CN114766510A - Domestic drinking water disinfection powder and preparation method thereof - Google Patents

Domestic drinking water disinfection powder and preparation method thereof Download PDF

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Publication number
CN114766510A
CN114766510A CN202210565901.XA CN202210565901A CN114766510A CN 114766510 A CN114766510 A CN 114766510A CN 202210565901 A CN202210565901 A CN 202210565901A CN 114766510 A CN114766510 A CN 114766510A
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China
Prior art keywords
powder
drinking water
sodium
domestic drinking
disinfection
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CN202210565901.XA
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Chinese (zh)
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刘利达
刘利方
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Shandong Runxing Environmental Protection Technology Co ltd
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Shandong Runxing Environmental Protection Technology Co ltd
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/06Aluminium; Calcium; Magnesium; Compounds thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/22Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing ingredients stabilising the active ingredients
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/64Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with three nitrogen atoms as the only ring hetero atoms
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds

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  • Life Sciences & Earth Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Dentistry (AREA)
  • Pest Control & Pesticides (AREA)
  • Plant Pathology (AREA)
  • Engineering & Computer Science (AREA)
  • Agronomy & Crop Science (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical & Material Sciences (AREA)
  • Toxicology (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention relates to the technical field of disinfection powder, in particular to domestic drinking water disinfection powder and a preparation method thereof, which can reduce the cost of domestic drinking water disinfection, improve the storage stability of the drinking water disinfection powder and improve the storage convenience of the disinfection powder; comprises sodium hypochlorite, calcium hydroxide, sodium dichloroisocyanurate, auxiliary powder and stabilizing powder, and the mass percentages are respectively as follows: 10-20% of sodium hypochlorite, 30-45% of calcium hydroxide, 10-25% of sodium dichloroisocyanurate and the balance of auxiliary powder and stable powder mixture.

Description

Domestic drinking water disinfection powder and preparation method thereof
Technical Field
The invention relates to the technical field of disinfection powder, in particular to domestic drinking water disinfection powder and a preparation method thereof.
Background
The disinfection powder is a sterilization drug, is suitable for the sterilization and disinfection of pathogenic microorganisms such as bacteria, viruses, fungi and the like, is mainly used in public places such as hospitals, hotels, hair salons and the like, and the conventional disinfection methods for drinking water such as ozone disinfection, ultraviolet disinfection and the like at present can effectively kill bacteria, but have the condition of higher equipment cost, and the conventional liquid disinfectant on the market has the conditions of inconvenient transportation and easy evaporation in the storage process, so the domestic drinking water disinfection powder which is convenient to store and improves the disinfection effect is provided.
Disclosure of Invention
In order to solve the technical problems, the invention provides the domestic drinking water disinfectant powder and the preparation method thereof, wherein the cost of disinfecting the domestic drinking water is reduced, the storage stability of the drinking water disinfectant powder is improved, and the storage convenience of the disinfectant powder is improved.
The invention relates to a domestic drinking water disinfection powder, which comprises sodium hypochlorite, calcium hydroxide, sodium dichloroisocyanurate, auxiliary powder and stable powder, and the domestic drinking water disinfection powder comprises the following components in percentage by mass: 10-20% of sodium hypochlorite, 30-45% of calcium hydroxide, 10-25% of sodium dichloroisocyanurate and the balance of auxiliary powder and stable powder mixture.
Preferably, the auxiliary powder comprises citric acid, sorbic acid and hygroscopic powder;
the weight percentages are respectively as follows: 1-8% of citric acid and 1-8% of sorbic acid.
Preferably, the stabilizing powder comprises one of sodium oxide or ethylenediamine tetraacetic acid;
the weight percentages are as follows: 1-4% of sodium oxide or ethylenediamine tetraacetic acid.
Preferably, the moisture absorbent comprises one of sodium sulfate or sodium chloride;
the weight percentages are respectively as follows: 1 to 3 percent of sodium sulfate or sodium chloride.
The invention relates to a preparation method of domestic drinking water disinfection powder, which comprises the following steps:
step 1, weighing raw materials: respectively weighing sodium hypochlorite, calcium hydroxide, sodium dichloroisocyanurate, citric acid, sorbic acid, sodium oxide or ethylenediamine tetraacetic acid, sodium sulfate or sodium chloride powder;
step 2, screening and filtering: respectively placing the raw material powder into screening equipment, screening the granular raw materials in a vibration screening mode, and placing the separated small granular raw materials into a container together for storage for later use;
step 3, crushing materials: putting the large particle raw materials subjected to vibration screening into a rolling crusher for rolling and crushing, returning the crushed particle raw materials to the vibration screening in the step 2 until the raw material particles are completely filtered, and putting the raw material particles into a container together for later use;
step 4, mixing and stirring: putting the raw material particles in the container into a stirrer for mixing and stirring;
step 5, air drying treatment: conveying dry air into the stirrer in a bottom air supply mode, and drying raw materials in the stirrer in a stirring process to obtain drinking water disinfection powder;
and 6, packaging: lifting and conveying the drinking water disinfectant powder to filling equipment in a spiral belt conveying mode, and sealing and packaging the drinking water disinfectant powder.
Preferably, the particle raw material in the step 2 is screened by a screen with 80-120 meshes for 2-3 times in a vibration mode.
Preferably, in the step 4, the stirrer adopts a single stirring paddle, the rotating speed of the stirring paddle is 60-90 r/min, clockwise stirring is adopted for 15-20 min, and anticlockwise stirring is adopted for 15-20 min.
Preferably, the air drying temperature in the step 5 is 5-12 ℃, the air drying is firstly carried out clockwise for 5-8 min, the air drying temperature is 9-12 ℃ clockwise, then the air drying is carried out counterclockwise for 5-8 min, and the air drying temperature is 5-7 ℃ counterclockwise.
Preferably, in the step 4, the height of the granular raw material put into the stirrer is not more than 1/2 of the stirrer.
Compared with the prior art, the invention has the beneficial effects that: through making sodium hypochlorite, calcium hydroxide, dichloro isocyanuric acid sodium, supplementary powder and stable powder mixed processing into the disinfection powder, effectively improve life drinking water disinfection effect, reduce the sterile cost of life drinking water, improve the storage stability of drinking water disinfection powder, simultaneously through with drinking water disinfection powder seal packing, reduce the condition that the disinfection powder stored or wet in the transportation, improve the storage convenience of disinfection powder.
Drawings
FIG. 1 is a schematic flow diagram of the present invention.
Detailed Description
To facilitate an understanding of the invention, the invention will now be described more fully hereinafter with reference to the accompanying drawings. The present invention may be embodied in many different forms and is not limited to the embodiments described herein. Rather, these embodiments are provided so that this disclosure will be thorough and complete.
Example 1
The weight percentages are respectively as follows: 10-20% of sodium hypochlorite, 30-45% of calcium hydroxide, 10-25% of sodium dichloroisocyanurate, 1-8% of citric acid, 1-8% of sorbic acid, 1-4% of sodium oxide or ethylene diamine tetraacetic acid and sodium sulfate or sodium chloride; the disinfectant powder is prepared by mixing sodium hypochlorite, calcium hydroxide, sodium dichloroisocyanurate, auxiliary powder and stabilizing powder, so that the disinfection effect of the drinking water is effectively improved, the disinfection cost of the drinking water is reduced, and the storage stability of the drinking water disinfectant powder is improved.
Example 2
The weight percentages are respectively as follows: 10 to 20 percent of sodium hypochlorite, 30 to 45 percent of calcium hydroxide, 10 to 25 percent of sodium dichloroisocyanurate, 1 to 8 percent of citric acid, 1 to 8 percent of sorbic acid, 1 to 4 percent of sodium oxide or ethylene diamine tetraacetic acid and sodium sulfate or sodium chloride are respectively weighed, the sodium hypochlorite, the calcium hydroxide, the sodium dichloroisocyanurate, the citric acid, the sorbic acid, the sodium oxide or ethylene diamine tetraacetic acid, the sodium sulfate or sodium chloride powder are respectively put into a screening device, the raw material powder is respectively placed into a screening device for screening by adopting a vibration screening mode, the separated small particle raw materials are together put into a container for storage, the large particle raw materials screened by vibration are put into a rolling crusher for rolling and crushing, the crushed particle raw materials are returned to the vibration screening in the step 2 until the raw material particles are completely filtered, and then the raw material particles are together put into the container for standby, putting raw material particles in a container into a stirrer for mixing and stirring, conveying dry air into the stirrer in a bottom air supply mode, drying the raw material in the stirrer in a stirring process to obtain drinking water disinfectant powder, lifting and conveying the drinking water disinfectant powder to filling equipment in a spiral belt conveying mode, and sealing and packaging the drinking water disinfectant powder; through making sodium hypochlorite, calcium hydroxide, dichloro isocyanuric acid sodium, supplementary powder and stable powder mixed processing into the disinfection powder, effectively improve life drinking water disinfection effect, reduce the sterile cost of life drinking water, improve the storage stability of drinking water disinfection powder, simultaneously through with drinking water disinfection powder seal packing, reduce the condition that the disinfection powder stored or wet in the transportation, improve the storage convenience of disinfection powder.
As shown in figure 1, the invention relates to a domestic drinking water disinfection powder and a preparation method thereof, during operation, sodium hypochlorite, calcium hydroxide, sodium dichloroisocyanurate, citric acid, sorbic acid, sodium oxide or ethylene diamine tetraacetic acid, sodium sulfate or sodium chloride powder are respectively weighed, the raw material powder is respectively placed in a screening device, particle raw materials are screened by adopting a vibration screening mode, separated small particle raw materials are together placed in a container for standby, then large particle raw materials screened by vibration are placed in a crusher for crushing by rolling, the crushed particle raw materials are screened by vibration until the raw material particles are completely filtered, the raw material particles are together placed in the container for standby, then the raw material particles in the container are placed in a stirrer for mixing and stirring, then dry air is conveyed into the stirrer by adopting a bottom air supply mode, so that the raw materials in the stirrer are dried during the stirring process, then obtaining the disinfection powder for drinking water.
The main functions realized by the invention are as follows: through with sodium hypochlorite, calcium hydroxide, dichloro isocyanuric acid sodium, the disinfection powder is made to supplementary powder and stable powder blending, effectively improves life drinking water disinfection effect, green reduces disinfection powder self to the health hazard of human body, reduces the disinfected cost of life drinking water, improves the storage stability of drinking water disinfection powder, simultaneously through with drinking water disinfection powder seal package, reduce the condition that the disinfection powder stored or wet in the transportation, improve the storage convenience of disinfection powder.
All technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs. The terminology used in the description of the invention herein is for the purpose of describing particular embodiments only and is not intended to be limiting of the invention. As used herein, the term "and/or" includes any and all combinations of one or more of the associated listed items.
The above description is only a preferred embodiment of the present invention, and it should be noted that, for those skilled in the art, several modifications and variations can be made without departing from the technical principle of the present invention, and these modifications and variations should also be regarded as the protection scope of the present invention.

Claims (9)

1. The domestic drinking water disinfection powder is characterized by comprising sodium hypochlorite, calcium hydroxide, sodium dichloroisocyanurate, auxiliary powder and stable powder, and the domestic drinking water disinfection powder comprises the following components in percentage by mass: 10-20% of sodium hypochlorite, 30-45% of calcium hydroxide, 10-25% of sodium dichloroisocyanurate and the balance of auxiliary powder and stable powder mixture.
2. The disinfection powder for domestic drinking water as claimed in claim 1, wherein said auxiliary powders comprise citric acid, sorbic acid and hygroscopic powders;
the weight percentages are as follows: 1-8% of citric acid and 1-8% of sorbic acid.
3. The domestic drinking water disinfectant powder according to claim 1, wherein said stabilizing powder comprises one of sodium oxide or ethylenediaminetetraacetic acid;
the weight percentages are respectively as follows: 1-4% of sodium oxide or ethylenediamine tetraacetic acid.
4. The domestic drinking water disinfectant powder according to claim 1, wherein said hygroscopic agent comprises one of sodium sulfate or sodium chloride;
the weight percentages are respectively as follows: 1 to 3 percent of sodium sulfate or sodium chloride.
5. A preparation method of domestic drinking water disinfection powder is characterized by comprising the following steps:
step 1, weighing raw materials: respectively weighing sodium hypochlorite, calcium hydroxide, sodium dichloroisocyanurate, citric acid, sorbic acid, sodium oxide or ethylene diamine tetraacetic acid, sodium sulfate or sodium chloride powder;
step 2, screening and filtering: respectively placing the raw material powder into screening equipment, screening the granular raw materials in a vibration screening mode, and placing the separated small granular raw materials into a container together for storage for later use;
step 3, crushing materials: putting the large particle raw materials subjected to vibration screening into a rolling crusher for rolling and crushing, returning the crushed particle raw materials to the vibration screening in the step 2 until the raw material particles are completely filtered, and putting the raw material particles into a container together for later use;
and step 4, mixing and stirring: putting the raw material particles in the container into a stirrer for mixing and stirring;
and 5, air drying treatment: conveying dry air into the stirrer in a bottom air supply mode, and drying raw materials in the stirrer in a stirring process to obtain drinking water disinfection powder;
and 6, packaging: lifting and conveying the drinking water disinfectant powder to filling equipment in a spiral belt conveying mode, and sealing and packaging the drinking water disinfectant powder.
6. The domestic drinking water disinfectant powder according to claim 5, wherein the raw material particles in step 2 are screened with a 80-120 mesh screen and vibrated for 2-3 times.
7. The domestic drinking water disinfectant powder according to claim 5, wherein in step 4, the stirrer is a single stirring paddle, the rotation speed of the stirring paddle is 60-90 r/min, and the stirring is performed clockwise for 15-20 min and counterclockwise for 15-20 min.
8. The disinfection powder for domestic drinking water as claimed in claim 5, wherein the air-drying temperature in step 5 is 5-12 ℃, and the air-drying temperature is 5-8 min clockwise, 9-12 ℃ clockwise, 5-8 min counterclockwise and 5-7 ℃ counterclockwise.
9. The domestic drinking water disinfectant powder according to claim 5, wherein in step 4, the height of the particulate material placed in the mixer is not more than 1/2 of the mixer.
CN202210565901.XA 2022-05-24 2022-05-24 Domestic drinking water disinfection powder and preparation method thereof Pending CN114766510A (en)

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Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1149396A (en) * 1995-10-25 1997-05-14 李殿波 Slow-release type sterilizing tablet and its production method
CN102283247A (en) * 2011-07-23 2011-12-21 中国农业科学院兰州畜牧与兽药研究所 Veterinary disinfection powder and preparation method thereof
CN103371178A (en) * 2012-04-24 2013-10-30 李家波 Food equipment disinfectant and preparation method thereof
CN107021550A (en) * 2017-05-11 2017-08-08 江苏苏沃尚新材料科技有限公司 A kind of domestic water disinfectant powder
CN107027806A (en) * 2017-06-08 2017-08-11 太仓优活生物技术有限公司 A kind of sterilized articles therefrom good with Disinfection Effect
CN207071333U (en) * 2017-04-27 2018-03-06 山东润兴环保科技有限公司 A kind of disinfectant preparation automatically configures device
CN111675294A (en) * 2020-06-05 2020-09-18 沈小燕 Degradable bactericide for sewage
CN112352786A (en) * 2020-12-01 2021-02-12 临沂京瑞新材料科技有限公司 Disinfection powder
CN112825851A (en) * 2021-01-11 2021-05-25 山东安捷高科消毒科技有限公司 High-stability 84 disinfectant with corrosion inhibition effect and preparation method thereof
CN114181789A (en) * 2020-09-12 2022-03-15 大城县宇昊卫生用品有限公司 Pipeline dredging agent with strong oxidizing property

Patent Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1149396A (en) * 1995-10-25 1997-05-14 李殿波 Slow-release type sterilizing tablet and its production method
CN102283247A (en) * 2011-07-23 2011-12-21 中国农业科学院兰州畜牧与兽药研究所 Veterinary disinfection powder and preparation method thereof
CN103371178A (en) * 2012-04-24 2013-10-30 李家波 Food equipment disinfectant and preparation method thereof
CN207071333U (en) * 2017-04-27 2018-03-06 山东润兴环保科技有限公司 A kind of disinfectant preparation automatically configures device
CN107021550A (en) * 2017-05-11 2017-08-08 江苏苏沃尚新材料科技有限公司 A kind of domestic water disinfectant powder
CN107027806A (en) * 2017-06-08 2017-08-11 太仓优活生物技术有限公司 A kind of sterilized articles therefrom good with Disinfection Effect
CN111675294A (en) * 2020-06-05 2020-09-18 沈小燕 Degradable bactericide for sewage
CN114181789A (en) * 2020-09-12 2022-03-15 大城县宇昊卫生用品有限公司 Pipeline dredging agent with strong oxidizing property
CN112352786A (en) * 2020-12-01 2021-02-12 临沂京瑞新材料科技有限公司 Disinfection powder
CN112825851A (en) * 2021-01-11 2021-05-25 山东安捷高科消毒科技有限公司 High-stability 84 disinfectant with corrosion inhibition effect and preparation method thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
曹佳等: "《程天民军事预防医学》", 人民军医出版社, pages: 104 - 107 *

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Application publication date: 20220722