CN114702347A - Water-soluble fertilizer purification treatment method - Google Patents

Water-soluble fertilizer purification treatment method Download PDF

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CN114702347A
CN114702347A CN202210327577.8A CN202210327577A CN114702347A CN 114702347 A CN114702347 A CN 114702347A CN 202210327577 A CN202210327577 A CN 202210327577A CN 114702347 A CN114702347 A CN 114702347A
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宋志星
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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05BPHOSPHATIC FERTILISERS
    • C05B1/00Superphosphates, i.e. fertilisers produced by reacting rock or bone phosphates with sulfuric or phosphoric acid in such amounts and concentrations as to yield solid products directly
    • C05B1/02Superphosphates
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05FORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F17/00Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation
    • C05F17/20Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation using specific microorganisms or substances, e.g. enzymes, for activating or stimulating the treatment
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05FORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F17/00Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation
    • C05F17/50Treatments combining two or more different biological or biochemical treatments, e.g. anaerobic and aerobic treatment or vermicomposting and aerobic treatment
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/40Mixtures of one or more fertilisers with additives not having a specially fertilising activity for affecting fertiliser dosage or release rate; for affecting solubility
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/80Soil conditioners
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G5/00Fertilisers characterised by their form
    • C05G5/20Liquid fertilisers

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Organic Chemistry (AREA)
  • Pest Control & Pesticides (AREA)
  • Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Engineering & Computer Science (AREA)
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  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Microbiology (AREA)
  • Tropical Medicine & Parasitology (AREA)
  • Soil Sciences (AREA)
  • Fertilizers (AREA)

Abstract

The invention belongs to the technical field of agricultural fertilizers, and particularly relates to a purification treatment method of a water-soluble fertilizer with few impurities and high purification degree. The water-soluble fertilizer is subjected to twice evaporation purification treatment, so that the impurities are few and the purification degree is high. Through evaporating the ground paste in the washing of evaporation process, with the process of ground paste evaporation condensation, effectively get rid of impurity, improve water-soluble fertilizer's purification degree, effectively improved water-soluble fertilizer's nutrient composition.

Description

Water-soluble fertilizer purification treatment method
Technical Field
The invention belongs to the technical field of agricultural fertilizers, and particularly relates to a purification treatment method of a water-soluble fertilizer with few impurities and high purification degree.
Background
The water-soluble fertilizer is a compound fertilizer containing nitrogen, phosphorus, potassium, calcium, magnesium, trace elements, amino acid, humic acid, alginic acid and the like, which can be completely dissolved in water. Compared with the traditional fertilizer, the water-soluble fertilizer has diversified formula, very flexible application method, and can be irrigated by soil to ensure that the roots of plants can contact the fertilizer comprehensively to absorb various nutrient elements; the fertilizer can be sprayed on the leaf surfaces and enters the interior of the plant through leaf surface pores, so that the absorption and utilization rate of the fertilizer is improved; can also be used for drip irrigation and soilless culture, saves irrigation water and improves the labor production efficiency.
Compared with the traditional granular fertilizer, the water-soluble fertilizer has high purification degree requirement, and the nutrition quality of the water-soluble fertilizer can be influenced by too many impurities. In the prior art, the purification technology of water-soluble fertilizers is still few. Therefore, there is a need for improvements in technology, structural improvements, and improvements in the purity of water-soluble fertilizers.
Disclosure of Invention
In order to solve the defects in the prior art, the technical scheme of the invention provides a purification treatment method of a water-soluble fertilizer with less impurities and high purification degree.
The water-soluble fertilizer comprises pea pods, luffa stems, swamp mahogany leaves, pig nails, an ethanol solution, monopotassium phosphate, magnesium aluminum silicate, bacillus subtilis, bacillus mucilaginosus, saccharomycetes, calcium superphosphate, liquid ammonia, ammonium polyphosphate, diethyl aminoethyl hexanoate, a liquid nitrogen fertilizer, a liquid potassium fertilizer, compound sodium nitrophenolate, ethylicin, polyaspartic acid, polyglutamic acid, alkyl glycoside, ferric sulfate, gibberellin, tetramethyl glutaric acid, ferrous sulfate heptahydrate, meperilate, potassium fulvate, polyacrylamide, boric acid, matrine, a disintegrating agent and a water-soluble synergist;
the purification treatment method of the water-soluble fertilizer comprises the following steps:
step 1: grinding pea pods, luffa stems and eucalyptus robusta leaves into 140-mesh powder of 120 meshes, pouring the powder into a boiling pot, adding an ethanol solution, heating the boiling pot to 87-95 ℃, boiling for 35-70 minutes, adding magnesium aluminum silicate and ammonium polyphosphate, uniformly stirring, and filtering out residues to obtain slurry;
step 2: carrying out first evaporation purification on the slurry obtained in the step 1, keeping the evaporation temperature at 109 ℃, keeping the evaporation time at 60-90 minutes, removing impurities on the surface of the slurry, and dripping washing liquid for washing to obtain purified slurry;
and step 3: grinding the pig nail, filtering the powder to 110-130 meshes, adding potassium dihydrogen phosphate and ethanol solution, soaking for 72-96 hours, uniformly stirring, and filtering out material residues to obtain slurry;
and 4, step 4: pouring the materials obtained in the step 2 and the step 3 into a reaction kettle, stirring the materials in the reaction kettle for 20-30 minutes at the speed of 75-90 revolutions per minute by using a stirrer, pouring bacillus subtilis, bacillus mucilaginosus, saccharomycetes and calcium superphosphate into the reaction kettle, fermenting for 80-96 hours for the first time at the temperature of 70-85 ℃, and turning the reactor during the fermentation process;
and 5: filtering the material residue of the slurry obtained after fermentation in the step 4, placing the obtained slurry in a second reaction kettle, stirring the filtrate in the reaction kettle at the speed of 55-70 r/min, and pouring liquid ammonia into the reaction kettle in the stirring process;
step 6: adding the material obtained in the step 5 into bacillus subtilis, bacillus mucilaginosus, saccharomycetes and calcium superphosphate for secondary fermentation, fermenting for 30-40 hours at the temperature of 70 ℃, and performing pile turning treatment in the fermentation process;
and 7: pouring the slurry obtained by the second fermentation into a third reaction kettle, simultaneously pouring diethyl aminoethyl hexanoate, a liquid nitrogen fertilizer, a liquid potassium fertilizer, compound sodium nitrophenolate, ethylicin, polyaspartic acid, polyglutamic acid, alkyl glycoside, ferric sulfate, gibberellin, tetramethylglutaric acid, ferrous sulfate heptahydrate, mepiquat chloride, potassium fulvate, polyacrylamide, boric acid, matrine, a disintegrating agent and a water-soluble synergist into the third reaction kettle, stirring the slurry in the reaction kettle for 30-45 minutes by using a stirrer at the speed of 55-65 revolutions per minute, and then placing the slurry in a normal temperature environment for 1 hour to obtain a semi-finished product;
and 8: and (3) carrying out secondary evaporation purification on the semi-finished product obtained in the step (7), keeping the evaporation temperature at 95-105 ℃ for 30-50 minutes, then condensing the slurry by using a condenser and removing impurities on the surface of the slurry to obtain purified slurry, and standing the slurry for 1 hour at normal temperature to obtain the finished product.
Preferably, the water-soluble fertilizer comprises, by weight, 40-50 parts of pea pods, 35-45 parts of luffa stems, 25-40 parts of eucalyptus robusta leaves, 50-60 parts of pig nails, 50-55 parts of ethanol solution, 20-30 parts of potassium dihydrogen phosphate, 20-25 parts of magnesium aluminum silicate, 50-60 parts of bacillus subtilis, 30-40 parts of bacillus mucilaginosus, 30-40 parts of saccharomycetes, 50-55 parts of calcium superphosphate, 45-55 parts of liquid ammonia, 20-30 parts of ammonium polyphosphate, 10-15 parts of diethyl aminoethyl hexanoate, 30-40 parts of liquid nitrogen fertilizer, 35-40 parts of liquid potash fertilizer, 10-15 parts of compound sodium nitrophenolate, 5-9 parts of ethylicin, 10-12 parts of polyaspartic acid, 15-20 parts of polyglutamic acid, 10-13 parts of alkyl glycoside, 15-20 parts of ferric sulfate, 15-20 parts of sodium sulfate, and, 10-13 parts of gibberellin, 25-30 parts of tetramethyl glutaric acid, 15-20 parts of ferrous sulfate heptahydrate, 10-15 parts of mepiquat chloride, 5-8 parts of potassium fulvate, 15-25 parts of polyacrylamide, 10-20 parts of boric acid, 5-9 parts of matrine, 10-15 parts of disintegrant and 25-35 parts of water-soluble synergist.
The water-soluble fertilizer comprises highland barley seedlings, asparagus lettuce seedlings, eucalyptus robusta leaves, ungula bovis seu Bubali, ethanol solution, potassium dihydrogen phosphate, magnesium aluminum silicate, ammonium polyphosphate, bacillus subtilis, bacillus mucilaginosus, saccharomycetes, calcium superphosphate, liquid ammonia, phosphoric acid solution, diethyl aminoethyl hexanoate, liquid nitrogen fertilizer, liquid potassium fertilizer, compound sodium nitrophenolate, ethylicin, polyaspartic acid, alkyl glycoside, a-sodium naphthalene acetate, gibberellin, forchlorfenuron, ferrous sulfate heptahydrate, meperilate, potassium fulvate, carbamide, soluble Mo salt, glycine and water-soluble synergist;
the purification treatment method of the water-soluble fertilizer comprises the following steps:
step 1: grinding highland barley seedlings, asparagus lettuce seedlings and swamp mahogany leaves into powder of 115 meshes, pouring the powder into a boiling pot, adding an ethanol solution, heating the boiling pot to 85-88 ℃, boiling for 70 minutes, adding magnesium aluminum silicate and ammonium polyphosphate, uniformly stirring, and filtering material residues to obtain slurry;
step 2: carrying out first evaporation purification on the slurry obtained in the step 1, keeping the evaporation temperature at 109 ℃, carrying out evaporation for 90 minutes, removing impurities on the surface of the slurry, and dripping washing liquid for washing to obtain purified slurry;
and step 3: grinding ungula bovis Seu Bubali, filtering to obtain powder of 105 meshes, adding potassium dihydrogen phosphate and ethanol solution, soaking for 75 hr, stirring, and filtering to remove residue to obtain slurry;
and 4, step 4: pouring the slurry obtained in the step 2 and the step 3 into a reaction kettle, stirring the materials in the reaction kettle for 27 minutes at the speed of 80 revolutions per minute by using a stirrer, pouring bacillus subtilis, bacillus mucilaginosus, saccharomycetes and calcium superphosphate into the reaction kettle, fermenting for the first time for 80 hours at the temperature of 80-90 ℃, and turning during the fermentation process;
and 5: filtering material residues of the slurry obtained after fermentation in the step 4, placing the obtained slurry in a second reaction kettle, stirring the filtrate in the reaction kettle at the speed of 57 revolutions per minute, and pouring liquid ammonia into the reaction kettle in the stirring process;
step 6: adding bacillus subtilis, bacillus mucilaginosus, saccharomycetes and calcium superphosphate into the slurry obtained in the step 5 for secondary fermentation, fermenting for 30 hours at the temperature of 90 ℃, and performing pile turning treatment in the fermentation process;
and 7: pouring the slurry obtained by the second fermentation into a third reaction kettle, and simultaneously pouring phosphoric acid solution, diethyl aminoethyl hexanoate, liquid nitrogen fertilizer, liquid potassium fertilizer, compound sodium nitrophenolate, ethylicin, polyaspartic acid, alkyl glycoside, alpha-sodium naphthalene acetate, gibberellin, forchlorfenuron, ferrous sulfate heptahydrate, meperilate, potassium fulvate, carbamide, soluble Mo salt, glycine and water-soluble synergist into the third reaction kettle, stirring the slurry in the reaction kettle for 45 minutes by using a stirrer at the speed of 55 revolutions per minute, and then placing the slurry in a normal temperature environment for 1 hour to obtain a semi-finished product;
and 8: and (3) carrying out secondary evaporation purification on the semi-finished product obtained in the step (7), keeping the evaporation temperature at 95-105 ℃, carrying out evaporation for 45 minutes, then condensing the slurry by using a condenser and removing impurities on the surface of the slurry to obtain purified slurry, and standing the slurry for 1 hour at normal temperature to obtain the finished product.
Preferably, the water-soluble fertilizer comprises, by weight, 30-45 parts of highland barley seedlings, 30-40 parts of asparagus lettuce seedlings, 25-30 parts of eucalyptus robusta leaves, 50-60 parts of bauhinia variegata, 35-45 parts of ethanol solution, 26-30 parts of monopotassium phosphate, 20-30 parts of magnesium aluminum silicate, 17-25 parts of ammonium polyphosphate, 25-35 parts of bacillus subtilis, 40-50 parts of bacillus mucilaginosus, 50-60 parts of saccharomycetes, 45-50 parts of calcium superphosphate, 35-45 parts of liquid ammonia, 35-40 parts of phosphoric acid solution, 10-15 parts of diethyl aminoethyl hexanoate, 20-30 parts of liquid nitrogen fertilizer, 25-30 parts of liquid potassium fertilizer, 20-27 parts of compound sodium nitrophenolate, 10-14 parts of ethylicin, 5-9 parts of polyaspartic acid, 25-35 parts of alkyl glycoside, and the like, 15-20 parts of alpha-sodium naphthalene acetate, 15-19 parts of gibberellin, 5-8 parts of forchlorfenuron, 15-19 parts of ferrous sulfate heptahydrate, 5-12 parts of radix aristolochiae, 15-20 parts of potassium fulvate, 26-30 parts of carbamide, 25-34 parts of soluble Mo salt, 15-18 parts of glycine and 30-35 parts of water-soluble synergist.
The water-soluble fertilizer is subjected to twice evaporation purification treatment, so that the impurities are few and the purification degree is high. Through evaporating and washing the slurry in the evaporation process, impurities are effectively removed in the process of evaporating and condensing the slurry, the purification degree of the water-soluble fertilizer is improved, and the nutrient quality of the water-soluble fertilizer is effectively improved.
The invention takes the waste crop seedling stems and fallen leaves as one of the raw materials, realizes the secondary reutilization of the waste, saves the energy and has good environmental protection effect. The water-soluble fertilizer has high nutritive value, and is added with biological components such as pig nail, cow nail and the like. The slurry is subjected to secondary fermentation, the nutrient content of the finished product is higher, and the slurry in the reaction kettle reacts more fully by pouring liquid ammonia into the reaction kettle in the stirring process. The water-soluble fertilizer can increase the soil nutrition, promote the growth of various enzymes, improve the fiber decomposability and other excellent biological characteristics, has good fertilizer effect, and can continuously improve the soil nutrition condition. The invention is suitable for popularization and application in related fields.
Detailed Description
The present invention will now be described in more detail, wherein preferred embodiments of the invention are shown, it being understood that one skilled in the art may modify the invention herein described while still achieving the advantageous results of the invention. Accordingly, the following description should be construed as broadly as possible to those skilled in the art and not as limiting the invention.
In the interest of clarity, not all features of an actual implementation are described. In the following description, well-known functions or constructions are not described in detail since they would obscure the invention in unnecessary detail. It will of course be appreciated that in the development of any such actual embodiment, numerous implementation-specific details may be set forth in order to achieve the developer's specific goals, such as compliance with system-related and business-related constraints, which may vary from one implementation to another. Moreover, it will be appreciated that such a development effort might be complex and time-consuming, but would nevertheless be a routine undertaking for those of ordinary skill in the art.
The purpose and features of the present invention will be more clearly understood through the following detailed description of the preferred embodiments of the present invention.
The first embodiment is as follows:
the water-soluble fertilizer comprises 45 parts of pea pods, 35 parts of luffa stems, 30 parts of eucalyptus robusta leaves, 50 parts of pig nails, 50 parts of ethanol solution, 30 parts of monopotassium phosphate, 25 parts of magnesium aluminum silicate, 60 parts of bacillus subtilis, 40 parts of bacillus mucilaginosus, 30 parts of yeast, 52 parts of calcium superphosphate, 48 parts of liquid ammonia, 25 parts of ammonium polyphosphate, 10 parts of diethyl aminoethyl hexanoate, 36 parts of liquid nitrogen fertilizer, 39 parts of liquid potash fertilizer, 10 parts of compound sodium nitrophenolate, 9 parts of ethylicin, 11 parts of polyaspartic acid, 15 parts of polyglutamic acid, 12 parts of alkyl glycoside, 15 parts of ferric sulfate, 11 parts of gibberellin, 27 parts of tetramethyl glutaric acid, 20 parts of ferrous sulfate heptahydrate, 15 parts of meperilate, 7 parts of potassium fulvic acid, 19 parts of polyacrylamide, 17 parts of boric acid, 9 parts of matrine, 13 parts of disintegrant and 29 parts of water-soluble synergist.
The purification treatment method of the water-soluble fertilizer comprises the following steps:
step 1: grinding pea pods, luffa stems and swamp mahogany leaves into powder of 130 meshes, pouring the powder into a boiling pot, adding an ethanol solution, heating the boiling pot to 90-95 ℃, boiling for 65 minutes, adding magnesium aluminum silicate and ammonium polyphosphate, uniformly stirring, and filtering out residues to obtain slurry;
step 2: carrying out first evaporation purification on the slurry obtained in the step 1, keeping the evaporation temperature at 109 ℃, keeping the evaporation time at 80 minutes, removing impurities on the surface of the slurry, and dripping washing liquid for washing to obtain the purified slurry;
and step 3: grinding ungula Sus Domestica, filtering to obtain powder of 130 meshes, adding potassium dihydrogen phosphate and ethanol solution, soaking for 90 hr, stirring, and filtering to remove residue to obtain slurry;
and 4, step 4: pouring the materials obtained in the step 2 and the step 3 into a reaction kettle, stirring the materials in the reaction kettle for 20 minutes at the speed of 90 revolutions per minute by using a stirrer, pouring bacillus subtilis, bacillus mucilaginosus, saccharomycetes and calcium superphosphate into the reaction kettle, fermenting for the first time for 90 hours at the temperature of 70-85 ℃, and turning the reactor during the fermentation process;
and 5: filtering material residues of the slurry obtained after fermentation in the step 4, placing the obtained slurry in a second reaction kettle, stirring the filtrate in the reaction kettle at the speed of 70 r/min, and pouring liquid ammonia into the reaction kettle in the stirring process;
step 6: adding the material obtained in the step 5 into bacillus subtilis, bacillus mucilaginosus, saccharomycetes and calcium superphosphate for secondary fermentation, fermenting for 40 hours at the temperature of 70 ℃, and performing pile turning treatment in the fermentation process;
and 7: pouring the slurry obtained by the second fermentation into a third reaction kettle, and simultaneously pouring diethyl aminoethyl hexanoate, a liquid nitrogen fertilizer, a liquid potassium fertilizer, compound sodium nitrophenolate, ethylicin, polyaspartic acid, polyglutamic acid, alkyl glycoside, ferric sulfate, gibberellin, tetramethylglutaric acid, ferrous sulfate heptahydrate, mepiquat, potassium fulvate, polyacrylamide, boric acid, matrine, a disintegrating agent and a water-soluble synergist into the third reaction kettle, stirring the slurry in the reaction kettle for 35 minutes by using a stirrer at the speed of 60 revolutions per minute, and then standing the slurry for 1 hour in a normal temperature environment to obtain a semi-finished product;
and 8: and (4) carrying out secondary evaporation purification on the semi-finished product obtained in the step (7), keeping the evaporation temperature at 95-105 ℃, carrying out evaporation for 40 minutes, condensing the slurry by using a condenser, removing impurities on the surface of the slurry to obtain purified slurry, and standing the slurry for 1 hour at normal temperature to obtain the finished product.
The content of nutrient elements of the water-soluble fertilizer subjected to purification treatment in the embodiment of the invention is compared with the content of nutrient elements of the water-soluble fertilizer not subjected to purification treatment in the prior art by the following table:
Figure BSA0000269662250000091
(watch one)
As can be seen from the table I, the content of the nutrient elements of the water-soluble fertilizer subjected to purification treatment in the embodiment of the invention is higher than that of the nutrient elements of the water-soluble fertilizer not subjected to purification treatment in the prior art. The water-soluble fertilizer purification treatment can obviously increase the content of nutrient elements of the water-soluble fertilizer.
Example two:
the water-soluble fertilizer comprises, by weight, 31 parts of highland barley seedlings, 37 parts of asparagus lettuce seedlings, 29 parts of eucalyptus robusta leaves, 60 parts of beef nails, 39 parts of ethanol solution, 30 parts of monopotassium phosphate, 21 parts of magnesium aluminum silicate, 25 parts of ammonium polyphosphate, 25 parts of bacillus subtilis, 41 parts of bacillus mucilaginosus, 50 parts of saccharomycetes, 50 parts of calcium superphosphate, 35 parts of liquid ammonia, 38 parts of phosphoric acid solution, 15 parts of diethyl aminoethyl hexanoate, 27 parts of liquid nitrogen fertilizer, 25 parts of liquid potash fertilizer, 27 parts of compound sodium nitrophenolate, 14 parts of ethylicin, 8 parts of polyaspartic acid, 27 parts of alkyl glycoside, 20 parts of a-sodium naphthalene acetate, 16 parts of gibberellin, 8 parts of forchlorfenuron, 19 parts of ferrous sulfate heptahydrate, 12 parts of piperazine, 17 parts of potassium fulvate, 26 parts of carbamide, 34 parts of soluble Mo salt, 18 parts of glycine and 30 parts of synergistic water-soluble agent.
The purification treatment method of the water-soluble fertilizer comprises the following steps:
step 1: grinding highland barley seedlings, asparagus lettuce seedlings and swamp mahogany leaves into powder of 115 meshes, pouring the powder into a boiling pot, adding an ethanol solution, heating the boiling pot to 85-88 ℃, boiling for 70 minutes, adding magnesium aluminum silicate and ammonium polyphosphate, uniformly stirring, and filtering material residues to obtain slurry;
step 2: carrying out first evaporation purification on the slurry obtained in the step 1, keeping the evaporation temperature at 109 ℃, carrying out evaporation for 90 minutes, removing impurities on the surface of the slurry, and dripping washing liquid for washing to obtain purified slurry;
and step 3: grinding ungula bovis Seu Bubali, filtering to obtain powder of 105 meshes, adding potassium dihydrogen phosphate and ethanol solution, soaking for 75 hr, stirring, and filtering to remove residue to obtain slurry;
and 4, step 4: pouring the slurry obtained in the step 2 and the step 3 into a reaction kettle, stirring the materials in the reaction kettle for 27 minutes at the speed of 80 revolutions per minute by using a stirrer, pouring bacillus subtilis, bacillus mucilaginosus, saccharomycetes and calcium superphosphate into the reaction kettle, fermenting for the first time for 80 hours at the temperature of 80-90 ℃, and turning during the fermentation process;
and 5: filtering material residues of the slurry obtained after fermentation in the step 4, placing the obtained slurry in a second reaction kettle, stirring the filtrate in the reaction kettle at the speed of 57 revolutions per minute, and pouring liquid ammonia into the reaction kettle in the stirring process;
step 6: adding bacillus subtilis, bacillus mucilaginosus, saccharomycetes and calcium superphosphate into the slurry obtained in the step 5 for secondary fermentation, fermenting for 30 hours at the temperature of 90 ℃, and performing pile turning treatment in the fermentation process;
and 7: pouring the slurry obtained by the second fermentation into a third reaction kettle, simultaneously pouring a phosphoric acid solution, diethyl aminoethyl hexanoate, a liquid nitrogen fertilizer, a liquid potassium fertilizer, compound sodium nitrophenolate, ethylicin, polyaspartic acid, alkyl glycoside, a-sodium naphthalene acetate, gibberellin, forchlorfenuron, ferrous sulfate heptahydrate, meperidine, potassium fulvate, carbonamide, soluble Mo salt, glycine and a water-soluble synergist, stirring the slurry in the reaction kettle for 45 minutes at the speed of 55 revolutions per minute by using a stirrer, and then standing for 1 hour under a normal temperature environment to obtain a semi-finished product;
and 8: and (3) carrying out secondary evaporation purification on the semi-finished product obtained in the step (7), keeping the evaporation temperature at 95-105 ℃, carrying out evaporation for 45 minutes, then condensing the slurry by using a condenser and removing impurities on the surface of the slurry to obtain purified slurry, and standing the slurry for 1 hour at normal temperature to obtain the finished product.
The nutrient element content of the water-soluble fertilizer subjected to purification treatment in the second embodiment of the invention is compared with the nutrient element content of the water-soluble fertilizer not subjected to purification treatment in the prior art as shown in the table:
Figure BSA0000269662250000121
(watch two)
As can be seen from the table II, the content of the nutrient elements of the water-soluble fertilizer subjected to purification treatment in the second embodiment of the invention is higher than that of the nutrient elements of the water-soluble fertilizer not subjected to purification treatment in the prior art. The water-soluble fertilizer purification treatment can obviously increase the content of nutrient elements of the water-soluble fertilizer.
Various modifications to these embodiments will be readily apparent to those skilled in the art, and the generic principles defined herein may be applied to other embodiments without departing from the spirit or scope of the embodiments. Thus, the present embodiments are not intended to be limited to the embodiments shown herein but are to be accorded the widest scope consistent with the principles and novel features disclosed herein.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and should not be taken as limiting the scope of the present invention, which is intended to cover any modifications, equivalents, improvements, etc. within the spirit and principle of the present invention.

Claims (4)

1. A purification treatment method of a water-soluble fertilizer is characterized in that the water-soluble fertilizer comprises pea pods, luffa stems, eucalyptus robusta leaves, pig nails, an ethanol solution, monopotassium phosphate, magnesium aluminum silicate, bacillus subtilis, bacillus mucilaginosus, saccharomycetes, calcium superphosphate, liquid ammonia, ammonium polyphosphate, diethyl aminoethyl hexanoate, a liquid nitrogen fertilizer, a liquid potassium fertilizer, compound sodium nitrophenolate, ethylicin, polyaspartic acid, polyglutamic acid, alkyl glycoside, ferric sulfate, gibberellin, tetramethyl glutaric acid, ferrous sulfate heptahydrate, mepiquat chloride, potassium fulvate, polyacrylamide, boric acid, matrine, a disintegrating agent and a water-soluble synergist;
the purification treatment method of the water-soluble fertilizer comprises the following steps:
step 1: grinding pea pods, luffa stems and eucalyptus robusta leaves into 140-mesh powder of 120 meshes, pouring the powder into a boiling pot, adding an ethanol solution, heating the boiling pot to 87-95 ℃, boiling for 35-70 minutes, adding magnesium aluminum silicate and ammonium polyphosphate, uniformly stirring, and filtering out residues to obtain slurry;
step 2: carrying out first evaporation purification on the slurry obtained in the step 1, keeping the evaporation temperature at 109 ℃, keeping the evaporation time at 60-90 minutes, removing impurities on the surface of the slurry, and dripping washing liquid for washing to obtain purified slurry;
and step 3: grinding the pig nail, filtering the powder to 110-130 meshes, adding potassium dihydrogen phosphate and ethanol solution, soaking for 72-96 hours, uniformly stirring, and filtering out material residues to obtain slurry;
and 4, step 4: pouring the materials obtained in the step (2) and the step (3) into a reaction kettle, stirring the materials in the reaction kettle for 20-30 minutes by using a stirrer at the speed of 75-90 revolutions per minute, pouring bacillus subtilis, bacillus mucilaginosus, saccharomycetes and calcium superphosphate into the reaction kettle, performing primary fermentation for 80-96 hours at the temperature of 70-85 ℃, and performing pile turning treatment in the fermentation process;
and 5: filtering the material residue of the slurry obtained after fermentation in the step 4, placing the obtained slurry in a second reaction kettle, stirring the filtrate in the reaction kettle at the speed of 55-70 r/min, and pouring liquid ammonia into the reaction kettle in the stirring process;
step 6: adding the material obtained in the step 5 into bacillus subtilis, bacillus mucilaginosus, saccharomycetes and calcium superphosphate for secondary fermentation, fermenting for 30-40 hours at the temperature of 70 ℃, and performing pile turning treatment in the fermentation process;
and 7: pouring the slurry obtained by the second fermentation into a third reaction kettle, and simultaneously pouring diethyl aminoethyl hexanoate, a liquid nitrogen fertilizer, a liquid potassium fertilizer, compound sodium nitrophenolate, ethylicin, polyaspartic acid, polyglutamic acid, alkyl glycoside, ferric sulfate, gibberellin, tetramethylglutaric acid, ferrous sulfate heptahydrate, mepiquat, potassium fulvate, polyacrylamide, boric acid, matrine, a disintegrating agent and a water-soluble synergist into the third reaction kettle, stirring the slurry in the reaction kettle for 30-45 minutes by using a stirrer at the speed of 55-65 revolutions per minute, and then standing the slurry for 1 hour under the normal temperature environment to obtain a semi-finished product;
and 8: and (3) carrying out secondary evaporation purification on the semi-finished product obtained in the step (7), keeping the evaporation temperature at 95-105 ℃ for 30-50 minutes, then condensing the slurry by using a condenser and removing impurities on the surface of the slurry to obtain purified slurry, and standing the slurry for 1 hour at normal temperature to obtain the finished product.
2. The purification treatment method of the water-soluble fertilizer as claimed in claim 1, wherein the water-soluble fertilizer comprises 40-50 parts of pea pod, 35-45 parts of luffa stem, 25-40 parts of eucalyptus robusta leaf, 50-60 parts of pig nail, 50-55 parts of ethanol solution, 20-30 parts of potassium dihydrogen phosphate, 20-25 parts of magnesium aluminum silicate, 50-60 parts of bacillus subtilis, 30-40 parts of bacillus mucilaginosus, 30-40 parts of saccharomycetes, 50-55 parts of calcium superphosphate, 45-55 parts of liquid ammonia, 20-30 parts of ammonium polyphosphate, 10-15 parts of diethyl aminoethyl hexanoate, 30-40 parts of liquid nitrogen fertilizer, 35-40 parts of liquid potassium fertilizer, 10-15 parts of compound sodium nitrophenolate, 5-9 parts of ethylicin, 10-12 parts of polyaspartic acid, 15-20 parts of polyglutamic acid, 10-13 parts of alkyl glycoside, 15-20 parts of ferric sulfate, 10-13 parts of gibberellin, 25-30 parts of tetramethyl glutaric acid, 15-20 parts of ferrous sulfate heptahydrate, 10-15 parts of radix pulsatillae, 5-8 parts of potassium fulvate, 15-25 parts of polyacrylamide, 10-20 parts of boric acid, 5-9 parts of matrine, 10-15 parts of disintegrant and 25-35 parts of water-soluble synergist.
3. A water-soluble fertilizer purification treatment method is characterized in that components of the water-soluble fertilizer comprise highland barley seedlings, asparagus lettuce seedlings, eucalyptus robusta leaves, ungula bovis seu Bubali, an ethanol solution, monopotassium phosphate, magnesium aluminum silicate, ammonium polyphosphate, bacillus subtilis, bacillus mucilaginosus, saccharomycetes, calcium superphosphate, liquid ammonia, a phosphoric acid solution, diethyl aminoethyl hexanoate, a liquid nitrogen fertilizer, a liquid potash fertilizer, compound sodium nitrophenolate, ethylicin, polyaspartic acid, alkyl glycoside, a-sodium naphthalene acetate, gibberellin, forchlorfenuron, ferrous sulfate heptahydrate, meperilate, potassium fulvate, carbamide, soluble Mo salt, glycine and a water-soluble synergist;
the purification treatment method of the water-soluble fertilizer comprises the following steps:
step 1: grinding highland barley seedlings, asparagus lettuce seedlings and swamp mahogany leaves into powder of 115 meshes, pouring the powder into a boiling pot, adding an ethanol solution, heating the boiling pot to 85-88 ℃, boiling for 70 minutes, adding magnesium aluminum silicate and ammonium polyphosphate, uniformly stirring, and filtering material residues to obtain slurry;
step 2: carrying out first evaporation purification on the slurry obtained in the step 1, keeping the evaporation temperature at 109 ℃, carrying out evaporation for 90 minutes, removing impurities on the surface of the slurry, and dripping washing liquid for washing to obtain purified slurry;
and step 3: grinding ungula bovis Seu Bubali, filtering to obtain powder of 105 meshes, adding potassium dihydrogen phosphate and ethanol solution, soaking for 75 hr, stirring, and filtering to remove residue to obtain slurry;
and 4, step 4: pouring the slurry obtained in the step 2 and the step 3 into a reaction kettle, stirring the materials in the reaction kettle for 27 minutes at the speed of 80 revolutions per minute by using a stirrer, pouring bacillus subtilis, bacillus mucilaginosus, saccharomycetes and calcium superphosphate into the reaction kettle, fermenting for the first time for 80 hours at the temperature of 80-90 ℃, and turning during the fermentation process;
and 5: filtering material residues of the slurry obtained after fermentation in the step 4, placing the obtained slurry in a second reaction kettle, stirring the filtrate in the reaction kettle at the speed of 57 revolutions per minute, and pouring liquid ammonia into the reaction kettle in the stirring process;
step 6: adding bacillus subtilis, bacillus mucilaginosus, saccharomycetes and calcium superphosphate into the slurry obtained in the step 5 for secondary fermentation, fermenting for 30 hours at the temperature of 90 ℃, and performing pile turning treatment in the fermentation process;
and 7: pouring the slurry obtained by the second fermentation into a third reaction kettle, and simultaneously pouring phosphoric acid solution, diethyl aminoethyl hexanoate, liquid nitrogen fertilizer, liquid potassium fertilizer, compound sodium nitrophenolate, ethylicin, polyaspartic acid, alkyl glycoside, alpha-sodium naphthalene acetate, gibberellin, forchlorfenuron, ferrous sulfate heptahydrate, meperilate, potassium fulvate, carbamide, soluble Mo salt, glycine and water-soluble synergist into the third reaction kettle, stirring the slurry in the reaction kettle for 45 minutes by using a stirrer at the speed of 55 revolutions per minute, and then placing the slurry in a normal temperature environment for 1 hour to obtain a semi-finished product;
and 8: and (3) carrying out secondary evaporation purification on the semi-finished product obtained in the step (7), keeping the evaporation temperature at 95-105 ℃, carrying out evaporation for 45 minutes, then condensing the slurry by using a condenser and removing impurities on the surface of the slurry to obtain purified slurry, and standing the slurry for 1 hour at normal temperature to obtain the finished product.
4. The water-soluble fertilizer purification treatment method as claimed in claim 3, wherein the water-soluble fertilizer comprises 30-45 parts of highland barley seedlings, 30-40 parts of asparagus lettuce seedlings, 25-30 parts of eucalyptus robusta leaves, 50-60 parts of bovine nails, 35-45 parts of ethanol solution, 26-30 parts of potassium dihydrogen phosphate, 20-30 parts of magnesium aluminum silicate, 17-25 parts of ammonium polyphosphate, 25-35 parts of bacillus subtilis, 40-50 parts of bacillus mucilaginosus, 50-60 parts of yeast, 45-50 parts of calcium superphosphate, 35-45 parts of liquid ammonia, 35-40 parts of phosphoric acid solution, 10-15 parts of diethyl aminoethyl hexanoate, 20-30 parts of liquid nitrogen fertilizer, 25-30 parts of liquid potassium fertilizer, 20-27 parts of compound sodium nitrophenolate, 10-14 parts of ethylicin, 5-9 parts of polyaspartic acid, 25-35 parts of alkyl glycoside, 15-20 parts of a-sodium naphthalene acetate, 15-19 parts of gibberellin, 5-8 parts of forchlorfenuron, 15-19 parts of ferrous sulfate heptahydrate, 5-12 parts of mepiquat chloride, 15-20 parts of potassium fulvate, 26-30 parts of carbamide, 25-34 parts of soluble Mo salt, 15-18 parts of glycine and 30-35 parts of water-soluble synergist.
CN202210327577.8A 2022-03-29 2022-03-29 Water-soluble fertilizer purification treatment method Pending CN114702347A (en)

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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104513108A (en) * 2013-09-30 2015-04-15 洪秋 Water-soluble fertilizer
CN105924314A (en) * 2016-04-22 2016-09-07 广西喷施宝股份有限公司 Water-soluble fertilizer and preparation method thereof
CN107445726A (en) * 2017-09-21 2017-12-08 阿米巴南京生物技术有限责任公司 A kind of organic water-soluble fertilizer and preparation method
CN107954796A (en) * 2017-11-25 2018-04-24 贵阳开磷化肥有限公司 A kind of novel soybean Water soluble fertilizer and preparation method thereof
CN111978130A (en) * 2019-05-22 2020-11-24 兰登国际科技有限公司 Water-soluble fertilizer
CN113603546A (en) * 2021-09-16 2021-11-05 宁夏天瑞鸣钟农化有限公司 Water-soluble fertilizer synergist and preparation method and application method thereof

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104513108A (en) * 2013-09-30 2015-04-15 洪秋 Water-soluble fertilizer
CN105924314A (en) * 2016-04-22 2016-09-07 广西喷施宝股份有限公司 Water-soluble fertilizer and preparation method thereof
CN107445726A (en) * 2017-09-21 2017-12-08 阿米巴南京生物技术有限责任公司 A kind of organic water-soluble fertilizer and preparation method
CN107954796A (en) * 2017-11-25 2018-04-24 贵阳开磷化肥有限公司 A kind of novel soybean Water soluble fertilizer and preparation method thereof
CN111978130A (en) * 2019-05-22 2020-11-24 兰登国际科技有限公司 Water-soluble fertilizer
CN113603546A (en) * 2021-09-16 2021-11-05 宁夏天瑞鸣钟农化有限公司 Water-soluble fertilizer synergist and preparation method and application method thereof

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