CN114316678A - Cloth painting water color pen coating ink and preparation method thereof - Google Patents

Cloth painting water color pen coating ink and preparation method thereof Download PDF

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Publication number
CN114316678A
CN114316678A CN202210173706.2A CN202210173706A CN114316678A CN 114316678 A CN114316678 A CN 114316678A CN 202210173706 A CN202210173706 A CN 202210173706A CN 114316678 A CN114316678 A CN 114316678A
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CN
China
Prior art keywords
cloth
mixing
coating
coating ink
forming agent
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Pending
Application number
CN202210173706.2A
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Chinese (zh)
Inventor
张伟
张艳
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Yancheng Institute of Industry Technology
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Yancheng Institute of Industry Technology
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Application filed by Yancheng Institute of Industry Technology filed Critical Yancheng Institute of Industry Technology
Priority to CN202210173706.2A priority Critical patent/CN114316678A/en
Publication of CN114316678A publication Critical patent/CN114316678A/en
Pending legal-status Critical Current

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Abstract

The invention discloses a cloth painting water color pen coating ink, which comprises the following raw materials in percentage by weight, 5-25% of coating; 5% -15% of film-forming agent; 30% -60% of a solvent; 5% -20% of a dispersant; 2 to 10 percent of humectant. The invention integrally adopts more environment-friendly raw materials, is beneficial to controlling the process flow, is simpler, reduces the cost, has good water solubility, is beneficial to cleaning, and has the advantages of fast dispersion, good uniformity, difficult fading and good painting effect when being coated with the pigment on the cloth.

Description

Cloth painting water color pen coating ink and preparation method thereof
Technical Field
The invention relates to the technical field of ink paint, in particular to paint ink for a cloth painting water color pen and a preparation method thereof.
Background
The water color pen, a drawing instrument, colored water pen's advantage is that the color is abundant, bright-colored, and the shortcoming is that the time of using is shorter, and moisture is inhomogeneous, and the transition is unnatural, and two colours are well harmonious together, are fit for the drawing, and in present daily work and study, water color pen's use is also very common, can directly write the drawing through printing ink, has made things convenient for work and amusement life.
At present, most of coatings of existing water color pens are suitable for drawing on paper, and when the existing water color pens draw on cloth, the coatings are easy to disperse quickly, fade easily and have poor drawing effect.
Disclosure of Invention
The invention aims to provide a cloth painting water color pen coating ink and a preparation method thereof, and solves the problems that the existing water color pen coating is more suitable for drawing on paper, and painting on cloth is easy to cause fast dispersion of the coating, easy fading and poor painting effect.
In order to solve the above problems, the present invention provides the following technical solutions: the paint ink for cloth painting water color pen includes the following components in certain weight proportion,
5% -25% of coating;
5% -15% of film-forming agent;
30% -60% of a solvent;
5% -20% of a dispersant;
2 to 10 percent of humectant.
As a further preferable mode of the invention, the coating specifically comprises 2-4 parts of talcum powder, 4-7 parts of calcium carbonate, 3.5-6 parts of sulfonated oil, 3-8 parts of crude alkali oil and 0.3-1 part of pigment.
In a further preferred embodiment of the present invention, the humectant is a mixture of glycerin and ethylene glycol.
In a further preferred embodiment of the present invention, the film forming agent is a mixture of an acrylic resin modified casein film forming agent, an acrylic resin polyurethane copolymer resin, polyethylene, an acrylate modified butadiene resin, and a polyurethane modified nitrocellulose film forming agent.
In a further preferred embodiment of the present invention, the dispersant is a mixture of phosphate ester, polyethylene wax, ethylene-acrylic acid copolymer, and ethylene-vinyl acetate copolymer.
In a further preferred embodiment of the present invention, the solvent is selected from NaCl, KCl and KH2PO4Dissolved in deionized water and purified by mixing according to a 1:1.6: 0.8: 100, and the pH is controlled to be 7.1.
In a further preferred embodiment of the present invention, the manufacturing process comprises the following steps:
s1, preparing materials, namely weighing the raw materials according to the weight percentage;
s2, mixing the coating and the film-forming agent, adding half amount of solvent, and then carrying out oscillation mixing, wherein the temperature is controlled at 68-78 ℃;
s3, adding the dispersing agent into the steps, and then fully stirring and mixing, wherein the stirring and mixing temperature is controlled at 82-86 ℃ and lasts for 45 min;
s4, adding the rest of solvent and humectant into the above steps, stirring and mixing again, keeping the temperature at 65-75 deg.C for 60min, and standing;
and S5, sterilizing the finished solution by ultraviolet rays, then refrigerating, controlling the refrigerating temperature at 2-5 ℃ for 2 hours, and removing precipitates to finish the processing.
In a more preferred embodiment of the present invention, in step S3, the stirring rotation speed is controlled to 120r/min to 260 r/min.
Compared with the prior art, the invention has the following beneficial effects:
the invention integrally adopts more environment-friendly raw materials, is beneficial to controlling the process flow, is simpler, reduces the cost, has good water solubility, is beneficial to cleaning, and has the advantages of fast dispersion, good uniformity, difficult fading and good painting effect when being coated with the pigment on the cloth.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below in conjunction with the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The utility model provides a technical scheme: the paint ink for cloth painting water color pen includes the following components in certain weight proportion,
5% -25% of coating;
5% -15% of film-forming agent;
30% -60% of a solvent;
5% -20% of a dispersant;
2 to 10 percent of humectant.
The coating specifically comprises 2-4 parts of talcum powder, 4-7 parts of calcium carbonate, 3.5-6 parts of sulfonated oil, 3-8 parts of crude alkali oil and 0.3-1 part of pigment.
The humectant is a mixture of glycerol and glycol.
The film forming agent is a mixture of an acrylic resin modified casein film forming agent, acrylic resin polyurethane copolymer resin, polyethylene, acrylic ester modified butadiene resin and a polyurethane modified nitrocellulose film forming agent.
The dispersing agent is a mixture composed of phosphate ester, polyethylene wax, ethylene-acrylic acid copolymer and ethylene-vinyl acetate copolymer.
The solvent is selected from NaCl, KCl and KH2PO4Dissolved in deionized water and purified by mixing according to a 1:1.6: 0.8: 100, and the pH is controlled to be 7.1.
The manufacturing process comprises the following steps:
s1, preparing materials, namely weighing the raw materials according to the weight percentage;
s2, mixing the coating and the film-forming agent, adding half amount of solvent, and then carrying out oscillation mixing, wherein the temperature is controlled at 68-78 ℃;
s3, adding the dispersing agent into the steps, and then fully stirring and mixing, wherein the stirring and mixing temperature is controlled at 82-86 ℃ and lasts for 45 min;
s4, adding the rest of solvent and humectant into the above steps, stirring and mixing again, keeping the temperature at 65-75 deg.C for 60min, and standing;
and S5, sterilizing the finished solution by ultraviolet rays, then refrigerating, controlling the refrigerating temperature at 2-5 ℃ for 2 hours, and removing precipitates to finish the processing.
In step S3, the stirring speed is controlled to be 120r/min-260 r/min.
The pigment includes white, yellow, red, blue, green, brown, purple, and black.
Example 1
5% of coating;
5% of film forming agent;
60% of a solvent;
20% of a dispersant;
10% of humectant.
Mixing the coating and the film forming agent, adding half amount of solvent, then carrying out oscillation mixing, controlling the temperature at 68 ℃, adding the dispersing agent into the steps, then carrying out full stirring and mixing, controlling the stirring and mixing temperature at 82 ℃ for 45min, adding the rest of solvent and humectant into the steps, carrying out stirring and mixing again, keeping the temperature at 65 ℃ for 60min, then standing, carrying out ultraviolet sterilization and disinfection on the finished solution, then carrying out refrigeration treatment, controlling the refrigeration temperature at 2 ℃ for 2h, and removing precipitates, thus finishing the processing.
Example 2
25% of coating;
15% of a film forming agent;
30% of a solvent;
20% of a dispersant;
10% of humectant.
Mixing the coating and the film forming agent, adding half amount of solvent, then carrying out oscillation mixing, controlling the temperature at 78 ℃, adding the dispersing agent into the steps, then carrying out full stirring and mixing, controlling the stirring and mixing temperature at 86 ℃ for 45min, adding the rest of solvent and humectant into the steps, stirring and mixing again, keeping the temperature at 75 ℃ for 60min, then standing, carrying out ultraviolet sterilization and disinfection on the finished solution, then carrying out refrigeration treatment, controlling the refrigeration temperature at 5 ℃ for 2h, and removing precipitates, thus finishing the processing.
Example 3
20% of coating;
13% of a film forming agent;
60% of a solvent;
5% of a dispersant;
2 percent of humectant.
Mixing the coating and the film forming agent, adding half amount of solvent, then carrying out oscillation mixing, controlling the temperature at 70 ℃, adding the dispersing agent into the steps, then carrying out full stirring and mixing, controlling the stirring and mixing temperature at 83 ℃ for 45min, adding the rest of solvent and humectant into the steps, stirring and mixing again, keeping the temperature at 70 ℃ for 60min, then standing, carrying out ultraviolet sterilization and disinfection on the finished solution, then carrying out refrigeration treatment, controlling the refrigeration temperature at 4 ℃ for 2h, and removing precipitates, thus finishing the processing.
Example 4
15% of coating;
10% of film forming agent;
55% of a solvent;
20% of a dispersant;
10% of humectant.
Mixing the coating and the film forming agent, adding half amount of solvent, then carrying out oscillation mixing, controlling the temperature at 70 ℃, adding the dispersing agent into the steps, then carrying out full stirring and mixing, controlling the stirring and mixing temperature at 83 ℃ for 45min, adding the rest of solvent and humectant into the steps, stirring and mixing again, keeping the temperature at 70 ℃ for 60min, then standing, carrying out ultraviolet sterilization and disinfection on the finished solution, then carrying out refrigeration treatment, controlling the refrigeration temperature at 4 ℃ for 2h, and removing precipitates, thus finishing the processing.
Example 5
20% of coating;
15% of a film forming agent;
45% of a solvent;
10% of a dispersant;
10% of humectant.
Mixing the coating and the film forming agent, adding half amount of solvent, then carrying out oscillation mixing, controlling the temperature at 70 ℃, adding the dispersing agent into the steps, then carrying out full stirring and mixing, controlling the stirring and mixing temperature at 83 ℃ for 45min, adding the rest of solvent and humectant into the steps, stirring and mixing again, keeping the temperature at 70 ℃ for 60min, then standing, carrying out ultraviolet sterilization and disinfection on the finished solution, then carrying out refrigeration treatment, controlling the refrigeration temperature at 4 ℃ for 2h, and removing precipitates, thus finishing the processing.
In conclusion, the invention integrally adopts more environment-friendly raw materials, is beneficial to controlling the process flow, is simpler, reduces the cost, has good water solubility, is beneficial to cleaning, and has the advantages of quicker dispersion of the pigment coated on the cloth, good uniformity, difficult fading and good painting effect.
While there have been shown and described what are at present considered the fundamental principles and essential features of the invention and its advantages, it will be apparent to those skilled in the art that the invention is not limited to the details of the foregoing exemplary embodiments, but is capable of other specific forms without departing from the spirit or essential characteristics thereof. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein.
Furthermore, it should be understood that although the present description refers to embodiments, not every embodiment may contain only a single embodiment, and such description is for clarity only, and those skilled in the art should integrate the description, and the embodiments may be combined as appropriate to form other embodiments understood by those skilled in the art.

Claims (8)

1. The cloth painting water color pen coating ink is characterized in that: the specific raw material proportion comprises the following components,
5% -25% of coating;
5% -15% of film-forming agent;
30% -60% of a solvent;
5% -20% of a dispersant;
2 to 10 percent of humectant.
2. The cloth-painting water color pen coating ink as claimed in claim 1, wherein the coating specifically comprises 2-4 parts of talcum powder, 4-7 parts of calcium carbonate, 3.5-6 parts of sulfonated oil, 3-8 parts of crude alkali oil and 0.3-1 part of pigment.
3. The cloth-drawing watercolor pen coating ink according to claim 1, wherein the humectant is a mixture of glycerin and ethylene glycol.
4. The cloth-drawing watercolor pen coating ink according to claim 1, wherein the film-forming agent is a mixture of an acrylic resin modified casein film-forming agent, an acrylic resin polyurethane copolymer resin, polyethylene, an acrylate modified butadiene resin, and a polyurethane modified nitrocellulose film-forming agent.
5. The cloth-painting watercolor pen coating ink according to claim 4, wherein the dispersant is a mixture of phosphate ester, polyethylene wax, ethylene-acrylic acid copolymer and ethylene-vinyl acetate copolymer.
6. The cloth-drawing watercolor pen coating ink according to claim 1, wherein the solvent is selected from NaCl, KCl and KH2PO4Dissolved in deionized water and purified by mixing according to a 1:1.6: 0.8: 100, and the pH is controlled to be 7.1.
7. The preparation method of the coating ink for the cloth-painted water color pen according to claim 1, wherein the preparation process comprises the following steps:
s1, preparing materials, namely weighing the raw materials according to the weight percentage;
s2, mixing the coating and the film-forming agent, adding half amount of solvent, and then carrying out oscillation mixing, wherein the temperature is controlled at 68-78 ℃;
s3, adding the dispersing agent into the steps, and then fully stirring and mixing, wherein the stirring and mixing temperature is controlled at 82-86 ℃ and lasts for 45 min;
s4, adding the rest of solvent and humectant into the above steps, stirring and mixing again, keeping the temperature at 65-75 ℃, keeping for 60min, and then standing;
and S5, sterilizing the finished solution by ultraviolet rays, then refrigerating, controlling the refrigerating temperature at 2-5 ℃ for 2 hours, and removing precipitates to finish the processing.
8. The method for preparing coating ink for a cloth-painted water color pen according to claim 7, wherein in step S3, the stirring rotation speed is controlled to 120r/min-260 r/min.
CN202210173706.2A 2022-02-24 2022-02-24 Cloth painting water color pen coating ink and preparation method thereof Pending CN114316678A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202210173706.2A CN114316678A (en) 2022-02-24 2022-02-24 Cloth painting water color pen coating ink and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202210173706.2A CN114316678A (en) 2022-02-24 2022-02-24 Cloth painting water color pen coating ink and preparation method thereof

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Publication Number Publication Date
CN114316678A true CN114316678A (en) 2022-04-12

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Citations (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1105373A (en) * 1994-01-13 1995-07-19 广州增城荔城佳彩文化用品二厂 Method for making semi-dry watercolour
CN103059644A (en) * 2013-01-09 2013-04-24 宁波新安涂料有限公司 Water-based painting brush and preparation method of water-based painting brush
CN103130448A (en) * 2011-11-30 2013-06-05 李建国 Efficient and environment-friendly emulsion paint
CN103319955A (en) * 2013-05-24 2013-09-25 贝碧欧美术颜料(昆山)有限公司 High cover up low viscosity textile hand drawing mark pen ink, preparation method and application thereof
CN104497737A (en) * 2014-12-15 2015-04-08 广东梅雁吉祥水电股份有限公司 Multifunctional anti-bacteria coating composition and preparation method thereof
CN104962116A (en) * 2015-05-29 2015-10-07 广东华兹卜化学工业有限公司 Environmentally friendly aqueous nanometer inorganic coating material and preparation method thereof
CN107699048A (en) * 2017-10-30 2018-02-16 华蓥市红军小学 A kind of preparation method for easily wiping teaching ink
CN109181434A (en) * 2018-09-25 2019-01-11 临沂大学 A kind of environment-friendly type coating and preparation method thereof
CN109732866A (en) * 2018-12-28 2019-05-10 太仓意欣智能科技有限公司 Multi-injection molding process one-step molding method for high-toughness household appliance panel
CN110776774A (en) * 2019-10-16 2020-02-11 江苏科技大学 Water-based ink composition containing ultraviolet-resistant pigment and preparation method and application thereof
CN111320888A (en) * 2020-03-25 2020-06-23 广东长鑫环保科技有限公司 Method for preparing anion paint with virus and bacteria removing function
CN112280381A (en) * 2020-11-17 2021-01-29 闫西安 Neutral erasable ink composition and preparation method thereof
CN112480744A (en) * 2020-12-25 2021-03-12 青岛点石文具用品有限公司 Water-based ink composition
CN113292644A (en) * 2021-05-19 2021-08-24 南京艾拓生命科技有限公司 Cytokine activity stabilizer and preparation method thereof

Patent Citations (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1105373A (en) * 1994-01-13 1995-07-19 广州增城荔城佳彩文化用品二厂 Method for making semi-dry watercolour
CN103130448A (en) * 2011-11-30 2013-06-05 李建国 Efficient and environment-friendly emulsion paint
CN103059644A (en) * 2013-01-09 2013-04-24 宁波新安涂料有限公司 Water-based painting brush and preparation method of water-based painting brush
CN103319955A (en) * 2013-05-24 2013-09-25 贝碧欧美术颜料(昆山)有限公司 High cover up low viscosity textile hand drawing mark pen ink, preparation method and application thereof
CN104497737A (en) * 2014-12-15 2015-04-08 广东梅雁吉祥水电股份有限公司 Multifunctional anti-bacteria coating composition and preparation method thereof
CN104962116A (en) * 2015-05-29 2015-10-07 广东华兹卜化学工业有限公司 Environmentally friendly aqueous nanometer inorganic coating material and preparation method thereof
CN107699048A (en) * 2017-10-30 2018-02-16 华蓥市红军小学 A kind of preparation method for easily wiping teaching ink
CN109181434A (en) * 2018-09-25 2019-01-11 临沂大学 A kind of environment-friendly type coating and preparation method thereof
CN109732866A (en) * 2018-12-28 2019-05-10 太仓意欣智能科技有限公司 Multi-injection molding process one-step molding method for high-toughness household appliance panel
CN110776774A (en) * 2019-10-16 2020-02-11 江苏科技大学 Water-based ink composition containing ultraviolet-resistant pigment and preparation method and application thereof
CN111320888A (en) * 2020-03-25 2020-06-23 广东长鑫环保科技有限公司 Method for preparing anion paint with virus and bacteria removing function
CN112280381A (en) * 2020-11-17 2021-01-29 闫西安 Neutral erasable ink composition and preparation method thereof
CN112480744A (en) * 2020-12-25 2021-03-12 青岛点石文具用品有限公司 Water-based ink composition
CN113292644A (en) * 2021-05-19 2021-08-24 南京艾拓生命科技有限公司 Cytokine activity stabilizer and preparation method thereof

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Application publication date: 20220412