stability:
TABLE 6
Example 4 and example 17
Comparison in the use sense dimensions:
TABLE 7
Finally, it should be noted that the above-mentioned contents are only used for illustrating the technical solutions of the present invention, and not for limiting the protection scope of the present invention, and that the simple modifications or equivalent substitutions of the technical solutions of the present invention by those of ordinary skill in the art can be made without departing from the spirit and scope of the technical solutions of the present invention.
Claims (10)
1. An air lip glaze composition, characterized in that: the method comprises the following steps: tribehenate, cetyl PEG/PPG-10/1 polydimethylsiloxane, bis-diglycerol polyacyladipate-2, diisostearyl malate, polydimethylsiloxane, vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane crosspolymer, diphenyl polydimethylsiloxane/vinyl diphenyl polydimethylsiloxane/silsesquioxane crosspolymer, barium sulfate, HDI/trimethylolhexyllactone crosspolymer, colorant, diisostearyl malate.
2. The air lip glaze composition of claim 1, wherein: comprises the following components in parts by weight: 1.5-3 parts of tribehenate, 1-2 parts of cetyl PEG/PPG-10/1 polydimethylsiloxane, 3-6 parts of bis-diglycerol polyacyladipate-2, 3-6 parts of diisostearyl malate, 53-70 parts of polydimethylsiloxane, 3-9 parts of vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane cross-linked polymer, 2-8 parts of diphenyl polydimethylsiloxane/vinyl diphenyl polydimethylsiloxane/silsesquioxane cross-linked polymer, 1.5-2 parts of barium sulfate, 1.5-3 parts of HDI/trihydroxymethyl hexyl lactone cross-linked polymer, 5 parts of colorant and 5 parts of diisostearyl malate.
3. The air lip glaze composition of claim 1, wherein: further comprises one or more of an emulsifier, a film former and a skin conditioner.
4. The air lip glaze composition of claim 3, wherein: the emulsifier comprises sorbitan isostearate and/or polyhydroxystearic acid, the film former comprises VP/hexadecene copolymer and/or dextrin isostearate, and the skin conditioner comprises tocopherol acetate.
5. The air lip glaze composition of claim 4, wherein: the adhesive also comprises the following components in parts by weight: 0.5-2 parts of sorbitan isostearate, 0.5-2 parts of VP/hexadecene copolymer, 0.5-1 part of tocopherol acetate, 0.5-2 parts of dextrin isostearate and 0.1-0.3 part of polyhydroxystearic acid.
6. The air lip glaze composition of claim 5, wherein: comprises the following components in parts by weight: 3 parts of tribehenate, 1 part of sorbitan isostearate, 1 part of VP/hexadecene copolymer, 1 part of cetyl PEG/PPG-10/1 polydimethylsiloxane, 6 parts of bis-diglycerol polyacyladipate-2, 3 parts of diisostearyl malate, 0.5 part of tocopheryl acetate, 1 part of dextrin isostearate, 55.4 parts of polydimethylsiloxane, 8 parts of vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane crosspolymer, 5 parts of diphenyl polydimethylsiloxane/vinyl diphenyl polydimethylsiloxane/silsesquioxane crosspolymer, 2 parts of barium sulfate, 3 parts of HDI/HDImethyl hexyl lactone crosspolymer, 5 parts of colorant, 5 parts of diisostearyl malate, and 0.1 part of polyhydroxystearic acid.
7. The air lip glaze composition of claim 1, wherein: the colorant includes iron oxide and/or organic toner.
8. The air lip glaze composition of claim 4, wherein: the weight ratio of the emulsifier to the cetyl PEG/PPG-10/1 polydimethylsiloxane is 0.5-2: 1-2.
9. The air lip glaze composition of claim 8, wherein: the weight ratio of the sorbitan isostearate to the cetyl PEG/PPG-10/1 polydimethylsiloxane is 0.5-2: 1-2.
10. A process for preparing an air lip glaze composition according to any one of claims 1 to 3 wherein: the method comprises the following steps:
(1) heating and stirring tribehenate, cetyl PEG/PPG-10/1 polydimethylsiloxane, di-diglycerol polyacyladipate-2, diisostearyl malate and polydimethylsiloxane, and melting to be uniform to obtain a mixture A;
(2) adding vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane cross-linked polymer, diphenyl polydimethylsiloxane/vinyl diphenyl polydimethylsiloxane/silsesquioxane cross-linked polymer, barium sulfate and HDI/trihydroxymethyl hexyl lactone cross-linked polymer into the mixture A in sequence, stirring uniformly, and preserving heat to obtain a mixture B;
(3) mixing a colorant and diisostearyl malate into color paste, and grinding until the color paste is uniform;
(4) stirring and mixing the uniform color paste obtained in the step (3) with the mixture B, preserving heat, and stirring until the material body is uniform;
(5) defoaming;
(6) cooling, stirring and cooling to obtain the final product.
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| CN111991248A (en) * | 2020-09-23 | 2020-11-27 | 上海市天乐日化厂 | Lip glaze and preparation method thereof |
| CN112870112A (en) * | 2019-11-29 | 2021-06-01 | 株式会社爱茉莉太平洋 | Lip cosmetic composition |
| CN113081885A (en) * | 2021-05-06 | 2021-07-09 | 美尚(广州)化妆品股份有限公司 | Non-makeup lip cosmetic and preparation method thereof |
| CN113143186A (en) * | 2021-04-27 | 2021-07-23 | 亳州市人民医院 | Special diplopore bite-block of intubate |
| CN113181083A (en) * | 2021-04-02 | 2021-07-30 | 科丝美诗(中国)化妆品有限公司 | Matte mud lip, cheek and eye three-purpose composition and preparation method thereof |
| CN114452239A (en) * | 2022-01-21 | 2022-05-10 | 广州卡洛莱化妆品有限公司 | Fog-feeling lip balm with soft mousse texture |
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| CN112870112A (en) * | 2019-11-29 | 2021-06-01 | 株式会社爱茉莉太平洋 | Lip cosmetic composition |
| CN111991248A (en) * | 2020-09-23 | 2020-11-27 | 上海市天乐日化厂 | Lip glaze and preparation method thereof |
| CN113181083A (en) * | 2021-04-02 | 2021-07-30 | 科丝美诗(中国)化妆品有限公司 | Matte mud lip, cheek and eye three-purpose composition and preparation method thereof |
| CN113143186A (en) * | 2021-04-27 | 2021-07-23 | 亳州市人民医院 | Special diplopore bite-block of intubate |
| CN113081885A (en) * | 2021-05-06 | 2021-07-09 | 美尚(广州)化妆品股份有限公司 | Non-makeup lip cosmetic and preparation method thereof |
| CN114452239A (en) * | 2022-01-21 | 2022-05-10 | 广州卡洛莱化妆品有限公司 | Fog-feeling lip balm with soft mousse texture |
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