CN115044406A - Efficient cutting fluid and preparation method thereof - Google Patents
Efficient cutting fluid and preparation method thereof Download PDFInfo
- Publication number
- CN115044406A CN115044406A CN202210806404.4A CN202210806404A CN115044406A CN 115044406 A CN115044406 A CN 115044406A CN 202210806404 A CN202210806404 A CN 202210806404A CN 115044406 A CN115044406 A CN 115044406A
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- China
- Prior art keywords
- component
- cutting fluid
- parts
- acid
- diethanolamine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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- 239000002173 cutting fluid Substances 0.000 title claims abstract description 28
- 238000002360 preparation method Methods 0.000 title description 7
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 33
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 12
- 239000004135 Bone phosphate Substances 0.000 claims abstract description 11
- 239000002253 acid Substances 0.000 claims abstract description 11
- ZBCBWPMODOFKDW-UHFFFAOYSA-N diethanolamine Chemical compound OCCNCCO ZBCBWPMODOFKDW-UHFFFAOYSA-N 0.000 claims abstract description 11
- 239000002994 raw material Substances 0.000 claims abstract description 10
- -1 phosphate ester Chemical class 0.000 claims abstract description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229910019142 PO4 Inorganic materials 0.000 claims abstract description 4
- 150000001412 amines Chemical class 0.000 claims abstract description 4
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims abstract description 4
- 239000010452 phosphate Substances 0.000 claims abstract description 4
- 238000003756 stirring Methods 0.000 claims description 6
- 238000000034 method Methods 0.000 claims description 4
- 239000013530 defoamer Substances 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 abstract description 7
- 230000007797 corrosion Effects 0.000 abstract description 6
- 238000005260 corrosion Methods 0.000 abstract description 6
- 238000004140 cleaning Methods 0.000 abstract description 5
- 238000001816 cooling Methods 0.000 abstract description 5
- 230000000694 effects Effects 0.000 abstract description 3
- 231100000956 nontoxicity Toxicity 0.000 abstract description 3
- 230000002265 prevention Effects 0.000 abstract description 3
- 239000002518 antifoaming agent Substances 0.000 abstract 1
- 238000003912 environmental pollution Methods 0.000 abstract 1
- 238000001514 detection method Methods 0.000 description 3
- 239000002184 metal Substances 0.000 description 3
- 229910052751 metal Inorganic materials 0.000 description 3
- 241000894006 Bacteria Species 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 238000005520 cutting process Methods 0.000 description 2
- 239000000839 emulsion Substances 0.000 description 2
- 238000000227 grinding Methods 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 230000001050 lubricating effect Effects 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000000344 soap Substances 0.000 description 2
- CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 239000003899 bactericide agent Substances 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000013329 compounding Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 239000003995 emulsifying agent Substances 0.000 description 1
- 238000011066 ex-situ storage Methods 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 238000003754 machining Methods 0.000 description 1
- 239000002480 mineral oil Substances 0.000 description 1
- 235000010446 mineral oil Nutrition 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 238000011179 visual inspection Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M173/00—Lubricating compositions containing more than 10% water
- C10M173/02—Lubricating compositions containing more than 10% water not containing mineral or fatty oils
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/02—Hydroxy compounds
- C10M2207/021—Hydroxy compounds having hydroxy groups bound to acyclic or cycloaliphatic carbon atoms
- C10M2207/022—Hydroxy compounds having hydroxy groups bound to acyclic or cycloaliphatic carbon atoms containing at least two hydroxy groups
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/10—Carboxylix acids; Neutral salts thereof
- C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
- C10M2207/121—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of seven or less carbon atoms
- C10M2207/123—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of seven or less carbon atoms polycarboxylic
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/10—Carboxylix acids; Neutral salts thereof
- C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
- C10M2207/121—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of seven or less carbon atoms
- C10M2207/124—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of seven or less carbon atoms containing hydroxy groups; Ethers thereof
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
- C10M2215/04—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms
- C10M2215/042—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms containing hydroxy groups; Alkoxylated derivatives thereof
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
- C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
- C10M2223/04—Phosphate esters
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/04—Detergent property or dispersant property
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/12—Inhibition of corrosion, e.g. anti-rust agents or anti-corrosives
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/52—Base number [TBN]
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/64—Environmental friendly compositions
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/20—Metal working
- C10N2040/22—Metal working with essential removal of material, e.g. cutting, grinding or drilling
Abstract
The invention discloses an efficient cutting fluid which comprises the following raw materials in percentage by weight: 1-3 parts of diethanolamine, 1-10 parts of tribasic acid and 0.5-2 parts of citric acid; t060.1-0.5, BK 1-3; 1-10 parts of CH020 special amine, 1-3 parts of semisynthetic phosphate ester, 10-20 parts of glycerol, 0.1-1 part of ether carboxylic acid and 0.1-1 part of water-based defoaming agent. Compared with the existing products, the cutting fluid has the characteristics of better cooling, cleaning, rust prevention and the like, has the characteristics of no toxicity, no smell, no corrosion to human bodies, no corrosion to equipment, no environmental pollution and the like, can meet the processing requirements of common loads, and has the characteristics of long service life and obvious technical effect.
Description
Technical Field
The invention relates to the technical field of machining, in particular to a high-efficiency cutting fluid and a preparation method of the high-efficiency cutting fluid.
Background
The cutting fluid is an important matched material for metal cutting processing, acts on industrial liquid of a cutter and a workpiece in the metal processing process, mainly plays roles in cooling, lubricating, cleaning and rust prevention, and mainly comprises a rust inhibitor, an emulsifier, an alkali value retaining agent, an oily lubricant, a bactericide, mineral oil, water and the like.
The cutting fluid is prepared by scientifically compounding and matching various additives, and has the characteristics of good cooling performance, lubricating performance, antirust performance, oil removal and cleaning functions, anticorrosion function and easiness in dilution. The defects that the traditional soap-based emulsion is easy to smell in summer, difficult to dilute in winter and poor in antirust effect are overcome, the lathe paint is not affected, and the soap-based emulsion is suitable for cutting and grinding ferrous metal and belongs to the current leading grinding product.
Most of the existing cutting fluids have the characteristics of good cooling, cleaning, rust prevention and the like, and have the characteristics of no toxicity, no odor, no corrosion to human bodies, no corrosion to equipment, no pollution to the environment and the like. In order to further improve the functions and performances of the cutting fluid, the raw materials and the proportion of the cutting fluid need to be continuously improved.
Disclosure of Invention
The invention aims to provide the cutting fluid which is scientific and reasonable in proportion and has higher functions and performances.
In order to solve the problem, the technical scheme adopted by the invention is as follows:
a high-efficiency cutting fluid comprises components A, B and C, wherein the components A, B and C comprise the following raw materials in percentage by weight:
1) component A
1-3 of diethanolamine
1-10% of tribasic acid
0.5-2 parts of citric acid;
2) component B
T06 0.1～0.5
BK 1～3；
3) Component C
On the basis of the technical scheme, the components A, B and C comprise the following raw materials in percentage by weight:
1) component A
Diethanolamine 1.5
Tribasic acid 5
1 part of citric acid;
2) component B
T06 0.3
BK 2；
3) Component C
The preparation method of the efficient cutting fluid specifically comprises the following steps:
adding diethanolamine, tribasic acid and citric acid in the component A according to the proportion;
then adding T06 and BK in the component B;
adding CH020 special amine in the component C, and stirring in a reaction kettle;
adding the semisynthetic phosphate ester, the glycerol, the ether carboxylic acid and the aqueous defoamer in the component C, mixing and stirring;
and finally adding the rest of water to obtain the high-efficiency cutting fluid.
The invention has the following beneficial effects:
the invention optimizes the raw materials and the proportion of the cutting fluid, greatly improves the smell, the base number and the rust resistance of the prepared cutting fluid, greatly improves the function and the performance of the cutting fluid, has the characteristics of better cooling, cleaning, rust resistance and the like compared with the prior product, has the characteristics of no toxicity, no odor, no corrosion to human bodies, no corrosion to equipment, no pollution to environment and the like, can meet the processing requirement of common load, and has the characteristics of long service life and obvious technical effect.
Detailed Description
For the purpose of facilitating an understanding of the present invention, the present invention will now be described by way of examples. It should be understood by those skilled in the art that the examples are only for the purpose of facilitating understanding of the present invention and should not be construed as specifically limiting the present invention.
Unless otherwise specified, various starting materials of the present invention are commercially available; or prepared according to conventional methods in the art. Unless defined or indicated otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs. In addition, any methods and materials similar or equivalent to those described herein can be used in the methods of the present invention. Unless otherwise defined, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs.
Example 1
A high-efficiency cutting fluid comprises components A, B and C, wherein the components A, B and C comprise the following raw materials in percentage by weight:
1) component A
Diethanolamine 1.5
Tribasic acid 5
1 part of citric acid;
2) component B
T06 0.3
BK 2；
3) Component C
The preparation method comprises the following steps:
adding diethanolamine, tribasic acid and citric acid in the component A according to the proportion;
then adding T06 and BK in the component B;
adding CH020 special amine in the component C, and stirring in a reaction kettle;
adding the semisynthetic phosphate ester, the glycerol, the ether carboxylic acid and the aqueous defoamer in the component C, mixing and stirring;
finally adding the rest water to obtain the product.
After 24 hours, the high-efficiency cutting fluid prepared in the embodiment is detected, and the performance detection standard and result of the cutting fluid are as follows:
| detecting items | Detection standard | |
| Ex-situ cash | Visual inspection of | Transparent liquid |
| Smell(s) | Snuff | Slight putrefactive odor |
| pH value | Reference SH/T0578 | 8-9 |
| Rust resistance (iron fillings filter paper) | Reference IP 287 | Level 0 |
| Bacteria, CFU/ml. | Bacterium detecting sheet | <10 2 |
According to the detection result, the pH value and the antirust property of the efficient cutting fluid are obviously improved, the antirust requirement is met, and the processing requirement of general loads can be met.
Example 2
A high-efficiency cutting fluid comprises components A, B and C, wherein the components A, B and C comprise the following raw materials in percentage by weight:
1) component A
Diethanolamine 3
Tribasic acid 10
2 parts of citric acid;
2) component B
T06 0.5
BK 3；
3) Component C
The preparation method is the same as that of example 1.
Example 3
A high-efficiency cutting fluid comprises components A, B and C, wherein the components A, B and C comprise the following raw materials in percentage by weight:
1) component A
Diethanolamine 2
Tribasic acid 5
1 part of citric acid;
2) component B
T06 0.1
BK 1；
3) Component C
The preparation method is the same as that of example 1.
Furthermore, it should be understood that although the present description refers to embodiments, not every embodiment may contain only a single embodiment, and such description is for clarity only, and those skilled in the art should integrate the description, and the embodiments may be combined as appropriate to form other embodiments understood by those skilled in the art.
Claims (3)
1. The efficient cutting fluid comprises components A, B and C, and is characterized in that the components A, B and C comprise the following raw materials in percentage by weight:
1) component A
1-3 of diethanolamine
1-10% of tribasic acid
0.5-2 parts of citric acid;
2) component B
T06 0.1～0.5
BK 1～3；
3) Component C
The balance being water.
2. The efficient cutting fluid as claimed in claim 1, wherein the components A, B and C comprise the following raw materials in percentage by weight:
1) component A
Diethanolamine 1.5
Tribasic acid 5
1 part of citric acid;
2) component B
T06 0.3
BK 2；
3) Component C
The balance being water.
3. The method for preparing the high-efficiency cutting fluid according to claim 1, which comprises the following steps:
adding diethanolamine, tribasic acid and citric acid in the component A according to the proportion;
then adding T06 and BK in the component B;
adding CH020 special amine in the component C, and stirring in a reaction kettle;
adding the semisynthetic phosphate ester, the glycerol, the ether carboxylic acid and the aqueous defoamer in the component C, mixing and stirring;
and finally, adding the rest of water to obtain the high-efficiency cutting fluid.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210806404.4A CN115044406A (en) | 2022-07-08 | 2022-07-08 | Efficient cutting fluid and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210806404.4A CN115044406A (en) | 2022-07-08 | 2022-07-08 | Efficient cutting fluid and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN115044406A true CN115044406A (en) | 2022-09-13 |
Family
ID=83164522
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202210806404.4A Pending CN115044406A (en) | 2022-07-08 | 2022-07-08 | Efficient cutting fluid and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN115044406A (en) |
-
2022
- 2022-07-08 CN CN202210806404.4A patent/CN115044406A/en active Pending
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
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Application publication date: 20220913 |