CN110331028A - A kind of long-acting extreme pressure emulsion cutting fluid of multifunctional water-soluble for intermetallic composite coating - Google Patents
A kind of long-acting extreme pressure emulsion cutting fluid of multifunctional water-soluble for intermetallic composite coating Download PDFInfo
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- CN110331028A CN110331028A CN201910672172.6A CN201910672172A CN110331028A CN 110331028 A CN110331028 A CN 110331028A CN 201910672172 A CN201910672172 A CN 201910672172A CN 110331028 A CN110331028 A CN 110331028A
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M173/00—Lubricating compositions containing more than 10% water
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/087—Boron oxides, acids or salts
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2203/00—Organic non-macromolecular hydrocarbon compounds and hydrocarbon fractions as ingredients in lubricant compositions
- C10M2203/10—Petroleum or coal fractions, e.g. tars, solvents, bitumen
- C10M2203/106—Naphthenic fractions
- C10M2203/1065—Naphthenic fractions used as base material
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/10—Carboxylix acids; Neutral salts thereof
- C10M2207/18—Tall oil acids
- C10M2207/183—Tall oil acids used as base material
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/10—Carboxylix acids; Neutral salts thereof
- C10M2207/22—Acids obtained from polymerised unsaturated acids
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
- C10M2215/04—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/06—Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/12—Inhibition of corrosion, e.g. anti-rust agents or anti-corrosives
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/18—Anti-foaming property
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/40—Low content or no content compositions
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/64—Environmental friendly compositions
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/20—Metal working
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/20—Metal working
- C10N2040/22—Metal working with essential removal of material, e.g. cutting, grinding or drilling
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/20—Metal working
- C10N2040/244—Metal working of specific metals
- C10N2040/246—Iron or steel
Abstract
The invention discloses a kind of long-acting extreme pressure emulsion cutting fluids of multifunctional water-soluble for intermetallic composite coating, belong to water soluble metal working fluids field, this is used for the long-acting extreme pressure emulsion cutting fluid of multifunctional water-soluble of intermetallic composite coating, is made of base oil, oiliness improver, complexing agent, emulsifier, antirust agent, copper alloy corrosion inhibiter, aluminum alloy corrosion inhibitor, fungicide, defoaming agent and water.Of the invention can resist hard water, have many advantages, such as excellent lubricity, cooling, rust-preventing characteristic, defoaming and long service life；Suitable for requiring the cutting and grinding of wide in range ferrous metal and non-ferrous metal, the especially processing of cast iron, copper, aluminium alloy component.Without poisonous and harmful substances such as nitrite, phenol, health is not damaged, it is free from environmental pollution.
Description
Technical field
The invention belongs to water soluble metal working fluids technical fields, and in particular to a kind of water solubility for intermetallic composite coating is more
The long-acting extreme pressure emulsion cutting fluid of function.
Background technique
Metal working fluid is a kind of in metal cutting, mill process, for cooling down and lubricating cutter and workpiece
Industrial type fluid, metal working fluid is made from a variety of powerful additives of scientific compatibility, is provided simultaneously with good cold
But performance, greasy property, rustless property, oil removing cleaning function, anti-corrosion function, easily dilutable feature.Overcome traditional soap base emulsification
Liquid summer easy smelly, winter difficult dilution rust-proof effect difference defect, also has no adverse effects to lathe paint.
Cutting fluid is essential processing aid in metal cutting process.With the development of industry, the increasing of machining
Cause the dosage of cutting fluid increasing more.The major issue for being treated as environmental protection of cutting fluid after use.Existing skill
Cutting fluid poorly water-soluble in art, it is difficult to meet the requirement of environmental protection, and applicability is low.
Summary of the invention
The purpose of the present invention is to provide a kind of long-acting extreme pressure emulsion cutting fluid of multifunctional water-soluble for intermetallic composite coating,
To solve the problems mentioned in the above background technology.
To achieve the above object, the invention provides the following technical scheme: a kind of multifunctional water-soluble for intermetallic composite coating
Long-acting extreme pressure emulsion cutting fluid, which includes such as the following group
Point:
The amount of being calculated in mass percent: diethanol amine 6-8%, dodecanedicarboxylic acid 2-3%, boric acid 5-6%, monoethanolamine 1-
2%, bicyclohexylamine 1-1.5%, tall oil M-28B 7-9%, four poly- oleic acid 2-3%, naphthenic oil 25-30%, white oil 5-8%,
Synthetic fat 5-6%, aluminium corrosion inhibiter and copper inhibitor 1-1.5%, MBM fungicide 1-1.5%, BK 1-1.5%, emulsifier 3-
3.5%, defoaming agent 0.05-1%, water surplus.
Further, the emulsifier is selected from one of sorbitol fatty acid ester, phospholipid.
Further, the defoaming agent is selected from one or both of GPE type, GPES type polyethers defoaming agent.
The preparation method of the long-acting extreme pressure emulsion cutting fluid of multifunctional water-soluble for intermetallic composite coating, which is characterized in that packet
Include the following steps:
(1) diethanol amine, monoethanolamine, bicyclohexylamine, water are taken respectively by weight, by the diethanol amine of acquirement, a second
Hydramine, sequentially adds in water bicyclohexylamine, heats while stirring, and temperature is controlled at 60 DEG C -80 DEG C, obtains reaction product A；
(2) dodecanedicarboxylic acid, boric acid, four poly- oleic acid are taken respectively by weight, are sequentially added in reaction product A, are stirred
15-30 minutes, temperature was controlled at 60 DEG C -80 DEG C, obtained reaction product B；
(3) tall oil M-28B, naphthenic oil, white oil, synthetic fat are taken respectively by weight, is sequentially added in reaction product B,
Stirring 15-30 minutes, temperature are controlled at 60 DEG C -80 DEG C, obtain reaction product C；
(4) aluminium corrosion inhibiter and copper inhibitor, MBM fungicide, fungicide, BK, emulsifier are taken respectively by weight, successively plus
Enter in reaction product C, stir 15-30 minutes, temperature is controlled at 60 DEG C -80 DEG C, obtains reaction product D；
(5) cancel infusion by weight, be added in reaction product D, stir 15-30 minutes, temperature is controlled at 60 DEG C -80
DEG C, obtain finished product.
Compared with prior art, the beneficial effects of the present invention are: of the invention can resist hard water, there is excellent lubrication
The advantages that property, cooling, rust-preventing characteristic, defoaming and long service life；Suitable for requiring wide in range ferrous metal and non-ferrous metal
Cutting and grinding, the especially processing of cast iron, alloy steel part.Without poisonous and harmful substances such as nitrite, phenol,
Health is not damaged, it is free from environmental pollution.
Specific embodiment
Below with reference to embodiment, the present invention will be further described.
The following examples are intended to illustrate the invention, but cannot be used to limit the scope of the invention.Item in embodiment
Part can be adjusted according to actual conditions are further, under concept thereof of the invention all to method simple modifications of the invention
Belong to the scope of protection of present invention.
Embodiment 1
The present invention provides a kind of long-acting extreme pressure emulsion cutting fluid of the multifunctional water-soluble for intermetallic composite coating, this is used for metal
The long-acting extreme pressure emulsion cutting fluid of the multifunctional water-soluble of processing includes following component:
The amount of being calculated in mass percent: diethanol amine 6%, dodecanedicarboxylic acid 2%, boric acid 5%, monoethanolamine 1%, two rings
Amine 1%, tall oil M-28B 7%, four poly- oleic acid 2%, naphthenic oil 25%, white oil 5-8%, synthetic fat 5%, aluminium corrosion inhibiter with
Copper inhibitor 1%, MBM fungicide 1%, BK 1%, emulsifier 3%, defoaming agent 0.05%, water surplus.
It is made of the following steps:
(1) diethanol amine, monoethanolamine, bicyclohexylamine, water are taken respectively by weight, by the diethanol amine of acquirement, a second
Hydramine, sequentially adds in water bicyclohexylamine, heats while stirring, and temperature is controlled at 80 DEG C, obtains reaction product A；
(2) dodecanedicarboxylic acid, boric acid, four poly- oleic acid are taken respectively by weight, are sequentially added in reaction product A, are stirred
15-30 minutes, temperature was controlled at 80 DEG C, obtained reaction product B；
(3) tall oil M-28B, naphthenic oil, white oil, synthetic fat are taken respectively by weight, is sequentially added in reaction product B,
Stirring 15-30 minutes, temperature are controlled at 80 DEG C, obtain reaction product C；
(4) aluminium corrosion inhibiter and copper inhibitor, MBM fungicide, fungicide, BK, emulsifier are taken respectively by weight, successively plus
Enter in reaction product C, stir 15-30 minutes, temperature is controlled at 80 DEG C, obtains reaction product D；
(5) cancel infusion by weight, be added in reaction product D, stir 15-30 minutes, temperature is controlled at 80 DEG C, is obtained into
Product.
Embodiment 2
The present invention provides a kind of long-acting extreme pressure emulsion cutting fluid of the multifunctional water-soluble for intermetallic composite coating, this is used for metal
The long-acting extreme pressure emulsion cutting fluid of the multifunctional water-soluble of processing includes following component:
The amount of being calculated in mass percent: diethanol amine 8%, dodecanedicarboxylic acid 3%, boric acid 6%, monoethanolamine 2%, two rings
Amine 1.5%, tall oil M-28B9%, four poly- oleic acid 3%, naphthenic oil 30%, white oil 8%, synthetic fat 6%, aluminium corrosion inhibiter with
Copper inhibitor 1.5%, MBM fungicide 1.5%, BK 1.5%, emulsifier 3.5%, defoaming agent 1%, water surplus.
It is made of the following steps:
(1) diethanol amine, monoethanolamine, bicyclohexylamine, water are taken respectively by weight, by the diethanol amine of acquirement, a second
Hydramine, sequentially adds in water bicyclohexylamine, heats while stirring, and temperature is controlled at 80 DEG C, obtains reaction product A；
(2) dodecanedicarboxylic acid, boric acid, four poly- oleic acid are taken respectively by weight, are sequentially added in reaction product A, are stirred
15-30 minutes, temperature was controlled at 80 DEG C, obtained reaction product B；
(3) tall oil M-28B, naphthenic oil, white oil, synthetic fat are taken respectively by weight, is sequentially added in reaction product B,
Stirring 15-30 minutes, temperature are controlled at 80 DEG C, obtain reaction product C；
(4) aluminium corrosion inhibiter and copper inhibitor, MBM fungicide, fungicide, BK, emulsifier are taken respectively by weight, successively plus
Enter in reaction product C, stir 15-30 minutes, temperature is controlled at 80 DEG C, obtains reaction product D；
(5) cancel infusion by weight, be added in reaction product D, stir 15-30 minutes, temperature is controlled at 80 DEG C, is obtained into
Product.
Embodiment 3
The present invention provides a kind of long-acting extreme pressure emulsion cutting fluid of the multifunctional water-soluble for intermetallic composite coating, this is used for metal
The long-acting extreme pressure emulsion cutting fluid of the multifunctional water-soluble of processing includes following component:
The amount of being calculated in mass percent: diethanol amine 6%, dodecanedicarboxylic acid 2%, boric acid 5%, monoethanolamine 1%, two rings
Amine 1%, tall oil M-28B 7%, four poly- oleic acid 2%, naphthenic oil 25%, white oil 5-8%, synthetic fat 5%, aluminium corrosion inhibiter with
Copper inhibitor 1%, MBM fungicide 1%, BK 1%, emulsifier 3%, defoaming agent 0.05%, water surplus.
It is made of the following steps:
(1) diethanol amine, monoethanolamine, bicyclohexylamine, water are taken respectively by weight, by the diethanol amine of acquirement, a second
Hydramine, sequentially adds in water bicyclohexylamine, heats while stirring, and temperature is controlled at 80 DEG C, obtains reaction product A；
(2) dodecanedicarboxylic acid, boric acid, four poly- oleic acid are taken respectively by weight, are sequentially added in reaction product A, are stirred
15-30 minutes, temperature was controlled at 80 DEG C, obtained reaction product B；
(3) tall oil M-28B, naphthenic oil, white oil, synthetic fat are taken respectively by weight, is sequentially added in reaction product B,
Stirring 15-30 minutes, temperature are controlled at 80 DEG C, obtain reaction product C；
(4) aluminium corrosion inhibiter and copper inhibitor, MBM fungicide, fungicide, BK, emulsifier are taken respectively by weight, successively plus
Enter in reaction product C, stir 15-30 minutes, temperature is controlled at 80 DEG C, obtains reaction product D；
(5) cancel infusion by weight, be added in reaction product D, stir 15-30 minutes, temperature is controlled at 80 DEG C, is obtained into
Product.
Embodiment 4
The present invention provides a kind of long-acting extreme pressure emulsion cutting fluid of the multifunctional water-soluble for intermetallic composite coating, this is used for metal
The long-acting extreme pressure emulsion cutting fluid of the multifunctional water-soluble of processing includes following component:
The amount of being calculated in mass percent: diethanol amine 8%, dodecanedicarboxylic acid 3%, boric acid 6%, monoethanolamine 2%, two rings
Amine 1.5%, tall oil M-28B9%, four poly- oleic acid 3%, naphthenic oil 30%, white oil 8%, synthetic fat 6%, aluminium corrosion inhibiter with
Copper inhibitor 1.5%, MBM fungicide 1.5%, BK 1.5%, emulsifier 3.5%, defoaming agent 1%, water surplus.
It is made of the following steps:
(1) diethanol amine, monoethanolamine, bicyclohexylamine, water are taken respectively by weight, by the diethanol amine of acquirement, a second
Hydramine, sequentially adds in water bicyclohexylamine, heats while stirring, and temperature is controlled at 80 DEG C, obtains reaction product A；
(2) dodecanedicarboxylic acid, boric acid, four poly- oleic acid are taken respectively by weight, are sequentially added in reaction product A, are stirred
15-30 minutes, temperature was controlled at 80 DEG C, obtained reaction product B；
(3) tall oil M-28B, naphthenic oil, white oil, synthetic fat are taken respectively by weight, is sequentially added in reaction product B,
Stirring 15-30 minutes, temperature are controlled at 80 DEG C, obtain reaction product C；
(4) aluminium corrosion inhibiter and copper inhibitor, MBM fungicide, fungicide, BK, emulsifier are taken respectively by weight, successively plus
Enter in reaction product C, stir 15-30 minutes, temperature is controlled at 80 DEG C, obtains reaction product D；
(5) cancel infusion by weight, be added in reaction product D, stir 15-30 minutes, temperature is controlled at 80 DEG C, is obtained into
Product.
In conclusion of the invention can resist hard water, have excellent lubricity, cooling, rust-preventing characteristic, defoaming and
The advantages that long service life；Suitable for require the cutting and grinding of wide in range ferrous metal and non-ferrous metal, especially cast iron,
The processing of alloy steel part.Without poisonous and harmful substances such as nitrite, phenol, health is not damaged, it is free from environmental pollution.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention is defined by the appended.
Claims (4)
1. a kind of long-acting extreme pressure emulsion cutting fluid of multifunctional water-soluble for intermetallic composite coating, which is characterized in that the water solubility is more
The long-acting extreme pressure emulsion cutting fluid of function includes following component:
The amount of being calculated in mass percent: diethanol amine 6-8%, dodecanedicarboxylic acid 2-3%, boric acid 5-6%, monoethanolamine 1-2%,
Bicyclohexylamine 1-1.5%, tall oil M-28B7-9%, four poly- oleic acid 2-3%, naphthenic oil 25-30%, white oil 5-8%, synthetic fat
5-6%, aluminium corrosion inhibiter and copper inhibitor 1-1.5%, MBM fungicide 1-1.5%, BK 1-1.5%, emulsifier 3-3.5%, disappear
Infusion 0.05-1%, water surplus.
2. the long-acting extreme pressure emulsion cutting fluid of a kind of multifunctional water-soluble for intermetallic composite coating according to claim 1,
It is characterized in that, the emulsifier is selected from one of sorbitol fatty acid ester, phospholipid.
3. the long-acting extreme pressure emulsion cutting fluid of a kind of multifunctional water-soluble for intermetallic composite coating according to claim 1,
It is characterized in that, the defoaming agent is selected from one or both of GPE type, GPES type polyethers defoaming agent.
4. a kind of system of the long-acting extreme pressure emulsion cutting fluid of multifunctional water-soluble for intermetallic composite coating according to claim 1
Preparation Method, characterized in that it comprises the following steps:
(1) diethanol amine, monoethanolamine, bicyclohexylamine, water are taken respectively by weight, by the diethanol amine of acquirement, monoethanolamine,
Bicyclohexylamine sequentially adds in water, heats while stirring, and temperature is controlled at 60 DEG C -80 DEG C, obtains reaction product A；
(2) dodecanedicarboxylic acid, boric acid, four poly- oleic acid are taken respectively by weight, are sequentially added in reaction product A, 15-30 is stirred
Minute, temperature is controlled at 60 DEG C -80 DEG C, obtains reaction product B；
(3) tall oil M-28B, naphthenic oil, white oil, synthetic fat are taken respectively by weight, is sequentially added in reaction product B, is stirred
15-30 minutes, temperature was controlled at 60 DEG C -80 DEG C, obtained reaction product C；
(4) aluminium corrosion inhibiter and copper inhibitor, MBM fungicide, fungicide, BK, emulsifier are taken respectively by weight, is sequentially added anti-
It answers in product C, stirs 15-30 minutes, temperature is controlled at 60 DEG C -80 DEG C, obtains reaction product D；
(5) cancel infusion by weight, be added in reaction product D, stir 15-30 minutes, temperature is controlled at 60 DEG C -80 DEG C, is obtained
Finished product.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111136771A (en) * | 2019-12-27 | 2020-05-12 | 湖南加美乐素新材料股份有限公司 | Release agent prepared from polyoxyethylene ether-20 oleoyl ricinoleate |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5985803A (en) * | 1997-12-05 | 1999-11-16 | The Lubrizol Corporation | Polyethoxylated alcohol-based phosphonates for metal working lubricants |
| CN105296120A (en) * | 2014-06-20 | 2016-02-03 | 周志雄 | Water-soluble cutting fluid |
| CN106833853A (en) * | 2017-01-11 | 2017-06-13 | 李弟和 | Water-soluble metalworking liquid |
| CN109504516A (en) * | 2019-01-22 | 2019-03-22 | 无锡科捷化学有限公司 | A kind of micro emulsion cutting fluid and preparation method thereof suitable for heavy load intermetallic composite coating |
-
2019
- 2019-07-24 CN CN201910672172.6A patent/CN110331028A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5985803A (en) * | 1997-12-05 | 1999-11-16 | The Lubrizol Corporation | Polyethoxylated alcohol-based phosphonates for metal working lubricants |
| CN105296120A (en) * | 2014-06-20 | 2016-02-03 | 周志雄 | Water-soluble cutting fluid |
| CN106833853A (en) * | 2017-01-11 | 2017-06-13 | 李弟和 | Water-soluble metalworking liquid |
| CN109504516A (en) * | 2019-01-22 | 2019-03-22 | 无锡科捷化学有限公司 | A kind of micro emulsion cutting fluid and preparation method thereof suitable for heavy load intermetallic composite coating |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111136771A (en) * | 2019-12-27 | 2020-05-12 | 湖南加美乐素新材料股份有限公司 | Release agent prepared from polyoxyethylene ether-20 oleoyl ricinoleate |
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Application publication date: 20191015 |