CN115089501B - Air lip glaze composition and preparation method thereof - Google Patents
Air lip glaze composition and preparation method thereof Download PDFInfo
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- CN115089501B CN115089501B CN202210919276.4A CN202210919276A CN115089501B CN 115089501 B CN115089501 B CN 115089501B CN 202210919276 A CN202210919276 A CN 202210919276A CN 115089501 B CN115089501 B CN 115089501B
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- 239000000203 mixture Substances 0.000 title claims abstract description 36
- 238000002360 preparation method Methods 0.000 title abstract description 9
- -1 polydimethylsiloxane Polymers 0.000 claims abstract description 58
- 239000004205 dimethyl polysiloxane Substances 0.000 claims abstract description 52
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims abstract description 52
- 229920006037 cross link polymer Polymers 0.000 claims abstract description 30
- 229920002554 vinyl polymer Polymers 0.000 claims abstract description 19
- TZCXTZWJZNENPQ-UHFFFAOYSA-L barium sulfate Chemical compound [Ba+2].[O-]S([O-])(=O)=O TZCXTZWJZNENPQ-UHFFFAOYSA-L 0.000 claims abstract description 18
- HGKOWIQVWAQWDS-UHFFFAOYSA-N bis(16-methylheptadecyl) 2-hydroxybutanedioate Chemical compound CC(C)CCCCCCCCCCCCCCCOC(=O)CC(O)C(=O)OCCCCCCCCCCCCCCCC(C)C HGKOWIQVWAQWDS-UHFFFAOYSA-N 0.000 claims abstract description 17
- 235000010290 biphenyl Nutrition 0.000 claims abstract description 16
- 239000004305 biphenyl Substances 0.000 claims abstract description 16
- ZUOUZKKEUPVFJK-UHFFFAOYSA-N phenylbenzene Natural products C1=CC=CC=C1C1=CC=CC=C1 ZUOUZKKEUPVFJK-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000003086 colorant Substances 0.000 claims abstract description 13
- 125000000913 palmityl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims abstract description 13
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 claims abstract description 10
- FGUZFFWTBWJBIL-XWVZOOPGSA-N [(1r)-1-[(2s,3r,4s)-3,4-dihydroxyoxolan-2-yl]-2-hydroxyethyl] 16-methylheptadecanoate Chemical compound CC(C)CCCCCCCCCCCCCCC(=O)O[C@H](CO)[C@H]1OC[C@H](O)[C@H]1O FGUZFFWTBWJBIL-XWVZOOPGSA-N 0.000 claims description 9
- 229940057429 sorbitan isostearate Drugs 0.000 claims description 9
- XDOFQFKRPWOURC-UHFFFAOYSA-N 16-methylheptadecanoic acid Chemical compound CC(C)CCCCCCCCCCCCCCC(O)=O XDOFQFKRPWOURC-UHFFFAOYSA-N 0.000 claims description 8
- 229920001353 Dextrin Polymers 0.000 claims description 8
- 239000004375 Dextrin Substances 0.000 claims description 8
- 229920001577 copolymer Polymers 0.000 claims description 8
- 235000019425 dextrin Nutrition 0.000 claims description 8
- GQEZCXVZFLOKMC-UHFFFAOYSA-N n-alpha-hexadecene Natural products CCCCCCCCCCCCCCC=C GQEZCXVZFLOKMC-UHFFFAOYSA-N 0.000 claims description 8
- ZAKOWWREFLAJOT-CEFNRUSXSA-N D-alpha-tocopherylacetate Chemical compound CC(=O)OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C ZAKOWWREFLAJOT-CEFNRUSXSA-N 0.000 claims description 7
- 239000002253 acid Substances 0.000 claims description 7
- 125000006267 biphenyl group Chemical group 0.000 claims description 7
- ZAKOWWREFLAJOT-UHFFFAOYSA-N d-alpha-Tocopheryl acetate Natural products CC(=O)OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C ZAKOWWREFLAJOT-UHFFFAOYSA-N 0.000 claims description 7
- FOYKKGHVWRFIBD-UHFFFAOYSA-N gamma-tocopherol acetate Natural products CC(=O)OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1 FOYKKGHVWRFIBD-UHFFFAOYSA-N 0.000 claims description 7
- 239000004135 Bone phosphate Substances 0.000 claims description 4
- 229920003217 poly(methylsilsesquioxane) Polymers 0.000 claims description 2
- 230000000694 effects Effects 0.000 abstract description 15
- 238000011161 development Methods 0.000 abstract description 5
- PAPBSGBWRJIAAV-UHFFFAOYSA-N ε-Caprolactone Chemical compound O=C1CCCCCO1 PAPBSGBWRJIAAV-UHFFFAOYSA-N 0.000 abstract description 3
- 239000002537 cosmetic Substances 0.000 abstract description 2
- 235000013870 dimethyl polysiloxane Nutrition 0.000 description 37
- 238000003756 stirring Methods 0.000 description 16
- 239000000463 material Substances 0.000 description 12
- 239000000049 pigment Substances 0.000 description 12
- 239000003921 oil Substances 0.000 description 10
- 239000000843 powder Substances 0.000 description 9
- 239000003995 emulsifying agent Substances 0.000 description 8
- 239000006185 dispersion Substances 0.000 description 7
- 239000003795 chemical substances by application Substances 0.000 description 6
- 238000001816 cooling Methods 0.000 description 6
- 238000002156 mixing Methods 0.000 description 6
- 229920002379 silicone rubber Polymers 0.000 description 4
- 210000003298 dental enamel Anatomy 0.000 description 3
- 239000003974 emollient agent Substances 0.000 description 3
- 238000000227 grinding Methods 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 230000003020 moisturizing effect Effects 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 238000013112 stability test Methods 0.000 description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 206010040844 Skin exfoliation Diseases 0.000 description 2
- 239000004902 Softening Agent Substances 0.000 description 2
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 2
- 230000002776 aggregation Effects 0.000 description 2
- 238000004220 aggregation Methods 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 238000011049 filling Methods 0.000 description 2
- 238000009472 formulation Methods 0.000 description 2
- 238000011835 investigation Methods 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 230000008447 perception Effects 0.000 description 2
- 238000004321 preservation Methods 0.000 description 2
- 229920002545 silicone oil Polymers 0.000 description 2
- 230000008719 thickening Effects 0.000 description 2
- 239000002562 thickening agent Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 239000001993 wax Substances 0.000 description 2
- 206010016322 Feeling abnormal Diseases 0.000 description 1
- 239000004166 Lanolin Substances 0.000 description 1
- 239000004743 Polypropylene Substances 0.000 description 1
- 229920002334 Spandex Polymers 0.000 description 1
- 235000021355 Stearic acid Nutrition 0.000 description 1
- 206010051788 Sticky skin Diseases 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- UKMSUNONTOPOIO-UHFFFAOYSA-M behenate Chemical compound CCCCCCCCCCCCCCCCCCCCCC([O-])=O UKMSUNONTOPOIO-UHFFFAOYSA-M 0.000 description 1
- 229940116224 behenate Drugs 0.000 description 1
- 238000005282 brightening Methods 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 239000000498 cooling water Substances 0.000 description 1
- 229940008099 dimethicone Drugs 0.000 description 1
- 238000007598 dipping method Methods 0.000 description 1
- 239000002270 dispersing agent Substances 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 230000006870 function Effects 0.000 description 1
- 239000001023 inorganic pigment Substances 0.000 description 1
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N iron oxide Inorganic materials [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 1
- 229940039717 lanolin Drugs 0.000 description 1
- 235000019388 lanolin Nutrition 0.000 description 1
- 230000001795 light effect Effects 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 230000001050 lubricating effect Effects 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 1
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 description 1
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 description 1
- 239000004482 other powder Substances 0.000 description 1
- NDLPOXTZKUMGOV-UHFFFAOYSA-N oxo(oxoferriooxy)iron hydrate Chemical compound O.O=[Fe]O[Fe]=O NDLPOXTZKUMGOV-UHFFFAOYSA-N 0.000 description 1
- 239000005022 packaging material Substances 0.000 description 1
- 239000003961 penetration enhancing agent Substances 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 229920001155 polypropylene Polymers 0.000 description 1
- 229920001296 polysiloxane Polymers 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 230000002335 preservative effect Effects 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 238000009877 rendering Methods 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 229920005573 silicon-containing polymer Polymers 0.000 description 1
- 239000004945 silicone rubber Substances 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 239000008117 stearic acid Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 239000004408 titanium dioxide Substances 0.000 description 1
- 238000004078 waterproofing Methods 0.000 description 1
- 230000037303 wrinkles Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
- A61K8/894—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone modified by a polyoxyalkylene group, e.g. cetyl dimethicone copolyol
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/895—Polysiloxanes containing silicon bound to unsaturated aliphatic groups, e.g. vinyl dimethicone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/04—Preparations containing skin colorants, e.g. pigments for lips
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/001—Preparations for care of the lips
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/42—Colour properties
- A61K2800/43—Pigments; Dyes
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Emergency Medicine (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Dermatology (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Cosmetics (AREA)
Abstract
The invention provides an air lip glaze composition and a preparation method thereof, and relates to the field of cosmetics, wherein the air lip glaze composition comprises the following components: tribehenine, cetyl PEG/PPG-10/1 polydimethylsiloxane, bis-diglycerol polyacyl adipate-2, diisostearyl malate, polydimethylsiloxane, vinyl polydimethylsiloxane/polydimethylsiloxane silsesquioxane cross-linked polymer, diphenylpolydimethylsiloxane/vinyl diphenyl polydimethylsiloxane/silsesquioxane cross-linked polymer, barium sulfate, HDI/trimethylol caprolactone cross-linked polymer, colorant, diisostearyl malate. The composition prepared finally has strong stability, good use feeling and good color development effect.
Description
Technical Field
The invention relates to the field of cosmetics, in particular to an air lip glaze composition and a preparation method thereof.
Background
The velvet lip glaze skin feel is mainly provided by a large amount of silicon elastomers in the formula, and the silicon elastomers are not easy to disperse and have poor compatibility with pigments, so that most velvet lip glazes on the market have two defects: (1) the dispersibility is poor, pigment marks and granular feel are easy to appear when the oil is filled into a container, small air holes are easy to appear after the oil is filled, and separated oil is easy to gather at the small air holes; (2) the skin feel is thick, sticky and greasy. For example, patent CN113143786a discloses a velvet matte texture lip glaze and a preparation method thereof, which is prepared from the following components: velvet texture composition, silicone rubber, first film forming agent, second film forming agent, first emollient, second emollient, third emollient, filler, thickener, and colorant; the velvet texture composition consists of silica, polypropylene silsesquioxane and polydimethylsiloxane crosslinked polymer, the lip glaze has good uniform color saturation and high-grade matte feel, good moistening degree, no phenomena of dry peeling and skin peeling after long-term use, good durability and light cup dipping effect, and the formula is added with related raw materials such as silicone elastane gel and the like.
Patent CN114425025a discloses a frosted matte lip glaze and a preparation method thereof, wherein the raw materials comprise phase a, phase B, phase C, phase D and phase E; the phase A comprises 0 to 14 parts of softening agent, 3 to 7 parts of emulsifying agent, 0.5 to 4 parts of adhesive, 0.05 to 0.25 part of preservative and 1 to 5 parts of rheological agent; the phase B comprises 30-70 parts of silicone polymer; the phase C comprises 7-10 parts of color paste; the phase D comprises 5-15 parts of powder; the E phase comprises 5-30 parts of rheological agent and 0.2-10 parts of softening agent. The lip glaze has special frosted powder texture, can turn powder after being smeared with make-up, is dry and free from shifting, and well solves the problem of uneven smearing of a material body; meanwhile, the lip gloss and moisturizing effects are achieved, and the lips are moisturized after the lip marks are covered by the matte gloss, so that multiple requirements of consumers are met.
Compared with the prior art, the air lip glaze has the advantages of better moisturizing effect, better glossiness and stronger durability, but the air lip glaze of the same type in the prior art has the following defects: uneven dispersion of pigment, smooth and sticky coating, and inadequate make-up effect, and lip marks.
Aiming at the problems of poor dispersibility and thick and sticky skin feel of velvet lip glaze in the prior art, it is necessary to find an air lip glaze which is easy to disperse uniformly, stable in pigment dispersion, and not sticky in make-up air feel and good in color development effect.
Disclosure of Invention
Aiming at the problems existing in the prior art, the invention provides an air lip glaze composition and a preparation method thereof, and the air lip glaze composition is easy to disperse uniformly, stable in pigment dispersion, and good in color development effect while the air feeling of makeup is not sticky.
In order to achieve the above purpose, the technical scheme adopted by the invention is as follows:
the invention provides an air lip glaze composition, which comprises the following components: tribehenine, cetyl PEG/PPG-10/1 polydimethylsiloxane, bis-diglycerol polyacyl adipate-2, diisostearyl malate, polydimethylsiloxane, vinyl polydimethylsiloxane/polydimethylsiloxane silsesquioxane cross-linked polymer, diphenylpolydimethylsiloxane/vinyl diphenyl polydimethylsiloxane/silsesquioxane cross-linked polymer, barium sulfate, HDI/trimethylol caprolactone cross-linked polymer, colorant, diisostearyl malate.
Further, the air lip gloss composition comprises the following components in parts by weight: 1.5 to 3 parts of tribasic behenine, 1 to 2 parts of cetyl PEG/PPG-10/1 polydimethylsiloxane, 3 to 6 parts of di-diglycerol polyacyl adipate-2, 3 to 6 parts of diisostearyl malate, 53 to 70 parts of polydimethylsiloxane, 3 to 9 parts of vinyl polydimethylsiloxane/polymethylsilsesquioxane cross-linked polymer, 2 to 8 parts of diphenyl polydimethylsiloxane/vinyl diphenyl polydimethylsiloxane/silsesquioxane cross-linked polymer, 1.5 to 2 parts of barium sulfate, 1.5 to 3 parts of HDI/trimethylol hexyl lactone cross-linked polymer, 5 parts of colorant and 5 parts of diisostearyl malate.
Wherein, the three-behenine is neutral nonionic wax with good compatibility; higher molecular weight, is an effective waterproofing agent; very mild and pleasant skin feel after use is suitable for use as an oil phase thickener and emulsion stabilizer.
The vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane cross-linked polymer has light touch, can absorb organic silicone oil, and has thickening property and soft light effect.
The organosilicon composite powder does not absorb organic silicone oil, has a matte effect and brings soft feeling to skin.
The VP/hexadecene copolymer is prepared by adding long-chain carbon olefin and VP, the VP group has extremely high safety, and the long-chain carbon alkyl has very good compatibility with oil and wax, can promote the dispersion of toner and provides compact moldability. Dextrin isostearate, a resin having excellent adhesion, can be rapidly formed into a film.
The di-diglycerol polyacyl adipate-2 has excellent water retention properties twice that of lanolin and excellent ability to prevent evaporation of water.
The diisostearyl malate has excellent pigment dispersibility and plasticity, can enhance the glossiness (lipstick and lip gloss brightening agent) of the surface of the product, has good skin moisturizing effect, and gives silk-like touch feeling.
The polydimethylsiloxane has the effects of lubricating skin and resisting ultraviolet rays, and has good air permeability and dustproof function.
Cetyl PEG/PPG-10/1 polydimethylsiloxane is an emulsifier and a permeation enhancer, as an organosilicon, which can lubricate and lock water, so that skin is silky and smooth, and active molecules, particularly pigments, can be released for a prolonged period due to good inclusion.
Polyhydroxystearic acid is a high-performance dispersing agent for inorganic pigment, titanium dioxide and other powder in make-up products, and the viscosity of the dispersion system can be obviously reduced by using a small dosage, so that the adding concentration of the powder can be improved, and the stability of the dispersion system can be improved.
The HDI/trimethylol hexyl lactone cross-linked polymer is a spherical powder with average particle diameter: the vacuum spherical powder with 10-15 mu m, high flexibility and excellent use feeling has the excellent effect of covering small wrinkles and hair holes, is uniformly smeared on the surface of skin, and has high and natural transparent feeling and soft touch feeling.
Further, the air lip glaze composition also includes one or more of an emulsifier, a film former, and a skin conditioner.
Further, the emulsifier comprises sorbitan isostearate and/or polyhydroxystearic acid, the film former comprises VP/hexadecene copolymer and/or dextrin isostearate, and the skin conditioner comprises tocopheryl acetate.
Preferably, the air lip glaze composition further comprises, in parts by weight: 0.5-2 parts of sorbitan isostearate, 0.5-2 parts of VP/hexadecene copolymer, 0.5-1 part of tocopheryl acetate, 0.5-2 parts of dextrin isostearate and 0.1-0.3 part of polyhydroxystearic acid.
In some specific embodiments, the air lip glaze composition comprises, in parts by weight: 3 parts of tribasic behenate, 1 part of sorbitan isostearate, 1 part of VP/hexadecene copolymer, 1 part of cetyl PEG/PPG-10/1 polydimethylsiloxane, 6 parts of di-diglycerol polyacyl adipate-2, 3 parts of diisostearyl malate, 0.5 part of tocopheryl acetate, 1 part of dextrin isostearate, 55.4 parts of polydimethylsiloxane, 8 parts of vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane cross-linked polymer, 5 parts of diphenyl polydimethylsiloxane/vinyl diphenyl polydimethylsiloxane/silsesquioxane cross-linked polymer, 2 parts of barium sulfate, 3 parts of HDI/trimethylol caprolactone cross-linked polymer, 5 parts of colorant, 5 parts of diisostearyl malate and 0.1 part of polyhydroxystearic acid.
Further, the colorant includes ferric oxide and/or organic toner.
Preferably, the colorant comprises one or more of CI15850, CI77492, CI19140, and CI 77491.
Further, the weight ratio of the emulsifying agent to the cetyl PEG/PPG-10/1 polydimethylsiloxane is 0.5-2:1-2.
Further, the weight ratio of the sorbitan isostearate to the cetyl PEG/PPG-10/1 polydimethylsiloxane is 0.5-2:1-2.
Further, the invention also provides a preparation method of the air lip glaze composition, which comprises the following steps:
(1) Heating and stirring tricresyl, cetyl PEG/PPG-10/1 polydimethylsiloxane, di-diglycerol polyacyl adipate-2, diisostearyl malate and polydimethylsiloxane, and melting until the mixture is uniform to obtain a mixture A;
(2) Sequentially adding vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane cross-linked polymer, diphenyl polydimethylsiloxane/vinyl diphenyl polydimethylsiloxane/silsesquioxane cross-linked polymer, barium sulfate and HDI/trimethylol hexyl lactone cross-linked polymer into the mixture A, uniformly stirring, and preserving heat to obtain a mixture B;
(3) Mixing a colorant and diisostearyl malate to form color paste, and grinding until the color paste is uniform;
(4) Stirring and mixing the uniform color paste obtained in the step (3) with the mixture B, preserving heat, and stirring until the material is uniform;
(5) Defoaming;
(6) Cooling, and continuously stirring and cooling to obtain the product.
In some specific embodiments, the method for preparing the air lip glaze composition comprises the following steps:
(1) Heating and stirring tricresyl essence, sorbitan isostearate, VP/hexadecene copolymer, cetyl PEG/PPG-10/1 polydimethylsiloxane, di-diglycerol polyacyl adipate-2, diisostearyl malate, tocopheryl acetate, dextrin isostearate and polydimethylsiloxane, and melting until the mixture is uniform to obtain a mixture A;
(2) Sequentially adding vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane cross-linked polymer, diphenyl polydimethylsiloxane/vinyl diphenyl polydimethylsiloxane/silsesquioxane cross-linked polymer, barium sulfate and HDI/trimethylol hexyl lactone cross-linked polymer into the mixture A, uniformly stirring, and preserving heat to obtain a mixture B;
(3) Mixing the colorant, the diisostearyl malate and the polyhydroxystearic acid into color paste, and grinding until the color paste is uniform;
(4) Stirring and mixing the uniform color paste obtained in the step (3) with the mixture B, preserving heat, and stirring until the material is uniform;
(5) Defoaming;
(6) Cooling, and continuously stirring and cooling to obtain the product.
Further, the temperature of the heating in step (1) is 90 ℃; the temperature of the heat preservation in the step (2) is 70-75 ℃, the temperature of the heat preservation in the step (4) is 60-65 ℃, and the stirring time is 20min; the temperature of the cooling in the step (6) is 38-40 ℃.
The invention has the technical effects that:
1. the silicon elastomer is not used, the dispersibility of the material body is good, and the material body can not be agglomerated after being placed for a long time;
2. the colorant is ground and dispersed for 3 times, so that the pigment has good compatibility with the material body, and pigment aggregation can not occur;
3. the hollow powder with soft focus effect is used for thickening, so that the lip glaze is soft and fog but not sticky and greasy, and the air feeling effect is achieved.
Detailed Description
Other advantages and effects of the present invention will become apparent to those skilled in the art from the following disclosure, which describes the embodiments of the present invention with reference to specific examples. The invention may be practiced or carried out in other embodiments that depart from the specific details, and the details of the present description may be modified or varied from the spirit and scope of the present invention.
Before the embodiments of the invention are explained in further detail, it is to be understood that the invention is not limited in its scope to the particular embodiments described below; it is also to be understood that the terminology used in the examples of the invention is for the purpose of describing particular embodiments only, and is not intended to limit the scope of the invention.
Where numerical ranges are provided in the examples, it is understood that unless otherwise stated herein, both endpoints of each numerical range and any number between the two endpoints are significant both in the numerical range. Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs.
It should be noted that the raw materials used in the present invention are all common commercial products, and therefore the sources thereof are not particularly limited.
The stability test method of each group of products comprises the following steps: the temperature of the incubator is respectively set: and (3) filling 5 samples of the lip glaze packaging material at 45 degrees, 25 degrees, 0 degree and-5 degrees, filling 1 bottle of each material body into 150ml wide-mouth bottles, putting the materials into an incubator for 1 month, taking out the materials, and observing the state of the materials after the materials return to room temperature, and evaluating according to the quality, the middle and the difference.
The formulations of examples 1-8 and the stability test results are detailed in Table 1 (amounts in parts by weight).
TABLE 1
The preparation method of the product in each embodiment comprises the following steps:
(1) Tribehenine (examples 2-8 also added with sorbitan isostearate and/or VP/hexadecene copolymer), cetyl PEG/PPG-10/1 polydimethylsiloxane, bis-diglycerol polyacyl adipate-2, diisostearyl malate (examples 3-8 also added with tocopheryl acetate and/or dextrin isostearate), and polydimethylsiloxane were heated with stirring to 90deg.C and melted to homogeneity to give mixture A;
(2) Sequentially adding vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane cross-linked polymer, diphenyl polydimethylsiloxane/vinyl diphenyl polydimethylsiloxane/silsesquioxane cross-linked polymer, barium sulfate and HDI/trimethylol hexyl lactone cross-linked polymer into the mixture A one by one, uniformly stirring, and controlling the temperature at 70-75 ℃ to obtain a mixture B;
(3) Mixing CI15850, CI77492, CI19140 and CI77491, diisostearyl malate (polyhydroxy stearic acid is also added in examples 3-8) into color paste, grinding for 3 times by a three-roller machine until the color paste is uniform;
(4) Stirring and mixing the uniform color paste obtained in the step (3) with the mixture B, controlling the temperature to be 60-65 ℃, and stirring for 20min until the material body is uniform;
(5) Defoaming;
(6) And (5) starting cooling water, and continuously stirring and cooling to 38-40 ℃.
The formulations of examples 9-16 and the stability test results are detailed in Table 2.
TABLE 2
Case 9 no significant aggregation of the emulsifier sorbitan isostearate and cetyl PEG/PPG-10/1 dimethicone pigment resulted in a very uneven mass.
Cases 10, 11, 12, and 13, in which either of the emulsifiers was added alone, the pigment dispersion was improved with increasing addition amount, but the optimum effect was not achieved.
Cases 14, 15, 16, total emulsifier addition was 2, in ratio 1: the optimal effect is achieved in the step 1; the addition ratio is 1:2 or 2:1, and the total addition of more than 2 pigments has poor dispersing effect.
Examples 4,5,6,7,8 were relatively good in stability, and each example was subjected to investigation tests for smoothness, air feel at the time of use, and color development, uniformity, graininess, and oil feel after use.
The investigation test method comprises the following steps: a panel of 20 female experts was composed, samples were applied to the lips, schemes 4,5,6,7,8 were scored according to the indices in table 3, the total score was 5 points, and the data results were combined to give table 4.
TABLE 3 Table 3
| Index (I) | Definition of the definition |
| Smoothness degree of smoothness | The easier the lip enamel is to be applied to a uniform degree when applying makeup with the lip enamel brush, the higher the score and vice versa. |
| Air feeling | The higher the degree of tackiness and impermeability of the lip enamel, the higher the score and vice versa. |
| Color rendering index | The degree of coloration is observed under standard lighting, the stronger the coloration the higher the score and vice versa. |
| Uniformity degree | The degree of uniformity of the coverage, with or without irregularities, or the texture, the higher the degree, the higher the score, and vice versa. |
| Particle size | The more powder the higher the fraction and vice versa, the more degree of particles is observed under standard light. |
| Feel of oil | The degree of oil perception is observed under standard lighting, the stronger the oil perception, the higher the score and vice versa. |
TABLE 4 Table 4
Example 4 exhibited relatively good results in terms of stability and smoothness during use, air feel, and color development after use, uniformity, graininess, and oil feel. Comparative experiments were also performed on the plain velvet lip glazes of example 4 and example 17.
TABLE 5 plain velvet lip glaze (example 17)
Comparison of example 4 and example 17 at respective temperatures of stability etc.:
TABLE 6
Example 4 and example 17
Comparison in each dimension of the sense of use:
TABLE 7
Finally, it should be noted that the above description is only for illustrating the technical solution of the present invention, and not for limiting the scope of the present invention, and that the simple modification and equivalent substitution of the technical solution of the present invention can be made by those skilled in the art without departing from the spirit and scope of the technical solution of the present invention.
Claims (2)
1. An air lip glaze composition, characterized in that: 1.5-3 parts of tribasic behenine, 1-2 parts of cetyl PEG/PPG-10/1 parts of polydimethylsiloxane, 3-6 parts of di-diglycerol polyacyl adipate-2, 53-70 parts of polydimethylsiloxane, 3-9 parts of vinyl polydimethylsiloxane/polymethylsilsesquioxane cross-linked polymer, 2-8 parts of diphenyl polydimethylsiloxane/vinyl diphenyl polydimethylsiloxane/silsesquioxane cross-linked polymer, 1.5-2 parts of barium sulfate, 1.5-3 parts of HDI/trimethylol hexyl lactone cross-linked polymer, 5 parts of colorant, 8-11 parts of diisostearyl malate, 0.5-2 parts of sorbitan isostearate, 0.5-2 parts of VP/hexadecene copolymer, 0.5-1 part of tocopheryl acetate, 0.5-2 parts of dextrin isostearate and 0.1-0.3 parts of polyhydroxystearic acid;
the colorant consisted of 0.35 parts CI15850, 1.5 parts CI77492, 2 parts CI19140, and 1.15 parts CI 77491.
2. An air lip glaze composition according to claim 1, wherein: the composition comprises, by weight, 3 parts of tribasic behenine, 1 part of sorbitan isostearate, 1 part of VP/hexadecene copolymer, 1 part of cetyl PEG/PPG-10/1 polydimethylsiloxane, 6 parts of bis-diglycerol polyacyl adipate-2, 0.5 part of tocopheryl acetate, 1 part of dextrin isostearate, 55.4 parts of polydimethylsiloxane, 8 parts of vinyl polydimethylsiloxane/polymethylsiloxane silsesquioxane cross-linked polymer, 5 parts of diphenyl polydimethylsiloxane/vinyl diphenyl polydimethylsiloxane/silsesquioxane cross-linked polymer, 2 parts of barium sulfate, 3 parts of HDI/trimethylol hexyl lactone cross-linked polymer, 5 parts of colorant, 8 parts of diisostearyl malate and 0.1 part of polyhydroxystearic acid.
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| CN111991248A (en) * | 2020-09-23 | 2020-11-27 | 上海市天乐日化厂 | Lip glaze and preparation method thereof |
| CN112870112A (en) * | 2019-11-29 | 2021-06-01 | 株式会社爱茉莉太平洋 | Lip cosmetic composition |
| CN113081885A (en) * | 2021-05-06 | 2021-07-09 | 美尚(广州)化妆品股份有限公司 | Non-makeup lip cosmetic and preparation method thereof |
| CN113143186A (en) * | 2021-04-27 | 2021-07-23 | 亳州市人民医院 | Special diplopore bite-block of intubate |
| CN113181083A (en) * | 2021-04-02 | 2021-07-30 | 科丝美诗(中国)化妆品有限公司 | Matte mud lip, cheek and eye three-purpose composition and preparation method thereof |
| CN114452239A (en) * | 2022-01-21 | 2022-05-10 | 广州卡洛莱化妆品有限公司 | Fog-feeling lip balm with soft mousse texture |
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| CN112870112A (en) * | 2019-11-29 | 2021-06-01 | 株式会社爱茉莉太平洋 | Lip cosmetic composition |
| CN111991248A (en) * | 2020-09-23 | 2020-11-27 | 上海市天乐日化厂 | Lip glaze and preparation method thereof |
| CN113181083A (en) * | 2021-04-02 | 2021-07-30 | 科丝美诗(中国)化妆品有限公司 | Matte mud lip, cheek and eye three-purpose composition and preparation method thereof |
| CN113143186A (en) * | 2021-04-27 | 2021-07-23 | 亳州市人民医院 | Special diplopore bite-block of intubate |
| CN113081885A (en) * | 2021-05-06 | 2021-07-09 | 美尚(广州)化妆品股份有限公司 | Non-makeup lip cosmetic and preparation method thereof |
| CN114452239A (en) * | 2022-01-21 | 2022-05-10 | 广州卡洛莱化妆品有限公司 | Fog-feeling lip balm with soft mousse texture |
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