CN1144599A - Treatment method and liquid for withered green plant recovering its active state - Google Patents
Treatment method and liquid for withered green plant recovering its active state Download PDFInfo
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- CN1144599A CN1144599A CN 95115411 CN95115411A CN1144599A CN 1144599 A CN1144599 A CN 1144599A CN 95115411 CN95115411 CN 95115411 CN 95115411 A CN95115411 A CN 95115411A CN 1144599 A CN1144599 A CN 1144599A
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Abstract
A method for restoring withered green plant to its living-like states in luster, form, flexibility, smooth-out and forcefulness features use of a processing liquid, which contains colouring and colour-gaining agent, extending agent, softening agent, etc. The living-like states of processed plant can continue for more than 2 years. Said method is suitable for dried flower, artistic articles and food packaging materials.
Description
The present invention relates to a kind of processing method and treatment fluid that makes green plant recovering and keep its activated state.Or rather, the invention provides a kind of is method and the Treatment Solution that withered plant is handled especially to the withered or fresh of green, by this processing, color and luster in the time of can making this green plant recovering and keep its condition of living organism, form, tall and straight property, softness and stretching, and above-mentioned feature long term maintenance can be reached more than 2 years.Can be widely used in the production of dried flower, handicraft production and packaging material for food.
The present invention is applicable to multiple green seed plant and spore producing plant.The for example oak in the spermatophyte, poplar, maple, bamboo, wormwood artemisia, eucalyptus, the tuber of dwarf lilyturf, cattail, Chinese ilex, little leaf boxwood, yulan, cloves, Chinese mahonia, barberry, asparagus fern or the like.Various plants in spore producing plant such as Lycopodiaceae, Pteridaceae, Aspleniaceae, the iron XIAN Pteridiaceae.
Home and abroad patent documentation by retrieval is even can not find the Perfected process of the multiple numerous features such as natural colour, form, tall and straight property, softness and stretching that can recover and keep plant leaf for a long time at present.Some patent of villous themeda relates to green branches and leaves handling problem to the greatest extent, and for example CN1058131A uses mantoquita and corresponding acid group that herbarium is handled, and can only obtain losing the transparent plant specimens of plant living body feature; CN1043857A emphasizes then that to plant treatment the time must be earlier cauline leaf being carried out drying processing carries out vacuum or aeration-drying not being higher than 50%, the plant water content is remained on below 10%, obviously, Yan Ge condition will increase the production difficulty like this, improve product cost greatly, and be helpless to recover and keep its above-mentioned active nature.
The plant tissue that the clear 61-41481 of Japan Patent mentions is preserved liquid, system is made up of multiple alcohols such as ethanol, isopropyl alcohol, the tert-butyl alcohol, sec-butyl alcohol, normal propyl alcohol and propyl alcohol, salicylic acid, magnesium sulfate, sodium sulphite, copper sulphate etc., used chemicals is of a great variety, cost is high as can't to accept, moreover use multiple dehydration of alcohols can cause vegetable material dry-shrinkage deformed, can't reach effect of the present invention.
The objective of the invention is to overcome the deficiency of above-mentioned prior art, propose a kind of treatment fluid that can recover and keep the processing method of vegetable active state for a long time and use for this method.
The present invention realizes like this.According to plant treatment method of the present invention, be that pending green plants is at first put in order and cleans, being placed on then in the color development treatment fluid, is 60-100 ℃ of down heating 1-30 minute in temperature, is presented on green effect under the nature thereby obtain this plant.
For making plant present more stable emerald green effect, through or without the plant that color development was handled, place hyperchromic treatment fluid, be to heat 1-8 minute under 60-100 ℃ the condition in temperature, just can obtain.
Through the plant of above processing, not only color is an emerald green, and colour stable.And in order to make branches and leaves keep tall and straight characteristics under the nature, the vegetable material of color development and/or hyperchromic processing can be dipped in the stiffening treatment fluid, be heating 1-6 minute under 60-100 ℃ the condition in temperature, thereby make the plant tissue sclerosis that it is stiffening that branches and leaves become.
No matter whether vegetable material needs through above step process, all can in softening treatment fluid, soften processing, be about to vegetable material in bating liquor, flooding the several seconds under the room temperature, so that it keeps soft characteristic to a few hours.(, adopting different dip times) according to floristic difference.
The purpose of unfolding processing be make that green plants keeps lifelike image unfold state naturally, its processing method is in unfolding in the liquid dipping several seconds to 2 minute under the greenhouse, to keep unfolding state with vegetable material.
According to green-plant treatment method of the present invention, wherein said color development treatment fluid is the simple substance of a kind of organic acid or inorganic acid and a kind of transition metal or the aqueous solution that compound is formed.Wherein organic acid can be malic acid, oxalic acid, sorbic acid, formic acid, fumaric acid, chloroacetic acid, dichloroacetic acid, trichloroacetic acid, tartaric acid, trifluoroacetic acid, acetate, malonic acid, propionic acid, peracetic acid, glycolic, lactic acid, succinic acid, citric acid, gallic acid, mellic acid, crotonic acid, pyrogallol, tetrahydroxysuccnic acid, o-toluene sulfonic acid, benzene sulfonic acid, maleic acid, fumaric acid, its consumption in the color development treatment fluid is 0.01-30 gram/every premium on currency, and optimum amount is 6-8 gram/every premium on currency.Wherein inorganic acid is hydrochloric acid, sulfuric acid, nitric acid, nitrous acid, sulfurous acid, phosphoric acid, phosphorous acid, hypophosphorous acid, peroxophosphoric acid, pyrosulfuric acid, arsenic acid, bromic acid, boric acid, acid iodide, selenous acid, chlorine bromic acid; Its consumption in the color development treatment fluid is 0.001-18 gram/every premium on currency, and optimum amount is 3-6 gram/every premium on currency.Wherein the simple substance of transition metal is zinc, copper, iron; Transistion metal compound is its oxide (as: zinc oxide, copper oxide, ferrous oxide), hydroxide (as: zinc hydroxide, Kocide SD, ferrous hydroxide) and salt, and wherein organic salt can be: zinc malate, formic acid zinc, zinc picrate, zinc acetate, zinc lactate, zinc glycerophosphate, zinc sulfanilate, zinc benzoate, zinc salicylate, zinc sulfocarbolate, zinc valerate, copper benzoate, copper phenolsulfonate, copper acetate, four ammonia copper sulphate; Wherein mineral salt can be zinc chloride, zinc sulphate, zinc carbonate, zinc nitrate, Firebrake ZB, zinc chlorate, zinc hypophosphite, hypophosphorous acid copper, copper chloride, copper sulphate, copper nitrate, copper chlorate, frerrous chloride.The simple substance of transition metal or the compound consumption in the color development treatment fluid is 0.001-30 gram/every premium on currency, and optimum amount is 15-25 gram/every premium on currency.
In addition, in the color development treatment fluid, when acid during with the salt compatibility of transition metal, the consumption of any acid can be controlled in 0-12 gram/every premium on currency, and optimum amount is 4-6 gram/every premium on currency.
The color development treatment mechanism of green plants is that the green in the natural plant material is to be determined by least stable chlorophyll.Chlorophyll can dissociate out after plant cell death, and free chlorophyll is very unstable, and the magnesium atom under acid condition in the chlorophyll molecule can be replaced by hydrogen and generate the pheophytin of brown.Under condition of compatibility, the magnesium atom in the chlorophyll can be replaced by zinc, copper, iron transition metal ions, generates the greenization compound, and this green matter can generate the chlorophyllin sodium of zinc, copper or iron with the sodium hydroxide reaction, thereby obtains stable emerald green color effects.
Therefore, according to green-plant treatment method of the present invention, wherein hyperchromic treatment fluid is a kind of aqueous solution of alkali-metal hydroxide, for example the aqueous solution of sodium hydroxide or potassium hydroxide.The consumption of alkali metal hydroxide is 0.01-20 gram/every premium on currency in the hyperchromic treatment fluid, and the hydroxide optimum amount that drops in every premium on currency is 3-6 gram/every premium on currency.
According to green-plant treatment method of the present invention, wherein stiffening treatment fluid is a kind of aqueous solution of calcium salt, and its consumption in treatment fluid is 0.1-15 gram/every premium on currency, and optimum amount is 6-8 gram/every premium on currency.This calcium salt can be nitrate of lime, calcium citrate, calcium chloride, calcium sulphate, calcium oxalate, calcium lactate, formic acid calcium, calcium molybdate, calcium chromate, calcium phosphate, calcium metaphosphate, calcium succinate, calcium pyrophosphate, calcium propionate, calcium sulfite, calcium lactobionate, calcium oleate, Lime Hypophosphate, calcium monohydrogen phosphate, calcium succinate, phytic acid calcium, calcium tartrate (most of at ambient temperature calcium salt is slightly soluble in water).
The stiffening mechanism of handling of green plants is that variation has taken place plant tissue after heat treatment its fibre structure, and the rockiness of these tissues depends on molecular linkage firm between cell-wall components.Pectin substance produces hard structure by the crosslinked action of its free hydroxyl group and polyvalent cation.The calcium salt that adds in the treatment fluid can increase more insoluble pectinic acid calcium salt and pectic acid calcium salt, strengthened crosslinked, thereby increased flintiness.These rock-steady structures are supporting to be organized, and makes it keep stiffening.
According to green-plant treatment method of the present invention, wherein softening treatment fluid is the aqueous solution of a kind of polyalcohol or fatty acid ester, and its consumption in softening treatment fluid is 1-500 milliliter/every premium on currency, and optimum amount is 5-300 milliliter/every premium on currency.Wherein polyalcohol can be glycerine, propane diols, two propyl alcohol, 1,3-butanediol; Wherein fatty acid ester is a polyoxyethylene sorboside fatty acid ester.
Selected its molecular structure of softening inorganic agent all has a plurality of hydrophilic radicals, can make plant tissue often keep moisture state and present pliability.
According to green-plant treatment method of the present invention, wherein unfolding treatment fluid is the xylene solution of a kind of aqueous solution resin aqueous solution or organic siliconresin.The consumption of water-soluble resin is 1-30 gram/every premium on currency in treatment fluid, and optimum amount is 5-10 gram/every premium on currency.The consumption of organic siliconresin is 1-20 gram/every liter of dimethylbenzene in treatment fluid, and optimum amount is 3-8 gram/every liter of dimethylbenzene (dimethylbenzene is as solvent).
The water-soluble resin of unfolding in the treatment fluid can be: poly-oxireme, polyacrylate, melamine resin and polyvinyl alcohol; Organic siliconresin can be methyl silicon resin, methyl phenyl silicone resin.
The constituent of unfolding treatment fluid can strengthen the enabling capabilities of vein, thereby makes branches and leaves keep the state of unfolding of nature.
As mentioned above, the present invention does not limit water content, baking temperature and the drying mode of vegetable material, need not earlier plant to be carried out drying before processing and handles.The transparent phenomenon of distortion can not appear in branches and leaves after treatment.Single with regard to the color development treatment fluid, even can only use a kind of inorganic compound to finish, thus can reduce product cost greatly.Moreover, kind surplus alternative treatment fluid constituent reaches 120, they can form numerous effective prescription.And can select different prescriptions for use to different plants, and in the hope of reaching optimum efficiency, can process floristic scope thereby widened, for more extensive, more effective development and use plant resources has been created condition, has also widened the range of application of product simultaneously.The present invention is not only applicable to the processing of fresh plant material, and be applicable to the processing of withered vegetable material, all can be to recovering and color and luster, form, tall and straight property, softness and stretching when keeping the vegetable active state provides remarkable result, and keep above-mentioned feature up to more than 2 years.
Example 1
Get 20 pieces in withered yulan branches and leaves and put, clean, be bundled into bundle in order, in pot, add 1 premium on currency, ZnO 5 grams, hydrochloric acid is made into the color development treatment fluid for 6 milliliters, place pot to boil after 5-18 minute in branches and leaves and take out, put into the hyperchromic treatment fluid heating 3 minutes that every premium on currency contains NaOH 5 grams.Place the stiffening treatment fluid of calcium citrate 5 grams per liters to boil to take out in 3 minutes then and clean, place every premium on currency to add glycerine 300 grams again, 1, soaked 8-10 hour in the softening treatment fluid of 3-butanediol 200 grams.Yulan leaf after softening the processing moves in the water-soluble resin and soaks 5-10 second.The proportioning of water-soluble resin is that a premium on currency adds 25 gram melamine resins.To dry packing at last.Example 2
Get the withered leaf of bamboo and be bundled into bundle for 30 pieces, and it is put in order cleaning.In pot, add Cu (OH) 25 grams by every premium on currency, industrial sulphuric acid is made into the color development treatment fluid for 6 milliliters, the leaf of bamboo inserted boil 5-6 minute in the pot, pull the back out for a moment with flushing with clean water, move in the softening treatment fluid thereupon and soaked about 24 hours, the proportioning of softening treatment fluid is that 1 premium on currency adds glycerine 100 grams, two propyl alcohol, 100 grams, 1,3-butanediol 100 grams, dry after taking out from softening treatment fluid, moving on to proportioning then is to add methyl silicon resin 15 unfolding of gram in every liter of dimethylbenzene (solution) to soak in the treatment fluid 5-10 second, dries (2-4 hour) packing at last.Example 3
Getting 20 of the fringe lycopods of hanging down is bundled into a branch of, arrangement is cleaned, in pot, add red fuming nitric acid (RFNA) 5ml by every premium on currency, zinc granule 5 grams are made into the color development treatment fluid, the fringe lycopod of will hanging down places pot to boil 5-10 minute, pull out with flushing with clean water for a moment, placed softening treatment fluid dipping 8-12 hour thereupon, the constituent and the proportioning of softening treatment fluid are identical with example 2.Lycopod after softening the processing can directly move to unfolding that example 1 adopted and soak in the treatment fluid 5-10 second, dries packing at last.
Claims (7)
1, a kind of processing method of color and luster, form, tall and straight property, softness and stretching when making withered or fresh green plant recovering and keeping its activated state is characterized in that comprising the steps:
(1) color development processing----is immersed green plants in the color development Treatment Solution, takes out after 1-30 minute in heating under 60-100 ℃ the temperature condition, and this color development treatment fluid is organic or inorganic acid and a kind of simple substance of transition metal or the aqueous solution of compound;
(2) hyperchromic processing----is immersed green plants in the hyperchromic Treatment Solution, take out after 1-8 minute in heating under 60-100 ℃ the temperature condition, this hyperchromic treatment fluid is a kind of aqueous solution of alkali metal hydroxide, and its content in treatment fluid is 0.01-20 gram/every premium on currency;
(3) stiffening processing----is immersed green plants in the stiffening Treatment Solution, takes out after 1-6 minute in heating under 60-100 ℃ the temperature condition, and this stiffening treatment fluid is a kind of aqueous solution of calcium salt, and its content in treatment fluid is 0.1-15 gram/every premium on currency;
(4) in flooding the several seconds to a few hours under the room temperature in softening Treatment Solution, this softening treatment fluid is the aqueous solution of a kind of polyalcohol or fatty acid ester with green plants in softening processing----, and its content in treatment fluid is 1-500 milliliter/every premium on currency;
(5) unfold processing----takes out green plants after unfolding in the Treatment Solution dipping number paper money to 2 minute under the room temperature, this unfolds treatment fluid is a kind of aqueous solution of water-soluble resin or the xylene solution of organic siliconresin, the content of its water-soluble resin in treatment fluid is 1-30 gram/every premium on currency, and the content of organic siliconresin is 1-20 gram/every liter of dimethylbenzene.
2, according to the processing method of claim 1, it is characterized in that: the organic acid in the described color development treatment fluid is selected from malic acid, oxalic acid, sorbic acid, formic acid, fumaric acid, chloroacetic acid, dichloroacetic acid, trichloroacetic acid, tartaric acid, trifluoroacetic acid, acetate, malonic acid, propionic acid, peracetic acid, glycolic, lactic acid, succinic acid, citric acid, gallic acid, mellic acid, crotonic acid, pyrogallol, tetrahydroxysuccnic acid, o-toluene sulfonic acid, benzene sulfonic acid, maleic acid, fumaric acid, and its content in treatment fluid is 0.01-30 gram/every premium on currency.
3, according to the processing method of claim 1, it is characterized in that: inorganic acid is selected from hydrochloric acid, sulfuric acid, nitric acid, nitrous acid, sulfurous acid, phosphoric acid, phosphorous acid, hypophosphorous acid, peroxophosphoric acid, pyrosulfuric acid, arsenic acid, bromic acid, boric acid, acid iodide, selenous acid, chlorine bromic acid in the described color development treatment fluid, and its content in treatment fluid is 0.001-18 gram/every premium on currency.
4, according to the processing method of claim 1, it is characterized in that: transition metal simple substance is zinc, copper, iron in the described color development treatment fluid, other compounds are oxide, hydroxide and the salt of transition metal zinc, copper, iron, and wherein organic salt is: zinc malate, formic acid zinc, zinc picrate, zinc acetate, zinc lactate, zinc glycerophosphate, zinc valerate, zinc benzoate, zinc salicylate, zinc sulfocarbolate, zinc sulfanilate, copper benzoate, copper phenolsulfonate, copper acetate, four ammonia copper sulphate; Wherein mineral salt are: zinc chloride, zinc chlorate, zinc hypophosphite, hypophosphorous acid copper, copper chloride, copper sulphate, copper nitrate, copper chlorate, frerrous chloride, above-mentioned simple substance or the compound content in the color development treatment fluid are 0.001-30 gram/every premium on currency.
5, according to the processing method of claim 1, it is characterized in that: calcium salt is selected from nitrate of lime, calcium citrate, calcium chloride, calcium sulphate, calcium oxalate, calcium lactate, formic acid calcium, calcium molybdate, calcium chromate, calcium phosphate, calcium metaphosphate, calcium succinate, calcium propionate, calcium sulfite, calcium lactobionate, calcium oleate, Lime Hypophosphate, calcium monohydrogen phosphate, calcium succinate, phytic acid calcium, calcium tartrate in the described stiffening treatment fluid.
6, according to the processing method of claim 1, it is characterized in that: the polyalcohol in the described softening treatment fluid is selected from glycerine, propane diols, two propyl alcohol, 1, and 3-butanediol, described fatty acid ester are polyoxyethylene sorboside fatty acid ester.
7, according to the processing method of claim 1, it is characterized in that: described water-soluble resin of unfolding in the treatment fluid is selected from PEO, polyacrylate, melamine resin and polyvinyl alcohol, and organic siliconresin is selected from methyl silicon resin and methyl phenyl silicone resin.
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| Application Number | Priority Date | Filing Date | Title |
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| CN 95115411 CN1144599A (en) | 1995-09-08 | 1995-09-08 | Treatment method and liquid for withered green plant recovering its active state |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 95115411 CN1144599A (en) | 1995-09-08 | 1995-09-08 | Treatment method and liquid for withered green plant recovering its active state |
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| CN1144599A true CN1144599A (en) | 1997-03-12 |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100396175C (en) * | 2003-11-13 | 2008-06-25 | 株式会社佐藤运送 | Method for restoring plant green or preserving plant green |
| CN101518368A (en) * | 2008-02-29 | 2009-09-02 | 谢富有 | Preservative tree prepared in accordance with supplementary preservative plant technology |
| CN103621494A (en) * | 2012-08-28 | 2014-03-12 | 张明焕 | Plant preserving treatment method and plant treatment liquid compositions |
| CN104589900A (en) * | 2015-01-05 | 2015-05-06 | 青岛农业大学 | Dried flower production method for aquatic flower plants |
| CN105052898A (en) * | 2015-08-26 | 2015-11-18 | 昆明紫色青阳生物科技有限公司 | Preserved hydrangea processing method |
| CN105252622A (en) * | 2015-09-02 | 2016-01-20 | 安徽省蓼源贸易有限责任公司 | Method for manufacturing craft through waste bamboo |
| CN108029682A (en) * | 2018-01-04 | 2018-05-15 | 云南欣绿茶花股份有限公司 | A kind of processing method of camellia immortality branches and leaves |
| CN110915436A (en) * | 2019-10-25 | 2020-03-27 | 内蒙古源生泰农牧业开发有限公司 | Cottonseed storage method |
-
1995
- 1995-09-08 CN CN 95115411 patent/CN1144599A/en active Pending
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100396175C (en) * | 2003-11-13 | 2008-06-25 | 株式会社佐藤运送 | Method for restoring plant green or preserving plant green |
| CN101518368A (en) * | 2008-02-29 | 2009-09-02 | 谢富有 | Preservative tree prepared in accordance with supplementary preservative plant technology |
| CN101518368B (en) * | 2008-02-29 | 2011-08-10 | 谢富有 | Preservative tree prepared in accordance with supplementary preservative plant technology |
| CN103621494A (en) * | 2012-08-28 | 2014-03-12 | 张明焕 | Plant preserving treatment method and plant treatment liquid compositions |
| CN104589900A (en) * | 2015-01-05 | 2015-05-06 | 青岛农业大学 | Dried flower production method for aquatic flower plants |
| CN104589900B (en) * | 2015-01-05 | 2018-04-27 | 青岛农业大学 | A kind of flower drying method for aquatic flowers plant |
| CN105052898A (en) * | 2015-08-26 | 2015-11-18 | 昆明紫色青阳生物科技有限公司 | Preserved hydrangea processing method |
| CN105252622A (en) * | 2015-09-02 | 2016-01-20 | 安徽省蓼源贸易有限责任公司 | Method for manufacturing craft through waste bamboo |
| CN108029682A (en) * | 2018-01-04 | 2018-05-15 | 云南欣绿茶花股份有限公司 | A kind of processing method of camellia immortality branches and leaves |
| CN110915436A (en) * | 2019-10-25 | 2020-03-27 | 内蒙古源生泰农牧业开发有限公司 | Cottonseed storage method |
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