CN114767761A - Preparation method of vinegar schisandra chinensis - Google Patents

Preparation method of vinegar schisandra chinensis Download PDF

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CN114767761A
CN114767761A CN202210618556.1A CN202210618556A CN114767761A CN 114767761 A CN114767761 A CN 114767761A CN 202210618556 A CN202210618556 A CN 202210618556A CN 114767761 A CN114767761 A CN 114767761A
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schisandra chinensis
vinegar
steaming
drying
preparation
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刘颖
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Anguo City Synonymous Chinese Herbal Medicine Ltd
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Anguo City Synonymous Chinese Herbal Medicine Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/79Schisandraceae (Schisandra family)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/57Magnoliaceae (Magnolia family)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P1/00Drugs for disorders of the alimentary tract or the digestive system
    • A61P1/12Antidiarrhoeals
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P11/00Drugs for disorders of the respiratory system
    • A61P11/06Antiasthmatics
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P13/00Drugs for disorders of the urinary system
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P25/00Drugs for disorders of the nervous system
    • A61P25/20Hypnotics; Sedatives
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P9/00Drugs for disorders of the cardiovascular system
    • A61P9/06Antiarrhythmics
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/10Preparation or pretreatment of starting material
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/10Preparation or pretreatment of starting material
    • A61K2236/17Preparation or pretreatment of starting material involving drying, e.g. sun-drying or wilting

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
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Abstract

The invention relates to the technical field of traditional Chinese medicine processing, in particular to a preparation method of vinegar schisandra chinensis. The method specifically comprises the following steps: (1) mixing fructus Schisandrae chinensis with rice vinegar, moistening, and air drying; (2) steaming the dried schisandra chinensis obtained in the step (1), and collecting a steaming liquid; (3) mixing the steamed fructus Schisandrae with the steam, and drying. The invention takes schisandra chinensis as a main material and prepares vinegar schisandra chinensis through roasting, wherein the vinegar schisandra chinensis is used for treating asthenic cough, nocturnal emission, spermatorrhea, enuresis, frequent micturition, chronic diarrhea, spontaneous perspiration, night sweat, thirst due to body fluid consumption, internal heat, thirst, palpitation and insomnia.

Description

Preparation method of vinegar schisandra chinensis
Technical Field
The invention relates to the technical field of traditional Chinese medicine processing, in particular to a preparation method of vinegar schisandra chinensis.
Background
Fructus Schisandrae is dried ripe fruit of Schisandra chinensis (Turcz.) Baill. Commonly known as "Bei Wu Wei Zi".
Picking in autumn when the fruit is mature, sun-drying or steaming and sun-drying, and removing fruit stalks and impurities. Tang et al, Xin Xiu Ben Cao, recorded that the five flavors of skin and meat are sweet and sour, and bitter and pungent in the kernel, all have salty flavor, so it is named as Wu Wei Zi. The schisandra chinensis is divided into a south part and a north part. The ancient medical book called him 33614c, mysterious union 34127, mysterious union, confluence, the earliest listed in the Shennong herbal meridian top-grade traditional Chinese medicines can nourish and strengthen the strength, has extremely high medicinal value and the effect of strengthening the body, and is used together with Qiongzhen lucid ganoderma to treat insomnia.
Vinegar fructus Schisandrae is processed product of fructus Schisandrae. The Chinese magnoliavine fruit processed with vinegar has stronger effects of astringency and stopping diarrhea. Can be used for treating spermatorrhea and diarrhea. The processing methods recorded in modern main literatures of schisandra chinensis include four methods of purification, vinegar steaming, wine steaming and honey roasting, and the processing method recorded in the 2005 edition of the chinese pharmacopoeia includes vinegar steaming. Vinegar processed schisandra fruit: taking the clean fructus Schisandrae, and steaming to black according to vinegar steaming method (appendix II D). It is administered by mashing. The processing method does not have reasonable process indexes, steaming time, vinegar adding amount, steaming conditions, temperature and the like, and is not controlled, wherein the steaming time is about 1-2 days, the time consumption is long, the process is relatively complex, and the industrial mass production is greatly restricted. Therefore, it is imperative to formulate feasible and quantificationally controllable processing parameters of fructus Schisandrae chinensis and reasonable quality inspection indexes of decoction pieces.
Therefore, how to provide a preparation method of vinegar schisandra chinensis is to solve the technical problems that in the prior art, the preparation process of vinegar schisandra chinensis is complicated, the preparation period is long, finished products produced by the prior production technology are seriously caked and peeled, and the product quality is low, and the problems to be solved by technical personnel in the field are urgently needed.
Disclosure of Invention
The invention aims to provide a preparation method of vinegar schisandra chinensis, which aims to solve the technical problems of complex preparation process, serious agglomeration and peeling of finished products and low product quality of the vinegar schisandra chinensis in the prior art.
In order to achieve the above object, the present invention provides the following technical solutions:
a preparation method of vinegar schisandra chinensis comprises the following steps:
(1) mixing fructus Schisandrae with rice vinegar, moistening, and air drying;
(2) steaming the dried schisandra chinensis obtained in the step (1), and collecting a steaming liquid;
(3) mixing the steamed fructus Schisandrae with the steam, and drying.
Preferably, the mass ratio of the schisandra chinensis to the rice vinegar in the step (1) is 4-6: 1.
Preferably, the moistening time in the step (1) is 2-4 h.
Preferably, the air drying in the step (1) is carried out until the water content of the schisandra chinensis is 25-35%.
Preferably, the steaming temperature in the step (2) is 80-100 ℃, and the steaming time is 2-4 h.
Preferably, the drying temperature in step (3) is less than 80 ℃.
Preferably, the drying in the step (3) is carried out until the moisture content of the schisandra chinensis is less than 16%.
Preferably, the thickness of the paving material in the drying process in the step (3) is less than 3cm, and the paving material is stirred for 2-4 times every day.
Compared with the prior art, the invention has the following beneficial effects:
the invention takes schisandra chinensis as a main material and prepares vinegar schisandra chinensis through roasting, wherein the vinegar schisandra chinensis is used for treating asthenic cough, nocturnal emission, spermatorrhea, enuresis, frequent micturition, chronic diarrhea, spontaneous perspiration, night sweat, thirst due to body fluid consumption, internal heat, thirst, palpitation and insomnia.
Drawings
In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings used in the description of the embodiments or the prior art will be briefly described below, it is obvious that the drawings in the following description are only embodiments of the present invention, and for those skilled in the art, other drawings can be obtained according to the provided drawings without creative efforts.
FIG. 1 is a flow chart of the present invention.
Detailed Description
The invention provides a preparation method of vinegar schisandra chinensis, which comprises the following steps:
(1) mixing fructus Schisandrae chinensis with rice vinegar, moistening, and air drying;
(2) steaming the dried schisandra chinensis obtained in the step (1), and collecting a steaming liquid;
(3) mixing the steamed fructus Schisandrae with the steam, and drying.
In the invention, the mass ratio of the schisandra chinensis to the rice vinegar in the step (1) is 4-6: 1.
In the invention, the moistening time in the step (1) is 2-4 h; preferably 3 hours.
In the invention, the step (1) is carried out until the water content of the schisandra chinensis is 25-35%; preferably 27-33%; further preferably 29-31%; more preferably 30%.
In the invention, the steaming temperature in the step (2) is 80-100 ℃; preferably 84-96 ℃; further preferably 88-92 ℃; more preferably 90 deg.c.
In the invention, the steaming time in the step (2) is 2-4 h; preferably for 3 hours.
In the invention, the drying temperature in the step (3) is less than 80 ℃; preferably 55-75 ℃; further preferably 60-70 ℃; more preferably 65 deg.c.
In the invention, the drying in the step (3) is carried out until the water content of the schisandra chinensis is less than 16 percent; preferably 13-15%; further preferably 14%.
In the invention, the thickness of the paving material in the drying process in the step (3) is less than 3cm, and the paving material is stirred for 2-4 times every day; preferably, the spreading thickness is 1.5-2.5 cm, and the mixture is stirred for 3 times every day; more preferably, the layer is 2cm thick and stirred 3 times a day.
The technical solutions provided by the present invention are described in detail below with reference to examples, but they should not be construed as limiting the scope of the present invention.
Example 1
A preparation method of vinegar schisandra chinensis comprises the following steps:
(1) placing the cleaned fructus Schisandrae (impurity ratio is less than 1%) in a clean medicine-mixing box, adding rice vinegar (mass ratio of fructus Schisandrae to rice vinegar is 4:1), stirring, moistening for 2 hr, and air drying until water content of fructus Schisandrae reaches 25%;
(2) steaming the dried schisandra chinensis obtained in the step (1) for 2 hours at 80 ℃, collecting steaming liquid in the steaming process, mixing the collected steaming liquid back when vinegar is completely absorbed and the surface is black, and cooling;
(3) drying cooled fructus Schisandrae at 55 deg.C until the water content of fructus Schisandrae is 13%, spreading to a thickness of 1.5cm during drying, stirring for 2 times per day, drying, packaging, sealing to obtain final product, and warehousing.
Example 2
A preparation method of vinegar schisandra chinensis comprises the following steps:
(1) placing the cleaned fructus Schisandrae (impurity ratio is less than 1%) in a clean medicine-mixing box, adding rice vinegar (mass ratio of fructus Schisandrae to rice vinegar is 6:1), stirring, moistening for 4 hr, and air drying until water content of fructus Schisandrae reaches 35%;
(2) steaming the dried schisandra chinensis obtained in the step (1) for 4 hours at 100 ℃ by using a steam box, collecting steam liquid in the steaming process, mixing the collected steam liquid back when vinegar is completely absorbed and the surface is black, and taking out the mixture and cooling the mixture;
(3) drying cooled fructus Schisandrae at 75 deg.C until the water content of fructus Schisandrae is 15%, spreading to a thickness of 2.5cm during drying, stirring for 4 times per day, drying, packaging, sealing to obtain final product, and warehousing.
Example 3
A preparation method of vinegar schisandra chinensis comprises the following steps:
(1) placing the cleaned fructus Schisandrae (impurity ratio is less than 1%) in a clean medicine mixing box, adding rice vinegar (mass ratio of fructus Schisandrae to rice vinegar is 5:1), stirring, moistening for 3 hr, and air drying until water content of fructus Schisandrae reaches 30%;
(2) steaming the dried schisandra chinensis in the step (1) for 3 hours at 90 ℃ by using a steam box, collecting the steam in the steaming process, mixing the collected steam back when the vinegar is completely absorbed and the surface is black, taking out, and cooling;
(3) drying cooled fructus Schisandrae at 65 deg.C until the water content of fructus Schisandrae is 14%, spreading with a thickness of 2cm during drying, stirring for 3 times per day, drying, automatically packaging, sealing to obtain final product, and warehousing.
The foregoing is only a preferred embodiment of the present invention, and it should be noted that, for those skilled in the art, various modifications and amendments can be made without departing from the principle of the present invention, and these modifications and amendments should also be considered as the protection scope of the present invention.

Claims (8)

1. The preparation method of vinegar schisandra chinensis is characterized by comprising the following steps:
(1) mixing fructus Schisandrae with rice vinegar, moistening, and air drying;
(2) steaming the dried schisandra chinensis obtained in the step (1), and collecting a steaming liquid;
(3) mixing the steamed fructus Schisandrae with the steam, and drying.
2. The method for preparing vinegar-processed schisandra chinensis as claimed in claim 1, wherein the moistening time in step (1) is 2-4 h.
3. The preparation method of vinegar-processed schisandra chinensis as claimed in claim 1, wherein the air-drying step (2) is performed until the moisture content of schisandra chinensis is 25-35%.
4. The preparation method of vinegar-processed schisandra chinensis as claimed in claim 1, wherein the steaming temperature in the step (2) is 80-100 ℃, and the steaming time is 2-4 h.
5. The method for preparing vinegar-processed schisandra chinensis as claimed in claim 1, wherein the temperature of drying in step (3) is less than 80 ℃.
6. The method for preparing vinegar-processed schisandra chinensis as claimed in claim 1, wherein the drying step (3) is performed until the moisture content of schisandra chinensis is less than 16%.
7. The preparation method of vinegar-processed schisandra chinensis as claimed in claim 1, wherein the thickness of the paving material in the drying process of step (3) is less than 3cm, and the stirring is performed 2-4 times per day.
8. The preparation method of vinegar-processed schisandra chinensis as claimed in claim 1, wherein the mass ratio of the schisandra chinensis to the rice vinegar in the step (1) is 4-6: 1.
CN202210618556.1A 2022-06-01 2022-06-01 Preparation method of vinegar schisandra chinensis Pending CN114767761A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116763845A (en) * 2023-08-03 2023-09-19 陕西中医药大学 Preparation method of shizandra berry decoction pieces

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110251583A (en) * 2019-07-23 2019-09-20 江苏红豆杉中药饮片有限公司 A kind of preparation method of steamed FRUCTUS SCHISANDRAE with vinegar medicine materical crude slice

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110251583A (en) * 2019-07-23 2019-09-20 江苏红豆杉中药饮片有限公司 A kind of preparation method of steamed FRUCTUS SCHISANDRAE with vinegar medicine materical crude slice

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116763845A (en) * 2023-08-03 2023-09-19 陕西中医药大学 Preparation method of shizandra berry decoction pieces

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