CN114748370A - Hand-protecting bacteriostatic cream and preparation method thereof - Google Patents
Hand-protecting bacteriostatic cream and preparation method thereof Download PDFInfo
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- CN114748370A CN114748370A CN202210532533.9A CN202210532533A CN114748370A CN 114748370 A CN114748370 A CN 114748370A CN 202210532533 A CN202210532533 A CN 202210532533A CN 114748370 A CN114748370 A CN 114748370A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/41—Amines
- A61K8/416—Quaternary ammonium compounds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/524—Preservatives
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Abstract
A hand-protecting bacteriostatic cream and a preparation method thereof belong to the technical field of skin care products, and mainly comprise phase A deionized water, methyl nicotinate, glycerol and surfactin sodium. B phase hexadecanol/octadecanol, monoglyceride, a first emulsifier, a second emulsifier, silicone oil, white oil and shea butter. The phase C comprises: benzethonium chloride. Phase D comprises: phenoxyethanol. Heating phase A and B. Mixing and emulsifying the AB phase and the AB phase, and cooling by stages. The CD phase was added during the process. The benzethonium chloride is added, so that the hand-protecting bacteriostatic cream has high-efficiency bacteriostasis and very little irritation to the epidermis of the hand, does not have irritant taste, and has better corrosion resistance, A B phase, so that the hand-protecting bacteriostatic cream has better affinity, lipid components can better avoid causing allergy to a user, provide nutrition for the skin, soften dead skin, resist oxidation and keep the skin soft and tender, can keep the skin moisturized for a long time, and does not add alcohol, so that the hand-protecting bacteriostatic cream can further ensure the water locking property.
Description
Technical Field
The invention belongs to the technical field of skin care products, and particularly relates to hand-protecting antibacterial cream and a preparation method thereof.
Background
Daily frequent cleaning and hand washing is one of the key means of epidemic prevention, hand disinfection and sterilization become a part of people's daily life, and hand products disinfected and sterilized by long-term use can bring adverse effects to hand skin, such as dryness, chapping or dermatitis, etc., so that moisturizing and nursing of hands after disinfection and sterilization are very necessary.
At present, the most commonly used component alcohol in common hand moisturizing cream has high volatility, takes away skin heat and skin moisture, reduces the natural moisturizing capability and immunity of the skin, and causes dry and rough skin. The alcohol also has super-strong permeability, and can permeate into cells to enable the proteins of the cells to be coagulated and denatured so as to dehydrate the cells, so that the traditional hand and bacteriostatic cream has a plurality of defects in actual use.
Disclosure of Invention
The invention aims to provide hand-protecting and bacteriostatic cream, and another aim of the invention is to provide a hand-protecting and bacteriostatic cream and a preparation method thereof, aiming at solving the problems that the most commonly used component alcohol in the prior hand-protecting and moisturizing cream products in the background art has high volatility, takes away the skin heat and the skin moisture, reduces the natural moisturizing capability and immunity of the skin, and causes the skin to be dry and rough.
The hand-protecting bacteriostatic cream is mainly prepared from a phase A, a phase B, a phase C and a phase D.
Wherein, the weight portion is:
the phase A comprises: 60-70 parts of deionized water, 0.1-0.3 part of nylon-methyl ester, 5-10 parts of glycerol and 0.01-1 part of surfactin sodium.
The phase B comprises: 1-5 parts of hexadecanol/octadecanol, 1-5 parts of monoglyceride, 1-5 parts of first emulsifier, 0.1-5 parts of second emulsifier, 1-5 parts of silicone oil, 5-20 parts of white oil and 0.5-5 parts of shea butter.
The phase C comprises: 0.01-1 part of benzethonium chloride.
Phase D comprises: 0.1-1 part of phenoxyethanol.
Wherein: the first emulsifier is M68 emulsifier, and the second emulsifier is A165 emulsifier.
The silicone oil is silicone oil 350.
The white oil is 26# white oil.
And the phase D can also comprise 0.1-1 part of cosmetic essence, such as known essence such as strawberry essence or apple essence.
The preparation method of the hand-protecting bacteriostatic cream is used for preparing the hand-protecting bacteriostatic cream, and comprises the following steps:
and S1, preparing materials.
And S2, checking raw materials and preparing materials.
And S3, heating.
S4, emulsification.
And S5, cooling.
And S6, checking.
And S7, discharging.
And S8, aging.
The preparation of the phase A comprises the following steps: accurately weighing deionized water of phase A, placing into a water phase tank, adding other components of phase A (0.1-0.3 part of methyl nicotinate, 5-10 parts of glycerol and 0.01-1 part of sodium surfactin), and heating to 90 deg.C for dissolving.
The preparation of the B phase is as follows: accurately weighing various raw materials of phase B (1-5 parts of hexadecanol/octadecanol, 1-5 parts of monoglyceride, 1-5 parts of first emulsifier, 0.1-5 parts of second emulsifier, 1-5 parts of silicone oil, 5-20 parts of white oil and 0.5-5 parts of shea butter), adding into an oil phase tank, heating to 90 ℃ for dissolving, and reserving for later use.
The emulsification process comprises the following steps: and (3) starting vacuum to-0.05 MPa, pumping two thirds of materials in the water phase tank into an emulsification tank, starting stirring at 800rpm, pumping all the oil phase into the emulsification tank, pumping the rest materials in the water phase tank into the emulsification tank, ending vacuum, continuing stirring at 800rpm for 1 minute, stopping stirring, homogenizing at 2800rpm for 5 minutes, starting stirring at 800rpm, and emulsifying for 5 minutes.
The cooling process comprises the following steps: stirring in an emulsification tank at 300rpm after emulsification is finished, introducing cooling water to cool to 75 ℃, vacuumizing to-0.05 MPa, maintaining the pressure for 10 minutes, continuously cooling to 50 ℃, adding the phase C, adding the phase D at 45 ℃, finishing vacuum, continuously stirring at 300rpm, cooling to 30 ℃, and stopping stirring and cooling water.
The checking process comprises the following steps: and (3) carrying out microbial inspection, sanitary chemical inspection, pH value determination, toxicology safety experiment and human safety and function test on the sample.
And the aged finished product is further packaged by a quantitative plastic sealing packaging bag.
The advantages are that:
1) the benzethonium chloride is added into the hand protection antibacterial cream, so that the hand protection antibacterial cream has high-efficiency antibacterial property and very little irritation to the skin of the hand, and is free of irritation taste, meanwhile, the hand protection antibacterial cream has good corrosion resistance, the hand protection antibacterial cream has better affinity by adding the phase A and the phase B, lipid components can be better prevented from causing allergy to a user, and nutrition is effectively provided for the skin, dead skin is softened, oxidation resistance is realized, the softness and tenderness of the skin can be kept, the skin can be moisturized for a long time, and the efficacy of the hand protection antibacterial cream is improved.
2) Alcohol is not added into the components of the hand-protecting bacteriostatic cream, so that the hand-protecting bacteriostatic cream can further ensure the water locking property and ensure the efficacy of the hand-protecting bacteriostatic cream.
Drawings
FIG. 1 is a schematic view of the preparation process of the present invention.
The accompanying drawings are included to provide a further understanding of the invention, and are incorporated in and constitute a part of this specification, illustrate embodiments of the invention and together with the description serve to explain the invention without limiting the invention.
Detailed Description
Example 1
The hand-protecting bacteriostatic cream is mainly made up by using A phase, B phase, C phase and D phase.
Wherein, the weight portion is:
the phase A comprises: 60 parts of deionized water, 0.1 part of nylon methyl ester, 5 parts of glycerol and 0.01 part of surfactin sodium.
The phase B comprises: 1 part of cetyl alcohol, 1 part of monoglyceride, 1 part of first emulsifier, 0.1 part of second emulsifier, 1 part of silicone oil, 5 parts of white oil and 0.5 part of shea butter.
The phase C comprises: 0.01 part of benzethonium chloride.
Phase D comprises: 0.1 part of phenoxyethanol.
Wherein: the first emulsifier is an M68 emulsifier and the second emulsifier is an A165 emulsifier.
The silicone oil is silicone oil 350.
The white oil is 26# white oil.
Further, 0.1 part of essence can be added into the phase D.
The benzethonium chloride component can enable the hand-protection antibacterial cream to have high-efficiency bacteriostasis, meanwhile, the irritation to the epidermis of the hand is very small, the hand-protection antibacterial cream does not have irritating taste, and meanwhile, the hand-protection antibacterial cream has good corrosion resistance.
The preparation method of the hand-protecting bacteriostatic cream is used for preparing the hand-protecting bacteriostatic cream, and comprises the following steps:
and S1, preparing materials.
And S2, checking raw materials and preparing materials.
And S3, heating.
S4, emulsification.
And S5, cooling.
And S6, checking.
And S7, discharging.
And S8, aging.
In this embodiment: the preparation of the phase A comprises the following steps: accurately weighing deionized water of phase A, placing into a water phase tank, adding other components of phase A (0.1 part of methyl nicotinate, 5 parts of glycerol and 0.01 part of surfactin sodium), and heating to 90 deg.C for dissolving.
The preparation of the B phase is as follows: accurately weighing various raw materials of phase B (1 part of cetyl alcohol, 1 part of monoglyceride, 1 part of first emulsifier, 0.1 part of second emulsifier, 1 part of silicone oil, 5 parts of white oil and 0.5 part of shea butter), adding into an oil phase tank, and heating to 90 deg.C for use.
The emulsification process comprises the following steps: and (3) starting vacuum to-0.05 MPa, pumping two thirds of materials in the water phase tank into an emulsification tank, starting stirring at 800rpm, pumping all the oil phase into the emulsification tank, pumping the rest materials in the water phase tank into the emulsification tank, ending vacuum, continuing stirring at 800rpm for 1 minute, stopping stirring, homogenizing at 2800rpm for 5 minutes, starting stirring at 800rpm, and emulsifying for 5 minutes.
The cooling process comprises the following steps: stirring in an emulsification tank at 300rpm after emulsification is finished, introducing cooling water to cool to 75 ℃, vacuumizing to-0.05 MPa, maintaining the pressure for 10 minutes, continuously cooling to 50 ℃, adding the phase C, adding the phase D at 45 ℃, finishing vacuum, continuously stirring at 300rpm, cooling to 30 ℃, and stopping stirring and cooling water.
The added lipid can effectively increase the regeneration capacity of skin cells, effectively avoid rough and wrinkled skin, and the added deionized water can adjust the viscosity of the emulsion in the preparation process of the hand-protection antibacterial cream, so that the hand-protection antibacterial cream can be better applied daily.
And the adopted step cooling mode ensures that emulsion liquid drops after final emulsification are finer and narrower in particle size distribution, so that the generated mixed liquid has better stability.
In this embodiment: the process of the inspection comprises: and (3) carrying out microbial inspection, sanitary chemical inspection, pH value determination, toxicology safety experiment and human safety and function test on the sample.
The use safety of the hand-protecting and bacteriostatic cream is ensured by carrying out multi-index inspection on the sample.
And packaging the aged finished product by using a quantitative plastic sealing packaging bag.
Specifically, through the encapsulation of the plastic sealing packaging bags, the amount of the hand protection antibacterial cream can be controlled to be 1-2g in each packaging bag, and the packaging bag can be used independently, so that the pollution to the unused hand protection antibacterial cream caused by a bottled filling mode is avoided.
Alternatively, 1 part of cetyl alcohol in the present example may be replaced with 1 part of stearyl alcohol.
Example 2
The hand-protecting bacteriostatic cream is mainly made up by using A phase, B phase, C phase and D phase.
Wherein, the weight portion is:
the phase A comprises: 70 parts of deionized water, 0.3 part of nylon methyl ester, 10 parts of glycerol and 1 part of surfactin sodium.
The phase B comprises: 5 parts of octadecanol, 5 parts of monoglyceride, 5 parts of a first emulsifier, 5 parts of a second emulsifier, 5 parts of silicone oil, 20 parts of white oil and 5 parts of shea butter.
The phase C comprises: 1 part of benzethonium chloride.
Phase D comprises: 1 part of phenoxyethanol
Wherein: the first emulsifier is an M68 emulsifier and the second emulsifier is an A165 emulsifier.
The silicone oil is silicone oil 350.
The white oil is 26# white oil.
The preparation method is as described above.
Further, 1 part of essence can be added into the phase D.
Alternatively, 5 parts of octadecanol in the present example may be replaced with 5 parts of hexadecanol.
Example 3
The hand-protecting bacteriostatic cream is mainly made up by using A phase, B phase, C phase and D phase.
Wherein, the weight portion is:
the phase A comprises: 65 parts of deionized water, 0.2 part of nylon methyl ester, 9 parts of glycerol and 0.5 part of surfactin sodium.
The phase B comprises: 3 parts of octadecanol, 3 parts of monoglyceride, 3 parts of a first emulsifier, 2 parts of a second emulsifier, 2 parts of silicone oil, 12 parts of white oil and 4 parts of shea butter.
The phase C comprises: 0.7 part of benzethonium chloride.
Phase D comprises: 0.6 part of phenoxyethanol.
Wherein: the first emulsifier is an M68 emulsifier and the second emulsifier is an A165 emulsifier.
The silicone oil is silicone oil 350.
The white oil is 26# white oil.
Further, 0.5 part of essence can be added into the phase D.
Alternatively, 3 parts of octadecanol in the present example may be replaced with 3 parts of hexadecanol.
Claims (7)
1. The hand-protecting bacteriostatic cream is mainly prepared from a phase A, a phase B, a phase C and a phase D, and is characterized in that: the weight portion is as follows:
the phase A comprises: 60-70 parts of deionized water, 0.1-0.3 part of nylon methyl ester, 5-10 parts of glycerol and 0.01-1 part of surfactin sodium;
the phase B comprises: 1-5 parts of hexadecanol/octadecanol, 1-5 parts of monoglyceride, 1-5 parts of first emulsifier, 0.1-5 parts of second emulsifier, 1-5 parts of silicone oil, 5-20 parts of white oil and 0.5-5 parts of shea butter;
the phase C comprises: 0.01-1 part of benzethonium chloride;
phase D comprises: 0.1-1 part of phenoxyethanol.
2. The hand-protecting bacteriostatic cream according to claim 1, which is characterized in that:
the first emulsifier is M68 emulsifier, and the second emulsifier is A165 emulsifier;
the silicone oil is 350;
the white oil is 26# white oil.
3. The hand protection and bacteriostasis cream according to claim 1, characterized in that:
the phase A comprises: 60 parts of deionized water, 0.1 part of nylon methyl ester, 5 parts of glycerol and 0.01 part of surfactin sodium;
the phase B comprises: 1 part of cetyl alcohol/stearyl alcohol, 1 part of monoglyceride, 1 part of a first emulsifier, 0.1 part of a second emulsifier, 1 part of silicone oil, 5 parts of white oil and 0.5 part of shea butter;
the phase C comprises: 0.01 part of benzethonium chloride;
phase D comprises: 0.1 part of phenoxyethanol.
4. The hand-protecting bacteriostatic cream according to claim 1, which is characterized in that:
the phase A comprises: 70 parts of deionized water, 0.3 part of nylon methyl ester, 10 parts of glycerol and 1 part of surfactin sodium;
the phase B comprises: 5 parts of octadecanol/octadecanol, 5 parts of monoglyceride, 5 parts of first emulsifier, 5 parts of second emulsifier, 5 parts of silicone oil, 20 parts of white oil and 5 parts of shea butter;
the phase C comprises: 1 part of benzethonium chloride;
phase D comprises: 1 part of phenoxyethanol.
5. The hand-protecting bacteriostatic cream according to claim 1, which is characterized in that:
the phase A comprises: 65 parts of deionized water, 0.2 part of nylon-methyl ester, 9 parts of glycerol and 0.5 part of surfactin sodium;
the phase B comprises: 3 parts of octadecanol/octadecanol, 3 parts of monoglyceride, 3 parts of a first emulsifier, 2 parts of a second emulsifier, 2 parts of silicone oil, 12 parts of white oil and 4 parts of shea butter;
the phase C comprises: 0.7 part of benzethonium chloride;
phase D comprises: 0.6 part of phenoxyethanol.
6. The preparation method of the hand-protecting bacteriostatic cream according to claim 1, characterized by comprising the following steps:
the preparation of the phase A is as follows: putting the phase A into a water phase tank, and heating until the phase A is dissolved;
the preparation of the B phase is as follows: adding phase B into oil phase tank, heating to dissolve;
mixing and emulsifying the two, and cooling the two by stages;
adding C phase and D phase.
7. The preparation method of the hand-protecting bacteriostatic cream according to claim 6, characterized by comprising the following steps:
heating phase A to 90 deg.C, and heating phase B to 90 deg.C;
the emulsification process comprises the following steps: starting vacuum to-0.05 MPa, pumping two thirds of materials in the water phase tank into an emulsification tank, starting stirring at 800rpm, pumping all oil phases into the emulsification tank, pumping the rest materials in the water phase tank into the emulsification tank, ending vacuum, continuing stirring at 800rpm for 1 minute, stopping stirring, homogenizing at 2800rpm for 5 minutes, starting stirring at 800rpm for 5 minutes, and emulsifying;
the cooling process comprises the following steps: stirring in an emulsification tank at 300rpm after emulsification is finished, introducing cooling water to cool to 75 ℃, vacuumizing to-0.05 MPa, maintaining the pressure for 10 minutes, continuously cooling to 50 ℃, adding the phase C, adding the phase D at 45 ℃, finishing vacuum, continuously stirring at 300rpm, cooling to 30 ℃, and stopping stirring and cooling water.
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| CN202210532533.9A CN114748370A (en) | 2022-05-17 | 2022-05-17 | Hand-protecting bacteriostatic cream and preparation method thereof |
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