CN114767599A - 一种滋养护肤洗手液及其制备方法 - Google Patents
一种滋养护肤洗手液及其制备方法 Download PDFInfo
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- CN114767599A CN114767599A CN202210577500.6A CN202210577500A CN114767599A CN 114767599 A CN114767599 A CN 114767599A CN 202210577500 A CN202210577500 A CN 202210577500A CN 114767599 A CN114767599 A CN 114767599A
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- skin
- nourishing
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Abstract
本申请公开了一种滋养护肤洗手液,其包括以下质量百分数的组分:表面活性剂1.5‑25wt%;pH调节剂0.05‑0.2wt%;保湿剂5‑12wt%;皮肤调理剂0.1‑0.2wt%;抗氧化剂0.5‑5wt%;余量为水;上述滋养护肤洗手液的制备方法,包括以下步骤:(1)将表面活性剂、pH调节剂及(65‑85)%保湿剂加到水中,搅拌至液体呈澄清透明状得到A相;(2)将皮肤调理剂、抗氧化剂及剩余的保湿剂添加至A相中,搅拌至液体呈澄清透明状,得到滋养护肤洗手液。本申请具有温和亲肤、保湿锁水、滋润肌肤的效果。
Description
技术领域
本申请涉及日用品领域,尤其是涉及一种滋养护肤洗手液及其制备方法。
背景技术
随着人们生活水平的提高,洗手液代替传统的香皂成为普遍使用的手部清洁用品。洗手液是一种用来清洁手部的护肤清洁液,通过以机械摩擦和表面活性剂的作用,配合水流或不需要水来清除手上的污垢和附着的细菌。
洗手液的主要成分为表面活性剂和增稠剂,表面活性剂的功能是去除手上的油污和污垢,增稠剂使产品具有适宜的粘度和稳定性。除此之外,现有大多数洗手液中都含有酒精,从而使细菌中的蛋白质变性从而起到杀菌消毒的作用,而洗手液中如果使用酒精浓度不足60%是达不到杀菌目的的,酒精浓度在60%-80%之间才能达到杀菌或抑菌效果,但发明人发现,如果长时间使用酒精浓度超过60%的洗手液容易对皮肤造成损伤,导致手部皮肤干燥、粗糙。
发明内容
针对上述现有技术,本申请目的是提供一种温和亲肤、保湿锁水、滋润肌肤的洗手液。
本申请的上述技术目的是通过以下技术方案得以实现的:
一种滋养护肤洗手液,包括以下质量百分数的组分:
表面活性剂1.5-25wt%;
pH调节剂0.05-0.2wt%;
保湿剂5-12wt%;
皮肤调理剂0.1-0.2wt%;
抗氧化剂0.5-5wt%;
余量为水。
上述滋养护肤洗手液的制备方法,包括以下步骤:
(1)将表面活性剂、pH调节剂及(65-85)%保湿剂加到水中,搅拌至液体呈澄清透明状得到A相;
(2)将皮肤调理剂、抗氧化剂及剩余的保湿剂添加至A相中,搅拌至液体呈澄清透明状,得到滋养护肤洗手液。
优选的,所述保湿剂和皮肤调理剂的质量比为(40-60):1。
优选的,所述保湿剂和抗氧化剂的质量比为(10-12):(1-5)。
优选的,所述保湿剂由甘油、1,2-己二醇、玉米谷蛋白氨基酸类、薰衣草花提取物、茶叶提取物、牛油果树提取物、玫瑰花提取物、泛醇复配而成。
优选的,所述皮肤调理剂为烟酰胺和腺苷的复配。
优选的,所述抗氧化剂为对米糠油或珊瑚菌提取物中的至少一种与对羟基苯乙酮的组合物。
优选的,所述抗氧化剂为对羟基苯乙酮、米糠油和珊瑚菌提取物的复配,所述对羟基苯乙酮、米糠油和珊瑚菌提取物三者复配的质量比为(30-40):(2-8)(2-8)
优选的,所述pH调节剂选自柠檬酸、甘草酸、琥珀酸中的至少一种。
优选的,所述表面活性剂选自月桂醇聚醚硫酸酯钠、椰油酰两性基乙酸钠、椰油酰胺丙基甜菜碱、月桂酰基谷氨酸钠、卵磷脂中的至少一种。
综上所述,本申请包括以下至少一种有益技术效果:
通过保湿剂和皮肤调理剂协同促进,能渗透进角质层发挥作用,起到了促进吸收、长效保湿和功能;同时还与抗氧化剂协同配合,起到抗氧化功能;而保湿剂、皮肤调理剂、抗氧化剂和表面活性剂之间相互协同,起到清洁、杀菌的同时,能够加倍提升肌肤含水量和储水功能,细致肌肤纹理,滋润肌肤。
具体实施方式
以下结合具体实施例对本申请作进一步详细说明。
本申请实施例中,一种滋养护肤洗手液,包括以下质量百分数的组分:
表面活性剂15-25wt%;
pH调节剂0.05-0.2wt%;
保湿剂5-12wt%;
皮肤调理剂0.1-0.2wt%;
抗氧化剂0.5-5wt%;
余量为水。
本申请中,通过调控表面活性剂、pH调节剂、保湿剂、皮肤调理剂、抗氧化剂和水之间的比例,各组分相互协同,获得一种具有优良清洁、杀菌抑菌效果,同时还能够加倍提升肌肤含水量和储水功能、细致肌肤纹理、滋润肌肤的洗手液。
在本申请实施例中,所述保湿剂和皮肤调理剂的质量比为(40-60):1。
本申请中,通过调节保湿剂和皮肤调理剂之间的比例,在皮肤调理剂的作用下,保湿剂能够快速渗透皮肤,从而发挥其深层清洁肌肤污垢,并发挥其保湿和锁水作用,有助于改善皮肤干燥状态;同时保湿剂中的营养物质还能够快速被肌肤吸收,使老化的表皮恢复弹性,延缓手部皮肤衰老,提高皮肤抗自由基能力,并为皮肤提供充足的营养,滋润手部肌肤。
在本申请实施例中,所述保湿剂和抗氧化剂的质量比为(10-12):(1-5)。
本申请中,抗氧化剂不仅能够帮助肌肤捕获并中和自由基,从而祛除自由基对皮肤的损害,而且能够和保湿剂组合,深入手部肌肤内部并保持高活性,保湿抗氧化。
在本申请实施例中,所述表面活性剂选自月桂醇聚醚硫酸酯钠、椰油酰两性基乙酸钠、椰油酰胺丙基甜菜碱、月桂酰基谷氨酸钠、卵磷脂中的至少一种;优选为其中三者以上配伍使用。
本申请中,采用表面活性剂自身的吸附、降低表面张力、渗透、乳化、增溶、分散等作用,使产品产生丰富的泡沫,赋予产品优良的脱脂、脱灰的去污力。采用阴离子表面活性剂和两性离子表面活性剂的配伍使用,不仅具有高效且均匀的渗透性,能够快速渗透油污到达皮肤表面,从而使由于快速剥离,加快清洁效率;而且表面活性剂水溶液呈弱酸性,对皮肤极为柔和,不引起过敏;同时,采用两性离子表面活性剂和阴离子表面活性剂配伍后能够和保湿剂、抗氧化剂、皮肤调理剂和水等其他物质形成均一、稳定的体系。
在本申请实施例中,所述pH调节剂选自柠檬酸、甘草酸、琥珀酸中的至少一种;优选为其中两种以上配伍使用。
本申请中,柠檬酸、甘草酸和琥珀酸均为有机酸,能够更好地和保湿剂、皮肤调理剂等配伍,除了作为pH调节剂外,柠檬酸、甘草酸和琥珀酸还能够使该洗手液获得抗炎、抗菌的作用,而且能够增强保湿剂、皮肤调理剂和抗氧化剂的活性,进而增强该洗手液的保湿、滋润、抗氧化、调理等疗效。
在本申请实施例中,所述保湿剂由甘油、1,2-己二醇、玉米谷蛋白氨基酸类、薰衣草花提取物、茶叶提取物、牛油果树提取物、玫瑰花提取物、泛醇复配而成。
本申请中,甘油和1,2-己二醇作为主要保湿成分,玉米谷蛋白氨基酸类、薰衣草花提取物、茶叶提取物、牛油果树提取物、玫瑰花提取物均为天然植物提取物,富含多种萜烯类化合物、黄酮类化合物、酚酸类化合物、酚类等活性成分,除了其本申请能够补充手部皮肤所需的维生素、微量元素等,起到活肤、保湿、防衰抗氧化、抗菌抗炎等作用外,还能够促进甘油、1,2-己二醇、泛醇以及皮肤调理剂的吸收。
在本申请优选实施例中,所述保湿剂中,玉米谷蛋白氨基酸类、薰衣草花提取物、茶叶提取物、牛油果树提取物、玫瑰花提取物复配的质量比为(3-5):(2-5):(2-5):(1-5):(1-5)。
在本申请实施例中,所述皮肤调理剂为烟酰胺和腺苷的复配;优选实施例为,所述烟酰胺占皮肤调理剂的85%-92%。
本申请中,腺苷能够直接深入肌肤内层,促进肌肤对烟酰胺的吸收,烟酰胺与保湿剂配伍使用后,能够有效滋润保湿肌肤,改善皮肤干燥、粗糙、脱皮等问题。
同时,保湿剂中的活性成分能够提高烟酰胺和腺苷进入皮肤的能力,同时降低高浓度烟酰胺的刺激性,对皮肤柔和,使皮肤不易过敏。
在本申请实施例中,所述抗氧化剂为对米糠油或珊瑚菌提取物中的至少一种与对羟基苯乙酮的组合物。
在本申请实施例中,所述抗氧化剂为对羟基苯乙酮、米糠油和珊瑚菌提取物的复配,所述对羟基苯乙酮、米糠油和珊瑚菌提取物三者复配的质量比为(30-40):(2-8)(2-8)。
本申请中,米糠油和珊瑚菌提取物作为提取物,富含丰富的维生素、氨基酸,不仅皮肤易吸收,而且其与皮肤调理剂和保湿剂配伍使用后,能够发挥协同作用,从而有效延缓手部皮肤衰老,提高皮肤抗自由基能力,并为皮肤提供充足的营养,滋润手部肌肤,增强保湿效果;同时还能够与pH调理剂、保湿剂配合,发挥协同作用,从而抵抗炎症、抗过敏。
与此同时,保湿剂、pH调理剂和抗氧化剂中含有多种具有芳香气味的物质,能够赋予该洗手液自然清香,无需额外添加香精即可获得扑鼻的清香感受。
在本申请实施例中,所述米糠油的通过下述方法制备得到:将新鲜米糠在65-78℃条件下预处理30min后降温至50℃,加入pH5-6的酸性水溶液,酸性水溶液的加入量为新鲜米糠的60-70倍,调节pH至6.0后加入纤维素酶和木瓜蛋白酶,搅拌60-90min后冷却离心,取上层液加入正己烷进行萃取后得到米糠油。
在本申请实施例中,上述方法中,纤维素酶的加入量为新鲜米糠的0.5%,木瓜蛋白酶的加入量为新鲜米糠的0.65%。
在上述方法中涉及到的酸性水溶液中的酸选自醋酸或柠檬酸。
对羟基苯乙酮一般作为防腐剂应用,但是当对羟基苯乙酮和由新鲜米糠制得的米糠油组合使用后,对羟基苯乙酮能够提升米糠油在洗手液中的抗氧化活性,同时由于对羟基苯乙酮的添加能够保持产品的新鲜度,避免细菌或真菌入侵导致米糠油变质,使洗手液具有长效抑菌、抗氧化、保湿和滋润肌肤的作用。
在本申请实施例中,所述珊瑚菌提取物通过下述方法制备得到:将阴干的珊瑚菌粉碎为粉末,加入pH值为4-5的酸性水溶液,酸性水溶液的加入量为珊瑚菌粉末的40-50倍,在45-55℃温度下水浴搅拌45-60min后过滤,取滤液进行减压浓缩后得到珊瑚菌提取物。
在上述方法中涉及到的酸性水溶液选自醋酸或柠檬酸。
由酸性水溶液浸提及减压浓缩的方法制得的珊瑚菌提取物中不引入其他对皮肤有害的物质,产品性质稳定;且对羟基苯乙酮的添加能够避免细菌或真菌入侵珊瑚菌提取物,使珊瑚菌提取物中的活性物质的保持其高活性,具有长效抗氧化、抗炎作用。
在本申请实施例中,所述洗手液还包括增稠剂,所述增稠剂选自EDTA二钠、海藻酸钠、羊毛脂、黄原胶、鲸蜡羟乙基纤维素中的至少一种;采用增稠剂后能够形成均一、稳定的体系。
在本申请实施例中,所述洗手液还包括Cl19140或Cl14700中的至少一种色素;在本申请实施例中,所述洗手液还包括香精。
本申请中,通过添加的色素和香精与其中的天然植物提取物以及部分有香味和颜色的物质配伍使用,赋予该洗手液浓郁的清香味道和颜色。
本申请还公开一种滋养护肤洗手液的制备方法,包括以下步骤:
(1)将表面活性剂、pH调节剂及(65-85)%保湿剂加到水中,搅拌至液体呈澄清透明状得到A相;
(2)将皮肤调理剂、抗氧化剂及剩余的保湿剂添加至A相中,搅拌至液体呈澄清透明状,得到滋养护肤洗手液。
以下根据具体实施例对本申请技术方案进行说明。
制备例1
米糠油的制备步骤如下:将1kg新鲜米糠在68℃条件下热烘预处理30min后降温至50℃,加入pH5的柠檬酸水溶液,柠檬酸水溶液的加入量为新鲜米糠重量的60倍,调节pH至6.0后加入纤维素酶和木瓜蛋白酶,搅拌60min后冷却离心,取上层液加入正己烷进行萃取后得到米糠油。
上述方法中,纤维素酶的加入量为新鲜米糠的0.5%,木瓜蛋白酶的加入量为新鲜米糠的0.65%。
制备例2
珊瑚菌提取物的制备方法如下:将1kg阴干的珊瑚菌粉碎为粉末,过80目筛,加入pH值为4的柠檬酸水溶液,柠檬酸水溶液的加入量为珊瑚菌粉末的40倍,在50℃温度下水浴搅拌45min后过滤,取滤液进行减压浓缩后得到珊瑚菌提取物。
实施例1-6
一种滋养护肤洗手液,采用以下步骤制备:
(1)乳化锅投入水、表面活性剂和甘油,搅拌溶解,搅拌速度为25±5r/min,搅拌约20min后添加pH调节剂,继续搅拌至液体澄清透明,得到A相;
(2)向A相中添加皮肤调理剂、抗氧剂、增稠剂、色素、香精及除甘油外的其他保湿剂,搅拌溶解,搅拌速度为25±5r/min,搅拌至液体澄清透明,得到滋养护肤洗手液。
实施例1-6中各组分添加量见下表。
表1
表2
对比例1
与实施例1的区别在于,采用等量的75%乙醇替换pH调节剂、保湿剂、皮肤调理剂和抗氧化剂。
对比例2
与实施例1的区别在于,采用等量的60%乙醇替换pH调节剂、保湿剂、皮肤调理剂和抗氧化剂。
以上实施例和对比例制得的产品各取50g作为样品进行以下测试:
1、在手背上用油性笔进行划线,划线数量为20条,在干燥状态下,将样品对划线处以打圈方式进行清洗,清洗3分钟,然后用清水冲洗;(1)观察记录划线清晰度;(2)测定初始皮肤表面水分含量,静置30分钟后,测定后期皮肤表面水分含量,通过公式:(初始皮肤表面水分含量-后期皮肤表面水分含量)/初始皮肤表面水分含量*100%计算水分流失率;
2、在手背上用水性笔进行划线,划线数量为20条,在干燥状态下,将样品对划线处以同样力道打圈方式进行清洗,清洗3分钟,然后用清水冲洗;(1)观察记录划线清晰度;(2)测定初始皮肤表面水分含量,静置30分钟后,测定后期皮肤表面水分含量,通过公式:(初始皮肤表面水分含量-后期皮肤表面水分含量)/初始皮肤表面水分含量*100%计算水分流失率;
3、将制得的产品放入盒内加盖遮光静置保存6个月,开盖后观察表面是否存在分层;
4、稳定性(耐寒、耐热性能测试):按照GB/T34855-2017中规定的方法检验;
5、抑菌试验:按照GB/T34857-2017中规定的方法检验;
1)菌种
大肠杆菌Escherichia coli ATCC24752
金黄色葡萄球菌Staphylocouusaureus ATCC 6538
白色念珠菌Moniliaalbican ATCC 10231
2)方法
将上述各菌种进行菌种复苏,培养至对数生长期,用培养基稀释到105~106CFU/ml,采用涂布器将稀释的菌液均匀涂在固体培养基上。
3)抑菌效果试验
在手背上进行试验,清洗手背前根据测定细菌总数的要求进行采样,然后用洗手液按一般洗手的方法进行清洗手背,清洗持续时间在40s~60s,最后在流动水下冲净。清洗完后进行采样,将采集的样品稀释后与液化的琼脂培养基混合,在37℃下培养24h后,根据培养基上的菌落数计算样品中的细菌总数;通过公式:(清洗前菌落数-清洗后菌落数)/清洗前菌落数*100%计算去菌率;
6、敏感测试:
选24个肤质一般的志愿者和选24个肤质敏感的志愿者,分别取样品,清洗手上皮肤,每天早晚各试用一次,连续试用三天,测试反馈填入下表。
测试结果如下:
表3
表4
综上,可以看出采用本申请技术方案制得的产品使用后,水分流失率保持在10%以下,可以很好地保持手部皮肤的湿度,避免产生手部干燥、粗糙的现象,而且产品稳定性好、抗菌抑菌效果好。
本具体实施例仅仅是对本申请的解释,其并不是对本申请的限制,本领域技术人员在阅读完本说明书后可以根据需要对本实施例做出没有创造性贡献的修改,但只要在本申请的权利要求范围内都受到专利法的保护。
Claims (10)
1.一种滋养护肤洗手液,其特征在于,包括以下质量百分数的各组分:
表面活性剂15-25wt%;
pH调节剂0.05-0.2wt%;
保湿剂5-12wt%;
皮肤调理剂0.1-0.2wt%;
抗氧化剂0.5-5wt%;
余量为水。
2.根据权利要求1所述的滋养护肤洗手液,其特征在于:所述保湿剂和皮肤调理剂的质量比为(40-60):1。
3.根据权利要求1所述的滋养护肤洗手液,其特征在于:所述保湿剂和抗氧化剂的质量比为(10-12):(1-5)。
4.根据权利要求1所述的滋养护肤洗手液,其特征在于:所述保湿剂由甘油、1,2-己二醇、玉米谷蛋白氨基酸类、薰衣草花提取物、茶叶提取物、牛油果树提取物、玫瑰花提取物、泛醇复配而成。
5.根据权利要求1所述的滋养护肤洗手液,其特征在于:所述皮肤调理剂为烟酰胺和腺苷的复配。
6.根据权利要求1所述的滋养护肤洗手液,其特征在于:所述抗氧化剂为对米糠油或珊瑚菌提取物中的至少一种与对羟基苯乙酮的组合物。
7.根据权利要求6所述的滋养护肤洗手液,其特征在于:所述抗氧化剂为对羟基苯乙酮、米糠油和珊瑚菌提取物的复配,所述对羟基苯乙酮、米糠油和珊瑚菌提取物三者复配的质量比为(30-40):(2-8)(2-8)。
8.根据权利要求1所述的滋养护肤洗手液,其特征在于:所述pH调节剂选自柠檬酸、甘草酸、琥珀酸中的至少一种。
9.根据权利要求1所述的滋养护肤洗手液,其特征在于:所述表面活性剂选自月桂醇聚醚硫酸酯钠、椰油酰两性基乙酸钠、椰油酰胺丙基甜菜碱、月桂酰基谷氨酸钠、卵磷脂中的至少一种。
10.权利要求1-9任一所述的一种滋养护肤洗手液的制备方法,其特征在于:
(1)将表面活性剂、pH调节剂及(65-85)%保湿剂加到水中,搅拌至液体呈澄清透明状得到A相;
(2)将皮肤调理剂、抗氧化剂及剩余的保湿剂添加至A相中,搅拌至液体呈澄清透明状,得到滋养护肤洗手液。
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