CN114432208A

CN114432208A - Softening and nourishing shampoo

Info

Publication number: CN114432208A
Application number: CN202210312814.3A
Authority: CN
Inventors: 王澍; 彭慧群; 易霞; 王莹
Original assignee: Hangzhou Yuexuantang Cosmetics Co ltd
Current assignee: Hangzhou Yuexuantang Cosmetics Co ltd
Priority date: 2022-03-28
Filing date: 2022-03-28
Publication date: 2022-05-06
Anticipated expiration: 2042-03-28
Also published as: CN114432208B

Abstract

The invention discloses a softening and nourishing shampoo, which is obtained by a large number of experiments and mainly comprises the following pharmacology: the rice washing water fermentation product, the polygonum multiflorum extract, the poria cocos extract and the semen cuscutae extract are used as nourishing components, and the rice washing water also has comprehensive performances of oxidation resistance and the like; cortex Phellodendri and Scutellariae radix as antibacterial and antipruritic components; the tea bran extract and the soapberry extract are used as antioxidant components and also have partial bactericidal effect; the liquorice, clove and borneol are compounded to form the permeation and absorption promoting component, so that the nourishing and absorption speed can be increased, the quick effect can be achieved, and the deep sterilization capability of the sterilization component and the like can be improved; rabbit hair keratin is used as a moisture-preserving and protecting component; then, the dosage of the surfactant, the castor oil and the thickening agent is continuously optimized and adjusted according to the feedback of the test result, and the shampoo in the formula has multiple effects of quickly nourishing hair, deeply sterilizing, keeping moisture for a long time, removing dandruff, relieving itching and the like.

Description

Softening and nourishing shampoo

Technical Field

The invention relates to the technical field of articles for daily use, and particularly relates to a softening and nourishing shampoo.

Background

For hair care, currently, related shampoos, hair conditioners, hair treatment creams and the like are combined by chemical preparations to solve related hair quality problems and the like, and the disadvantage is that the side effect is large. In contrast, in China, related traditional Chinese medicine combined products are explored according to the traditional Chinese medicine concept, taking shampoo as an example, and researches are carried out on the market according to the phenomena of improving hair quality and the like of rice washing water commonly used by Yunnan minority, so that related hair washing products are provided, for example, a scheme for fermenting arborvitae mixed with brown sugar, privet, ginger, rice washing water and the like is disclosed in a patent document with the authorization number of CN104382809B, and a rice washing plant fermentation product is disclosed in a patent document with the authorization number of CN112522150B, and aloe, ginger and the like are mixed with purified strains for fermentation. However, the specific action mechanism of the rice washing water on hair after fermentation is not clear, and all the people are exploring, so that the department intends to develop a collocation scheme of the rice washing water and the traditional Chinese medicine components by taking quick effect, itching relieving, scurf removing, hair blacking and the like as utility indexes according to the lack of the phenomena of products such as hair blacking, hair blacking and the like related to rice washing water fermentation in the market.

Disclosure of Invention

In order to solve at least one technical defect, the invention provides the following technical scheme:

the application document discloses a softening and nourishing shampoo which comprises the following components in parts by mass:

a lot of experiments are carried out to explore diversified collocation schemes of rice washing water fermentation products and traditional Chinese medicines, the schemes are obtained by continuously adjusting according to test results, and the main pharmacology is as follows: the rice washing water fermentation product, the polygonum multiflorum extract, the poria cocos extract and the semen cuscutae extract are used as nourishing components, and the rice washing water also has comprehensive performances of oxidation resistance and the like; cortex Phellodendri and Scutellariae radix as antibacterial and antipruritic components; the tea bran extract and the soapberry extract are used as antioxidant components and also have partial bactericidal effect; the liquorice, clove and borneol are compounded to form the permeation and absorption promoting component, so that the nourishing and absorption speed can be increased, the quick effect can be achieved, and the deep sterilization capability of the sterilization component and the like can be improved; rabbit hair keratin is used as a moisture-preserving and protecting component; then, the dosage of the surfactant, the castor oil and the thickening agent is continuously optimized and adjusted according to the feedback of the test result, and the shampoo in the formula has multiple effects of quickly nourishing hair, deeply sterilizing, keeping moisture for a long time, removing dandruff, relieving itching and the like.

Further, mixing cortex Phellodendri, Scutellariae radix, and Glycyrrhrizae radix, and fermenting with Aspergillus niger to obtain fermentation liquid as mixture of Glycyrrhrizae radix extract, cortex Phellodendri extract, and Scutellariae radix extract. According to the scheme, the extract is prepared from the golden cypress, the radix scutellariae and the liquorice in a mixed fermentation mode, so that the preparation process and time are saved, and the golden cypress, the radix scutellariae and the liquorice are specifically prepared into the extract by the following steps in a mass ratio of (10-12): 10-12: 0.06-0.2 is mixed in 4-6 times of water, after soaking for 2h, 5-8% of aspergillus niger is inoculated for fermentation, the fermentation temperature is 28-30 ℃, the rotation speed is 180-220rpm, the fermentation time can be 40-60h, then sterilization and filtration are carried out to obtain fermentation liquor, the fermentation liquor is concentrated to 1-2 times of the mass of the medicinal herbs, namely extract mixed liquor, according to detection, the concentrations of berberine, baicalin, glycyrrhetinic acid and the like in the mixed liquor are greatly improved compared with the common water extraction and the like, and the effect is obvious when the extract mixed liquor is applied to shampoo.

Further, adding yeast strain 2-5% by mass into the rice washing water, fermenting at 25-32 deg.C for 50-70 hr, sterilizing, and filtering to obtain rice washing water fermented product. Washing rice water such as rice or glutinous rice, soaking rice accounting for 20-35% of the water solution by mass at 20-22 ℃, stirring for 40-80min, filtering to obtain rice washing water, autoclaving the rice washing water at 120 ℃ for more than 10min, inoculating 2-5% yeast strain, fermenting at 25-32 ℃, keeping the rotation speed of 180-220rpm, stirring and fermenting for 50-70h, and sterilizing to obtain rice washing water fermentation liquor.

Further, the tea bran after the pressure treatment under 0.8-1.0MPa is extracted by water, and is filtered and separated to obtain an extract, and the extract is concentrated to 0.5-0.8 time of the weight of the tea bran, namely the tea bran extract. The pressurizing treatment is helpful for improving the concentration of active ingredients of the extract in the tea bran, the tea polyphenol, the tea saponin and the like in the tea bran extract have the effects of absorbing ultraviolet rays, sterilizing, resisting oxidation and the like, and when the tea bran extract is compounded into the formula, the effect is greatly increased.

Further, 8-12% of rhizopus oryzae is inoculated in the polygonum multiflorum particle suspension for fermentation for 30-36h, sterilization and filtration are carried out, and the polygonum multiflorum extract is obtained, similarly, the beneficial components of polygonum multiflorum are extracted in a fermentation mode, and the polygonum multiflorum is a common preparation for traditional Chinese medicine hair blackening.

For the polygonum multiflorum particle suspension, for example, polygonum multiflorum is crushed into particles, then the particles are mixed with distilled water to form a mixed solution with the concentration of 3-8 percent, namely the suspension, rhizopus oryzae strains can be inoculated after high-pressure sterilization, fermentation is carried out at the temperature of 25-28 ℃, the rotating speed is 100-150rpm, the time is 40-50h, the polygonum multiflorum extract is obtained after sterilization and filtration and is concentrated to 1-2 times of the mass of the medicine, and the content of substances such as alkene glycosides, anthraquinone, lecithin and the like is improved through detection.

In the scheme, the traditional Chinese medicine extract is mostly carried out in a fermentation mode, so that the active ingredients of the traditional Chinese medicine extract are utilized to a higher degree, and the hair washing effect is further improved.

Further, the extract is prepared by extracting semen cuscutae, fructus sapindus mukorossi, clove and poria cocos by water, and the mixed water extraction method is helpful for reducing time and saving working procedures, for example, the extract is prepared by extracting semen cuscutae, poria cocos, fructus sapindus mukorossi and clove by mass according to the ratio of 10-26: mixing at a mass ratio of 10-26:12-18:1, adding 5 times of water, soaking for 4 hr, decocting, concentrating to about 2.5 times of the weight of the medicinal materials, filtering, and heating and concentrating the filtrate to 0.6-0.8 times of the weight of the medicinal materials. In addition, the product is basically consistent with the mixed extract in a single extraction mode.

Further, the surfactant comprises sodium laureth sulfate, cocamidopropyl betaine and coconut oil diethanolamide, and the surfactant is prepared by matching various surfactants, wherein the mass ratio of the sodium laureth sulfate, the cocamidopropyl betaine and the coconut oil diethanolamide is 12-18: mixing at a ratio of 2-4: 4-8.

Further, the thickener is prepared by compounding sodium chloride and Versath ix, the Versath ix is a mixture prepared from Dazao, PEG-150 pentaerythritol tetrastearate and PPG-2 hydroxyethyl cocamide are commonly used in the industry, and the mass ratio of the sodium chloride to the Versath ix is 1: 1.

Compared with the prior art, the invention has the beneficial effects that:

1. the invention improves the matching combination of the rice washing water fermentation product and the traditional Chinese medicine, can effectively nurse, nourish and smooth the hair, and has the advantages of quick effect taking and the like.

Detailed Description

The present invention will be further described with reference to the following specific examples.

During preparation, the different components of the softening and nourishing shampoo are as follows: 30 parts of rice-washing water fermentation product, 0.05 part of licorice extract, 0.03 part of clove extract, 0.04 part of borneol, 0.3 part of phellodendron extract, 0.3 part of radix scutellariae extract, 0.8 part of tea bran extract, 0.4 part of Chinese soapberry extract, 1 part of polygonum multiflorum extract, 0.6 part of poria cocos extract, 0.6 part of semen cuscutae extract, 0.2 part of rabbit hair keratin, 3 parts of surfactant, 0.1 part of hydrogenated castor oil and 0.6 part of thickener. Wherein the surfactant is sodium laureth sulfate, cocamidopropyl betaine, and coconut oil diethanolamide 12: mixing at a ratio of 2: 4. The thickening agent is compounded by sodium chloride and Versath ix according to the mass ratio of 1: 1.

Or 40 parts of rice-washing water fermentation product, 0.08 part of liquorice extract, 0.05 part of clove extract, 0.06 part of borneol, 1.2 parts of phellodendron extract, 0.8 part of radix scutellariae extract, 1.2 parts of tea bran extract, 0.8 part of soapberry extract, 2 parts of polygonum multiflorum extract, 1.2 parts of poria cocos extract, 1.2 parts of semen cuscutae extract, 1.2 parts of rabbit hair keratin, 7 parts of surfactant, 0.3 part of hydrogenated castor oil and 1.5 parts of thickening agent. Wherein the surfactant is sodium laureth sulfate, cocamidopropyl betaine, and coconut oil diethanolamide 12: mixing at a ratio of 2: 4. The thickening agent is compounded by sodium chloride and Versath ix according to the mass ratio of 1: 1.

Or 35 parts of rice-washing water fermentation product, 0.07 part of liquorice extract, 0.04 part of clove extract, 0.05 part of borneol, 0.8 part of phellodendron extract, 0.6 part of radix scutellariae extract, 1 part of tea bran extract, 0.6 part of Chinese soapberry extract, 1.5 parts of polygonum multiflorum extract, 0.9 part of poria cocos extract, 1.0 part of semen cuscutae extract, 0.5 part of rabbit hair keratin, 5 parts of surfactant, 0.2 part of hydrogenated castor oil and 1.1 part of thickener. Wherein the surfactant is sodium laureth sulfate, cocamidopropyl betaine, coconut oil diethanolamide according to the proportion of 12: mixing at a ratio of 2: 4. The thickening agent is compounded by sodium chloride and Versath ix according to the mass ratio of 1: 1.

Or 40 parts of rice-washing water fermentation product, 0.07 part of licorice extract, 0.04 part of clove extract, 0.06 part of borneol, 1.2 parts of phellodendron extract, 0.6 part of radix scutellariae extract, 1.1 part of tea bran extract, 0.4 part of Chinese soapberry extract, 2 parts of polygonum multiflorum extract, 0.7 part of poria cocos extract, 0.6 part of semen cuscutae extract, 0.6 part of rabbit hair keratin, 6 parts of surfactant, 0.3 part of hydrogenated castor oil and 1.2 parts of thickener. Wherein the surfactant is sodium laureth sulfate, cocamidopropyl betaine, and coconut oil diethanolamide 12: mixing at a ratio of 2: 4. The thickening agent is compounded by sodium chloride and Versath ix according to the mass ratio of 1: 1.

Or 36 parts of rice-washing water fermentation product, 0.06 part of liquorice extract, 0.05 part of clove extract, 0.03 part of borneol, 0.5 part of phellodendron extract, 0.6 part of radix scutellariae extract, 0.9 part of tea bran extract, 0.6 part of Chinese soapberry extract, 1.2 parts of polygonum multiflorum extract, 0.8 part of poria cocos extract, 0.8 part of semen cuscutae extract, 0.4 part of rabbit hair keratin, 4.5 parts of surfactant, 0.2 part of hydrogenated castor oil and 1.3 parts of thickener. Wherein the surfactant is sodium laureth sulfate, cocamidopropyl betaine, and coconut oil diethanolamide 12: mixing at a ratio of 2: 4. The thickening agent is compounded by sodium chloride and Versath ix according to the mass ratio of 1: 1.

In the following preparation examples, the mixture of phellodendron extract, scutellaria extract and glycyrrhiza extract was prepared as follows: mixing cortex Phellodendri, Scutellariae radix and Glycyrrhrizae radix in 5 times of water according to the formula, soaking for 2h, inoculating 6% Aspergillus niger (purchased from the market directly) for fermentation at 28 + -0.5 deg.C under 180rpm for 40h, sterilizing, filtering to obtain fermentation liquid, and concentrating to 1.2 times of the herb mass to obtain extract mixed solution.

In the preparation example, rice accounting for 25% of the water solution is soaked at 20-22 ℃ by mass, stirred for 50min and filtered to obtain rice washing water, the rice washing water is autoclaved at 120 ℃ for more than 10min, then 4% of yeast strains are inoculated, the fermentation temperature is 28 +/-0.5 ℃, the rotation speed is kept at 220rpm, stirring and fermentation are carried out for 60h, and the rice washing water fermentation liquor is obtained after sterilization.

In the preparation example, the tea bran is added into a pot, the pressure is increased to 1.0MP by heating, the holding time is 10min, the tea bran is taken out and put into 3 times of water for leaching, the temperature is 50 ℃, the time is 20min, leaching liquor is obtained after filtration and separation, and the leaching liquor is concentrated to 0.6 time of the weight of the tea bran, namely the tea bran extract.

In the preparation example, the polygonum multiflorum is crushed into particles (screened by a 60-mesh sieve), then is mixed with distilled water to form a mixed solution with the concentration of 4 percent, namely a suspension, and is inoculated with rhizopus oryzae strains (the type commonly purchased from the market) after being sterilized under high pressure, the fermentation is carried out at the temperature of 25 ℃ and the rotating speed of 150rpm for 40 hours, and the polygonum multiflorum extract is obtained after the sterilization and filtration and is concentrated to the mass which is 1.2 times of the mass of the medicine.

In the preparation example, the dodder, the tuckahoe, the sapindus mukorossi and the clove are directly mixed according to the mass ratio shown in the formula by mass, 5 times of water is added for soaking for 4 hours, the mixture is decocted and concentrated to be about 2.5 times of the weight of the medicine, the filtration is carried out, and the filtrate is heated and concentrated to be 0.6 time of the weight of the medicine.

Rabbit hair keratin is purchased directly on the market, is prepared by an L-cysteine method, and has the parameters of 15.86 percent of nitrogen mass fraction and 99.3 percent of keratin content.

Hydrogenated castor oil, borneol, surfactant, thickener and the like are directly purchased from the market.

The surfactant is prepared from sodium laureth sulfate, cocamidopropyl betaine and coconut oil diethanolamide according to the proportion of 12: mixing at a ratio of 2: 4. The thickening agent is compounded by sodium chloride and Versath ix according to the mass ratio of 1: 1.

The shampoo was prepared as follows:

mixing the Chinese medicinal extract components at 40 + -1 deg.C in rice washing water fermentation broth, stirring for 20min, and mixing.

Sequentially adding surfactant, thickener, hydrogenated castor oil, etc. into the above Chinese medicinal mixed solution, stirring for 40min, and mixing to obtain shampoo.

The shampoo is prepared by the components and the preparation method, and the components of each specific example and comparative example are shown in the table 1:

TABLE 1

Performance tests were performed on shampoos prepared in the above examples and comparative examples

First, combing test, measuring the anti-tangling performance for hair with the maximum combing force, measuring the conditioning performance of hair by the total combing work, according to the current standard, wherein the wet combing test procedure: the hair was wetted, rubbed with about 2g of the prepared shampoo for 2-3min, rinsed with running water, combed once with a comb to remove excess water, wet combability was tested on a mini tensile tester at a tensile rate of 300mm/min for 6 tests per sample, the results are shown in table 2, with a blank (untreated) control.

Dry combing test: after the wet combing test was completed, the hair samples were dried in air and after drying, the dry combing property was measured as shown in table 2. A smaller value of dry and wet combing work indicates a better smoothness of the product on the hair.

TABLE 2

The reduction is compared with a blank group, and the shampoo with the formula has obvious increase on the combing performance.

Secondly, the shampoo prepared in the above examples and comparative examples performs common drug core cylindrical zone tests on staphylococcus aureus, escherichia coli, candida albicans and malassezia with bacteriostatic performance, and the average value (mm) of the diameters of the zone is shown in table 3.

TABLE 3

It can be seen that each example and comparative example have strong bacteriostatic performance.

Thirdly, clinical practice tests show that 5 groups of testees are selected, 5 men and 5 women in each group have the phenomena of much dandruff, alopecia and white hair, the degree difference is not more than 10%, the frequency of washing the shampoo once every two days is carried out, the shampoo is applied to the hair and the scalp for 5-10min every time, the shampoo is continuously used for 4 weeks, the phenomena are observed, and the using effect is judged: and (3) relieving: after the shampoo is used, dandruff is reduced, and hair loss and blackness are not obviously improved; obviously improve the following steps: scalp itch and alopecia are eliminated, new hairs grow at the serious alopecia part, and white hairs turn black;

invalid; as shown in table 4.

TABLE 4

In addition, the problems of itching, scurf and the like of the shampoos prepared in examples 1, 2 and 3 are relieved after the shampoos are used for 2 times on average, the hair is long in moisture retention time after the shampoos are used, and the shampoos are more flexible and do not have the feeling of drooping, and the data in table 4 shows that the shampoos in the formula have quick response and remarkable effect.

The above are only preferred embodiments of the present invention, and the scope of the present invention is not limited to the above examples, and all technical solutions that fall under the spirit of the present invention belong to the scope of the present invention. It should be noted that modifications and embellishments within the scope of the invention may occur to those skilled in the art without departing from the principle of the invention, and are considered to be within the scope of the invention.

Claims

1. The softening and nourishing shampoo is characterized by comprising the following components in parts by mass:

2. the softening and nourishing shampoo as defined in claim 1, wherein: mixing cortex Phellodendri, Scutellariae radix, and Glycyrrhrizae radix, and fermenting with Aspergillus niger to obtain fermentation liquid as mixture of Glycyrrhrizae radix extract, cortex Phellodendri extract, and Scutellariae radix extract.

3. The softening and nourishing shampoo as defined in claim 2, wherein: adding yeast strain 2-5 wt% into the rice washing water, fermenting at 25-32 deg.C for 50-70 hr, sterilizing, and filtering to obtain rice washing water fermented product.

4. The softening and nourishing shampoo as defined in claim 1, wherein: extracting the tea bran treated under pressure of 0.8-1.0MPa with water, filtering, separating to obtain extractive solution, and concentrating to 0.5-0.8 times of the weight of tea bran to obtain tea bran extract.

5. The softening and nourishing shampoo as defined in claim 1, wherein: inoculating 8-12% Rhizopus oryzae in the Polygoni Multiflori radix granule suspension, fermenting for 30-36 hr, sterilizing, and filtering to obtain Polygoni Multiflori radix extract.

6. The softening and nourishing shampoo as defined in claim 1, wherein: extracting semen Cuscutae, fructus Sapindi Mukouossi, flos Caryophylli and Poria with water to obtain extract.

7. The softening and nourishing shampoo as defined in claim 1, wherein: the surfactant comprises sodium laureth sulfate, cocamidopropyl betaine and coconut oil diethanolamide.

8. The softening and nourishing shampoo as defined in claim 1, wherein: the thickening agent is formed by compounding sodium chloride and Versathix.