CN114702347A - Water-soluble fertilizer purification treatment method - Google Patents
Water-soluble fertilizer purification treatment method Download PDFInfo
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- CN114702347A CN114702347A CN202210327577.8A CN202210327577A CN114702347A CN 114702347 A CN114702347 A CN 114702347A CN 202210327577 A CN202210327577 A CN 202210327577A CN 114702347 A CN114702347 A CN 114702347A
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- 239000003337 fertilizer Substances 0.000 title claims abstract description 76
- 238000000746 purification Methods 0.000 title claims abstract description 48
- 238000000034 method Methods 0.000 title claims abstract description 27
- 238000001704 evaporation Methods 0.000 claims abstract description 42
- 230000008020 evaporation Effects 0.000 claims abstract description 39
- 239000012535 impurity Substances 0.000 claims abstract description 20
- 238000005406 washing Methods 0.000 claims abstract description 14
- 230000008569 process Effects 0.000 claims abstract description 11
- 239000002002 slurry Substances 0.000 claims description 93
- 238000006243 chemical reaction Methods 0.000 claims description 55
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 44
- 239000007788 liquid Substances 0.000 claims description 38
- -1 compound sodium nitrophenolate Chemical class 0.000 claims description 37
- 238000003756 stirring Methods 0.000 claims description 37
- 238000000855 fermentation Methods 0.000 claims description 32
- 230000004151 fermentation Effects 0.000 claims description 32
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 29
- 239000011591 potassium Substances 0.000 claims description 29
- 229910052700 potassium Inorganic materials 0.000 claims description 29
- 238000001914 filtration Methods 0.000 claims description 24
- 239000000463 material Substances 0.000 claims description 23
- 244000063299 Bacillus subtilis Species 0.000 claims description 22
- 235000014469 Bacillus subtilis Nutrition 0.000 claims description 22
- 241000881860 Paenibacillus mucilaginosus Species 0.000 claims description 22
- 239000007633 bacillus mucilaginosus Substances 0.000 claims description 22
- YYRMJZQKEFZXMX-UHFFFAOYSA-L calcium bis(dihydrogenphosphate) Chemical compound [Ca+2].OP(O)([O-])=O.OP(O)([O-])=O YYRMJZQKEFZXMX-UHFFFAOYSA-L 0.000 claims description 22
- 229910000389 calcium phosphate Inorganic materials 0.000 claims description 22
- 235000019691 monocalcium phosphate Nutrition 0.000 claims description 22
- 241000235342 Saccharomycetes Species 0.000 claims description 20
- 238000009835 boiling Methods 0.000 claims description 18
- 239000000843 powder Substances 0.000 claims description 18
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 17
- OICGFSUWXCJLCO-UHFFFAOYSA-N 1-ethylsulfonylsulfanylethane Chemical compound CCSS(=O)(=O)CC OICGFSUWXCJLCO-UHFFFAOYSA-N 0.000 claims description 16
- 239000004114 Ammonium polyphosphate Substances 0.000 claims description 16
- OORIKNJWZHTXDC-UHFFFAOYSA-N CCCC(CC)C(CC)(C(=O)OCC)N Chemical compound CCCC(CC)C(CC)(C(=O)OCC)N OORIKNJWZHTXDC-UHFFFAOYSA-N 0.000 claims description 16
- 229930191978 Gibberellin Natural products 0.000 claims description 16
- DHMQDGOQFOQNFH-UHFFFAOYSA-N Glycine Chemical compound NCC(O)=O DHMQDGOQFOQNFH-UHFFFAOYSA-N 0.000 claims description 16
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 16
- 229920000805 Polyaspartic acid Polymers 0.000 claims description 16
- SNAAJJQQZSMGQD-UHFFFAOYSA-N aluminum magnesium Chemical compound [Mg].[Al] SNAAJJQQZSMGQD-UHFFFAOYSA-N 0.000 claims description 16
- 235000019826 ammonium polyphosphate Nutrition 0.000 claims description 16
- 229920001276 ammonium polyphosphate Polymers 0.000 claims description 16
- IXORZMNAPKEEDV-UHFFFAOYSA-N gibberellic acid GA3 Natural products OC(=O)C1C2(C3)CC(=C)C3(O)CCC2C2(C=CC3O)C1C3(C)C(=O)O2 IXORZMNAPKEEDV-UHFFFAOYSA-N 0.000 claims description 16
- 239000003448 gibberellin Substances 0.000 claims description 16
- 229930182470 glycoside Natural products 0.000 claims description 16
- SURQXAFEQWPFPV-UHFFFAOYSA-L iron(2+) sulfate heptahydrate Chemical compound O.O.O.O.O.O.O.[Fe+2].[O-]S([O-])(=O)=O SURQXAFEQWPFPV-UHFFFAOYSA-L 0.000 claims description 16
- 229910000402 monopotassium phosphate Inorganic materials 0.000 claims description 16
- 235000019796 monopotassium phosphate Nutrition 0.000 claims description 16
- 239000000618 nitrogen fertilizer Substances 0.000 claims description 16
- 108010064470 polyaspartate Proteins 0.000 claims description 16
- 244000239645 swamp mahogany Species 0.000 claims description 16
- 235000005221 swamp mahogany Nutrition 0.000 claims description 16
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims description 14
- 238000000227 grinding Methods 0.000 claims description 12
- 239000011265 semifinished product Substances 0.000 claims description 12
- PJNZPQUBCPKICU-UHFFFAOYSA-N phosphoric acid;potassium Chemical compound [K].OP(O)(O)=O PJNZPQUBCPKICU-UHFFFAOYSA-N 0.000 claims description 10
- ZBJKOZDGZGTMJX-UHFFFAOYSA-N 2,2,4,4-tetramethylpentanedioic acid Chemical compound OC(=O)C(C)(C)CC(C)(C)C(O)=O ZBJKOZDGZGTMJX-UHFFFAOYSA-N 0.000 claims description 8
- 239000005979 Forchlorfenuron Substances 0.000 claims description 8
- 239000004471 Glycine Substances 0.000 claims description 8
- 240000005979 Hordeum vulgare Species 0.000 claims description 8
- 235000007340 Hordeum vulgare Nutrition 0.000 claims description 8
- ZSBXGIUJOOQZMP-UHFFFAOYSA-N Isomatrine Natural products C1CCC2CN3C(=O)CCCC3C3C2N1CCC3 ZSBXGIUJOOQZMP-UHFFFAOYSA-N 0.000 claims description 8
- 235000003956 Luffa Nutrition 0.000 claims description 8
- 244000050983 Luffa operculata Species 0.000 claims description 8
- ZSBXGIUJOOQZMP-JLNYLFASSA-N Matrine Chemical compound C1CC[C@H]2CN3C(=O)CCC[C@@H]3[C@@H]3[C@H]2N1CCC3 ZSBXGIUJOOQZMP-JLNYLFASSA-N 0.000 claims description 8
- 108010020346 Polyglutamic Acid Proteins 0.000 claims description 8
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 8
- 244000046738 asparagus lettuce Species 0.000 claims description 8
- 235000006705 asparagus lettuce Nutrition 0.000 claims description 8
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 claims description 8
- 239000004327 boric acid Substances 0.000 claims description 8
- GPXLRLUVLMHHIK-UHFFFAOYSA-N forchlorfenuron Chemical compound C1=NC(Cl)=CC(NC(=O)NC=2C=CC=CC=2)=C1 GPXLRLUVLMHHIK-UHFFFAOYSA-N 0.000 claims description 8
- RUTXIHLAWFEWGM-UHFFFAOYSA-H iron(3+) sulfate Chemical compound [Fe+3].[Fe+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O RUTXIHLAWFEWGM-UHFFFAOYSA-H 0.000 claims description 8
- 229910000360 iron(III) sulfate Inorganic materials 0.000 claims description 8
- 229930014456 matrine Natural products 0.000 claims description 8
- 229920002401 polyacrylamide Polymers 0.000 claims description 8
- 229920002643 polyglutamic acid Polymers 0.000 claims description 8
- 150000003839 salts Chemical class 0.000 claims description 8
- 239000004202 carbamide Substances 0.000 claims description 7
- 235000013877 carbamide Nutrition 0.000 claims description 7
- 239000000047 product Substances 0.000 claims description 7
- 239000003795 chemical substances by application Substances 0.000 claims description 6
- 239000000706 filtrate Substances 0.000 claims description 6
- 238000010438 heat treatment Methods 0.000 claims description 6
- GNSKLFRGEWLPPA-UHFFFAOYSA-M potassium dihydrogen phosphate Chemical compound [K+].OP(O)([O-])=O GNSKLFRGEWLPPA-UHFFFAOYSA-M 0.000 claims description 6
- LWIHDJKSTIGBAC-UHFFFAOYSA-K potassium phosphate Substances [K+].[K+].[K+].[O-]P([O-])([O-])=O LWIHDJKSTIGBAC-UHFFFAOYSA-K 0.000 claims description 6
- 238000002791 soaking Methods 0.000 claims description 6
- DARPYRSDRJYGIF-PTNGSMBKSA-N (Z)-3-ethoxy-2-naphthalen-2-ylsulfonylprop-2-enenitrile Chemical compound C1=CC=CC2=CC(S(=O)(=O)C(\C#N)=C/OCC)=CC=C21 DARPYRSDRJYGIF-PTNGSMBKSA-N 0.000 claims description 4
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 4
- 229940072033 potash Drugs 0.000 claims description 4
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Substances [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 claims description 4
- 235000015320 potassium carbonate Nutrition 0.000 claims description 4
- 239000007884 disintegrant Substances 0.000 claims description 3
- 239000000243 solution Substances 0.000 claims description 3
- 239000005984 Mepiquat Substances 0.000 claims description 2
- 240000004808 Saccharomyces cerevisiae Species 0.000 claims description 2
- NNCAWEWCFVZOGF-UHFFFAOYSA-N mepiquat Chemical compound C[N+]1(C)CCCCC1 NNCAWEWCFVZOGF-UHFFFAOYSA-N 0.000 claims description 2
- 241000283690 Bos taurus Species 0.000 claims 1
- 239000009806 pulsatillae Substances 0.000 claims 1
- 235000015097 nutrients Nutrition 0.000 abstract description 13
- 238000009833 condensation Methods 0.000 abstract 1
- 230000005494 condensation Effects 0.000 abstract 1
- 241000282898 Sus scrofa Species 0.000 description 5
- 235000016709 nutrition Nutrition 0.000 description 3
- 230000035764 nutrition Effects 0.000 description 3
- 239000002689 soil Substances 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 2
- GLUUGHFHXGJENI-UHFFFAOYSA-N Piperazine Chemical compound C1CNCCN1 GLUUGHFHXGJENI-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- PUKLDDOGISCFCP-JSQCKWNTSA-N 21-Deoxycortisone Chemical compound C1CC2=CC(=O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@@](C(=O)C)(O)[C@@]1(C)CC2=O PUKLDDOGISCFCP-JSQCKWNTSA-N 0.000 description 1
- QJZYHAIUNVAGQP-UHFFFAOYSA-N 3-nitrobicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid Chemical compound C1C2C=CC1C(C(=O)O)C2(C(O)=O)[N+]([O-])=O QJZYHAIUNVAGQP-UHFFFAOYSA-N 0.000 description 1
- 244000259585 Bauhinia variegata Species 0.000 description 1
- 235000009759 Bauhinia variegata Nutrition 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- FCYKAQOGGFGCMD-UHFFFAOYSA-N Fulvic acid Natural products O1C2=CC(O)=C(O)C(C(O)=O)=C2C(=O)C2=C1CC(C)(O)OC2 FCYKAQOGGFGCMD-UHFFFAOYSA-N 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- XADCESSVHJOZHK-UHFFFAOYSA-N Meperidine Chemical compound C=1C=CC=CC=1C1(C(=O)OCC)CCN(C)CC1 XADCESSVHJOZHK-UHFFFAOYSA-N 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
- 241000282894 Sus scrofa domesticus Species 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000000783 alginic acid Substances 0.000 description 1
- 235000010443 alginic acid Nutrition 0.000 description 1
- 229920000615 alginic acid Polymers 0.000 description 1
- 229960001126 alginic acid Drugs 0.000 description 1
- 150000004781 alginic acids Chemical class 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 235000015278 beef Nutrition 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 125000005521 carbonamide group Chemical group 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000002509 fulvic acid Substances 0.000 description 1
- 229940095100 fulvic acid Drugs 0.000 description 1
- 239000004021 humic acid Substances 0.000 description 1
- 230000002262 irrigation Effects 0.000 description 1
- 238000003973 irrigation Methods 0.000 description 1
- 239000003621 irrigation water Substances 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 235000021049 nutrient content Nutrition 0.000 description 1
- 230000000050 nutritive effect Effects 0.000 description 1
- 229960000482 pethidine Drugs 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 229910052938 sodium sulfate Inorganic materials 0.000 description 1
- 235000011152 sodium sulphate Nutrition 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 239000011573 trace mineral Substances 0.000 description 1
- 235000013619 trace mineral Nutrition 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B1/00—Superphosphates, i.e. fertilisers produced by reacting rock or bone phosphates with sulfuric or phosphoric acid in such amounts and concentrations as to yield solid products directly
- C05B1/02—Superphosphates
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
- C05F17/00—Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation
- C05F17/20—Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation using specific microorganisms or substances, e.g. enzymes, for activating or stimulating the treatment
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
- C05F17/00—Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation
- C05F17/50—Treatments combining two or more different biological or biochemical treatments, e.g. anaerobic and aerobic treatment or vermicomposting and aerobic treatment
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/40—Mixtures of one or more fertilisers with additives not having a specially fertilising activity for affecting fertiliser dosage or release rate; for affecting solubility
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/20—Liquid fertilisers
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Organic Chemistry (AREA)
- Pest Control & Pesticides (AREA)
- Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Biotechnology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Microbiology (AREA)
- Tropical Medicine & Parasitology (AREA)
- Soil Sciences (AREA)
- Fertilizers (AREA)
Abstract
The invention belongs to the technical field of agricultural fertilizers, and particularly relates to a purification treatment method of a water-soluble fertilizer with few impurities and high purification degree. The water-soluble fertilizer is subjected to twice evaporation purification treatment, so that the impurities are few and the purification degree is high. Through evaporating the ground paste in the washing of evaporation process, with the process of ground paste evaporation condensation, effectively get rid of impurity, improve water-soluble fertilizer's purification degree, effectively improved water-soluble fertilizer's nutrient composition.
Description
Technical Field
The invention belongs to the technical field of agricultural fertilizers, and particularly relates to a purification treatment method of a water-soluble fertilizer with few impurities and high purification degree.
Background
The water-soluble fertilizer is a compound fertilizer containing nitrogen, phosphorus, potassium, calcium, magnesium, trace elements, amino acid, humic acid, alginic acid and the like, which can be completely dissolved in water. Compared with the traditional fertilizer, the water-soluble fertilizer has diversified formula, very flexible application method, and can be irrigated by soil to ensure that the roots of plants can contact the fertilizer comprehensively to absorb various nutrient elements; the fertilizer can be sprayed on the leaf surfaces and enters the interior of the plant through leaf surface pores, so that the absorption and utilization rate of the fertilizer is improved; can also be used for drip irrigation and soilless culture, saves irrigation water and improves the labor production efficiency.
Compared with the traditional granular fertilizer, the water-soluble fertilizer has high purification degree requirement, and the nutrition quality of the water-soluble fertilizer can be influenced by too many impurities. In the prior art, the purification technology of water-soluble fertilizers is still few. Therefore, there is a need for improvements in technology, structural improvements, and improvements in the purity of water-soluble fertilizers.
Disclosure of Invention
In order to solve the defects in the prior art, the technical scheme of the invention provides a purification treatment method of a water-soluble fertilizer with less impurities and high purification degree.
The water-soluble fertilizer comprises pea pods, luffa stems, swamp mahogany leaves, pig nails, an ethanol solution, monopotassium phosphate, magnesium aluminum silicate, bacillus subtilis, bacillus mucilaginosus, saccharomycetes, calcium superphosphate, liquid ammonia, ammonium polyphosphate, diethyl aminoethyl hexanoate, a liquid nitrogen fertilizer, a liquid potassium fertilizer, compound sodium nitrophenolate, ethylicin, polyaspartic acid, polyglutamic acid, alkyl glycoside, ferric sulfate, gibberellin, tetramethyl glutaric acid, ferrous sulfate heptahydrate, meperilate, potassium fulvate, polyacrylamide, boric acid, matrine, a disintegrating agent and a water-soluble synergist;
the purification treatment method of the water-soluble fertilizer comprises the following steps:
step 1: grinding pea pods, luffa stems and eucalyptus robusta leaves into 140-mesh powder of 120 meshes, pouring the powder into a boiling pot, adding an ethanol solution, heating the boiling pot to 87-95 ℃, boiling for 35-70 minutes, adding magnesium aluminum silicate and ammonium polyphosphate, uniformly stirring, and filtering out residues to obtain slurry;
step 2: carrying out first evaporation purification on the slurry obtained in the step 1, keeping the evaporation temperature at 109 ℃, keeping the evaporation time at 60-90 minutes, removing impurities on the surface of the slurry, and dripping washing liquid for washing to obtain purified slurry;
and step 3: grinding the pig nail, filtering the powder to 110-130 meshes, adding potassium dihydrogen phosphate and ethanol solution, soaking for 72-96 hours, uniformly stirring, and filtering out material residues to obtain slurry;
and 4, step 4: pouring the materials obtained in the step 2 and the step 3 into a reaction kettle, stirring the materials in the reaction kettle for 20-30 minutes at the speed of 75-90 revolutions per minute by using a stirrer, pouring bacillus subtilis, bacillus mucilaginosus, saccharomycetes and calcium superphosphate into the reaction kettle, fermenting for 80-96 hours for the first time at the temperature of 70-85 ℃, and turning the reactor during the fermentation process;
and 5: filtering the material residue of the slurry obtained after fermentation in the step 4, placing the obtained slurry in a second reaction kettle, stirring the filtrate in the reaction kettle at the speed of 55-70 r/min, and pouring liquid ammonia into the reaction kettle in the stirring process;
step 6: adding the material obtained in the step 5 into bacillus subtilis, bacillus mucilaginosus, saccharomycetes and calcium superphosphate for secondary fermentation, fermenting for 30-40 hours at the temperature of 70 ℃, and performing pile turning treatment in the fermentation process;
and 7: pouring the slurry obtained by the second fermentation into a third reaction kettle, simultaneously pouring diethyl aminoethyl hexanoate, a liquid nitrogen fertilizer, a liquid potassium fertilizer, compound sodium nitrophenolate, ethylicin, polyaspartic acid, polyglutamic acid, alkyl glycoside, ferric sulfate, gibberellin, tetramethylglutaric acid, ferrous sulfate heptahydrate, mepiquat chloride, potassium fulvate, polyacrylamide, boric acid, matrine, a disintegrating agent and a water-soluble synergist into the third reaction kettle, stirring the slurry in the reaction kettle for 30-45 minutes by using a stirrer at the speed of 55-65 revolutions per minute, and then placing the slurry in a normal temperature environment for 1 hour to obtain a semi-finished product;
and 8: and (3) carrying out secondary evaporation purification on the semi-finished product obtained in the step (7), keeping the evaporation temperature at 95-105 ℃ for 30-50 minutes, then condensing the slurry by using a condenser and removing impurities on the surface of the slurry to obtain purified slurry, and standing the slurry for 1 hour at normal temperature to obtain the finished product.
Preferably, the water-soluble fertilizer comprises, by weight, 40-50 parts of pea pods, 35-45 parts of luffa stems, 25-40 parts of eucalyptus robusta leaves, 50-60 parts of pig nails, 50-55 parts of ethanol solution, 20-30 parts of potassium dihydrogen phosphate, 20-25 parts of magnesium aluminum silicate, 50-60 parts of bacillus subtilis, 30-40 parts of bacillus mucilaginosus, 30-40 parts of saccharomycetes, 50-55 parts of calcium superphosphate, 45-55 parts of liquid ammonia, 20-30 parts of ammonium polyphosphate, 10-15 parts of diethyl aminoethyl hexanoate, 30-40 parts of liquid nitrogen fertilizer, 35-40 parts of liquid potash fertilizer, 10-15 parts of compound sodium nitrophenolate, 5-9 parts of ethylicin, 10-12 parts of polyaspartic acid, 15-20 parts of polyglutamic acid, 10-13 parts of alkyl glycoside, 15-20 parts of ferric sulfate, 15-20 parts of sodium sulfate, and, 10-13 parts of gibberellin, 25-30 parts of tetramethyl glutaric acid, 15-20 parts of ferrous sulfate heptahydrate, 10-15 parts of mepiquat chloride, 5-8 parts of potassium fulvate, 15-25 parts of polyacrylamide, 10-20 parts of boric acid, 5-9 parts of matrine, 10-15 parts of disintegrant and 25-35 parts of water-soluble synergist.
The water-soluble fertilizer comprises highland barley seedlings, asparagus lettuce seedlings, eucalyptus robusta leaves, ungula bovis seu Bubali, ethanol solution, potassium dihydrogen phosphate, magnesium aluminum silicate, ammonium polyphosphate, bacillus subtilis, bacillus mucilaginosus, saccharomycetes, calcium superphosphate, liquid ammonia, phosphoric acid solution, diethyl aminoethyl hexanoate, liquid nitrogen fertilizer, liquid potassium fertilizer, compound sodium nitrophenolate, ethylicin, polyaspartic acid, alkyl glycoside, a-sodium naphthalene acetate, gibberellin, forchlorfenuron, ferrous sulfate heptahydrate, meperilate, potassium fulvate, carbamide, soluble Mo salt, glycine and water-soluble synergist;
the purification treatment method of the water-soluble fertilizer comprises the following steps:
step 1: grinding highland barley seedlings, asparagus lettuce seedlings and swamp mahogany leaves into powder of 115 meshes, pouring the powder into a boiling pot, adding an ethanol solution, heating the boiling pot to 85-88 ℃, boiling for 70 minutes, adding magnesium aluminum silicate and ammonium polyphosphate, uniformly stirring, and filtering material residues to obtain slurry;
step 2: carrying out first evaporation purification on the slurry obtained in the step 1, keeping the evaporation temperature at 109 ℃, carrying out evaporation for 90 minutes, removing impurities on the surface of the slurry, and dripping washing liquid for washing to obtain purified slurry;
and step 3: grinding ungula bovis Seu Bubali, filtering to obtain powder of 105 meshes, adding potassium dihydrogen phosphate and ethanol solution, soaking for 75 hr, stirring, and filtering to remove residue to obtain slurry;
and 4, step 4: pouring the slurry obtained in the step 2 and the step 3 into a reaction kettle, stirring the materials in the reaction kettle for 27 minutes at the speed of 80 revolutions per minute by using a stirrer, pouring bacillus subtilis, bacillus mucilaginosus, saccharomycetes and calcium superphosphate into the reaction kettle, fermenting for the first time for 80 hours at the temperature of 80-90 ℃, and turning during the fermentation process;
and 5: filtering material residues of the slurry obtained after fermentation in the step 4, placing the obtained slurry in a second reaction kettle, stirring the filtrate in the reaction kettle at the speed of 57 revolutions per minute, and pouring liquid ammonia into the reaction kettle in the stirring process;
step 6: adding bacillus subtilis, bacillus mucilaginosus, saccharomycetes and calcium superphosphate into the slurry obtained in the step 5 for secondary fermentation, fermenting for 30 hours at the temperature of 90 ℃, and performing pile turning treatment in the fermentation process;
and 7: pouring the slurry obtained by the second fermentation into a third reaction kettle, and simultaneously pouring phosphoric acid solution, diethyl aminoethyl hexanoate, liquid nitrogen fertilizer, liquid potassium fertilizer, compound sodium nitrophenolate, ethylicin, polyaspartic acid, alkyl glycoside, alpha-sodium naphthalene acetate, gibberellin, forchlorfenuron, ferrous sulfate heptahydrate, meperilate, potassium fulvate, carbamide, soluble Mo salt, glycine and water-soluble synergist into the third reaction kettle, stirring the slurry in the reaction kettle for 45 minutes by using a stirrer at the speed of 55 revolutions per minute, and then placing the slurry in a normal temperature environment for 1 hour to obtain a semi-finished product;
and 8: and (3) carrying out secondary evaporation purification on the semi-finished product obtained in the step (7), keeping the evaporation temperature at 95-105 ℃, carrying out evaporation for 45 minutes, then condensing the slurry by using a condenser and removing impurities on the surface of the slurry to obtain purified slurry, and standing the slurry for 1 hour at normal temperature to obtain the finished product.
Preferably, the water-soluble fertilizer comprises, by weight, 30-45 parts of highland barley seedlings, 30-40 parts of asparagus lettuce seedlings, 25-30 parts of eucalyptus robusta leaves, 50-60 parts of bauhinia variegata, 35-45 parts of ethanol solution, 26-30 parts of monopotassium phosphate, 20-30 parts of magnesium aluminum silicate, 17-25 parts of ammonium polyphosphate, 25-35 parts of bacillus subtilis, 40-50 parts of bacillus mucilaginosus, 50-60 parts of saccharomycetes, 45-50 parts of calcium superphosphate, 35-45 parts of liquid ammonia, 35-40 parts of phosphoric acid solution, 10-15 parts of diethyl aminoethyl hexanoate, 20-30 parts of liquid nitrogen fertilizer, 25-30 parts of liquid potassium fertilizer, 20-27 parts of compound sodium nitrophenolate, 10-14 parts of ethylicin, 5-9 parts of polyaspartic acid, 25-35 parts of alkyl glycoside, and the like, 15-20 parts of alpha-sodium naphthalene acetate, 15-19 parts of gibberellin, 5-8 parts of forchlorfenuron, 15-19 parts of ferrous sulfate heptahydrate, 5-12 parts of radix aristolochiae, 15-20 parts of potassium fulvate, 26-30 parts of carbamide, 25-34 parts of soluble Mo salt, 15-18 parts of glycine and 30-35 parts of water-soluble synergist.
The water-soluble fertilizer is subjected to twice evaporation purification treatment, so that the impurities are few and the purification degree is high. Through evaporating and washing the slurry in the evaporation process, impurities are effectively removed in the process of evaporating and condensing the slurry, the purification degree of the water-soluble fertilizer is improved, and the nutrient quality of the water-soluble fertilizer is effectively improved.
The invention takes the waste crop seedling stems and fallen leaves as one of the raw materials, realizes the secondary reutilization of the waste, saves the energy and has good environmental protection effect. The water-soluble fertilizer has high nutritive value, and is added with biological components such as pig nail, cow nail and the like. The slurry is subjected to secondary fermentation, the nutrient content of the finished product is higher, and the slurry in the reaction kettle reacts more fully by pouring liquid ammonia into the reaction kettle in the stirring process. The water-soluble fertilizer can increase the soil nutrition, promote the growth of various enzymes, improve the fiber decomposability and other excellent biological characteristics, has good fertilizer effect, and can continuously improve the soil nutrition condition. The invention is suitable for popularization and application in related fields.
Detailed Description
The present invention will now be described in more detail, wherein preferred embodiments of the invention are shown, it being understood that one skilled in the art may modify the invention herein described while still achieving the advantageous results of the invention. Accordingly, the following description should be construed as broadly as possible to those skilled in the art and not as limiting the invention.
In the interest of clarity, not all features of an actual implementation are described. In the following description, well-known functions or constructions are not described in detail since they would obscure the invention in unnecessary detail. It will of course be appreciated that in the development of any such actual embodiment, numerous implementation-specific details may be set forth in order to achieve the developer's specific goals, such as compliance with system-related and business-related constraints, which may vary from one implementation to another. Moreover, it will be appreciated that such a development effort might be complex and time-consuming, but would nevertheless be a routine undertaking for those of ordinary skill in the art.
The purpose and features of the present invention will be more clearly understood through the following detailed description of the preferred embodiments of the present invention.
The first embodiment is as follows:
the water-soluble fertilizer comprises 45 parts of pea pods, 35 parts of luffa stems, 30 parts of eucalyptus robusta leaves, 50 parts of pig nails, 50 parts of ethanol solution, 30 parts of monopotassium phosphate, 25 parts of magnesium aluminum silicate, 60 parts of bacillus subtilis, 40 parts of bacillus mucilaginosus, 30 parts of yeast, 52 parts of calcium superphosphate, 48 parts of liquid ammonia, 25 parts of ammonium polyphosphate, 10 parts of diethyl aminoethyl hexanoate, 36 parts of liquid nitrogen fertilizer, 39 parts of liquid potash fertilizer, 10 parts of compound sodium nitrophenolate, 9 parts of ethylicin, 11 parts of polyaspartic acid, 15 parts of polyglutamic acid, 12 parts of alkyl glycoside, 15 parts of ferric sulfate, 11 parts of gibberellin, 27 parts of tetramethyl glutaric acid, 20 parts of ferrous sulfate heptahydrate, 15 parts of meperilate, 7 parts of potassium fulvic acid, 19 parts of polyacrylamide, 17 parts of boric acid, 9 parts of matrine, 13 parts of disintegrant and 29 parts of water-soluble synergist.
The purification treatment method of the water-soluble fertilizer comprises the following steps:
step 1: grinding pea pods, luffa stems and swamp mahogany leaves into powder of 130 meshes, pouring the powder into a boiling pot, adding an ethanol solution, heating the boiling pot to 90-95 ℃, boiling for 65 minutes, adding magnesium aluminum silicate and ammonium polyphosphate, uniformly stirring, and filtering out residues to obtain slurry;
step 2: carrying out first evaporation purification on the slurry obtained in the step 1, keeping the evaporation temperature at 109 ℃, keeping the evaporation time at 80 minutes, removing impurities on the surface of the slurry, and dripping washing liquid for washing to obtain the purified slurry;
and step 3: grinding ungula Sus Domestica, filtering to obtain powder of 130 meshes, adding potassium dihydrogen phosphate and ethanol solution, soaking for 90 hr, stirring, and filtering to remove residue to obtain slurry;
and 4, step 4: pouring the materials obtained in the step 2 and the step 3 into a reaction kettle, stirring the materials in the reaction kettle for 20 minutes at the speed of 90 revolutions per minute by using a stirrer, pouring bacillus subtilis, bacillus mucilaginosus, saccharomycetes and calcium superphosphate into the reaction kettle, fermenting for the first time for 90 hours at the temperature of 70-85 ℃, and turning the reactor during the fermentation process;
and 5: filtering material residues of the slurry obtained after fermentation in the step 4, placing the obtained slurry in a second reaction kettle, stirring the filtrate in the reaction kettle at the speed of 70 r/min, and pouring liquid ammonia into the reaction kettle in the stirring process;
step 6: adding the material obtained in the step 5 into bacillus subtilis, bacillus mucilaginosus, saccharomycetes and calcium superphosphate for secondary fermentation, fermenting for 40 hours at the temperature of 70 ℃, and performing pile turning treatment in the fermentation process;
and 7: pouring the slurry obtained by the second fermentation into a third reaction kettle, and simultaneously pouring diethyl aminoethyl hexanoate, a liquid nitrogen fertilizer, a liquid potassium fertilizer, compound sodium nitrophenolate, ethylicin, polyaspartic acid, polyglutamic acid, alkyl glycoside, ferric sulfate, gibberellin, tetramethylglutaric acid, ferrous sulfate heptahydrate, mepiquat, potassium fulvate, polyacrylamide, boric acid, matrine, a disintegrating agent and a water-soluble synergist into the third reaction kettle, stirring the slurry in the reaction kettle for 35 minutes by using a stirrer at the speed of 60 revolutions per minute, and then standing the slurry for 1 hour in a normal temperature environment to obtain a semi-finished product;
and 8: and (4) carrying out secondary evaporation purification on the semi-finished product obtained in the step (7), keeping the evaporation temperature at 95-105 ℃, carrying out evaporation for 40 minutes, condensing the slurry by using a condenser, removing impurities on the surface of the slurry to obtain purified slurry, and standing the slurry for 1 hour at normal temperature to obtain the finished product.
The content of nutrient elements of the water-soluble fertilizer subjected to purification treatment in the embodiment of the invention is compared with the content of nutrient elements of the water-soluble fertilizer not subjected to purification treatment in the prior art by the following table:
(watch one)
As can be seen from the table I, the content of the nutrient elements of the water-soluble fertilizer subjected to purification treatment in the embodiment of the invention is higher than that of the nutrient elements of the water-soluble fertilizer not subjected to purification treatment in the prior art. The water-soluble fertilizer purification treatment can obviously increase the content of nutrient elements of the water-soluble fertilizer.
Example two:
the water-soluble fertilizer comprises, by weight, 31 parts of highland barley seedlings, 37 parts of asparagus lettuce seedlings, 29 parts of eucalyptus robusta leaves, 60 parts of beef nails, 39 parts of ethanol solution, 30 parts of monopotassium phosphate, 21 parts of magnesium aluminum silicate, 25 parts of ammonium polyphosphate, 25 parts of bacillus subtilis, 41 parts of bacillus mucilaginosus, 50 parts of saccharomycetes, 50 parts of calcium superphosphate, 35 parts of liquid ammonia, 38 parts of phosphoric acid solution, 15 parts of diethyl aminoethyl hexanoate, 27 parts of liquid nitrogen fertilizer, 25 parts of liquid potash fertilizer, 27 parts of compound sodium nitrophenolate, 14 parts of ethylicin, 8 parts of polyaspartic acid, 27 parts of alkyl glycoside, 20 parts of a-sodium naphthalene acetate, 16 parts of gibberellin, 8 parts of forchlorfenuron, 19 parts of ferrous sulfate heptahydrate, 12 parts of piperazine, 17 parts of potassium fulvate, 26 parts of carbamide, 34 parts of soluble Mo salt, 18 parts of glycine and 30 parts of synergistic water-soluble agent.
The purification treatment method of the water-soluble fertilizer comprises the following steps:
step 1: grinding highland barley seedlings, asparagus lettuce seedlings and swamp mahogany leaves into powder of 115 meshes, pouring the powder into a boiling pot, adding an ethanol solution, heating the boiling pot to 85-88 ℃, boiling for 70 minutes, adding magnesium aluminum silicate and ammonium polyphosphate, uniformly stirring, and filtering material residues to obtain slurry;
step 2: carrying out first evaporation purification on the slurry obtained in the step 1, keeping the evaporation temperature at 109 ℃, carrying out evaporation for 90 minutes, removing impurities on the surface of the slurry, and dripping washing liquid for washing to obtain purified slurry;
and step 3: grinding ungula bovis Seu Bubali, filtering to obtain powder of 105 meshes, adding potassium dihydrogen phosphate and ethanol solution, soaking for 75 hr, stirring, and filtering to remove residue to obtain slurry;
and 4, step 4: pouring the slurry obtained in the step 2 and the step 3 into a reaction kettle, stirring the materials in the reaction kettle for 27 minutes at the speed of 80 revolutions per minute by using a stirrer, pouring bacillus subtilis, bacillus mucilaginosus, saccharomycetes and calcium superphosphate into the reaction kettle, fermenting for the first time for 80 hours at the temperature of 80-90 ℃, and turning during the fermentation process;
and 5: filtering material residues of the slurry obtained after fermentation in the step 4, placing the obtained slurry in a second reaction kettle, stirring the filtrate in the reaction kettle at the speed of 57 revolutions per minute, and pouring liquid ammonia into the reaction kettle in the stirring process;
step 6: adding bacillus subtilis, bacillus mucilaginosus, saccharomycetes and calcium superphosphate into the slurry obtained in the step 5 for secondary fermentation, fermenting for 30 hours at the temperature of 90 ℃, and performing pile turning treatment in the fermentation process;
and 7: pouring the slurry obtained by the second fermentation into a third reaction kettle, simultaneously pouring a phosphoric acid solution, diethyl aminoethyl hexanoate, a liquid nitrogen fertilizer, a liquid potassium fertilizer, compound sodium nitrophenolate, ethylicin, polyaspartic acid, alkyl glycoside, a-sodium naphthalene acetate, gibberellin, forchlorfenuron, ferrous sulfate heptahydrate, meperidine, potassium fulvate, carbonamide, soluble Mo salt, glycine and a water-soluble synergist, stirring the slurry in the reaction kettle for 45 minutes at the speed of 55 revolutions per minute by using a stirrer, and then standing for 1 hour under a normal temperature environment to obtain a semi-finished product;
and 8: and (3) carrying out secondary evaporation purification on the semi-finished product obtained in the step (7), keeping the evaporation temperature at 95-105 ℃, carrying out evaporation for 45 minutes, then condensing the slurry by using a condenser and removing impurities on the surface of the slurry to obtain purified slurry, and standing the slurry for 1 hour at normal temperature to obtain the finished product.
The nutrient element content of the water-soluble fertilizer subjected to purification treatment in the second embodiment of the invention is compared with the nutrient element content of the water-soluble fertilizer not subjected to purification treatment in the prior art as shown in the table:
(watch two)
As can be seen from the table II, the content of the nutrient elements of the water-soluble fertilizer subjected to purification treatment in the second embodiment of the invention is higher than that of the nutrient elements of the water-soluble fertilizer not subjected to purification treatment in the prior art. The water-soluble fertilizer purification treatment can obviously increase the content of nutrient elements of the water-soluble fertilizer.
Various modifications to these embodiments will be readily apparent to those skilled in the art, and the generic principles defined herein may be applied to other embodiments without departing from the spirit or scope of the embodiments. Thus, the present embodiments are not intended to be limited to the embodiments shown herein but are to be accorded the widest scope consistent with the principles and novel features disclosed herein.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and should not be taken as limiting the scope of the present invention, which is intended to cover any modifications, equivalents, improvements, etc. within the spirit and principle of the present invention.
Claims (4)
1. A purification treatment method of a water-soluble fertilizer is characterized in that the water-soluble fertilizer comprises pea pods, luffa stems, eucalyptus robusta leaves, pig nails, an ethanol solution, monopotassium phosphate, magnesium aluminum silicate, bacillus subtilis, bacillus mucilaginosus, saccharomycetes, calcium superphosphate, liquid ammonia, ammonium polyphosphate, diethyl aminoethyl hexanoate, a liquid nitrogen fertilizer, a liquid potassium fertilizer, compound sodium nitrophenolate, ethylicin, polyaspartic acid, polyglutamic acid, alkyl glycoside, ferric sulfate, gibberellin, tetramethyl glutaric acid, ferrous sulfate heptahydrate, mepiquat chloride, potassium fulvate, polyacrylamide, boric acid, matrine, a disintegrating agent and a water-soluble synergist;
the purification treatment method of the water-soluble fertilizer comprises the following steps:
step 1: grinding pea pods, luffa stems and eucalyptus robusta leaves into 140-mesh powder of 120 meshes, pouring the powder into a boiling pot, adding an ethanol solution, heating the boiling pot to 87-95 ℃, boiling for 35-70 minutes, adding magnesium aluminum silicate and ammonium polyphosphate, uniformly stirring, and filtering out residues to obtain slurry;
step 2: carrying out first evaporation purification on the slurry obtained in the step 1, keeping the evaporation temperature at 109 ℃, keeping the evaporation time at 60-90 minutes, removing impurities on the surface of the slurry, and dripping washing liquid for washing to obtain purified slurry;
and step 3: grinding the pig nail, filtering the powder to 110-130 meshes, adding potassium dihydrogen phosphate and ethanol solution, soaking for 72-96 hours, uniformly stirring, and filtering out material residues to obtain slurry;
and 4, step 4: pouring the materials obtained in the step (2) and the step (3) into a reaction kettle, stirring the materials in the reaction kettle for 20-30 minutes by using a stirrer at the speed of 75-90 revolutions per minute, pouring bacillus subtilis, bacillus mucilaginosus, saccharomycetes and calcium superphosphate into the reaction kettle, performing primary fermentation for 80-96 hours at the temperature of 70-85 ℃, and performing pile turning treatment in the fermentation process;
and 5: filtering the material residue of the slurry obtained after fermentation in the step 4, placing the obtained slurry in a second reaction kettle, stirring the filtrate in the reaction kettle at the speed of 55-70 r/min, and pouring liquid ammonia into the reaction kettle in the stirring process;
step 6: adding the material obtained in the step 5 into bacillus subtilis, bacillus mucilaginosus, saccharomycetes and calcium superphosphate for secondary fermentation, fermenting for 30-40 hours at the temperature of 70 ℃, and performing pile turning treatment in the fermentation process;
and 7: pouring the slurry obtained by the second fermentation into a third reaction kettle, and simultaneously pouring diethyl aminoethyl hexanoate, a liquid nitrogen fertilizer, a liquid potassium fertilizer, compound sodium nitrophenolate, ethylicin, polyaspartic acid, polyglutamic acid, alkyl glycoside, ferric sulfate, gibberellin, tetramethylglutaric acid, ferrous sulfate heptahydrate, mepiquat, potassium fulvate, polyacrylamide, boric acid, matrine, a disintegrating agent and a water-soluble synergist into the third reaction kettle, stirring the slurry in the reaction kettle for 30-45 minutes by using a stirrer at the speed of 55-65 revolutions per minute, and then standing the slurry for 1 hour under the normal temperature environment to obtain a semi-finished product;
and 8: and (3) carrying out secondary evaporation purification on the semi-finished product obtained in the step (7), keeping the evaporation temperature at 95-105 ℃ for 30-50 minutes, then condensing the slurry by using a condenser and removing impurities on the surface of the slurry to obtain purified slurry, and standing the slurry for 1 hour at normal temperature to obtain the finished product.
2. The purification treatment method of the water-soluble fertilizer as claimed in claim 1, wherein the water-soluble fertilizer comprises 40-50 parts of pea pod, 35-45 parts of luffa stem, 25-40 parts of eucalyptus robusta leaf, 50-60 parts of pig nail, 50-55 parts of ethanol solution, 20-30 parts of potassium dihydrogen phosphate, 20-25 parts of magnesium aluminum silicate, 50-60 parts of bacillus subtilis, 30-40 parts of bacillus mucilaginosus, 30-40 parts of saccharomycetes, 50-55 parts of calcium superphosphate, 45-55 parts of liquid ammonia, 20-30 parts of ammonium polyphosphate, 10-15 parts of diethyl aminoethyl hexanoate, 30-40 parts of liquid nitrogen fertilizer, 35-40 parts of liquid potassium fertilizer, 10-15 parts of compound sodium nitrophenolate, 5-9 parts of ethylicin, 10-12 parts of polyaspartic acid, 15-20 parts of polyglutamic acid, 10-13 parts of alkyl glycoside, 15-20 parts of ferric sulfate, 10-13 parts of gibberellin, 25-30 parts of tetramethyl glutaric acid, 15-20 parts of ferrous sulfate heptahydrate, 10-15 parts of radix pulsatillae, 5-8 parts of potassium fulvate, 15-25 parts of polyacrylamide, 10-20 parts of boric acid, 5-9 parts of matrine, 10-15 parts of disintegrant and 25-35 parts of water-soluble synergist.
3. A water-soluble fertilizer purification treatment method is characterized in that components of the water-soluble fertilizer comprise highland barley seedlings, asparagus lettuce seedlings, eucalyptus robusta leaves, ungula bovis seu Bubali, an ethanol solution, monopotassium phosphate, magnesium aluminum silicate, ammonium polyphosphate, bacillus subtilis, bacillus mucilaginosus, saccharomycetes, calcium superphosphate, liquid ammonia, a phosphoric acid solution, diethyl aminoethyl hexanoate, a liquid nitrogen fertilizer, a liquid potash fertilizer, compound sodium nitrophenolate, ethylicin, polyaspartic acid, alkyl glycoside, a-sodium naphthalene acetate, gibberellin, forchlorfenuron, ferrous sulfate heptahydrate, meperilate, potassium fulvate, carbamide, soluble Mo salt, glycine and a water-soluble synergist;
the purification treatment method of the water-soluble fertilizer comprises the following steps:
step 1: grinding highland barley seedlings, asparagus lettuce seedlings and swamp mahogany leaves into powder of 115 meshes, pouring the powder into a boiling pot, adding an ethanol solution, heating the boiling pot to 85-88 ℃, boiling for 70 minutes, adding magnesium aluminum silicate and ammonium polyphosphate, uniformly stirring, and filtering material residues to obtain slurry;
step 2: carrying out first evaporation purification on the slurry obtained in the step 1, keeping the evaporation temperature at 109 ℃, carrying out evaporation for 90 minutes, removing impurities on the surface of the slurry, and dripping washing liquid for washing to obtain purified slurry;
and step 3: grinding ungula bovis Seu Bubali, filtering to obtain powder of 105 meshes, adding potassium dihydrogen phosphate and ethanol solution, soaking for 75 hr, stirring, and filtering to remove residue to obtain slurry;
and 4, step 4: pouring the slurry obtained in the step 2 and the step 3 into a reaction kettle, stirring the materials in the reaction kettle for 27 minutes at the speed of 80 revolutions per minute by using a stirrer, pouring bacillus subtilis, bacillus mucilaginosus, saccharomycetes and calcium superphosphate into the reaction kettle, fermenting for the first time for 80 hours at the temperature of 80-90 ℃, and turning during the fermentation process;
and 5: filtering material residues of the slurry obtained after fermentation in the step 4, placing the obtained slurry in a second reaction kettle, stirring the filtrate in the reaction kettle at the speed of 57 revolutions per minute, and pouring liquid ammonia into the reaction kettle in the stirring process;
step 6: adding bacillus subtilis, bacillus mucilaginosus, saccharomycetes and calcium superphosphate into the slurry obtained in the step 5 for secondary fermentation, fermenting for 30 hours at the temperature of 90 ℃, and performing pile turning treatment in the fermentation process;
and 7: pouring the slurry obtained by the second fermentation into a third reaction kettle, and simultaneously pouring phosphoric acid solution, diethyl aminoethyl hexanoate, liquid nitrogen fertilizer, liquid potassium fertilizer, compound sodium nitrophenolate, ethylicin, polyaspartic acid, alkyl glycoside, alpha-sodium naphthalene acetate, gibberellin, forchlorfenuron, ferrous sulfate heptahydrate, meperilate, potassium fulvate, carbamide, soluble Mo salt, glycine and water-soluble synergist into the third reaction kettle, stirring the slurry in the reaction kettle for 45 minutes by using a stirrer at the speed of 55 revolutions per minute, and then placing the slurry in a normal temperature environment for 1 hour to obtain a semi-finished product;
and 8: and (3) carrying out secondary evaporation purification on the semi-finished product obtained in the step (7), keeping the evaporation temperature at 95-105 ℃, carrying out evaporation for 45 minutes, then condensing the slurry by using a condenser and removing impurities on the surface of the slurry to obtain purified slurry, and standing the slurry for 1 hour at normal temperature to obtain the finished product.
4. The water-soluble fertilizer purification treatment method as claimed in claim 3, wherein the water-soluble fertilizer comprises 30-45 parts of highland barley seedlings, 30-40 parts of asparagus lettuce seedlings, 25-30 parts of eucalyptus robusta leaves, 50-60 parts of bovine nails, 35-45 parts of ethanol solution, 26-30 parts of potassium dihydrogen phosphate, 20-30 parts of magnesium aluminum silicate, 17-25 parts of ammonium polyphosphate, 25-35 parts of bacillus subtilis, 40-50 parts of bacillus mucilaginosus, 50-60 parts of yeast, 45-50 parts of calcium superphosphate, 35-45 parts of liquid ammonia, 35-40 parts of phosphoric acid solution, 10-15 parts of diethyl aminoethyl hexanoate, 20-30 parts of liquid nitrogen fertilizer, 25-30 parts of liquid potassium fertilizer, 20-27 parts of compound sodium nitrophenolate, 10-14 parts of ethylicin, 5-9 parts of polyaspartic acid, 25-35 parts of alkyl glycoside, 15-20 parts of a-sodium naphthalene acetate, 15-19 parts of gibberellin, 5-8 parts of forchlorfenuron, 15-19 parts of ferrous sulfate heptahydrate, 5-12 parts of mepiquat chloride, 15-20 parts of potassium fulvate, 26-30 parts of carbamide, 25-34 parts of soluble Mo salt, 15-18 parts of glycine and 30-35 parts of water-soluble synergist.
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