CN101033481A - Preparing process of extracting bone collagen from pig, cattle and sheep bone - Google Patents
Preparing process of extracting bone collagen from pig, cattle and sheep bone Download PDFInfo
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- CN101033481A CN101033481A CN 200710017623 CN200710017623A CN101033481A CN 101033481 A CN101033481 A CN 101033481A CN 200710017623 CN200710017623 CN 200710017623 CN 200710017623 A CN200710017623 A CN 200710017623A CN 101033481 A CN101033481 A CN 101033481A
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Abstract
The invention relates to a method for extracting bone collagen protein from bone of pig, cow and sheep, including: It removes the impurities of the bone. And then it warms up and extracts the bone under high-pressure in the high-pressure extraction tank. And then it separates the oil and melting soup by using oil-water separator. And then it transfers the separated liquid into the enzymolysis can for enzymatic hydrolysis. And then it cools the liquid to 50 deg.C, and then adds liquid complex flavor protease to enzymolysis for eight hours. And then it warms the liquid up to 90 deg.C, and it eliminate enzyme for 30 minutes. And then it adds natural spice and salt. And then it filters the liquid. And then it sterilizes the liquid with a high-temperature sterilization machine. And then it condenses the liquid to dry materials by using double-effect falling film evaporator. And then it dries the dry materials into power by using pressure-type sprayer.
Description
Technical field
The present invention relates to a kind of preparation technology who extracts bone collagen, particularly a kind of preparation technology who from pig, ox, sheep bone, extracts bone collagen.
Background technology
As everyone knows, contain the multiple nutrients composition in the animal bone, maximum with collagen protein (also claiming polypeptide) content, contain calcium, phosphorus, mineral substance 19 seed amino acids simultaneously, in the past owing to nutrition in the bone is extracted dangerous, collagen protein be high molecular several ten thousand to hundreds of thousands of dalton, human body extremely difficulty is assimilated, moreover does not have the low molecule of collagen protein (polypeptide) of bone soup fragrance on the market.
So,, can allow people drink bone collagen (polypeptide) soup of strong, mellow long, the high nutrition of bone flavor if can extract and mass production by certain special process.
Summary of the invention
Technical problem to be solved by this invention is at deficiency of the prior art, a kind of preparation technology who extracts bone collagen from the pig, cattle and sheep bone is provided, utilize compound biological enzyme from pig, ox, sheep bone, to extract bone collagen (polypeptide), use the product biological nutrition product extremely useful of this explained hereafter human body.
For this reason, the invention provides a kind of preparation technology who from the pig, cattle and sheep bone, extracts bone collagen, it is characterized in that, comprise the steps:
Step 1, with the bone of pig, ox, sheep as raw material, remove impurity after, soak with cold water, after the stirring, water is bled off;
Soup after step 3, usefulness water-and-oil separator separating oil and the heating and melting;
Step 8, usefulness flash-sterilization machine are to described soup sterilization;
Bone collagen (polypeptide) content of the product of the present invention preparation more than 86% (because of containing compositions such as salt and calcium) be lower molecular weight 3000 left and right sides dalton, be that absorption of human body collagen molecules amount is optimal, specific absorption is up to 98%.As there not being collagen protein to make calcium be difficult to be deposited in the bone, have only under the competent situation of collagen protein in the human body bone, just can make calcium deposit in bone, bone density is increased, hardness strengthens.Micromolecular collagen (polypeptide) can make skin delicacy, smooth, recovers human body elasticity.Improve hair quality, prevent the hair bifurcated, make the pitch-black beautiful high resilience of hair.Effectively eliminate skin speckle, anti-wrinkle promotes the metabolism of nail, makes breast have anchorage force and elasticity.Particularly has bone flavor strong, mellow long, delicious bone collagen (polypeptide) soup.
Below by drawings and Examples, technical scheme of the present invention is described in further detail.
Description of drawings
Fig. 1 is the schema of the preferred embodiments of the present invention.
Embodiment
Fig. 1 is the schema of the preferred embodiments of the present invention.As shown in Figure 1, the present invention is a kind of preparation technology who extracts bone collagen from the pig, cattle and sheep bone, comprises the steps:
Step 1, with the bone of pig, ox, sheep as raw material, remove impurity after, soak with cold water, after the stirring, water is bled off;
Soup after step 3, usefulness water-and-oil separator separating oil and the heating and melting;
Step 8, usefulness flash-sterilization machine are to described soup sterilization;
In the foregoing description, the soak time in rapid 1 is preferably 3 hours, and described churning time is preferably 30 minutes.
The powdery bone collagen of the last generation in the foregoing description can be again by carrying out packing at aseptic indoor wrapping machine, processes such as vanning; Put goods on the market through after the assay was approved and to sell.
It should be noted last that, above embodiment is only unrestricted in order to technical scheme of the present invention to be described, although the present invention is had been described in detail with reference to preferred embodiment, those of ordinary skill in the art is to be understood that, can make amendment or be equal to replacement technical scheme of the present invention, and not break away from the spirit and scope of technical solution of the present invention.
Claims (2)
1. a preparation technology who extracts bone collagen from the pig, cattle and sheep bone is characterized in that, comprises the steps:
Step 1, with the bone of pig, ox, sheep as raw material, remove impurity after, soak with cold water, after the stirring, water is bled off;
Step 2, the ratio according to five tons of water of one ton of bone in the high pressure extract jar add bone and water, are warming up to 100 ℃, after 30 minutes sump oil are emitted; High pressure extract was warming up to 95 ℃ and extracted 4 hours again after 6 hours then;
Soup after step 3, usefulness water-and-oil separator separating oil and the heating and melting;
Step 4, the soup of separator well is put into enzymatic vessel, with citric acid and edible alkali the pH value of described soup is transferred to PH and equals 7.5, add compound protease after being warming up to 55 ℃ then, enzymolysis makes the PH of described soup equal 6.0 to 6.5 after 2 hours; Again described soup is cooled to 50 ℃ and adds compound protease, enzymolysis 8 hours;
Step 5, described soup is warming up to 90 ℃ of enzymes 30 minutes of going out again;
Step 6, in described soup, add natural flavoring agent again, after 1 hour with the salt seasoning;
Step 7, the described soup in the described step 6 is filtered with flame filter press;
Step 8, usefulness flash-sterilization machine are to described soup sterilization;
Step 9, described soup is concentrated into 35% to 40% dry-matter with double-effect falling film evaporator;
Step 10, the dry-matter in the step 9 is dried to powdery with pressure-type spray day with fog drying unit.
2. the preparation technology who extracts bone collagen from the pig, cattle and sheep bone according to claim 1 is characterized in that the soak time in the described step 1 is 3 hours, and described churning time is 30 minutes.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200710017623 CN101033481A (en) | 2007-04-05 | 2007-04-05 | Preparing process of extracting bone collagen from pig, cattle and sheep bone |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200710017623 CN101033481A (en) | 2007-04-05 | 2007-04-05 | Preparing process of extracting bone collagen from pig, cattle and sheep bone |
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| CN101033481A true CN101033481A (en) | 2007-09-12 |
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| CN 200710017623 Pending CN101033481A (en) | 2007-04-05 | 2007-04-05 | Preparing process of extracting bone collagen from pig, cattle and sheep bone |
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Cited By (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101366494A (en) * | 2008-09-17 | 2009-02-18 | 广东汇香源生物科技股份有限公司 | Peptide-rich flavour development based material and preparation method |
| CN101857891A (en) * | 2010-06-12 | 2010-10-13 | 西南林业大学 | Method for preparing donkey bone protein by enzymatic method and donkey bone protein instant soup |
| CN102206271A (en) * | 2011-04-12 | 2011-10-05 | 李海彰 | Preparation method of pure-natural collagen product |
| CN102429891A (en) * | 2011-12-13 | 2012-05-02 | 河南科技大学 | Preparation method of low-molecular-weight sheep bone collagen polypeptide calcium chelate microcapsule |
| CN103014105A (en) * | 2012-06-11 | 2013-04-03 | 四川农业大学 | Method for preparing antihypertensive peptide by using porcine thighbones |
| CN103689212A (en) * | 2013-12-27 | 2014-04-02 | 冯启训 | Method for extracting small molecule peptide from fresh animal bone |
| CN103783254A (en) * | 2013-07-02 | 2014-05-14 | 吴长海 | Preparation method of yak bone collagen peptide |
| CN103843970A (en) * | 2012-11-30 | 2014-06-11 | 闫云霞 | Production method for preparing ossein oligopeptide meal, bone oil and bone meal |
| CN103920173A (en) * | 2014-04-10 | 2014-07-16 | 广州康洛信生物科技有限公司 | Collagen safe sterilizing method |
| CN104095141A (en) * | 2014-06-16 | 2014-10-15 | 中国农业科学院农产品加工研究所 | Method for coproducing collagen activity peptides and flavoured base materials with chicken bones |
| CN104223214A (en) * | 2014-09-16 | 2014-12-24 | 天津春发生物科技集团有限公司 | Bovine bone soup paste and preparation method thereof |
| CN104336636A (en) * | 2013-08-07 | 2015-02-11 | 青岛博研达工业技术研究所(普通合伙) | Method of extracting nutrients from pig bones |
| CN105326861A (en) * | 2015-09-23 | 2016-02-17 | 长春世鹿鹿业集团有限公司 | Extraction method of deer bone collagen polypeptide and active calcium composition |
| CN106343146A (en) * | 2016-08-23 | 2017-01-25 | 慈晓丽 | Preparation method of turtle peptide |
| CN107125770A (en) * | 2017-05-10 | 2017-09-05 | 烟台开发区绿源生物工程有限公司 | A kind of method that utilization fish-bone produces fish-bone peptide |
| CN108208739A (en) * | 2018-01-05 | 2018-06-29 | 广州市雅禾生物科技有限公司 | A kind of beef flavor and preparation method thereof |
| CN110960618A (en) * | 2018-09-30 | 2020-04-07 | 辽宁上药科技开发有限公司 | Preparation method of composition for joint protection |
| CN111363030A (en) * | 2020-03-20 | 2020-07-03 | 青岛小度信息科技有限公司 | Collagen peptide production and purification system |
-
2007
- 2007-04-05 CN CN 200710017623 patent/CN101033481A/en active Pending
Cited By (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101366494A (en) * | 2008-09-17 | 2009-02-18 | 广东汇香源生物科技股份有限公司 | Peptide-rich flavour development based material and preparation method |
| CN101857891A (en) * | 2010-06-12 | 2010-10-13 | 西南林业大学 | Method for preparing donkey bone protein by enzymatic method and donkey bone protein instant soup |
| CN102206271A (en) * | 2011-04-12 | 2011-10-05 | 李海彰 | Preparation method of pure-natural collagen product |
| CN102429891A (en) * | 2011-12-13 | 2012-05-02 | 河南科技大学 | Preparation method of low-molecular-weight sheep bone collagen polypeptide calcium chelate microcapsule |
| CN102429891B (en) * | 2011-12-13 | 2013-02-27 | 河南科技大学 | A kind of preparation method of low molecular weight sheep bone collagen polypeptide calcium chelate microcapsule |
| CN103014105A (en) * | 2012-06-11 | 2013-04-03 | 四川农业大学 | Method for preparing antihypertensive peptide by using porcine thighbones |
| CN103843970A (en) * | 2012-11-30 | 2014-06-11 | 闫云霞 | Production method for preparing ossein oligopeptide meal, bone oil and bone meal |
| CN103783254A (en) * | 2013-07-02 | 2014-05-14 | 吴长海 | Preparation method of yak bone collagen peptide |
| CN104336636A (en) * | 2013-08-07 | 2015-02-11 | 青岛博研达工业技术研究所(普通合伙) | Method of extracting nutrients from pig bones |
| CN104336636B (en) * | 2013-08-07 | 2018-07-13 | 青岛博研达工业技术研究所(普通合伙) | A method of extracting nutriment from pig bone |
| CN103689212A (en) * | 2013-12-27 | 2014-04-02 | 冯启训 | Method for extracting small molecule peptide from fresh animal bone |
| CN103920173B (en) * | 2014-04-10 | 2016-11-02 | 广州康洛信生物科技有限公司 | Collagen protein safe sterilization method |
| CN103920173A (en) * | 2014-04-10 | 2014-07-16 | 广州康洛信生物科技有限公司 | Collagen safe sterilizing method |
| CN104095141B (en) * | 2014-06-16 | 2016-06-08 | 中国农业科学院农产品加工研究所 | A kind of method of chicken bone coproduction collagen active peptide and flavor base material |
| CN104095141A (en) * | 2014-06-16 | 2014-10-15 | 中国农业科学院农产品加工研究所 | Method for coproducing collagen activity peptides and flavoured base materials with chicken bones |
| CN104223214A (en) * | 2014-09-16 | 2014-12-24 | 天津春发生物科技集团有限公司 | Bovine bone soup paste and preparation method thereof |
| CN105326861A (en) * | 2015-09-23 | 2016-02-17 | 长春世鹿鹿业集团有限公司 | Extraction method of deer bone collagen polypeptide and active calcium composition |
| CN106343146A (en) * | 2016-08-23 | 2017-01-25 | 慈晓丽 | Preparation method of turtle peptide |
| CN107125770A (en) * | 2017-05-10 | 2017-09-05 | 烟台开发区绿源生物工程有限公司 | A kind of method that utilization fish-bone produces fish-bone peptide |
| CN108208739A (en) * | 2018-01-05 | 2018-06-29 | 广州市雅禾生物科技有限公司 | A kind of beef flavor and preparation method thereof |
| CN110960618A (en) * | 2018-09-30 | 2020-04-07 | 辽宁上药科技开发有限公司 | Preparation method of composition for joint protection |
| CN111363030A (en) * | 2020-03-20 | 2020-07-03 | 青岛小度信息科技有限公司 | Collagen peptide production and purification system |
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Open date: 20070912 |