CN114681382A - Flower toothpaste and preparation method thereof - Google Patents
Flower toothpaste and preparation method thereof Download PDFInfo
- Publication number
- CN114681382A CN114681382A CN202210490763.3A CN202210490763A CN114681382A CN 114681382 A CN114681382 A CN 114681382A CN 202210490763 A CN202210490763 A CN 202210490763A CN 114681382 A CN114681382 A CN 114681382A
- Authority
- CN
- China
- Prior art keywords
- toothpaste
- fresh flower
- flower
- agent
- essential oil
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
- A61K8/498—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/99—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from microorganisms other than algae or fungi, e.g. protozoa or bacteria
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P1/00—Drugs for disorders of the alimentary tract or the digestive system
- A61P1/02—Stomatological preparations, e.g. drugs for caries, aphtae, periodontitis
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P29/00—Non-central analgesic, antipyretic or antiinflammatory agents, e.g. antirheumatic agents; Non-steroidal antiinflammatory drugs [NSAID]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P37/00—Drugs for immunological or allergic disorders
- A61P37/08—Antiallergic agents
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P7/00—Drugs for disorders of the blood or the extracellular fluid
- A61P7/04—Antihaemorrhagics; Procoagulants; Haemostatic agents; Antifibrinolytic agents
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/28—Rubbing or scrubbing compositions; Peeling or abrasive compositions; Containing exfoliants
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
Abstract
The invention relates to a fresh flower toothpaste and a preparation method thereof, wherein the toothpaste is prepared from the following raw materials: fresh flower hydrolat, fresh flower essential oil, honeysuckle extract, Pu' er tea polyphenol, an abrasive, a wetting agent, a thickening agent, a surfactant, a sweetening agent, a preservative, an active additive, probiotics and deionized water. The toothpaste prepared by the combined action of the fresh flower hydrolat, the fresh flower essential oil, the honeysuckle extract and the Pu' er tea polyphenol has the effects of refreshing breath, clearing heat, stopping bleeding, resisting bacteria and allergy, preventing caries, strengthening teeth and removing halitosis; if the temperature is too high in summer, the cooling water is introduced into the jacket of the paste making pot to reduce the temperature, and in winter, the liquid raw material is heated and kept warm.
Description
Technical Field
The invention belongs to the technical field of toothpaste, and particularly relates to fresh flower toothpaste and a preparation method thereof.
Background
Toothpaste is one of tooth cleaning products, is generally in a gel shape, is usually smeared on a toothbrush, cleans the surfaces of teeth by the mechanical friction action of the toothbrush, cleans the teeth and the periphery of the teeth and purifies and refreshes the oral cavity. The definition of the chinese toothpaste industry association is: the toothpaste is used together with the toothbrush for cleaning teeth and protecting oral hygiene, and is a daily necessity for protecting human body safety. Dental cleaning is of paramount importance for the aesthetic appearance of teeth, the protection of gum health and the prevention of bad breath. Toothpaste has become a necessity in human daily life. The toothpaste body is a suspended colloid mixture which is composed of water, hydrophilic liquid raw materials, water-soluble solid raw materials, insoluble solid raw materials and oil-soluble essence as main bodies and has stable system, complex components and uniform distribution under the action of a thickening agent and a surfactant (foaming agent). According to the 'Chinese resident oral health guide' published by the Ministry of health in 2009 in China, the basic functions of toothpaste are as follows: enhance the friction force of tooth brushing, help to remove food scraps, soft dirt and dental plaque, help to eliminate or reduce the peculiar smell of the oral cavity and make the breath fresh.
The toothpaste is a daily necessity which is not neglected in life of people, the function of the toothpaste is more and more diversified, the performance of the toothpaste directly influences the oral hygiene of people, and the oral hygiene is an important link for preventing odontopathy. The existing toothpaste in the market is various in types, but has single function and cannot meet the requirements of people.
The present invention has been made in view of the above circumstances.
Disclosure of Invention
In order to solve the problems in the prior art, the invention provides fresh flower toothpaste and a preparation method thereof.
The invention provides fresh flower toothpaste, which is prepared from the following raw materials in parts by weight: 5-10 parts of fresh flower hydrolat, 0.002-0.015 part of fresh flower essential oil, 0.05-0.15 part of honeysuckle extract, 0.05-0.15 part of Pu' er tea polyphenol, 16-20 parts of abrasive, 40-60 parts of wetting agent, 0.5-1.5 parts of thickening agent, 1-3 parts of surfactant, 0.05-0.15 part of sweetening agent, 0.3-0.7 part of preservative, 0.1-0.5 part of active additive, 0.05-0.15 part of probiotics and 15-25 parts of deionized water.
Furthermore, the fresh flower in the fresh flower hydrolat and the fresh flower essential oil is one or more of rose, jasmine, sweet osmanthus, gardenia, orange flower, cherry flower and peach flower.
Further, the abrasive is hydrated silicon dioxide; the wetting agent is 70% of sorbitol by mass; the thickening agent is xanthan gum and sodium carboxymethyl cellulose; the surfactant is sodium lauryl sulfate; the sweetening agent is sucralose; the preservative is sodium benzoate; the active matter additive is sodium fluoride, stannous fluoride and tranexamic acid.
The second object of the present invention provides a method for preparing said toothpaste, said method comprising the steps of:
(1) weighing the raw materials according to the weight of the raw materials for later use;
(2) adding a sweetening agent, a preservative and an active substance additive into deionized water in a pre-dissolving pot, and stirring and dissolving uniformly to obtain a material A;
(3) adding a wetting agent and a thickening agent into a pre-dispersion pot, and uniformly stirring and dispersing to obtain a material B;
(4) mixing the material A and the material B under a vacuum condition, uniformly stirring, adding a friction agent and a surfactant, and uniformly stirring to obtain a material C;
(5) adding fresh flower hydrolat, fresh flower essential oil, honeysuckle extract, Pu' er tea polyphenol and probiotics into the material C, stirring uniformly, degassing in vacuum, and homogenizing to obtain the fresh flower toothpaste.
Further, the stirring and dissolving time in the step (2) is 2-4 min.
Further, stirring and dispersing for 1-3min in the step (3).
Furthermore, the vacuum degree in the step (4) is-0.04 to-0.02 MPa.
Further, in the step (5), vacuum degassing is carried out until the vacuum degree is more than-0.094 MPa.
The flower hydrolat disclosed in the invention is prepared by adopting a preparation method of the edible flower hydrolat disclosed in patent CN 111728109A.
Compared with the prior art, the invention has the beneficial effects that:
the fresh flower hydrolat has the functions of relieving bad emotions such as depression, tension, anxiety and the like, and simultaneously can prevent bacteria and viruses, thereby playing the roles of sterilization and inflammation diminishing. The toothpaste prepared by utilizing the combined action of the fresh flower hydrolat, the fresh flower essential oil, the honeysuckle extract and the Pu' er tea polyphenol has the effects of refreshing breath, clearing heat, stopping bleeding, resisting bacteria and allergy, preventing caries, strengthening teeth and removing halitosis; if the temperature is too high in summer, the cooling water is introduced into the jacket of the paste making pot to reduce the temperature, and in winter, the liquid raw material is heated and kept warm.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the technical solutions of the present invention will be described in detail below. It is to be understood that the described embodiments are merely exemplary of the invention, and not restrictive of the full scope of the invention. All other embodiments, which can be derived by a person skilled in the art from the examples given herein without any inventive step, are within the scope of the present invention.
Example 1
The fresh flower toothpaste of the embodiment comprises the following raw materials: 5kg of fresh flower hydrolat, 0.015kg of fresh flower essential oil, 0.05kg of honeysuckle extract, 0.15kg of Pu' er tea polyphenol, 20kg of abrasive, 40kg of wetting agent, 1.5kg of thickening agent, 1kg of surfactant, 0.08kg of sweetening agent, 0.3kg of preservative, 0.5kg of active additive, 0.05kg of probiotics and 25kg of deionized water;
wherein the abrasive is hydrated silicon dioxide; the wetting agent is 70% of sorbitol by mass; the thickening agent is formed by mixing xanthan gum and sodium carboxymethyl cellulose according to the ratio of 1: 1; the surfactant is sodium lauryl sulfate; the sweetening agent is sucralose; the preservative is sodium benzoate; the active matter additive is formed by mixing sodium fluoride, stannous fluoride and tranexamic acid according to the ratio of 1:1: 1;
the flower hydrolat of this example is rose hydrolat prepared according to the method of example 3 in patent CN111728109A, and the flower essential oil is rose essential oil;
the preparation method of the toothpaste of the embodiment comprises the following steps:
(1) weighing the raw materials according to the weight of the raw materials for later use;
(2) adding a sweetening agent, a preservative and an active substance additive into deionized water in a pre-dissolving pot, and stirring and dissolving uniformly for 2min to obtain a material A;
(3) adding a wetting agent and a thickening agent into a pre-dispersion pot, uniformly stirring and dispersing, and stirring and dispersing for 1min to obtain a material B;
(4) under the vacuum condition, the vacuum degree is-0.04 MPa, the material A and the material B are mixed and stirred uniformly, and then a friction agent and a surfactant are added and stirred uniformly to obtain a material C;
(5) adding fresh flower hydrolat, fresh flower essential oil, honeysuckle extract, Pu' er tea polyphenol and probiotics into the material C, stirring uniformly, vacuum degassing until the vacuum degree is more than-0.094 MPa, and homogenizing to obtain the fresh flower toothpaste.
Example 2
The fresh flower toothpaste of the embodiment comprises the following raw materials: 7.5kg of fresh flower hydrolat, 0.01kg of fresh flower essential oil, 0.1kg of honeysuckle extract, 0.1kg of Pu' er tea polyphenol, 18kg of abrasive, 50kg of wetting agent, 1kg of thickening agent, 2kg of surfactant, 0.1kg of sweetening agent, 0.45kg of preservative, 0.3kg of active additive, 0.1kg of probiotics and 20kg of deionized water;
wherein the abrasive is hydrated silicon dioxide; the wetting agent is 70% of sorbitol by mass; the thickening agent is formed by mixing xanthan gum and sodium carboxymethyl cellulose according to the ratio of 1: 1; the surfactant is sodium lauryl sulfate; the sweetening agent is sucralose; the preservative is sodium benzoate; the active matter additive is formed by mixing sodium fluoride, stannous fluoride and tranexamic acid according to the ratio of 1:1: 1;
the fresh flower hydrolat of the embodiment is prepared according to the method of embodiment 3 in patent CN111728109A, only the rose is replaced by jasmine, and the fresh flower essential oil is jasmine essential oil;
the preparation method of the toothpaste of the embodiment comprises the following steps:
(1) weighing the raw materials according to the weight of the raw materials for later use;
(2) adding a sweetening agent, a preservative and an active substance additive into deionized water in a pre-dissolving pot, and stirring and dissolving uniformly for 3min to obtain a material A;
(3) adding a wetting agent and a thickening agent into a pre-dispersion pot, uniformly stirring and dispersing, and stirring and dispersing for 2min to obtain a material B;
(4) under the vacuum condition, the vacuum degree is-0.03 MPa, the material A and the material B are mixed and stirred uniformly, and then a friction agent and a surfactant are added and stirred uniformly to obtain a material C;
(5) adding fresh flower hydrolat, fresh flower essential oil, honeysuckle extract, Pu' er tea polyphenol and probiotics into the material C, stirring uniformly, vacuum degassing until the vacuum degree is more than-0.094 MPa, and homogenizing to obtain the fresh flower toothpaste.
Example 3
The fresh flower toothpaste of the embodiment comprises the following raw materials: 10kg of fresh flower hydrolat, 0.005kg of fresh flower essential oil, 0.15kg of honeysuckle extract, 0.05kg of Pu' er tea polyphenol, 16kg of abrasive, 60kg of wetting agent, 0.5kg of thickening agent, 3kg of surfactant, 0.09kg of sweetening agent, 0.7kg of preservative, 0.1kg of active additive, 0.15kg of probiotics and 15kg of deionized water;
wherein the abrasive is hydrated silicon dioxide; the wetting agent is 70% of sorbitol by mass; the thickening agent is formed by mixing xanthan gum and sodium carboxymethyl cellulose according to the ratio of 1: 1; the surfactant is sodium lauryl sulfate; the sweetening agent is sucralose; the preservative is sodium benzoate; the active matter additive is formed by mixing sodium fluoride, stannous fluoride and tranexamic acid according to the ratio of 1:1: 1;
the flower hydrolat of this example was prepared according to the method of example 3 in patent CN111728109A, only the roses were replaced with the cherry flowers, and the flower essential oil was cherry flower essential oil;
the preparation method of the toothpaste of the embodiment comprises the following steps:
(1) weighing the raw materials according to the weight of the raw materials for later use;
(2) adding a sweetening agent, a preservative and an active substance additive into deionized water in a pre-dissolving pot, and stirring and dissolving uniformly for 4min to obtain a material A;
(3) adding a wetting agent and a thickening agent into a pre-dispersion pot, uniformly stirring and dispersing, and stirring and dispersing for 3min to obtain a material B;
(4) under the vacuum condition, the vacuum degree is-0.02 MPa, the material A and the material B are mixed and stirred uniformly, and then a friction agent and a surfactant are added and stirred uniformly to obtain a material C;
(5) adding fresh flower hydrolat, fresh flower essential oil, honeysuckle extract, Pu' er tea polyphenol and probiotics into the material C, stirring uniformly, vacuum degassing until the vacuum degree is more than-0.094 MPa, and homogenizing to obtain the fresh flower toothpaste.
Example 4
The fresh flower toothpaste of the embodiment comprises the following raw materials: 7kg of fresh flower hydrolat, 0.01kg of fresh flower essential oil, 0.1kg of honeysuckle extract, 0.1kg of Pu' er tea polyphenol, 18.59kg of abrasive agent, 50kg of wetting agent, 1.0kg of thickening agent, 2kg of surfactant, 0.1kg of sweetening agent, 0.5kg of preservative, 0.3kg of active matter additive, 0.1kg of probiotics and 20kg of deionized water;
wherein the abrasive is hydrated silicon dioxide; the wetting agent is 70% of sorbitol by mass; the thickening agent is formed by mixing xanthan gum and sodium carboxymethyl cellulose according to the ratio of 1: 1; the surfactant is sodium lauryl sulfate; the sweetening agent is sucralose; the preservative is sodium benzoate; the active matter additive is formed by mixing sodium fluoride, stannous fluoride and tranexamic acid according to the ratio of 1:1: 1;
the flower hydrolat of this example is rose hydrolat prepared according to the method of example 3 in patent CN111728109A, and the flower essential oil is rose essential oil;
the preparation method of the toothpaste of the embodiment comprises the following steps:
(1) weighing the raw materials according to the weight of the raw materials for later use;
(2) adding a sweetening agent, a preservative and an active substance additive into deionized water in a pre-dissolving pot, and stirring and dissolving uniformly for 2.5min to obtain a material A;
(3) adding a wetting agent and a thickening agent into a pre-dispersion pot, uniformly stirring and dispersing, and stirring and dispersing for 1.5min to obtain a material B;
(4) under the vacuum condition, the vacuum degree is-0.04 MPa, the material A and the material B are mixed and stirred uniformly, and then a friction agent and a surfactant are added and stirred uniformly to obtain a material C;
(5) adding fresh flower hydrolat, fresh flower essential oil, honeysuckle extract, Pu' er tea polyphenol and probiotics into the material C, stirring uniformly, vacuum degassing until the vacuum degree is more than-0.094 MPa, and homogenizing to obtain the fresh flower toothpaste.
Example 5
The fresh flower toothpaste of the embodiment comprises the following raw materials: 7kg of fresh flower hydrolat, 0.01kg of fresh flower essential oil, 0.1kg of honeysuckle extract, 0.15kg of Pu' er tea polyphenol, 18.29kg of abrasive agent, 50kg of wetting agent, 1kg of thickening agent, 2kg of surfactant, 0.1kg of sweetening agent, 0.5kg of preservative, 0.3kg of active additive, 0.1kg of probiotics and 20kg of deionized water;
wherein the abrasive is hydrated silicon dioxide; the wetting agent is 70% of sorbitol by mass; the thickening agent is formed by mixing xanthan gum and sodium carboxymethyl cellulose according to the ratio of 1: 1; the surfactant is sodium lauryl sulfate; the sweetening agent is sucralose; the preservative is sodium benzoate; the active matter additive is formed by mixing sodium fluoride, stannous fluoride and tranexamic acid according to the ratio of 1:1: 1;
the fresh flower hydrolat of the embodiment is prepared according to the method of embodiment 3 in patent CN111728109A, only the rose is replaced by jasmine, and the fresh flower essential oil is jasmine essential oil;
the preparation method of the toothpaste of the embodiment comprises the following steps:
(1) weighing the raw materials according to the weight of the raw materials for later use;
(2) adding a sweetening agent, a preservative and an active substance additive into deionized water in a pre-dissolving pot, and stirring and dissolving uniformly for 2min to obtain a material A;
(3) adding a wetting agent and a thickening agent into a pre-dispersion pot, uniformly stirring and dispersing, and stirring and dispersing for 1min to obtain a material B;
(4) under the vacuum condition, the vacuum degree is-0.04 MPa, the material A and the material B are mixed and stirred uniformly, and then a friction agent and a surfactant are added and stirred uniformly to obtain a material C;
(5) adding fresh flower hydrolat, fresh flower essential oil, honeysuckle extract, Pu' er tea polyphenol and probiotics into the material C, stirring uniformly, vacuum degassing until the vacuum degree is more than-0.094 MPa, and homogenizing to obtain the fresh flower toothpaste.
Comparative example 1
The toothpaste raw materials and the preparation method of the comparative example are the same as those of example 4, except that rose hydrolat is not added to the raw materials.
Comparative example 2
The toothpaste raw material and the preparation method of the comparative example are the same as those of example 4, except that the honeysuckle extract is not added to the raw material.
Comparative example 3
The raw materials and the preparation method of the toothpaste of the comparative example are the same as those of the example 4, except that the raw materials are not added with the Pu' er tea polyphenol.
Test example 1
Test subjects: the middle-aged population, 400 men and 400 women, was divided into 8 groups of 50 men and 50 women on average.
The using method comprises the following steps: brushing 1-2g of toothpaste for 3 minutes each time, and using for 10 days 3 times a day (once in the morning, in the middle and at night).
The results of using the toothpastes prepared in examples 1 to 5 for test groups 1 to 5 and the toothpastes prepared in comparative examples 1 to 3 for control groups 1 to 3, respectively, are shown in table 1, wherein the effect is that no bleeding of gum occurs during the whole tooth brushing process, the tooth surface is smooth, the mouth feeling is obvious, fresh flower fragrance is provided, the fragrance is maintained for a long time, and no allergy or toothache occurs.
TABLE 1
Group of | Effective rate (%) |
Test group 1 | 90 |
Test group 2 | 93 |
Test group 3 | 91 |
Test group 4 | 90 |
Test group 5 | 92 |
Control group 1 | 50 |
Control group 2 | 60 |
Control group 3 | 80 |
As can be seen from Table 1, only by adopting the raw materials of the invention, the toothpaste has the effects of no gum bleeding in the whole tooth brushing process, smooth tooth surface, fresh flower fragrance with obvious mouth feeling after tooth brushing, lasting fragrance, no allergy and toothache, and because the toothpaste prepared by utilizing the combined action of the fresh flower hydrolat, the fresh flower essential oil, the honeysuckle extract and the Pu' er tea polyphenol has the effects of refreshing breath, clearing heat, stopping bleeding, resisting bacteria and allergy, preventing caries, strengthening teeth and removing halitosis.
The above description is only for the specific embodiments of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art can easily conceive of the changes or substitutions within the technical scope of the present invention, and all the changes or substitutions should be covered within the scope of the present invention. Therefore, the protection scope of the present invention shall be subject to the protection scope of the appended claims.
Claims (8)
1. The flower toothpaste is characterized by comprising the following raw materials in parts by weight: 5-10 parts of fresh flower hydrolat, 0.002-0.015 part of fresh flower essential oil, 0.05-0.15 part of honeysuckle extract, 0.05-0.15 part of Pu' er tea polyphenol, 16-20 parts of abrasive, 40-60 parts of wetting agent, 0.5-1.5 parts of thickening agent, 1-3 parts of surfactant, 0.05-0.15 part of sweetening agent, 0.3-0.7 part of preservative, 0.1-0.5 part of active additive, 0.05-0.15 part of probiotics and 15-25 parts of deionized water.
2. The flower toothpaste according to claim 1, wherein the flower of the flower hydrolat and flower essential oil is one or more of rose, jasmine, sweet osmanthus, gardenia, orange flower, cherry and peach flower.
3. The flower toothpaste of claim 1, wherein the abrasive is hydrated silica; the wetting agent is 70% of sorbitol by mass; the thickening agent is xanthan gum and sodium carboxymethyl cellulose; the surfactant is sodium lauryl sulfate; the sweetening agent is sucralose; the preservative is sodium benzoate; the active matter additive is sodium fluoride, stannous fluoride and tranexamic acid.
4. A method of preparing a toothpaste as claimed in any one of claims 1 to 3, said method comprising the steps of:
(1) weighing the raw materials according to the weight of the raw materials for later use;
(2) adding a sweetening agent, a preservative and an active additive into deionized water in a pre-dissolving pot, and stirring and dissolving uniformly to obtain a material A;
(3) adding a wetting agent and a thickening agent into a pre-dispersion pot, and uniformly stirring and dispersing to obtain a material B;
(4) mixing the material A and the material B under a vacuum condition, uniformly stirring, adding a friction agent and a surfactant, and uniformly stirring to obtain a material C;
(5) adding fresh flower hydrolat, fresh flower essential oil, honeysuckle extract, Pu' er tea polyphenol and probiotics into the material C, uniformly stirring, degassing in vacuum, and homogenizing to obtain the fresh flower toothpaste.
5. The method for preparing fresh flower toothpaste according to claim 4, wherein the dissolution time in step (2) is 2-4min under stirring.
6. The method for preparing fresh flower toothpaste according to claim 4, wherein the step (3) is performed by stirring and dispersing for 1-3 min.
7. The method for preparing fresh flower toothpaste according to claim 4, wherein the vacuum degree in step (4) is-0.04 to-0.02 MPa.
8. The method for preparing fresh flower toothpaste according to claim 4, wherein in step (5), vacuum degassing is performed until the vacuum degree is-0.094 MPa or more.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202210490763.3A CN114681382A (en) | 2022-05-07 | 2022-05-07 | Flower toothpaste and preparation method thereof |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202210490763.3A CN114681382A (en) | 2022-05-07 | 2022-05-07 | Flower toothpaste and preparation method thereof |
Publications (1)
Publication Number | Publication Date |
---|---|
CN114681382A true CN114681382A (en) | 2022-07-01 |
Family
ID=82144015
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN202210490763.3A Pending CN114681382A (en) | 2022-05-07 | 2022-05-07 | Flower toothpaste and preparation method thereof |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN114681382A (en) |
Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102764207A (en) * | 2012-06-12 | 2012-11-07 | 云南云道茶业有限公司 | Pu'er tea toothpaste and preparation method thereof |
CN104825350A (en) * | 2015-04-22 | 2015-08-12 | 林晓莉 | Toothpaste using plant hydrosol and essential oil to substitute essence components |
CN107802579A (en) * | 2017-12-06 | 2018-03-16 | 湖南省雅迭香科技有限公司 | Rosemary toothpaste and preparation method thereof |
CN108670902A (en) * | 2018-06-14 | 2018-10-19 | 佛山市渊泊鑫科技有限公司 | A kind of toothpaste except halitosis |
CN111728109A (en) * | 2020-06-19 | 2020-10-02 | 红河大自然水业有限责任公司 | Preparation method of edible flower hydrolat |
CN112662478A (en) * | 2021-01-14 | 2021-04-16 | 四川绿色本草科技发展有限公司 | Chrysanthemum essence, oral cleaning product containing chrysanthemum essence and preparation method of oral cleaning product |
-
2022
- 2022-05-07 CN CN202210490763.3A patent/CN114681382A/en active Pending
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102764207A (en) * | 2012-06-12 | 2012-11-07 | 云南云道茶业有限公司 | Pu'er tea toothpaste and preparation method thereof |
CN104825350A (en) * | 2015-04-22 | 2015-08-12 | 林晓莉 | Toothpaste using plant hydrosol and essential oil to substitute essence components |
CN107802579A (en) * | 2017-12-06 | 2018-03-16 | 湖南省雅迭香科技有限公司 | Rosemary toothpaste and preparation method thereof |
CN108670902A (en) * | 2018-06-14 | 2018-10-19 | 佛山市渊泊鑫科技有限公司 | A kind of toothpaste except halitosis |
CN111728109A (en) * | 2020-06-19 | 2020-10-02 | 红河大自然水业有限责任公司 | Preparation method of edible flower hydrolat |
CN112662478A (en) * | 2021-01-14 | 2021-04-16 | 四川绿色本草科技发展有限公司 | Chrysanthemum essence, oral cleaning product containing chrysanthemum essence and preparation method of oral cleaning product |
Non-Patent Citations (5)
Title |
---|
(美)RICHARD C.DART等: "《5分钟毒理学会诊》", 31 October 2001, 中国医药科技出版社 * |
(美)赫夫纳格尔等: "《益生菌健康宝典》", 31 October 2009, 南海出版社 * |
熊昌云: "《茶叶深加工与综合利用》", 31 March 2015, 云南大学出版社 * |
耿洪森等: "《养生秘典》", 31 July 2004, 安徽人民出版社 * |
贵州省科学技术情报研究所等: "《贵州省中药材大品种产业链》", 30 September 2017, 贵州科技出版社 * |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
Van der Weijden et al. | The effect of herbal extracts in an experimental mouthrinse on established plaque and gingivitis | |
TWI330089B (en) | Enzyme containing oral composition having enhanced stability | |
KR100294515B1 (en) | Effervescent tablet for oral cleaning and preparation method thereof | |
CN105310960B (en) | A kind of novel polysaccharide antimicrobial mouthwash and preparation method thereof | |
US5308611A (en) | Antiseptic composition | |
US5244652A (en) | Viscous surface active composition | |
SK44898A3 (en) | Antimicrobial compositions containing a c3-c6 alcohol | |
US11026881B2 (en) | Sedative laced toothpaste | |
US5885551A (en) | Treatment for dentinal hypersensitivity | |
CN111000772A (en) | New use of exocarpium Citri Grandis extract | |
WO2020054996A1 (en) | Foamable mouthwash solid formulation and preparation method therefor | |
CN107362121A (en) | A kind of anti-inflammatory antiulcer toothpaste of American-cockroach-extract-containing | |
CN105748380A (en) | Full-effective repairing toothpaste containing varied functional compositions | |
WO2016010284A1 (en) | Toothpaste composition containing curcuma longa l., and preparation method therefor | |
CN114681382A (en) | Flower toothpaste and preparation method thereof | |
CN117100676A (en) | Toothpaste containing centella asiatica extract and probiotics and preparation method thereof | |
KR20010036152A (en) | A method for preparation of plant extract powder and oral compositions containing plant extract powder prepared by the same | |
EP4044996A1 (en) | Oral care composition | |
CN110755297A (en) | High-molecular desensitizing paste and preparation method thereof | |
CN103599182A (en) | Traditional Chinese medicine composition and preparation method thereof, and oral cavity cleaning and nursing product and preparation method thereof | |
EA011254B1 (en) | Gel for remineralization of tooth tissues | |
CN108030742A (en) | A kind of warm-natured antibacterial decontamination skin-protection hand cleanser and preparation method thereof | |
CN107260559A (en) | A kind of desensitizing toothpaste and preparation method thereof | |
JP2003012483A (en) | Composition for oral cavity application | |
CN113244121B (en) | Whitening and antibacterial toothpaste |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination |