CN114681382A - Flower toothpaste and preparation method thereof - Google Patents

Flower toothpaste and preparation method thereof Download PDF

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Publication number
CN114681382A
CN114681382A CN202210490763.3A CN202210490763A CN114681382A CN 114681382 A CN114681382 A CN 114681382A CN 202210490763 A CN202210490763 A CN 202210490763A CN 114681382 A CN114681382 A CN 114681382A
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China
Prior art keywords
toothpaste
fresh flower
flower
agent
essential oil
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Pending
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CN202210490763.3A
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Chinese (zh)
Inventor
高国梁
孙顺文
高子昂
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Yunnan Huawang Biotechnology Co ltd
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Yunnan Huawang Biotechnology Co ltd
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Priority to CN202210490763.3A priority Critical patent/CN114681382A/en
Publication of CN114681382A publication Critical patent/CN114681382A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/4973Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
    • A61K8/498Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/99Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from microorganisms other than algae or fungi, e.g. protozoa or bacteria
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P1/00Drugs for disorders of the alimentary tract or the digestive system
    • A61P1/02Stomatological preparations, e.g. drugs for caries, aphtae, periodontitis
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P29/00Non-central analgesic, antipyretic or antiinflammatory agents, e.g. antirheumatic agents; Non-steroidal antiinflammatory drugs [NSAID]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P37/00Drugs for immunological or allergic disorders
    • A61P37/08Antiallergic agents
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P7/00Drugs for disorders of the blood or the extracellular fluid
    • A61P7/04Antihaemorrhagics; Procoagulants; Haemostatic agents; Antifibrinolytic agents
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q11/00Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/20Chemical, physico-chemical or functional or structural properties of the composition as a whole
    • A61K2800/28Rubbing or scrubbing compositions; Peeling or abrasive compositions; Containing exfoliants
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

Abstract

The invention relates to a fresh flower toothpaste and a preparation method thereof, wherein the toothpaste is prepared from the following raw materials: fresh flower hydrolat, fresh flower essential oil, honeysuckle extract, Pu' er tea polyphenol, an abrasive, a wetting agent, a thickening agent, a surfactant, a sweetening agent, a preservative, an active additive, probiotics and deionized water. The toothpaste prepared by the combined action of the fresh flower hydrolat, the fresh flower essential oil, the honeysuckle extract and the Pu' er tea polyphenol has the effects of refreshing breath, clearing heat, stopping bleeding, resisting bacteria and allergy, preventing caries, strengthening teeth and removing halitosis; if the temperature is too high in summer, the cooling water is introduced into the jacket of the paste making pot to reduce the temperature, and in winter, the liquid raw material is heated and kept warm.

Description

Flower toothpaste and preparation method thereof
Technical Field
The invention belongs to the technical field of toothpaste, and particularly relates to fresh flower toothpaste and a preparation method thereof.
Background
Toothpaste is one of tooth cleaning products, is generally in a gel shape, is usually smeared on a toothbrush, cleans the surfaces of teeth by the mechanical friction action of the toothbrush, cleans the teeth and the periphery of the teeth and purifies and refreshes the oral cavity. The definition of the chinese toothpaste industry association is: the toothpaste is used together with the toothbrush for cleaning teeth and protecting oral hygiene, and is a daily necessity for protecting human body safety. Dental cleaning is of paramount importance for the aesthetic appearance of teeth, the protection of gum health and the prevention of bad breath. Toothpaste has become a necessity in human daily life. The toothpaste body is a suspended colloid mixture which is composed of water, hydrophilic liquid raw materials, water-soluble solid raw materials, insoluble solid raw materials and oil-soluble essence as main bodies and has stable system, complex components and uniform distribution under the action of a thickening agent and a surfactant (foaming agent). According to the 'Chinese resident oral health guide' published by the Ministry of health in 2009 in China, the basic functions of toothpaste are as follows: enhance the friction force of tooth brushing, help to remove food scraps, soft dirt and dental plaque, help to eliminate or reduce the peculiar smell of the oral cavity and make the breath fresh.
The toothpaste is a daily necessity which is not neglected in life of people, the function of the toothpaste is more and more diversified, the performance of the toothpaste directly influences the oral hygiene of people, and the oral hygiene is an important link for preventing odontopathy. The existing toothpaste in the market is various in types, but has single function and cannot meet the requirements of people.
The present invention has been made in view of the above circumstances.
Disclosure of Invention
In order to solve the problems in the prior art, the invention provides fresh flower toothpaste and a preparation method thereof.
The invention provides fresh flower toothpaste, which is prepared from the following raw materials in parts by weight: 5-10 parts of fresh flower hydrolat, 0.002-0.015 part of fresh flower essential oil, 0.05-0.15 part of honeysuckle extract, 0.05-0.15 part of Pu' er tea polyphenol, 16-20 parts of abrasive, 40-60 parts of wetting agent, 0.5-1.5 parts of thickening agent, 1-3 parts of surfactant, 0.05-0.15 part of sweetening agent, 0.3-0.7 part of preservative, 0.1-0.5 part of active additive, 0.05-0.15 part of probiotics and 15-25 parts of deionized water.
Furthermore, the fresh flower in the fresh flower hydrolat and the fresh flower essential oil is one or more of rose, jasmine, sweet osmanthus, gardenia, orange flower, cherry flower and peach flower.
Further, the abrasive is hydrated silicon dioxide; the wetting agent is 70% of sorbitol by mass; the thickening agent is xanthan gum and sodium carboxymethyl cellulose; the surfactant is sodium lauryl sulfate; the sweetening agent is sucralose; the preservative is sodium benzoate; the active matter additive is sodium fluoride, stannous fluoride and tranexamic acid.
The second object of the present invention provides a method for preparing said toothpaste, said method comprising the steps of:
(1) weighing the raw materials according to the weight of the raw materials for later use;
(2) adding a sweetening agent, a preservative and an active substance additive into deionized water in a pre-dissolving pot, and stirring and dissolving uniformly to obtain a material A;
(3) adding a wetting agent and a thickening agent into a pre-dispersion pot, and uniformly stirring and dispersing to obtain a material B;
(4) mixing the material A and the material B under a vacuum condition, uniformly stirring, adding a friction agent and a surfactant, and uniformly stirring to obtain a material C;
(5) adding fresh flower hydrolat, fresh flower essential oil, honeysuckle extract, Pu' er tea polyphenol and probiotics into the material C, stirring uniformly, degassing in vacuum, and homogenizing to obtain the fresh flower toothpaste.
Further, the stirring and dissolving time in the step (2) is 2-4 min.
Further, stirring and dispersing for 1-3min in the step (3).
Furthermore, the vacuum degree in the step (4) is-0.04 to-0.02 MPa.
Further, in the step (5), vacuum degassing is carried out until the vacuum degree is more than-0.094 MPa.
The flower hydrolat disclosed in the invention is prepared by adopting a preparation method of the edible flower hydrolat disclosed in patent CN 111728109A.
Compared with the prior art, the invention has the beneficial effects that:
the fresh flower hydrolat has the functions of relieving bad emotions such as depression, tension, anxiety and the like, and simultaneously can prevent bacteria and viruses, thereby playing the roles of sterilization and inflammation diminishing. The toothpaste prepared by utilizing the combined action of the fresh flower hydrolat, the fresh flower essential oil, the honeysuckle extract and the Pu' er tea polyphenol has the effects of refreshing breath, clearing heat, stopping bleeding, resisting bacteria and allergy, preventing caries, strengthening teeth and removing halitosis; if the temperature is too high in summer, the cooling water is introduced into the jacket of the paste making pot to reduce the temperature, and in winter, the liquid raw material is heated and kept warm.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the technical solutions of the present invention will be described in detail below. It is to be understood that the described embodiments are merely exemplary of the invention, and not restrictive of the full scope of the invention. All other embodiments, which can be derived by a person skilled in the art from the examples given herein without any inventive step, are within the scope of the present invention.
Example 1
The fresh flower toothpaste of the embodiment comprises the following raw materials: 5kg of fresh flower hydrolat, 0.015kg of fresh flower essential oil, 0.05kg of honeysuckle extract, 0.15kg of Pu' er tea polyphenol, 20kg of abrasive, 40kg of wetting agent, 1.5kg of thickening agent, 1kg of surfactant, 0.08kg of sweetening agent, 0.3kg of preservative, 0.5kg of active additive, 0.05kg of probiotics and 25kg of deionized water;
wherein the abrasive is hydrated silicon dioxide; the wetting agent is 70% of sorbitol by mass; the thickening agent is formed by mixing xanthan gum and sodium carboxymethyl cellulose according to the ratio of 1: 1; the surfactant is sodium lauryl sulfate; the sweetening agent is sucralose; the preservative is sodium benzoate; the active matter additive is formed by mixing sodium fluoride, stannous fluoride and tranexamic acid according to the ratio of 1:1: 1;
the flower hydrolat of this example is rose hydrolat prepared according to the method of example 3 in patent CN111728109A, and the flower essential oil is rose essential oil;
the preparation method of the toothpaste of the embodiment comprises the following steps:
(1) weighing the raw materials according to the weight of the raw materials for later use;
(2) adding a sweetening agent, a preservative and an active substance additive into deionized water in a pre-dissolving pot, and stirring and dissolving uniformly for 2min to obtain a material A;
(3) adding a wetting agent and a thickening agent into a pre-dispersion pot, uniformly stirring and dispersing, and stirring and dispersing for 1min to obtain a material B;
(4) under the vacuum condition, the vacuum degree is-0.04 MPa, the material A and the material B are mixed and stirred uniformly, and then a friction agent and a surfactant are added and stirred uniformly to obtain a material C;
(5) adding fresh flower hydrolat, fresh flower essential oil, honeysuckle extract, Pu' er tea polyphenol and probiotics into the material C, stirring uniformly, vacuum degassing until the vacuum degree is more than-0.094 MPa, and homogenizing to obtain the fresh flower toothpaste.
Example 2
The fresh flower toothpaste of the embodiment comprises the following raw materials: 7.5kg of fresh flower hydrolat, 0.01kg of fresh flower essential oil, 0.1kg of honeysuckle extract, 0.1kg of Pu' er tea polyphenol, 18kg of abrasive, 50kg of wetting agent, 1kg of thickening agent, 2kg of surfactant, 0.1kg of sweetening agent, 0.45kg of preservative, 0.3kg of active additive, 0.1kg of probiotics and 20kg of deionized water;
wherein the abrasive is hydrated silicon dioxide; the wetting agent is 70% of sorbitol by mass; the thickening agent is formed by mixing xanthan gum and sodium carboxymethyl cellulose according to the ratio of 1: 1; the surfactant is sodium lauryl sulfate; the sweetening agent is sucralose; the preservative is sodium benzoate; the active matter additive is formed by mixing sodium fluoride, stannous fluoride and tranexamic acid according to the ratio of 1:1: 1;
the fresh flower hydrolat of the embodiment is prepared according to the method of embodiment 3 in patent CN111728109A, only the rose is replaced by jasmine, and the fresh flower essential oil is jasmine essential oil;
the preparation method of the toothpaste of the embodiment comprises the following steps:
(1) weighing the raw materials according to the weight of the raw materials for later use;
(2) adding a sweetening agent, a preservative and an active substance additive into deionized water in a pre-dissolving pot, and stirring and dissolving uniformly for 3min to obtain a material A;
(3) adding a wetting agent and a thickening agent into a pre-dispersion pot, uniformly stirring and dispersing, and stirring and dispersing for 2min to obtain a material B;
(4) under the vacuum condition, the vacuum degree is-0.03 MPa, the material A and the material B are mixed and stirred uniformly, and then a friction agent and a surfactant are added and stirred uniformly to obtain a material C;
(5) adding fresh flower hydrolat, fresh flower essential oil, honeysuckle extract, Pu' er tea polyphenol and probiotics into the material C, stirring uniformly, vacuum degassing until the vacuum degree is more than-0.094 MPa, and homogenizing to obtain the fresh flower toothpaste.
Example 3
The fresh flower toothpaste of the embodiment comprises the following raw materials: 10kg of fresh flower hydrolat, 0.005kg of fresh flower essential oil, 0.15kg of honeysuckle extract, 0.05kg of Pu' er tea polyphenol, 16kg of abrasive, 60kg of wetting agent, 0.5kg of thickening agent, 3kg of surfactant, 0.09kg of sweetening agent, 0.7kg of preservative, 0.1kg of active additive, 0.15kg of probiotics and 15kg of deionized water;
wherein the abrasive is hydrated silicon dioxide; the wetting agent is 70% of sorbitol by mass; the thickening agent is formed by mixing xanthan gum and sodium carboxymethyl cellulose according to the ratio of 1: 1; the surfactant is sodium lauryl sulfate; the sweetening agent is sucralose; the preservative is sodium benzoate; the active matter additive is formed by mixing sodium fluoride, stannous fluoride and tranexamic acid according to the ratio of 1:1: 1;
the flower hydrolat of this example was prepared according to the method of example 3 in patent CN111728109A, only the roses were replaced with the cherry flowers, and the flower essential oil was cherry flower essential oil;
the preparation method of the toothpaste of the embodiment comprises the following steps:
(1) weighing the raw materials according to the weight of the raw materials for later use;
(2) adding a sweetening agent, a preservative and an active substance additive into deionized water in a pre-dissolving pot, and stirring and dissolving uniformly for 4min to obtain a material A;
(3) adding a wetting agent and a thickening agent into a pre-dispersion pot, uniformly stirring and dispersing, and stirring and dispersing for 3min to obtain a material B;
(4) under the vacuum condition, the vacuum degree is-0.02 MPa, the material A and the material B are mixed and stirred uniformly, and then a friction agent and a surfactant are added and stirred uniformly to obtain a material C;
(5) adding fresh flower hydrolat, fresh flower essential oil, honeysuckle extract, Pu' er tea polyphenol and probiotics into the material C, stirring uniformly, vacuum degassing until the vacuum degree is more than-0.094 MPa, and homogenizing to obtain the fresh flower toothpaste.
Example 4
The fresh flower toothpaste of the embodiment comprises the following raw materials: 7kg of fresh flower hydrolat, 0.01kg of fresh flower essential oil, 0.1kg of honeysuckle extract, 0.1kg of Pu' er tea polyphenol, 18.59kg of abrasive agent, 50kg of wetting agent, 1.0kg of thickening agent, 2kg of surfactant, 0.1kg of sweetening agent, 0.5kg of preservative, 0.3kg of active matter additive, 0.1kg of probiotics and 20kg of deionized water;
wherein the abrasive is hydrated silicon dioxide; the wetting agent is 70% of sorbitol by mass; the thickening agent is formed by mixing xanthan gum and sodium carboxymethyl cellulose according to the ratio of 1: 1; the surfactant is sodium lauryl sulfate; the sweetening agent is sucralose; the preservative is sodium benzoate; the active matter additive is formed by mixing sodium fluoride, stannous fluoride and tranexamic acid according to the ratio of 1:1: 1;
the flower hydrolat of this example is rose hydrolat prepared according to the method of example 3 in patent CN111728109A, and the flower essential oil is rose essential oil;
the preparation method of the toothpaste of the embodiment comprises the following steps:
(1) weighing the raw materials according to the weight of the raw materials for later use;
(2) adding a sweetening agent, a preservative and an active substance additive into deionized water in a pre-dissolving pot, and stirring and dissolving uniformly for 2.5min to obtain a material A;
(3) adding a wetting agent and a thickening agent into a pre-dispersion pot, uniformly stirring and dispersing, and stirring and dispersing for 1.5min to obtain a material B;
(4) under the vacuum condition, the vacuum degree is-0.04 MPa, the material A and the material B are mixed and stirred uniformly, and then a friction agent and a surfactant are added and stirred uniformly to obtain a material C;
(5) adding fresh flower hydrolat, fresh flower essential oil, honeysuckle extract, Pu' er tea polyphenol and probiotics into the material C, stirring uniformly, vacuum degassing until the vacuum degree is more than-0.094 MPa, and homogenizing to obtain the fresh flower toothpaste.
Example 5
The fresh flower toothpaste of the embodiment comprises the following raw materials: 7kg of fresh flower hydrolat, 0.01kg of fresh flower essential oil, 0.1kg of honeysuckle extract, 0.15kg of Pu' er tea polyphenol, 18.29kg of abrasive agent, 50kg of wetting agent, 1kg of thickening agent, 2kg of surfactant, 0.1kg of sweetening agent, 0.5kg of preservative, 0.3kg of active additive, 0.1kg of probiotics and 20kg of deionized water;
wherein the abrasive is hydrated silicon dioxide; the wetting agent is 70% of sorbitol by mass; the thickening agent is formed by mixing xanthan gum and sodium carboxymethyl cellulose according to the ratio of 1: 1; the surfactant is sodium lauryl sulfate; the sweetening agent is sucralose; the preservative is sodium benzoate; the active matter additive is formed by mixing sodium fluoride, stannous fluoride and tranexamic acid according to the ratio of 1:1: 1;
the fresh flower hydrolat of the embodiment is prepared according to the method of embodiment 3 in patent CN111728109A, only the rose is replaced by jasmine, and the fresh flower essential oil is jasmine essential oil;
the preparation method of the toothpaste of the embodiment comprises the following steps:
(1) weighing the raw materials according to the weight of the raw materials for later use;
(2) adding a sweetening agent, a preservative and an active substance additive into deionized water in a pre-dissolving pot, and stirring and dissolving uniformly for 2min to obtain a material A;
(3) adding a wetting agent and a thickening agent into a pre-dispersion pot, uniformly stirring and dispersing, and stirring and dispersing for 1min to obtain a material B;
(4) under the vacuum condition, the vacuum degree is-0.04 MPa, the material A and the material B are mixed and stirred uniformly, and then a friction agent and a surfactant are added and stirred uniformly to obtain a material C;
(5) adding fresh flower hydrolat, fresh flower essential oil, honeysuckle extract, Pu' er tea polyphenol and probiotics into the material C, stirring uniformly, vacuum degassing until the vacuum degree is more than-0.094 MPa, and homogenizing to obtain the fresh flower toothpaste.
Comparative example 1
The toothpaste raw materials and the preparation method of the comparative example are the same as those of example 4, except that rose hydrolat is not added to the raw materials.
Comparative example 2
The toothpaste raw material and the preparation method of the comparative example are the same as those of example 4, except that the honeysuckle extract is not added to the raw material.
Comparative example 3
The raw materials and the preparation method of the toothpaste of the comparative example are the same as those of the example 4, except that the raw materials are not added with the Pu' er tea polyphenol.
Test example 1
Test subjects: the middle-aged population, 400 men and 400 women, was divided into 8 groups of 50 men and 50 women on average.
The using method comprises the following steps: brushing 1-2g of toothpaste for 3 minutes each time, and using for 10 days 3 times a day (once in the morning, in the middle and at night).
The results of using the toothpastes prepared in examples 1 to 5 for test groups 1 to 5 and the toothpastes prepared in comparative examples 1 to 3 for control groups 1 to 3, respectively, are shown in table 1, wherein the effect is that no bleeding of gum occurs during the whole tooth brushing process, the tooth surface is smooth, the mouth feeling is obvious, fresh flower fragrance is provided, the fragrance is maintained for a long time, and no allergy or toothache occurs.
TABLE 1
Group of Effective rate (%)
Test group 1 90
Test group 2 93
Test group 3 91
Test group 4 90
Test group 5 92
Control group 1 50
Control group 2 60
Control group 3 80
As can be seen from Table 1, only by adopting the raw materials of the invention, the toothpaste has the effects of no gum bleeding in the whole tooth brushing process, smooth tooth surface, fresh flower fragrance with obvious mouth feeling after tooth brushing, lasting fragrance, no allergy and toothache, and because the toothpaste prepared by utilizing the combined action of the fresh flower hydrolat, the fresh flower essential oil, the honeysuckle extract and the Pu' er tea polyphenol has the effects of refreshing breath, clearing heat, stopping bleeding, resisting bacteria and allergy, preventing caries, strengthening teeth and removing halitosis.
The above description is only for the specific embodiments of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art can easily conceive of the changes or substitutions within the technical scope of the present invention, and all the changes or substitutions should be covered within the scope of the present invention. Therefore, the protection scope of the present invention shall be subject to the protection scope of the appended claims.

Claims (8)

1. The flower toothpaste is characterized by comprising the following raw materials in parts by weight: 5-10 parts of fresh flower hydrolat, 0.002-0.015 part of fresh flower essential oil, 0.05-0.15 part of honeysuckle extract, 0.05-0.15 part of Pu' er tea polyphenol, 16-20 parts of abrasive, 40-60 parts of wetting agent, 0.5-1.5 parts of thickening agent, 1-3 parts of surfactant, 0.05-0.15 part of sweetening agent, 0.3-0.7 part of preservative, 0.1-0.5 part of active additive, 0.05-0.15 part of probiotics and 15-25 parts of deionized water.
2. The flower toothpaste according to claim 1, wherein the flower of the flower hydrolat and flower essential oil is one or more of rose, jasmine, sweet osmanthus, gardenia, orange flower, cherry and peach flower.
3. The flower toothpaste of claim 1, wherein the abrasive is hydrated silica; the wetting agent is 70% of sorbitol by mass; the thickening agent is xanthan gum and sodium carboxymethyl cellulose; the surfactant is sodium lauryl sulfate; the sweetening agent is sucralose; the preservative is sodium benzoate; the active matter additive is sodium fluoride, stannous fluoride and tranexamic acid.
4. A method of preparing a toothpaste as claimed in any one of claims 1 to 3, said method comprising the steps of:
(1) weighing the raw materials according to the weight of the raw materials for later use;
(2) adding a sweetening agent, a preservative and an active additive into deionized water in a pre-dissolving pot, and stirring and dissolving uniformly to obtain a material A;
(3) adding a wetting agent and a thickening agent into a pre-dispersion pot, and uniformly stirring and dispersing to obtain a material B;
(4) mixing the material A and the material B under a vacuum condition, uniformly stirring, adding a friction agent and a surfactant, and uniformly stirring to obtain a material C;
(5) adding fresh flower hydrolat, fresh flower essential oil, honeysuckle extract, Pu' er tea polyphenol and probiotics into the material C, uniformly stirring, degassing in vacuum, and homogenizing to obtain the fresh flower toothpaste.
5. The method for preparing fresh flower toothpaste according to claim 4, wherein the dissolution time in step (2) is 2-4min under stirring.
6. The method for preparing fresh flower toothpaste according to claim 4, wherein the step (3) is performed by stirring and dispersing for 1-3 min.
7. The method for preparing fresh flower toothpaste according to claim 4, wherein the vacuum degree in step (4) is-0.04 to-0.02 MPa.
8. The method for preparing fresh flower toothpaste according to claim 4, wherein in step (5), vacuum degassing is performed until the vacuum degree is-0.094 MPa or more.
CN202210490763.3A 2022-05-07 2022-05-07 Flower toothpaste and preparation method thereof Pending CN114681382A (en)

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CN104825350A (en) * 2015-04-22 2015-08-12 林晓莉 Toothpaste using plant hydrosol and essential oil to substitute essence components
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