CN114569497A

CN114569497A - Healthy nourishing hair mask and preparation method thereof

Info

Publication number: CN114569497A
Application number: CN202110979547.0A
Authority: CN
Inventors: 杨一帆; 莫美玲
Original assignee: Zhongshan Zhongyan Cosmetic Co ltd
Current assignee: Zhongshan Zhongyan Cosmetic Co ltd
Priority date: 2021-08-25
Filing date: 2021-08-25
Publication date: 2022-06-03
Anticipated expiration: 2041-08-25
Also published as: CN114569497B

Abstract

The invention provides a healthy nourishing hair mask which comprises the following raw materials in percentage by weight: 78-90% of alcohol compound, 0.5-2% of grease compound, 0.5-1.5% of silicone oil, 0.2-10% of cationic emulsifier and the balance of water. According to the hair conditioner, the specific cationic emulsifier, the alcohol compound and the grease are adopted for proportioning, so that the prepared hair mask is transparent and flowing texture at normal temperature, can be converted into cream texture in the using process, and the cationic surfactant in the hair care ingredients is deposited on the hair in the using process, so that the residue on the scalp is reduced, the irritation is reduced, and the repairing effect is improved.

Description

Healthy nourishing hair mask and preparation method thereof

Technical Field

The invention relates to the field of daily necessities, in particular to a product with an IPC (International patent Classification) code: A61Q5/00, and more particularly relates to a healthy hair nourishing film and a preparation method thereof.

Background

The hair care product is a daily article used in life, can repair and nourish hair, enables the dry and tangled hair to be easily treated, and can endow certain brightness and elasticity.

However, some conventional hair care products on the market, including hair conditioners and hair films, are usually cream in texture, and can cause the cationic surfactant to deposit on the scalp in the using process, so that the scalp is stimulated, and meanwhile, the oil balance of hair follicles is lost, so that the hair is seriously oiled, and a good repairing effect cannot be achieved. Chinese patent CN107569423B discloses a ginseng hair conditioner for repairing damaged hair and a preparation method thereof, wherein 3-10% of ginseng extract, 0.1-2% of D-panthenol, 0.1-0.5% of methylcellulose, 1-5% of monoglyceride, 3-10% of cetostearyl alcohol, 3-10% of silicone oil, 1-5% of behenyl trimethyl ammonium chloride, 3-10% of glycerol, 5-15% of black beans, 2-6% of coffee and the balance of water have the advantages of better repairing the damaged hair and promoting the yellow hair after permanent dyeing to become black hair. But neglects irritation to the scalp and may cause problems with scalp oil production.

Disclosure of Invention

In order to solve the above-mentioned technical problems, the invention provides, in one aspect, a healthy hair nourishing mask, which comprises the following raw materials in percentage by weight:

78-90% of alcohol compounds;

0.5-2% of oil compounds;

0.5-1.5% of silicone oil;

0.2-10% of cationic emulsifier;

the balance of water.

In some embodiments, the alcohol compound comprises one or more of a monohydric alcohol, a polyhydric alcohol, a fatty alcohol.

Preferably, the alcohol compound comprises monohydric alcohol, polyhydric alcohol and fatty alcohol, and the weight ratio is (0.2-0.3): 1: (0.2-0.3).

More preferably, the alcohol compound includes monohydric alcohol, polyhydric alcohol and fatty alcohol, and the weight ratio is 0.24: 1: 0.276.

in some embodiments, the monohydric alcohol comprises at least one of ethanol, isopropanol.

Preferably, the monohydric alcohol is ethanol.

In some embodiments, the polyol comprises at least one of propylene glycol, glycerin, butylene glycol, dipropylene glycol.

Preferably, the polyhydric alcohol comprises glycerol and butylene glycol in a weight ratio of (0.1-0.2): 1.

more preferably, the polyol comprises glycerol and 1, 3-butanediol in a weight ratio of 0.16: 1.

in some embodiments, the fatty alcohol comprises at least one of lauryl alcohol, myristyl alcohol, cetyl alcohol, stearyl alcohol, and octyldodecanol.

Preferably, the fatty alcohol comprises lauryl alcohol, myristyl alcohol and octyldodecanol, and the weight ratio of the lauryl alcohol to the myristyl alcohol is 1: (1.5-2.5): (0.1-0.3).

More preferably, the fatty alcohol comprises lauryl alcohol, myristyl alcohol and octyldodecanol in a weight ratio of 1: 2: 0.2.

in some embodiments, the oil-based compound includes at least one of a synthetic oil, a vegetable oil, and a modified oil.

In some embodiments, the synthetic oil or fat comprises at least one of caprylic/capric triglyceride, tri (ethyl hexanoic) ester, isononyl isononanoate.

Preferably, the synthetic oil is caprylic/capric triglyceride.

In some embodiments, the vegetable oil or fat comprises at least one of olive oil, jojoba oil, macadamia nut oil.

In some embodiments, the cationic emulsifier comprises at least one of oleylamidopropyl dimethylamine, stearyl trimethyl ammonium chloride, palmitylamidopropyl trimethyl ammonium chloride, distearyldimethyl ammonium chloride.

Preferably, the cationic emulsifier is rape oil amidopropyl dimethylamine.

In some embodiments, the silicone oil comprises at least one of polydimethylsiloxane, cyclopolysiloxane, octylpolydimethylsiloxane.

The conventional hair care products exist in cream texture, and the condition can cause the residue of the cationic surfactant on the scalp in the actual use process and influence the hair repairing effect, and after a great deal of research, the applicant finds that the specific cationic emulsifier, the alcohol compound and the oil are adopted for matching, and particularly, the alcohol compound comprises (0.2-0.3): 1: (0.2-0.3) the monohydric alcohol, the polyhydric alcohol and the fatty alcohol are compounded for use, and the oil and fat is caprylic/capric triglyceride, so that the prepared hair mask has transparent flowing texture at normal temperature, can be converted into cream texture in the using process, and can deposit the cationic surfactant in the hair care ingredients on the hair in the process, thereby reducing the residue on the scalp, reducing the irritation and improving the repairing effect, and the applicant considers that the possible reasons are as follows: during the preparation of the hair mask, a specific solvent system can be formed by the proportion of monohydric alcohol, polyhydric alcohol and fatty alcohol, so that the cationic emulsifier and the grease can be stably dissolved in the system, a transparent flowing texture can be formed at normal temperature, the dissolution state of the hair mask is changed after the hair mask is contacted with water in the actual use process, the hair mask finally becomes a cream texture, and the main cationic emulsifier is deposited on the hair just in the technical conversion process, so that the residue on the scalp is reduced, the stimulation is reduced, and the imbalance of the grease secretion of hair follicles is avoided. In addition, through the synergistic effect of the components, the prepared hair mask has excellent mildness and moistening feeling, good wet and dry combing performance and obvious flying resistance effect.

In some embodiments, the feedstock further comprises an adjuvant comprising at least one of a preservative, a chelating agent, a pH adjusting agent.

Preferably, the auxiliary agent comprises a preservative, a chelating agent and a pH regulator.

In some embodiments, the preservative is a cosmetic liquid preservative formulated with phenoxyethanol and ethylhexylglycerin.

In some embodiments, the chelating agent comprises disodium EDTA.

In some embodiments, the pH adjusting agent comprises one of an organic acid including, but not limited to, one of arginine, glutamic acid, aspartic acid, an organic salt including one of citrate, phosphate, or an organic base.

In another aspect of the present invention, there is provided a method for preparing a healthy hair nourishing mask, comprising the steps of: mixing water, alcohol compound, silicone oil and oil compound, heating to 90-95 deg.C, and stirring to uniform state; then stirring and cooling to 40-45 ℃, adjusting the pH value, filtering and discharging to obtain the product.

Has the advantages that:

(1) according to the hair conditioner, the specific cationic emulsifier, the alcohol compound and the grease are adopted for proportioning, so that the prepared hair mask is transparent and flowing at normal temperature and can be converted into cream texture in the using process, and the cationic surfactant in the hair care component is deposited on the hair in the using process, so that the residue on the scalp is reduced, the irritation is reduced, and the repairing effect is improved;

(2) in addition, through the synergistic effect of the components, the prepared hair mask has excellent mildness and moistening feeling, good wet and dry combing performance and obvious anti-flying effect;

(3) the hair care products prepared by the method have the particularity of form and novelty of use feeling.

Drawings

FIG. 1 is a graph showing the sensory evaluation effect of the hair mask prepared in example 1;

FIG. 2 is a graph showing the effect of the anti-flying test of the hair film prepared in example 1;

FIG. 3 is a graph comparing the sensory evaluation effects of example 1 and comparative example 1;

fig. 4 is a graph comparing the sensory evaluation effects of example 1 and comparative example 2.

Detailed Description

Example 1

The embodiment provides a healthy nourishing hair mask, which comprises the following raw materials in percentage by weight:

88% of alcohol compound;

1% of oil and fat compounds;

1% of silicone oil;

5% of cationic emulsifier;

0.8% of preservative;

0.05% of chelating agent;

0.5 percent of pH regulator;

the balance of water.

The alcohol compound comprises monohydric alcohol, polyhydric alcohol and fatty alcohol, and the weight ratio of the monohydric alcohol to the polyhydric alcohol to the fatty alcohol is 0.24: 1: 0.276.

the monohydric alcohol is ethanol, the polyhydric alcohol is glycerol and 1, 3-butanediol, and the weight ratio of the monohydric alcohol to the polyhydric alcohol is 0.16: 1, the fatty alcohol comprises lauryl alcohol, myristyl alcohol and octyldodecanol, and the weight ratio of the lauryl alcohol to the myristyl alcohol is 1: 2: 0.2.

the oil is caprylic/capric triglyceride.

The cationic emulsifier is rape oil amide propyl dimethylamine.

The silicone oil is polydimethylsiloxane which is purchased from Kunshan sanden bioscience and technology Limited and has the model number of 1311.

The preservative is a liquid preservative for cosmetics compounded by phenoxyethanol and ethylhexyl glycerin, and the type of the liquid preservative is German Shumei PE 9010; the chelating agent is EDTA disodium; the pH regulator is aspartic acid.

Another aspect of the present invention provides a method for preparing a healthy hair nourishing mask, including the steps of: mixing water, glycerol, 1, 3-butanediol, polydimethylsiloxane, caprylic/capric triglyceride, octyldodecanol, lauryl alcohol, myristyl alcohol, rape oil amide propyl dimethylamine, antiseptic and chelating agent, heating to 92 deg.C, and stirring to obtain uniform mixture; then cooling to 43 deg.C under stirring, adding ethanol and stirring, adding aspartic acid to adjust pH, and filtering with 600 mesh filter cloth.

Example 2

This example provides a health-care hair mask and a method for preparing the same, and the specific embodiment is the same as example 1, except that the alcohol compound does not include ethanol, but is replaced with water.

Example 3

This example provides a healthy hair nourishing membrane and a method for preparing the same, and the specific embodiment is the same as example 1, except that ethanol is replaced by ethoxydiglycol.

Example 4

The present example provides a healthy hair nourishing membrane and a method for preparing the same, and the specific embodiment is the same as example 1, except that the alcohol compound includes monohydric alcohol, polyhydric alcohol and fatty alcohol, and the weight ratio is 0.1: 1: 0.4.

Comparative example 1

This comparative example is a commercially available high end silicone-free conditioner.

Comparative example 2

The comparative example is a silicon-containing moisturizing hair conditioner on the market.

Performance testing

1. Sensory evaluation

The specific test method is as follows: 10 volunteers were tested, on the first day, using a common anti-dandruff shampoo without using a hair mask, on the second day, using a common anti-dandruff shampoo with the hair mask prepared in example 1, and scoring (1 to 10 points) from five dimensions of wet-thinning property, dry-thinning property, after-use moist feeling, hair-lightening degree and mildness, and then calculating the average score of each item, and the evaluation results are shown in fig. 1.

And (4) conclusion: the results shown in fig. 1 show that the hair mask of the present invention is excellent in mildness and moist feeling, excellent in wet-drying-and-drying performance, and moderately improved in hair gloss after use.

2. Flying resistance test

The specific test method comprises the following steps: two bundles of hair with similar weight are adopted, after the same cleaning operation, one bundle of hair is used with the hair mask prepared in the embodiment 1 of the invention, the other bundle of hair is not used, after the hair mask is washed clean and dried, the hair mask is combed straight, the two bundles of hair are hung side by side naturally, the flying condition of the two bundles of hair is observed, and the hair mask is photographed and recorded, and the test effect is shown in figure 2.

And (4) conclusion: as can be seen from comparison of fig. 2, the hair piece of the present invention has a significant anti-flying effect.

3. State of hair film

The state of the hair film obtained in examples 1 to 4 was observed, and the results are shown in Table 1.

TABLE 1

4. Compared with the effect of the commercial hair conditioner

The hair mask prepared in example 1 was evaluated for effects with the conditioners provided in comparative examples 1 and 2, respectively, and the results are shown in fig. 3 and 4, respectively.

Claims

1. The healthy hair nourishing film is characterized by comprising the following raw materials in percentage by weight:

78-90% of alcohol compounds;

0.5-2% of oil compounds;

0.5-1.5% of silicone oil;

0.2-10% of cationic emulsifier;

the balance of water.

2. The health-care hair nourishing film as claimed in claim 1, wherein the alcohol compound comprises one or more of monohydric alcohol, polyhydric alcohol and fatty alcohol.

3. The hair tonic according to claim 2, wherein the monohydric alcohol comprises at least one of ethanol and isopropanol.

4. The health hair nourishing film of claim 2, wherein the polyol comprises at least one of propylene glycol, glycerin, butylene glycol, dipropylene glycol.

5. The health hair nourishing film of claim 2, wherein the fatty alcohol comprises at least one of lauryl alcohol, myristyl alcohol, cetyl alcohol, stearyl alcohol, and octyldodecanol.

6. A health-promoting hair mask as claimed in any one of claims 1 to 5, wherein said oil compound includes at least one of synthetic oil, vegetable oil and modified oil.

7. The hair tonic according to claim 6, wherein the synthetic oil or fat includes at least one of caprylic/capric triglyceride, tri (ethyl hexanoic) glyceride, and isononyl isononanoate.

8. The health hair nourishing film of claim 1, wherein the cationic emulsifier comprises at least one of oleyl amidopropyl dimethylamine, stearyl trimethyl ammonium chloride, palmitamidopropyl trimethyl ammonium chloride, and distearyl dimethyl ammonium chloride.

9. The hair tonic film according to claim 1, wherein the raw material further comprises an auxiliary agent, and the auxiliary agent comprises at least one of a preservative, a chelating agent, and a pH adjuster.

10. A method for preparing the health nourishing hair mask according to any one of claims 1 to 9, comprising the steps of: mixing water, alcohol compound, silicone oil and oil compound, heating to 90-95 deg.C, and stirring to uniform state; then stirring and cooling to 40-45 ℃, adjusting the pH value, filtering and discharging to obtain the product.