CN114271532A - Solid electronic cigarette oil containing tamarind seed polysaccharide and preparation method thereof - Google Patents
Solid electronic cigarette oil containing tamarind seed polysaccharide and preparation method thereof Download PDFInfo
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- CN114271532A CN114271532A CN202210015512.XA CN202210015512A CN114271532A CN 114271532 A CN114271532 A CN 114271532A CN 202210015512 A CN202210015512 A CN 202210015512A CN 114271532 A CN114271532 A CN 114271532A
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- tamarind seed
- seed polysaccharide
- electronic cigarette
- tobacco tar
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- 229920001282 polysaccharide Polymers 0.000 title claims abstract description 69
- 239000005017 polysaccharide Substances 0.000 title claims abstract description 69
- 235000004298 Tamarindus indica Nutrition 0.000 title claims abstract description 63
- 150000004676 glycans Chemical class 0.000 title claims abstract description 53
- 239000007787 solid Substances 0.000 title claims abstract description 44
- 239000003571 electronic cigarette Substances 0.000 title claims abstract description 37
- 238000002360 preparation method Methods 0.000 title abstract description 13
- 240000004584 Tamarindus indica Species 0.000 title 1
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 62
- 241000596504 Tamarindus Species 0.000 claims abstract description 62
- 239000007788 liquid Substances 0.000 claims abstract description 28
- -1 polysaccharide compound Chemical class 0.000 claims abstract description 17
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 16
- 238000010438 heat treatment Methods 0.000 claims abstract description 12
- 229920002558 Curdlan Polymers 0.000 claims abstract description 7
- 239000001879 Curdlan Substances 0.000 claims abstract description 7
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 claims abstract description 7
- 229940078035 curdlan Drugs 0.000 claims abstract description 7
- 235000019316 curdlan Nutrition 0.000 claims abstract description 7
- 235000013599 spices Nutrition 0.000 claims abstract description 7
- 229920001817 Agar Polymers 0.000 claims abstract description 6
- 239000008272 agar Substances 0.000 claims abstract description 6
- 239000000779 smoke Substances 0.000 claims abstract description 6
- 241000208125 Nicotiana Species 0.000 claims description 61
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 57
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 42
- 239000000499 gel Substances 0.000 claims description 24
- 238000002156 mixing Methods 0.000 claims description 22
- 239000000203 mixture Substances 0.000 claims description 15
- 230000018044 dehydration Effects 0.000 claims description 10
- 238000006297 dehydration reaction Methods 0.000 claims description 10
- CDQSJQSWAWPGKG-UHFFFAOYSA-N butane-1,1-diol Chemical compound CCCC(O)O CDQSJQSWAWPGKG-UHFFFAOYSA-N 0.000 claims description 9
- 238000005266 casting Methods 0.000 claims description 9
- 238000000465 moulding Methods 0.000 claims description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 9
- 239000011259 mixed solution Substances 0.000 claims description 8
- ZIBGPFATKBEMQZ-UHFFFAOYSA-N triethylene glycol Chemical compound OCCOCCOCCO ZIBGPFATKBEMQZ-UHFFFAOYSA-N 0.000 claims description 8
- 235000019640 taste Nutrition 0.000 claims description 6
- 239000000796 flavoring agent Substances 0.000 claims description 3
- 235000019634 flavors Nutrition 0.000 claims description 3
- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 claims description 2
- 238000000034 method Methods 0.000 claims 2
- 239000003995 emulsifying agent Substances 0.000 abstract description 3
- 230000000391 smoking effect Effects 0.000 abstract description 3
- 241000196324 Embryophyta Species 0.000 abstract description 2
- 235000019504 cigarettes Nutrition 0.000 abstract description 2
- 239000002994 raw material Substances 0.000 abstract description 2
- 230000001953 sensory effect Effects 0.000 abstract description 2
- 239000000126 substance Substances 0.000 abstract description 2
- 244000061176 Nicotiana tabacum Species 0.000 abstract 1
- 239000000686 essence Substances 0.000 description 17
- 235000006679 Mentha X verticillata Nutrition 0.000 description 5
- 235000002899 Mentha suaveolens Nutrition 0.000 description 5
- 235000001636 Mentha x rotundifolia Nutrition 0.000 description 5
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 5
- 241000723353 Chrysanthemum Species 0.000 description 4
- 235000007516 Chrysanthemum Nutrition 0.000 description 4
- 240000004307 Citrus medica Species 0.000 description 3
- 229920005862 polyol Polymers 0.000 description 3
- 150000003077 polyols Chemical class 0.000 description 3
- 229920000858 Cyclodextrin Polymers 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000003205 fragrance Substances 0.000 description 2
- HFHDHCJBZVLPGP-UHFFFAOYSA-N schardinger α-dextrin Chemical compound O1C(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(O)C2O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC2C(O)C(O)C1OC2CO HFHDHCJBZVLPGP-UHFFFAOYSA-N 0.000 description 2
- 235000005979 Citrus limon Nutrition 0.000 description 1
- 244000131522 Citrus pyriformis Species 0.000 description 1
- 244000166675 Cymbopogon nardus Species 0.000 description 1
- 235000018791 Cymbopogon nardus Nutrition 0.000 description 1
- XINCECQTMHSORG-UHFFFAOYSA-N Isoamyl isovalerate Chemical compound CC(C)CCOC(=O)CC(C)C XINCECQTMHSORG-UHFFFAOYSA-N 0.000 description 1
- 244000061322 Nicotiana alata Species 0.000 description 1
- 241000220317 Rosa Species 0.000 description 1
- 229930003427 Vitamin E Natural products 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 239000000443 aerosol Substances 0.000 description 1
- 238000000889 atomisation Methods 0.000 description 1
- 230000000903 blocking effect Effects 0.000 description 1
- GVJHHUAWPYXKBD-UHFFFAOYSA-N d-alpha-tocopherol Natural products OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 description 1
- 238000000265 homogenisation Methods 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 230000008520 organization Effects 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 235000019505 tobacco product Nutrition 0.000 description 1
- 229940046009 vitamin E Drugs 0.000 description 1
- 235000019165 vitamin E Nutrition 0.000 description 1
- 239000011709 vitamin E Substances 0.000 description 1
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- Manufacture Of Tobacco Products (AREA)
Abstract
A solid electronic cigarette oil containing tamarind seed polysaccharide and a preparation method thereof are disclosed, wherein the solid electronic cigarette oil comprises the following components in parts by mass: 85-98 parts of smoke agent, 1-10 parts of curing agent and 1-14 parts of essence and spice; the curing agent is tamarind seed polysaccharide or tamarind seed polysaccharide compound gum; the tamarind seed polysaccharide compound gum comprises the following components in parts by mass: 55-90 parts of tamarind seed polysaccharide, 10-15 parts of curdlan, 0-10 parts of agar and 0-20 parts of algal polysaccharide. The tamarind seed polysaccharide or tamarind seed polysaccharide compound gum prepared from natural plant raw materials is used as a curing agent, the curing efficiency of the curing agent on tobacco tar is 93-98%, no residue is reserved after heating, and the smoking sensory quality is not affected. The solid electronic cigarette oil does not contain emulsifier and other chemical components which can cause harm to human bodies, is safe and reliable, and effectively solves the technical problem that the cigarette liquid is easy to leak.
Description
Technical Field
The invention relates to the technical field of electronic cigarette oil, in particular to solid electronic cigarette oil containing tamarind seed polysaccharide and application thereof in electronic cigarettes.
Background
Since the tobacco control framework convention promoted by the world health organization became effective, the control of the tobacco industry is continuously strengthened by various countries. With the increasing severity of the global smoking control environment and the growing concern of consumers on health, the research and development of novel tobacco products such as electronic cigarettes for reducing the release amount of harmful components in tobacco gradually become the key development point of the tobacco industry of all countries in the world.
Currently, most of commercially available electronic cigarettes use tobacco juice with good fluidity, but the tobacco juice easily leaks from the atomizer base, the joint between the oil bin and the base, the suction nozzle and other parts. Although people carry out the continuous improvement to the structure of atomizer, developed closed atomizer, adopted the formula design of blocking of air current passageway and tobacco juice passageway, also only solved the weeping problem of product transportation better, once the product is used, air current passageway and tobacco juice passageway will remain the intercommunication throughout, in the later stage use, the weeping condition still inevitably can appear. Meanwhile, vitamin E ester is widely used as an emulsifier in the electronic cigarette oil, and aims to solve the problem of homogenization of the electronic cigarette oil, fat-soluble and alcohol-soluble essence and spice and a smoke agent.
At present, some solid-state-like electronic tobacco tar products for adsorbing tobacco tar in the market utilize the porous structure of cyclodextrin to adsorb the tobacco tar in the pores of the cyclodextrin, but the adsorption rate is only 60% -80%, and residues are left after heating, so the consumption experience of consumers is not ideal.
Disclosure of Invention
The invention aims to solve the problem that the liquid leakage is easily caused by using the cigarette liquid of the existing electronic cigarette and the adverse effect of the electronic cigarette liquid on the human health, and provides solid electronic cigarette oil containing tamarind seed polysaccharide which is in a solid state at normal temperature and is converted from a solid state into a liquid state after being heated to a certain temperature and a preparation method thereof.
The technical scheme adopted by the invention is as follows:
a solid electronic cigarette oil containing tamarind seed polysaccharide comprises the following components in parts by mass: 85-98 parts of smoke agent, 1-10 parts of curing agent and 1-14 parts of essence and spice; the curing agent is tamarind seed polysaccharide or tamarind seed polysaccharide compound gum; the tamarind seed polysaccharide compound gum comprises the following components in parts by mass: 55-90 parts of tamarind seed polysaccharide, 10-15 parts of curdlan, 0-10 parts of agar and 0-20 parts of algal polysaccharide; the smoke agent is a mixture prepared by mixing more than one of glycerol, propylene glycol, butanediol and triethylene glycol.
The preparation method of the solid electronic cigarette oil comprises the following steps:
a. preparing a basic gel liquid: mixing glycerol and any one or two of propylene glycol, butanediol and triethylene glycol uniformly to form base tobacco tar, adding tamarind seed polysaccharide or tamarind seed polysaccharide complex gum to form a mixed solution, finally adding hot water of 80-100 ℃ to prepare into 3-5% of mass concentration, and continuously heating under the condition of keeping 80-100 ℃ to form base gel liquid;
b. preparing tobacco tar: adding different flavors of essence and spice into the basic gel liquid according to different taste requirements, and mixing and homogenizing at 60 +/-3 ℃, 2000-3000r/min and 10-50MPa to form tobacco tar with different tastes;
c. and (3) casting molding: and (3) pouring the homogenized tobacco tar into a mold, and carrying out vacuum freeze dehydration at-20 ℃ under the condition of 10bar to obtain the solid electronic tobacco tar.
Further, the base gel liquid prepared in the step a is a mixture prepared by mixing glycerol and more than one of propylene glycol, butanediol and triethylene glycol according to a mass ratio of 1: 4-5: 5.
According to the invention, the hydroxyl groups of the tamarind seed polysaccharide, the branch chains and the polyol are combined, and the polyol is solidified into gel without fluidity after dehydration to form the solid electronic cigarette oil. When the solid tobacco tar is used by consumers, the solid tobacco tar is filled into an atomizer, and the solid tobacco tar is heated by the atomizer to a temperature of over 120 ℃ and is converted into liquid to promote the polyol to form aerosol, so that the effect of tobacco tar atomization is achieved. The tamarind seed polysaccharide or tamarind seed polysaccharide compound gum prepared from natural plant raw materials is used as a curing agent, the curing efficiency of the curing agent on tobacco tar is 93-98%, no residue is reserved after heating, and the smoking sensory quality is not affected. The solid electronic cigarette oil does not contain emulsifier and other chemical components which can cause harm to human bodies, and is safe and reliable. The solid electronic tobacco tar effectively solves the technical problem that tobacco juice is easy to leak.
The solid electronic cigarette oil with various tastes can be prepared by adding the essences and spices with different tastes, so that the diversified demands of consumers are met.
The preparation method is simple and efficient, and is easy to realize industrialization.
Detailed Description
The present invention will be further illustrated with reference to the following examples.
Example 1
A solid electronic cigarette oil containing tamarind seed polysaccharide comprises the following components in parts by mass: 70 parts of glycerol, 20 parts of propylene glycol, 5 parts of tamarind seed polysaccharide and 5 parts of chrysanthemum essence.
The preparation method of the solid electronic cigarette oil comprises the following steps:
a. mixing glycerol and propylene glycol uniformly according to the mass ratio of 1:4 to form base tobacco tar, adding tamarind seed polysaccharide to form a mixed solution, adding 80 ℃ hot water to prepare a mixture with the mass concentration of 3%, continuously heating the mixture under the condition of keeping the temperature of 80 ℃, and completely dissolving the tamarind seed polysaccharide to form a base gel solution;
b, adding chrysanthemum essence into the basic gel liquid, and mixing and homogenizing the chrysanthemum essence and the basic gel liquid by using a high-pressure homogenizer at the conditions of 60 ℃, 2000r/min and 30MPa to form tobacco tar containing chrysanthemum fragrance;
c. and (3) casting molding: and (3) pouring the homogenized tobacco tar into a mold, and carrying out vacuum freeze dehydration at-20 ℃ under the condition of 10bar to obtain the solid electronic tobacco tar.
Example 2
A solid electronic cigarette oil containing tamarind seed polysaccharide comprises the following components in parts by mass: 89 parts of glycerol, 10 parts of tamarind seed polysaccharide and 1 part of tobacco extract.
The preparation method of the solid electronic cigarette oil comprises the following steps:
a. mixing glycerol and butanediol according to the proportion of 1:5 to form base tobacco tar, adding tamarind seed polysaccharide to form a mixed solution, adding 90 ℃ hot water to prepare a mixture with the mass concentration of 5%, continuously heating the mixture under the condition of keeping the temperature of 90 ℃, and completely dissolving the tamarind seed polysaccharide to form base gel liquid;
b, adding the tobacco extract into the basic gel liquid, and mixing and homogenizing by a homogenizer at 57 ℃, 2500r/min and 50MPa to form tobacco tar with tobacco fragrance;
c. and (3) casting molding: and (3) pouring the homogenized tobacco tar into a mold, and carrying out vacuum freeze dehydration at-20 ℃ under the condition of 10bar to obtain the solid electronic tobacco tar.
Example 3
A solid electronic cigarette oil containing tamarind seed polysaccharide comprises the following components in parts by mass: 80 parts of glycerol, 18 parts of butanediol, 1 part of tamarind seed polysaccharide, 0.5 part of lemon essence and 0.5 part of citronella essence.
The preparation method of the solid electronic cigarette oil comprises the following steps:
a. mixing glycerol and butanediol according to the proportion of 1: 2 to form base tobacco tar, adding tamarind seed polysaccharide to form a mixed solution, adding hot water at 95 ℃ to prepare a mixture with a mass concentration of 4%, continuously heating the mixture under the condition of keeping the temperature at 95 ℃, and completely dissolving the tamarind seed polysaccharide to form base gel liquid;
b, adding the tobacco extract into the basic gel liquid, and mixing and homogenizing by a homogenizer at 63 ℃, 3000r/min and 10MPa to form lemon-flavored tobacco tar;
c. and (3) casting molding: and (3) pouring the homogenized tobacco tar into a mold, and carrying out vacuum freeze dehydration at-20 ℃ under the condition of 10bar to obtain the solid electronic tobacco tar.
Example 4
A solid electronic cigarette oil containing tamarind seed polysaccharide comprises the following components in parts by mass: 60 parts of propylene glycol, 15 parts of glycerol, 10 parts of triethylene glycol, 8 parts of tamarind seed polysaccharide compound gum and 7 parts of mint essence. The tamarind seed polysaccharide compound gum is prepared from 55 parts of tamarind seed polysaccharide, 15 parts of curdlan, 10 parts of agar and 20 parts of algal polysaccharide.
The preparation method of the solid electronic cigarette oil comprises the following steps:
a. mixing glycerol: (propylene glycol + butylene glycol) as 1:0.25 mass ratio to form base tobacco tar, adding tamarind seed polysaccharide complex gum to form a mixed solution, adding 85 ℃ hot water to prepare 4% mass concentration, and continuously heating under the condition of keeping 85 ℃ to form base gel liquid;
b, adding the mint essence into the basic gel liquid, and mixing and homogenizing by using a homogenizer at the temperature of 61 ℃, 2500r/min and under the pressure of 20MPa to form mint-flavored tobacco tar;
c. and (3) casting molding: and (3) pouring the homogenized tobacco tar into a mold, and carrying out vacuum freeze dehydration at-20 ℃ under the condition of 10bar to obtain the solid electronic tobacco tar.
Example 5
A solid electronic cigarette oil containing tamarind seed polysaccharide comprises the following components in parts by mass: 90 parts of glycerol, 8 parts of tamarind seed polysaccharide compound gum, 0.5 part of rose essence and 1.5 parts of apple essence. The tamarind seed polysaccharide compound gum is prepared from 70 parts of tamarind seed polysaccharide, 10 parts of curdlan, 10 parts of agar and 10 parts of algal polysaccharide.
The preparation method of the solid electronic cigarette oil comprises the following steps:
a. mixing glycerol: (butanediol + triethylene glycol) as 1: 1 to form base tobacco tar, adding tamarind seed polysaccharide complex gum to form a mixed solution, adding 100 ℃ hot water to prepare a mixture with the mass concentration of 5%, and continuously heating the mixture under the condition that the temperature is not lower than 80 ℃ to form base gel liquid;
b, adding the mint essence into the basic gel liquid, and mixing and homogenizing the mixture by using a homogenizer at the temperature of 62 ℃, 3000r/min and 50MPa to form fragrant and sweet tobacco tar;
c. and (3) casting molding: and (3) pouring the homogenized tobacco tar into a mold, and carrying out vacuum freeze dehydration at-20 ℃ under the condition of 10bar to obtain the solid electronic tobacco tar.
Example 6
A solid electronic cigarette oil containing tamarind seed polysaccharide comprises the following components in parts by mass: 85 parts of propylene glycol, 1 part of tamarind seed polysaccharide compound gum, 3 parts of tobacco extract and 11 parts of mint essence. The tamarind seed polysaccharide compound gum is prepared from 90 parts of tamarind seed polysaccharide and 10 parts of curdlan.
The preparation method of the solid electronic cigarette oil comprises the following steps:
a. mixing glycerol and propylene glycol uniformly according to the mass ratio of 1:3 to form base tobacco tar, adding tamarind seed polysaccharide complex gum to form mixed liquor, adding hot water at 80 ℃ to prepare 3% of mass concentration, and continuously heating under the condition of keeping 80 ℃ to form base gel liquid;
b, adding the tobacco extract and the mint essence into the basic gel liquid, and mixing and homogenizing by a homogenizer at 58 ℃, 3000r/min and 50MPa to form mixed tobacco tar;
c. and (3) casting molding: and (3) pouring the homogenized mixed tobacco tar into a mold, and carrying out vacuum freeze dehydration at-20 ℃ under the condition of 10bar to obtain the solid electronic tobacco tar.
Example 7
A solid electronic cigarette oil containing tamarind seed polysaccharide comprises the following components in parts by mass: 80 parts of propylene glycol, 10 parts of glycerol, 5 parts of tamarind seed polysaccharide compound gum and 5 parts of citron essence. The tamarind seed polysaccharide compound gum is prepared from 75 parts of tamarind seed polysaccharide, 10 parts of curdlan, 5 parts of agar and 10 parts of algal polysaccharide.
The preparation method of the solid electronic cigarette oil comprises the following steps:
a. mixing glycerol and propylene glycol uniformly according to the mass ratio of 1:0.5 to form base tobacco tar, adding tamarind seed polysaccharide complex gum to form a mixed solution, adding 100 ℃ hot water to prepare a mixture with the mass concentration of 4%, and continuously heating the mixture under the condition of keeping the temperature of 100 ℃ to form base gel liquid;
b, adding citron essence into the basic gel liquid, and mixing and homogenizing by a homogenizer at 63 ℃, 2500r/min and 20MPa to form citron flavor tobacco tar;
c. and (3) casting molding: and (3) pouring the homogenized tobacco tar into a mold, and carrying out vacuum freeze dehydration at-20 ℃ under the condition of 10bar to obtain the solid electronic tobacco tar.
The tamarind polysaccharide described in the above examples was prepared by the prior art and is also commercially available.
Claims (3)
1. The solid electronic cigarette oil containing tamarind seed polysaccharide is characterized by comprising the following components in parts by mass: 85-98 parts of smoke agent, 1-10 parts of curing agent and 1-14 parts of essence and spice; the curing agent is tamarind seed polysaccharide or tamarind seed polysaccharide compound gum; the tamarind seed polysaccharide compound gum comprises the following components in parts by mass: 55-90 parts of tamarind seed polysaccharide, 10-15 parts of curdlan, 0-10 parts of agar and 0-20 parts of algal polysaccharide; the smoke agent is a mixture prepared by mixing more than one of glycerol, propylene glycol, butanediol and triethylene glycol.
2. The method for preparing a solid electronic cigarette oil containing tamarind seed polysaccharide according to claim 1, comprising the steps of:
a. preparing a basic gel liquid: mixing glycerol and any one or two of propylene glycol, butanediol and triethylene glycol uniformly to form base tobacco tar, adding tamarind seed polysaccharide or tamarind seed polysaccharide complex gum to form a mixed solution, finally adding hot water of 80-100 ℃ to prepare into 3-5% of mass concentration, and continuously heating under the condition of keeping 80-100 ℃ to form base gel liquid;
b. preparing tobacco tar: adding different flavors of essence and spice into the basic gel liquid according to different taste requirements, and mixing and homogenizing at 60 +/-3 ℃, 2000-3000r/min and 10-50MPa to form tobacco tar with different tastes;
c. and (3) casting molding: and (3) pouring the homogenized tobacco tar into a mold, and carrying out vacuum freeze dehydration at-20 ℃ under the condition of 10bar to obtain the solid electronic tobacco tar.
3. The method for preparing a solid electronic cigarette oil containing tamarind seed polysaccharide according to claim 2, wherein the base gel liquid prepared in step a is a mixture prepared by mixing glycerol and at least one of propylene glycol, butylene glycol and triethylene glycol in a mass ratio of 1: 0.25-1: 5.
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CN202210015512.XA CN114271532A (en) | 2022-01-07 | 2022-01-07 | Solid electronic cigarette oil containing tamarind seed polysaccharide and preparation method thereof |
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CN202210015512.XA CN114271532A (en) | 2022-01-07 | 2022-01-07 | Solid electronic cigarette oil containing tamarind seed polysaccharide and preparation method thereof |
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Citations (5)
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CN1933744A (en) * | 2004-02-19 | 2007-03-21 | 三荣源有限公司 | Nicotine-reducing agent and nicotine reduction method |
CN103501641A (en) * | 2011-03-02 | 2014-01-08 | 日本烟草产业株式会社 | Method for producing flavoring-containing sheet for smoking article, flavoring-containing sheet for smoking article produced thereby, and smoking article comprising same |
CN104382224A (en) * | 2014-10-22 | 2015-03-04 | 浙江中烟工业有限责任公司 | Solid state cartridge for electronic cigarettes and preparation method thereof |
CN105342013A (en) * | 2015-11-06 | 2016-02-24 | 浙江中烟工业有限责任公司 | Solid smoke cartridge of novel electronic cigarette |
CN112087959A (en) * | 2018-05-17 | 2020-12-15 | 株式会社东亚产业 | Aromatic cigarette cartridge |
-
2022
- 2022-01-07 CN CN202210015512.XA patent/CN114271532A/en active Pending
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1933744A (en) * | 2004-02-19 | 2007-03-21 | 三荣源有限公司 | Nicotine-reducing agent and nicotine reduction method |
CN103501641A (en) * | 2011-03-02 | 2014-01-08 | 日本烟草产业株式会社 | Method for producing flavoring-containing sheet for smoking article, flavoring-containing sheet for smoking article produced thereby, and smoking article comprising same |
JP5514951B2 (en) * | 2011-03-02 | 2014-06-04 | 日本たばこ産業株式会社 | Method for producing fragrance-containing sheet for smoking article, fragrance-containing sheet for smoking article produced by the method, and smoking article including the same |
CN104382224A (en) * | 2014-10-22 | 2015-03-04 | 浙江中烟工业有限责任公司 | Solid state cartridge for electronic cigarettes and preparation method thereof |
CN105342013A (en) * | 2015-11-06 | 2016-02-24 | 浙江中烟工业有限责任公司 | Solid smoke cartridge of novel electronic cigarette |
CN112087959A (en) * | 2018-05-17 | 2020-12-15 | 株式会社东亚产业 | Aromatic cigarette cartridge |
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