CN1147553C - Working technology for extracting ossein from animal cartilage - Google Patents
Working technology for extracting ossein from animal cartilageInfo
- Publication number
- CN1147553C CN1147553C CNB021204330A CN02120433A CN1147553C CN 1147553 C CN1147553 C CN 1147553C CN B021204330 A CNB021204330 A CN B021204330A CN 02120433 A CN02120433 A CN 02120433A CN 1147553 C CN1147553 C CN 1147553C
- Authority
- CN
- China
- Prior art keywords
- obtained product
- animal cartilage
- complete processing
- cartilage
- gained
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 210000000845 cartilage Anatomy 0.000 title claims abstract description 21
- 241001465754 Metazoa Species 0.000 title claims abstract description 17
- 238000005516 engineering process Methods 0.000 title description 3
- 238000012545 processing Methods 0.000 claims abstract description 15
- 150000001875 compounds Chemical class 0.000 claims abstract description 8
- 238000001035 drying Methods 0.000 claims abstract description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract 5
- 239000000463 material Substances 0.000 claims abstract 4
- 238000001556 precipitation Methods 0.000 claims abstract 3
- 239000002253 acid Substances 0.000 claims abstract 2
- 238000001816 cooling Methods 0.000 claims abstract 2
- 241000272201 Columbiformes Species 0.000 claims description 7
- 210000000481 breast Anatomy 0.000 claims description 7
- 239000002994 raw material Substances 0.000 claims description 5
- 230000007062 hydrolysis Effects 0.000 claims description 3
- 238000006460 hydrolysis reaction Methods 0.000 claims description 3
- 239000000284 extract Substances 0.000 claims description 2
- 238000012856 packing Methods 0.000 claims description 2
- 238000005507 spraying Methods 0.000 claims description 2
- 239000000243 solution Substances 0.000 claims 4
- 239000012535 impurity Substances 0.000 claims 2
- 239000011505 plaster Substances 0.000 claims 2
- 102000011759 adducin Human genes 0.000 claims 1
- 108010076723 adducin Proteins 0.000 claims 1
- 239000007864 aqueous solution Substances 0.000 claims 1
- 238000001704 evaporation Methods 0.000 claims 1
- 230000008020 evaporation Effects 0.000 claims 1
- 238000006386 neutralization reaction Methods 0.000 claims 1
- 230000003068 static effect Effects 0.000 claims 1
- 238000000034 method Methods 0.000 abstract description 9
- 239000000126 substance Substances 0.000 abstract description 8
- 235000013305 food Nutrition 0.000 abstract description 7
- 102000008186 Collagen Human genes 0.000 abstract description 5
- 108010035532 Collagen Proteins 0.000 abstract description 5
- 235000015097 nutrients Nutrition 0.000 abstract description 5
- 150000001413 amino acids Chemical class 0.000 abstract description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 4
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 abstract description 3
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 abstract description 3
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 abstract description 3
- 239000011575 calcium Substances 0.000 abstract description 3
- 229910052791 calcium Inorganic materials 0.000 abstract description 3
- 229920001436 collagen Polymers 0.000 abstract description 3
- 239000011777 magnesium Substances 0.000 abstract description 3
- 229910052749 magnesium Inorganic materials 0.000 abstract description 3
- 239000011591 potassium Substances 0.000 abstract description 3
- 229910052700 potassium Inorganic materials 0.000 abstract description 3
- 235000013619 trace mineral Nutrition 0.000 abstract description 3
- 239000011573 trace mineral Substances 0.000 abstract description 3
- 239000000654 additive Substances 0.000 abstract description 2
- 230000000996 additive effect Effects 0.000 abstract description 2
- 229910052785 arsenic Inorganic materials 0.000 abstract description 2
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 abstract description 2
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 abstract description 2
- 229910052753 mercury Inorganic materials 0.000 abstract description 2
- 230000001256 tonic effect Effects 0.000 abstract description 2
- 210000000988 bone and bone Anatomy 0.000 abstract 2
- 229920002567 Chondroitin Polymers 0.000 abstract 1
- 230000009286 beneficial effect Effects 0.000 abstract 1
- DLGJWSVWTWEWBJ-HGGSSLSASA-N chondroitin Chemical compound CC(O)=N[C@@H]1[C@H](O)O[C@H](CO)[C@H](O)[C@@H]1OC1[C@H](O)[C@H](O)C=C(C(O)=O)O1 DLGJWSVWTWEWBJ-HGGSSLSASA-N 0.000 abstract 1
- 238000004140 cleaning Methods 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- WABPQHHGFIMREM-UHFFFAOYSA-N lead(0) Chemical compound [Pb] WABPQHHGFIMREM-UHFFFAOYSA-N 0.000 abstract 1
- 238000004806 packaging method and process Methods 0.000 abstract 1
- 235000016709 nutrition Nutrition 0.000 description 4
- 230000035764 nutrition Effects 0.000 description 4
- 210000001519 tissue Anatomy 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 235000008935 nutritious Nutrition 0.000 description 2
- 230000000050 nutritive effect Effects 0.000 description 2
- 239000001888 Peptone Substances 0.000 description 1
- 108010080698 Peptones Proteins 0.000 description 1
- 239000002250 absorbent Substances 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000029087 digestion Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- 238000011017 operating method Methods 0.000 description 1
- 235000019319 peptone Nutrition 0.000 description 1
- 108090000765 processed proteins & peptides Proteins 0.000 description 1
- 150000003384 small molecules Chemical class 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Images
Landscapes
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The present invention discloses a processing technique for extracting compound bone collagen from animal cartilage. Biologic nutrient tonic foods beneficial to human bodies can be produced by the technique, and extracted compound bone collagen can also be used as an additive of chemical products for daily use. The technique comprises the following steps: material selection, cleaning, hydrolyzation by an alkaline water solution, cooling, acid addition, filtration, concentration, alcohol precipitation, dewatering, drying and packaging. A molecule structure of an original substance can be changed by the processing technique of the present invention, and nutrient components and proportions are basically not damaged or lost; an obtained product is low in fat content, high in collagen protein and contains trace elements, such as calcium, magnesium, potassium, etc., and 19 kinds of amino acid, the chondroitin content is about 20%, and the contents of harmful substances, such as plumbum, arsenic, mercury, etc., are lower than the national food safety standards; on the other hand, the obtained product can be completely dissolved in water and can be easily digested absorbed. Various health care nutrient foods can be produced by the obtained product, and the obtained product can also be widely added to various foods; in addition, the obtained product has high water absorbability, and therefore, the obtained product can be used for the industry, such as chemical industry for daily use articles, etc.
Description
Technical field
The present invention relates to a kind of complete processing of from animal tissues, extracting nutritive substance, refer to a kind of complete processing of from animal cartilage, extracting compound osso-albumin especially.
Background technology
As everyone knows, contain the multiple nutrients composition in the cartilaginous tissue of animal, especially abundant with the content of chrondroitin, collagen protein, also contain trace element, ten multiple amino acids such as calcium, magnesium, potassium simultaneously.Past, the utmost point was not easy to digestion and absorbed, and therefore went out of use, and was very unfortunate, also was a kind of waste because the above-mentioned nutrition in the animal cartilage is present in the macromole combination.
If so can pass through certain industrialization processing extraction technique, change its molecular structure, the useful matter in the animal cartilage tissue is extracted, the composition height of nutritious value is concentrated, and be easy to the human consumption absorption, it is required to help to replenish health undoubtedly.Complete processing of the present invention is promptly under this guiding theory and develop.
Summary of the invention
The present invention aims to provide a kind of complete processing of extracting compound osso-albumin from animal cartilage, makes and utilizes this technology can produce the biological nutrition tonic extremely useful to human body, also can be used as the additive of daily chemical product.
Complete processing of the present invention is as follows: a kind of complete processing of extracting compound osso-albumin from animal cartilage is characterized in that it in turn includes the following steps:
Steps A: clean, select the healthy animal cartilage, remove the surface impurity of attachment removal as raw material;
Step B: add the alkaline aqueous solution hydrolysis, promote the dissolving of nutrition;
Step C: cooling adds the acid neutralization;
Step D: filter, remove decorticate, skeletal grain and other impurity;
Step e: concentrate, evaporation moisture content reduces volume;
Step F: alcohol precipitation, the precipitation of the useful matter in rare plaster material is separated out;
Step G: dehydration, add 95 degree (surveying) alcohol repeatedly to the throw out of collecting with alcoholometer, the moisture content in the material is oozed out the purpose that reaches dehydration;
Step H: dry and pack.
Wherein preferably earlier fresh feed is carried out bubble in the steps A and send out, so that can descend the basic hydrolysis in step more fully;
Be to extract evaporable moisture content and alcohol out in 65 ℃～70 ℃ exhausting among the step H, temperature is too high to have destruction to product, crosses the low drying effect that influences.
Said animal cartilage is good with fresh pigeon breast cartilage.
In addition, the present invention also can be after completing steps E, use spraying drying instead after crushing packing substitute original step F, G and H.
Utilize above-mentioned production technique of the present invention, taking raw material is the pigeon breast cartilage, nutritious, in process of production with about raw material volume-diminished to 12%, and contained nutrition and ratio are not destroyed substantially or lose, and utilize the basic hydrolysis step and will be present in the macromole combination nutrition that is difficult for being digested and absorbing originally and become water miscible small molecules, even be hydrolyzed into the water-soluble nutrient substance that digests and absorb of being easy to of fat class, peptone class, peptide class and amino acids, so just can fully be absorbed by human body and be used; The products obtained therefrom lipid content is low, the collagen content height, chrondroitin content reaches about 20% (measuring by the method for being put down in writing on the American Pharmacopeia 25 editions), and contains trace element, 19 seed amino acids such as calcium, magnesium, potassium, and objectionable impuritiess such as lead, arsenic, mercury are lower than the state food safety standards.On the other hand, products obtained therefrom can be water-soluble fully, is easy to digest and assimilate.Utilize resulting product can produce the plurality kinds of health care nutritive food, and can extensively make an addition in the various food.Moreover products obtained therefrom has very strong water-absorbent, thus also can apply in the industries such as daily-use chemical industry, as add to and have humidity-holding effect in the makeup.
Description of drawings
Fig. 1 is a process flow sheet of the present invention.
Embodiment
Example one is an example to extract compound osso-albumin from the pigeon breast cartilage, but the present invention is not that being only applicable to the pigeon breast cartilage is raw material, in fact the cartilaginous tissue of other animal also can be used as raw material, but because of pigeon breast cartilage ratio is easier to obtain, so preferred pigeon breast cartilage.Please refer to shown in Figure 1ly, the present invention carries out following operating procedure step in regular turn.
Steps A: the pigeon breast cartilage with health is a raw material, goes into retort and adds water to fully and flood, and bubble is sent out 4 hours; Stirring and washing after 20 minutes bleeds off water;
Step B: add the water of 10 times of charging capacitys earlier, add 30% aqueous sodium hydroxide solution again and regulate pH value to 11, start stirring, temperature is raised to 30 ℃～35 ℃ hydrolysis 4 hours;
Step C: treat that hydrolysis finishes, the whole dissolvings of material add 10% hydrochloric acid again and transfer pH value to 6.5～7;
Step D: blowing filters, remove decorticate, skeletal grain and other impurity;
Step e: filtered liquid is squeezed into concentration tank, and heating is condensed into rare paste blowing cooling;
Step F: more spissated material is moved into settling tank, add alcohol precipitation while stirring, the ethanol concn of the solution in settling tank reaches 85 degree (measuring with alcoholometer, as follows) times and stops, and capping was left standstill 1 hour;
Step G: then the upper strata Diluted Alcohol is extracted out, following throw out is collected in the bucket, adding 95 degree alcohol are added to while stirring and flood till the material, and centrifuge dehydration after 2 hours is left standstill in capping; And then the material after the centrifuge dehydration gone into bucket again, the alcohol that adds 95 degree stirs the adding capping and left standstill 2 hours, 3～4 times repeatedly, under the alcohol condition, progressively become solid discrete particle up to material by rare thick paste shape, the ethanol concn that centrifuge dehydration is come out is carried out next step oven dry when 92 degree are above;
Step H: the drip pan of splendid attire material is placed on temperature is controlled in 65 ℃～70 ℃ baking ovens, dry under the exhausting condition, moisture content is controlled at finishes drying 10% below; Again dried material being pulverized 100 orders packs.Resulting nutrition accounts for about 12% of bright wet feed material weight, and promptly yield rate about 12%.
Above-mentioned step F, G and H also can change spraying drying and crushing packing into and replace, and wherein spraying drying is routine techniques (technology that is adopted when making milk powder), is just no longer described in detail at this.
Claims (5)
1, extracts the complete processing of compound osso-albumin in a kind of animal cartilage, comprise the steps:
Steps A: selecting the healthy animal cartilage is raw material, cleans, and removes the surface impurity of attachment removal;
Step B: add the alkaline aqueous solution hydrolysis to the steps A products therefrom, promote the dissolving of animal cartilage;
Step C: after the cooling of step B gained solution, add this solution of acid neutralization;
Step D: step C gained solution is filtered, remove decorticate, skeletal grain and other impurity;
Step e: with step D gained solution evaporation moisture content, be concentrated into and be rare plaster material,, be easy to precipitation and collect to reduce volume;
Step F: in the concentrated material of step e gained, add alcohol to ethanol concn and be 85 degree, static, precipitation;
Step G: in step F gained throw out, add 95 degree alcohol, the moisture content in the throw out is oozed out to dewater, get granular disintegration;
Step H: collect step G products therefrom, with its oven dry and pack.
2, complete processing according to claim 1 is characterized in that, the described animal cartilage of steps A carries out bubble earlier to be sent out, so that can carry out next step basic hydrolysis more fully.
3, complete processing according to claim 1 is characterized in that, the described oven dry of step H is dry under 65-70 ℃ of exhausting condition.
4, complete processing according to claim 1 is characterized in that, described animal cartilage is fresh pigeon breast cartilage.
5, complete processing according to claim 1 is characterized in that, crushing packing after rare plaster material spraying drying of step e gained.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB021204330A CN1147553C (en) | 2002-05-22 | 2002-05-22 | Working technology for extracting ossein from animal cartilage |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB021204330A CN1147553C (en) | 2002-05-22 | 2002-05-22 | Working technology for extracting ossein from animal cartilage |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1385489A CN1385489A (en) | 2002-12-18 |
| CN1147553C true CN1147553C (en) | 2004-04-28 |
Family
ID=4744773
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB021204330A Expired - Lifetime CN1147553C (en) | 2002-05-22 | 2002-05-22 | Working technology for extracting ossein from animal cartilage |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1147553C (en) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100485002C (en) * | 2005-10-18 | 2009-05-06 | 中国人民解放军第三军医大学第一附属医院 | Bone collagen gel liquid preparation method |
| CN100402088C (en) * | 2006-04-26 | 2008-07-16 | 周立军 | Method for preparing low molecular weighted glucidamin collagen composition, its product and use |
| CN104413406A (en) * | 2013-09-09 | 2015-03-18 | 西南民族大学 | Processing craft for extracting composite bone collagen from yak bone |
| CN107125612B (en) * | 2017-03-13 | 2020-09-15 | 鹤壁中农供应链管理有限公司 | Method for separating cartilage and bone powder from chicken leg bone |
-
2002
- 2002-05-22 CN CNB021204330A patent/CN1147553C/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| CN1385489A (en) | 2002-12-18 |
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Legal Events
| Date | Code | Title | Description |
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| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C56 | Change in the name or address of the patentee | ||
| CP02 | Change in the address of a patent holder |
Address after: 434300, room 1107, building C6, office building, Wanda Plaza, Hanyang District, Wuhan, Hubei Patentee after: Zhao Chengjun Address before: 434300 Gongan County General Chamber of Commerce in Hubei Patentee before: Zhao Chengjun |
|
| C56 | Change in the name or address of the patentee | ||
| CP02 | Change in the address of a patent holder |
Address after: 430056, room 1107, building C6, office building, Wanda Plaza, Hanyang District, Wuhan, Hubei Patentee after: Zhao Chengjun Address before: 434300, room 1107, building C6, office building, Wanda Plaza, Hanyang District, Wuhan, Hubei Patentee before: Zhao Chengjun |
|
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20171220 Address after: 430056 Hubei Province Economic and Technological Development Zone of Wuhan Wanda Plaza was opened in two sixth 11 storey 2 room Patentee after: Wuhan crystal Erli biological Polytron Technologies Inc Address before: 430056, room 1107, building C6, office building, Wanda Plaza, Hanyang District, Wuhan, Hubei Patentee before: Zhao Chengjun |
|
| CX01 | Expiry of patent term | ||
| CX01 | Expiry of patent term |
Granted publication date: 20040428 |