CN114224820A - Oil-control antioxidant makeup removing cream and preparation method thereof - Google Patents

Oil-control antioxidant makeup removing cream and preparation method thereof Download PDF

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CN114224820A
CN114224820A CN202210103239.6A CN202210103239A CN114224820A CN 114224820 A CN114224820 A CN 114224820A CN 202210103239 A CN202210103239 A CN 202210103239A CN 114224820 A CN114224820 A CN 114224820A
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oil
parts
fermentation product
product filtrate
antioxidant
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CN114224820B (en
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王辉
陈新征
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Nanjing Xiayue Biotechnology Co ltd
Shanghai Heya Cosmetic Co ltd
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Nanjing Xiayue Biotechnology Co ltd
Shanghai Heya Cosmetic Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/63Steroids; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9728Fungi, e.g. yeasts
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
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    • A61K8/99Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from microorganisms other than algae or fungi, e.g. protozoa or bacteria
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00Make-up preparations; Body powders; Preparations for removing make-up
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    • AHUMAN NECESSITIES
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    • A61Q19/00Preparations for care of the skin
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    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/008Preparations for oily skin
    • AHUMAN NECESSITIES
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    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
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    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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    • A61K2800/78Enzyme modulators, e.g. Enzyme agonists
    • A61K2800/782Enzyme inhibitors; Enzyme antagonists
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A40/00Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
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Abstract

The application relates to the field of makeup removing products, and particularly discloses an oil-control antioxidant makeup removing cream and a preparation method thereof, wherein the oil-control antioxidant makeup removing cream comprises 800 parts of an emollient 500-; the preparation method comprises the following steps: mixing other raw materials except the emollient to obtain a mixture A after stirring, adding the emollient to the mixture A after uniformly stirring at 75-85 ℃, obtaining a mixture B after uniformly stirring, and cooling the mixture B to 25 ℃ to obtain the oil-control antioxidant cleansing cream. The application has the effect of improving the defect that the skin is easily damaged due to over-cleaning of the oil control product.

Description

Oil-control antioxidant makeup removing cream and preparation method thereof
Technical Field
The application relates to the field of makeup removing products, in particular to oil-control antioxidant makeup removing cream and a preparation method thereof.
Background
The makeup can improve the appearance and promote confidence on one hand, and is also a presentation of politeness and respect on the other hand. However, when the pores are filled with cosmetics for a long time, the metabolism of the skin is affected, resulting in accelerated aging of the skin, and the cosmetics generally contain irritant substances, which are liable to cause various skin problems for a long time. Therefore, with the popularity of makeup, post-makeup cleaning becomes a topic of increasing concern.
The makeup removing product can effectively clean cosmetics in skin pores, including makeup removing oil, makeup removing water, makeup removing cream and the like. The cleansing cream has relatively thick texture, can be used for removing relatively complete makeup, and has good cleaning effect.
For people with oily skin, sebaceous glands of the people are more vigorous than other people, more sebum is secreted, and fat-soluble harmful substances are easy to accumulate, so that a cleaning product with stronger oil control capability is needed. However, over-cleansing tends to damage the barrier layer of the skin, causing more skin problems. Therefore, how to keep the skin from being damaged while controlling oil is an urgent problem to be solved for cleansing products such as makeup removing cream.
Disclosure of Invention
In order to overcome the defect that skin is easily damaged due to over-cleaning of an oil control product, the application provides an oil control antioxidant cleansing cream and a preparation method thereof.
In a first aspect, the application provides an oil-control antioxidant makeup remover, which adopts the following technical scheme:
the oil-control antioxidant makeup remover cream comprises the following components in parts by weight:
Figure BDA0003492929510000011
wherein the lactobacillus/soy milk fermentation product filtrate composition comprises 0.002-0.03 weight parts of lactobacillus/soy milk fermentation product filtrate, and the yeast for bifidus fermentation product filtrate composition comprises 0.197-2.967 weight parts of yeast for bifidus fermentation product filtrate.
By adopting the technical scheme, the aescin has the effects of controlling oil, calming and resisting oxidation, can relieve swelling and pain by promoting the exchange of water in capillaries, can inhibit the activity of hyaluronidase, reduce the degradation of hyaluronic acid and maintain the water of skin, and has a stabilizing effect on the structures of collagen and elastin, so that the skin aging is delayed;
the lactobacillus/soybean milk fermentation product filtrate is rich in vitamins and proteins, and has the effects of protecting and repairing while moisturizing and relieving;
the secondary fission yeast fermentation product filtrate can nourish the skin, promote the metabolism of cells, provide basic components for skin to synthesize protein, and play roles in moisturizing, resisting oxidation and whitening;
by compounding aescin, lactobacillus/soybean milk fermentation product filtrate and saccharomyces bifidus fermentation product filtrate, the cleansing cream has excellent oil control performance, can maintain the moisture of the skin, enables the barrier layer of the skin not to be easily damaged, and repairs the damaged skin through the lactobacillus/soybean milk fermentation product filtrate, so that the defect that the skin is easily damaged due to over-cleaning of the oil control product is overcome.
Optionally, the lactobacillus/soy milk fermentation product filtrate composition comprises the following components in percentage by mass:
Lactobacillus/Soybean milk fermentation product filtrate 1%
49.5 percent of water
And 49.5 percent of butanediol.
By adopting the technical scheme, the usage amount of the lactobacillus/soybean milk fermentation product filtrate is less, and the in-process for preparing the makeup removing cream is not convenient to weigh, so that the lactobacillus/soybean milk fermentation product filtrate is mixed with water and butanediol, the convenience for preparing the makeup removing cream is improved, in addition, the butanediol not only plays a role of a solvent, but also can improve the moisturizing effect of the makeup removing cream, and the makeup removing cream is not easy to damage when controlling oil to skin.
Optionally, the split yeast fermentation product filtrate composition comprises the following components in percentage by mass:
98.9 percent of secondary fission yeast fermentation product filtrate
0.8 percent of 1, 2-hexanediol
0.3 percent of p-hydroxyacetophenone.
By adopting the technical scheme, the secondary fission yeast fermentation product filtrate contains active ingredients, and is easy to deteriorate and lose efficacy in the preparation process of the makeup removing cream, so that the 1, 2-hexanediol and the p-hydroxyacetophenone are added as preservatives, the breeding of bacteria in the makeup removing cream can be inhibited, and the capacity of improving the moisturizing effect of the makeup removing cream is realized.
Optionally, the oil-control antioxidant makeup remover also comprises 0.2-3 parts by weight of beta-glucan composition, and the beta-glucan composition comprises 0.002-0.033 parts by weight of beta-glucan.
By adopting the technical scheme, the beta-glucan is the vegetable gum glycan, so that the cleansing cream not only has the effects of moisturizing and resisting oxidation, but also can reduce the damage of ultraviolet rays to the skin, and simultaneously endows the cleansing cream with good use skin feel, and the beta-glucan, the aescin, the lactobacillus/soybean milk fermentation product filtrate and the saccharomyces cerevisiae fermentation product filtrate are compounded, so that the defect that the skin is easily damaged due to over-cleaning of an oil control product can be further improved, and the cleansing cream can keep the moisture of the skin while controlling the oil.
Optionally, the beta-glucan composition comprises the following components in percentage by mass:
Figure BDA0003492929510000031
by adopting the technical scheme, the beta-glucan is less in dosage and inconvenient to weigh in the process of preparing the makeup removing cream, so that the beta-glucan is mixed with water and butanediol to improve the convenience of preparing the makeup removing cream, and in addition, the butanediol not only plays a role of a solvent, but also can improve the moisturizing effect of the makeup removing cream, so that the makeup removing cream is not easy to damage while controlling oil to skin;
because the beta-glucan contains active ingredients, the beta-glucan is easy to deteriorate and lose efficacy in the preparation process of the makeup removing cream, and the 1, 2-hexanediol and the p-hydroxyacetophenone are added as the preservative, so that the breeding of bacteria in the makeup removing cream can be inhibited, and the capacity of improving the moisturizing effect of the makeup removing cream is realized.
Optionally, the oil-control antioxidant cleansing cream further comprises 1-5 parts by weight of vitamin C.
By adopting the technical scheme, the vitamin C can inhibit the activity of tyrosinase, block the generation of melanin, improve the skin darkness, simultaneously has the effect of promoting the generation of collagen, plays the roles of oxidation resistance and aging resistance, and can improve the oxidation resistance and the repair capability of the makeup removing cream and further improve the defect that the skin is easily damaged due to the over-cleaning of an oil control product by compounding the vitamin C with aescin, lactobacillus/soybean milk fermentation product filtrate and saccharomyces cerevisiae fermentation product filtrate.
Optionally, the emollient comprises the following components in parts by weight:
cocoanol-caprylate/caprate 370-500 parts
100 portions of cetyl ethyl hexanoate and 200 portions of
30-100 parts of caprylic/capric triglyceride.
By adopting the technical scheme, the coconut oil alcohol-caprylate/caprate has good ductility, can make the makeup removing cream easy to smear, and has the effects of reducing skin moisture evaporation and enhancing skin hydration; the cetyl ethyl hexanoate can reduce the greasy feeling of the makeup removing cream, enhance the permeability of skin care components and ensure that the makeup removing cream is uniform and fine; the caprylic acid/capric acid triglyceride can play a role in stabilizing the components of the makeup removing cream and simultaneously improve the moisturizing effect of the makeup removing cream; by compounding the coconut oil alcohol-caprylate/caprate, the cetyl ethyl hexanoate and the caprylic/capric triglyceride, the uniform and fine makeup removing cream matrix which is easy to smear is formed, and the experience of a user is improved.
Optionally, the emulsifier comprises the following components in parts by weight:
30-100 parts of sorbitol polyether-30 tetraoleate
30-100 parts of PEG-12 diisostearate
30-100 parts of PEG-20 glycerol triisostearate.
By adopting the technical scheme, the sorbierite polyether-30 tetraoleate, the PEG-12 diisostearate and the PEG-20 glycerol triisostearate are excellent emulsifiers, and the cleansing cream is uniform and stable through compounding of the sorbierite polyether-30 tetraoleate, the PEG-12 diisostearate and the PEG-20 glycerol triisostearate, can form a mild and mild emulsion after meeting water, and is easy to clean.
Optionally, the thickener comprises the following components in percentage by mass:
80 percent of synthetic wax
Candelilla wax 17%
3% of carnauba wax.
By adopting the technical scheme, the synthetic wax can improve the viscosity of the makeup removing cream and simultaneously plays the roles of a stabilizer and a softening agent; the candelilla wax and the carnauba wax can play a role in hardening the synthetic wax, and through compounding of the candelilla wax and the carnauba wax, the viscosity of the makeup removing cream is improved, and meanwhile, the moisturizing effect and the anti-aging capability of the makeup removing cream are improved, so that the defect that skin is easily damaged due to over-cleaning of an oil control product is further overcome.
In a second aspect, the application provides a preparation method of the oil-control antioxidant cleansing cream, which adopts the following technical scheme: a preparation method of oil-control antioxidant cleansing cream comprises the following steps:
s1, weighing the raw materials according to the proportion, mixing the raw materials except the emollient, and stirring to obtain a mixture A;
s2, uniformly stirring the emollient at 75-85 ℃ to obtain the emollient after heating and stirring;
s3, adding the mixture A into the heated and stirred emollient, and stirring uniformly to obtain a mixture B;
and S4, cooling the mixture B to 25 ℃ to obtain the oil-control antioxidant cleansing cream.
By adopting the technical scheme, the emollient serving as the base material is melted at the temperature of 75-85 ℃, other raw materials are added and uniformly stirred, and the uniform, soft and moist oil-control antioxidant makeup remover can be obtained after cooling.
In summary, the present application includes at least one of the following beneficial technical effects:
1. by compounding aescin, lactobacillus/soybean milk fermentation product filtrate and saccharomyces cerevisiae fermentation product filtrate, the cleansing cream has excellent oil control performance, can maintain the moisture of the skin, enables the barrier layer of the skin not to be easily damaged, and repairs the damaged skin through the lactobacillus/soybean milk fermentation product filtrate, so that the defect that the skin is easily damaged due to over-cleaning of the oil control product is overcome;
2. the beta-glucan is vegetable gum glycan, so that the moisturizing and antioxidant effects are achieved, the damage of ultraviolet rays to the skin can be reduced, the makeup removing cream is endowed with good use skin feel, the beta-glucan is compounded with aescin, lactobacillus/soybean milk fermentation product filtrate and saccharomyces cerevisiae fermentation product filtrate, the defect that the skin is easily damaged due to over-cleaning of an oil control product can be further improved, and the makeup removing cream keeps the moisture of the skin while controlling the oil;
3. the vitamin C can inhibit the activity of tyrosinase, block the generation of melanin, improve the skin darkness, simultaneously has the effect of promoting the generation of collagen, has the functions of antioxidation and ageing resistance, can improve the antioxidation and repair capability of the makeup removing cream by compounding the vitamin C with aescin, lactobacillus/soybean milk fermentation product filtrate and saccharomyces cerevisiae fermentation product filtrate, and further improves the defect that the skin is easily damaged due to the over-cleaning of an oil control product.
Detailed Description
Source of raw materials
Unless otherwise specified, the specifications and sources of the raw materials in the following examples and comparative examples are shown in Table 1 below.
TABLE 1 raw material specifications and sources
Raw materials Specification of Source
Hydrogenated soybean oil CAS number: 68334-28-1 Shanxi brocade medicinal auxiliary materials Co Ltd
Citrus aurantium peel oil (also known as sweet orange oil) CAS number: 8008-57-9 Jiangxi Hengcheng Natural Fragrance Oil Co.,Ltd.
Tangerine peel oil (also known as tangerine oil) CAS number: 223748-44-5 Jiangxi Hairui Natural Plant Co.,Ltd.
Synthetic wax CAS number: 8002-74-2 Cangzhou Mulan wax Co Ltd
Candelilla wax CAS number: 8006-44-8 Cangzhou Mulan wax Co Ltd
Carnauba wax CAS number: 8015-86-9 Cangzhou Mulan wax Co Ltd
Beta-glucan CAS number: 160872-27-5 Shaanxi Saen Biotech Co Ltd
Lactobacillus/soymilk fermentation product filtrate The content is as follows: 99 percent Wuhanhua detailed scientific biotechnology limited
Secondary split yeast fermentation product filtrate CAS number: 96507-89-0 Shanghai Lizi Biotech Co., Ltd
Examples
Example 1
The oil-control antioxidant cleansing cream comprises the components and the corresponding using amounts shown in the table 2, and is prepared by the following steps:
p1, mixing the hydrogenated soybean oil required for the first taste-modifying composition, the sweet almond oil required for the first taste-modifying composition, and the lime peel oil to obtain a first taste-modifying composition;
p2, mixing the hydrogenated soybean oil required for the second odor modifying composition, the sweet almond oil required for the second odor modifying composition, and the cranberry peel oil to provide a second odor modifying composition;
p3, mixing water required by the lactobacillus/soybean milk fermentation product filtrate composition, butanediol required by the lactobacillus/soybean milk fermentation product filtrate composition and lactobacillus/soybean milk fermentation product filtrate to obtain a lactobacillus/soybean milk fermentation product filtrate composition;
p4, mixing 1, 2-hexanediol required by the secondary fission yeast fermentation product filtrate composition, P-hydroxyacetophenone required by the secondary fission yeast fermentation product filtrate composition and the secondary fission yeast fermentation product filtrate to obtain the secondary fission yeast fermentation product filtrate composition;
p5, weighing the raw materials according to the proportion, mixing the emulsifier, the first odor regulating composition, the second odor regulating composition, the thickening agent, the solvent, the preservative, the antioxidant, the aescin, the lactobacillus/soybean milk fermentation product filtrate composition and the saccharomyces cerevisiae fermentation product filtrate composition, and stirring to obtain a mixture A;
p6, uniformly stirring the emollient at 75-85 ℃ to obtain the emollient after heating and stirring;
p7, adding the mixture A into the heated and stirred emollient, and stirring uniformly to obtain a mixture B;
and P8, cooling the mixture B at the temperature of 25 ℃ to obtain the oil-control antioxidant cleansing cream.
Examples 2 to 3
Examples 2-3 differ from example 1 in the components included and their respective amounts, as shown in table 2 below.
Table 2 examples 1-3 include the components and their respective amounts
Figure BDA0003492929510000061
Example 4
The oil-control antioxidant cleansing cream comprises the components and the corresponding using amounts shown in Table 3, and is prepared by the following steps:
q1, mixing the hydrogenated soybean oil required by the first flavor modifying composition, the sweet almond oil required by the first flavor modifying composition and the lime peel oil to obtain a first flavor modifying composition;
q2, mixing the hydrogenated soybean oil required for the second odor modifying composition, the sweet almond oil required for the second odor modifying composition, and the cranberry peel oil to provide a second odor modifying composition;
q3, mixing water required by the lactobacillus/soy milk fermentation product filtrate composition, butanediol required by the lactobacillus/soy milk fermentation product filtrate composition and lactobacillus/soy milk fermentation product filtrate to obtain a lactobacillus/soy milk fermentation product filtrate composition;
q4, mixing 1, 2-hexanediol required by the secondary fission yeast fermentation product filtrate composition, p-hydroxyacetophenone required by the secondary fission yeast fermentation product filtrate composition and the secondary fission yeast fermentation product filtrate to obtain the secondary fission yeast fermentation product filtrate composition;
q5, mixing water required by the beta-glucan composition, butanediol required by the beta-glucan composition, 1, 2-hexanediol required by the beta-glucan composition, p-hydroxyacetophenone required by the beta-glucan composition and beta-glucan to obtain the beta-glucan composition;
q6, weighing the raw materials according to the proportion, mixing the emulsifier, the first odor regulating composition, the second odor regulating composition, the thickening agent, the solvent, the preservative, the antioxidant, the aescin, the lactobacillus/soybean milk fermentation product filtrate composition, the saccharomyces cerevisiae fermentation product filtrate composition and the beta-glucan composition, and stirring to obtain a mixture A;
q7, uniformly stirring the emollient at 75-85 ℃ to obtain the emollient after heating and stirring;
q8, adding the mixture A into the heated and stirred emollient, and stirring uniformly to obtain a mixture B;
q9, cooling the mixture B at the temperature of 25 ℃ to obtain the oil-control antioxidant cleansing cream.
Examples 5 to 6
Examples 5-6 differ from example 4 in the components included and their respective amounts, as shown in table 3 below.
Table 3 examples 4-6 include the components and their respective amounts
Figure BDA0003492929510000071
Figure BDA0003492929510000081
Example 7
Example 7 differs from example 4 in that 2g of vitamin C was also added in the Q6 step.
Example 8
Example 8 differs from example 5 in that 6g of vitamin C was also added in the Q6 step.
Example 9
Example 9 differs from example 6 in that 10g of vitamin C was also added in the Q6 step.
Comparative example
Comparative examples 1 to 3
Comparative examples 1-3 differ from example 1 in the amounts of the emollient components as shown in table 4 below.
TABLE 4 emollients included in comparative examples 1-3 and the corresponding amounts
Figure BDA0003492929510000082
Comparative example 4
Comparative example 4 differs from example 1 in that escin was not added in the P5 step.
Comparative example 5
Comparative example 5 is different from example 1 in that the lactobacillus/soybean milk fermentation product filtrate composition is replaced with an equal mass of the yeast for secondary fission fermentation product filtrate composition in the P5 step.
Comparative example 6
Comparative example 6 differs from example 1 in that the lactic acid bacteria/soybean milk fermentation product filtrate composition of equal mass was used instead of the yeast for secondary fission in the P5 step.
Performance test
Test one: oil control test
The test conditions are as follows: the test environment temperature is 20-22 ℃, and the relative humidity is 40-60%.
The test method comprises the following steps: selecting 75 healthy women in the same area and age range of 18-45 years as testees, randomly dividing the testees into 15 groups, marking 5 people in each group as 1-15 groups of testees, cleaning the face of each group of testees by using the same alkaline soap-based cleaning product, washing the face by using clear water, then sucking the face by using a non-scrap water-absorbing dry paper towel, statically sitting in a test environment, and testing the skin surface sebum amount of the forehead of each tester by using a skin surface sebum tester SebumeterAveraging the data obtained from each group to obtain the average initial forehead sebum amount of each group of subjects; each subject then used the same foundation at 0.1ml/cm2The amount of the oil-controlling antioxidant cleansing cream is uniformly applied to the forehead, after 30min, 1-9 groups use the oil-controlling antioxidant cleansing cream corresponding to examples 1-9, 10-15 groups use the oil-controlling antioxidant cleansing cream corresponding to comparative examples 1-6, the amount is 5ml, makeup is removed, the forehead is cleaned with clear water after being rubbed for 30s, water is sucked dry with a non-crumbs water-absorbing dry paper towel, the skin surface sebum amount of the forehead of each subject is tested by using a skin surface sebum tester Sebumeter, and the average value of the data obtained in each group is taken as the average final forehead sebum amount of each group of subjects.
And (3) test results: the amount of sebum on the forehead skin surface of the subject before and after application of the oil-controlling antioxidant cleansing cream corresponding to examples 1 to 9 and comparative examples 1 to 6 is shown in Table 5 below.
TABLE 5 oil control test results
Sample (I) Initial forehead sebum amount (. mu.g/cm)2) Final forehead sebum amount (. mu.g/cm)2)
Example 1 120 96
Example 2 125 95
Example 3 117 92
Example 4 109 90
Example 5 116 91
Example 6 121 97
Example 7 124 93
Example 8 109 89
Example 9 130 96
Comparative example 1 125 101
Comparative example 2 116 103
Comparative example 3 118 103
Comparative example 4 123 115
Comparative example 5 115 90
Comparative example 6 127 113
As can be seen by combining examples 1-9 and Table 5, the amount of sebum on the forehead of the subjects was reduced after removing makeup with the oil-control antioxidant makeup remover cream, indicating that examples 1-9 all had better oil-control ability.
As can be seen by combining examples 1-9 and comparative examples 1-3 with Table 5, the amount of each component of the emollient was adjusted in comparative examples 1-3 to have less effect on the oil control ability of the cream.
It can be seen by combining examples 1-9 and comparative example 4 and combining table 5 that the oil control ability of the cleansing cream is obviously affected by not adding aescin, which indicates that aescin is a key oil control component in the oil control antioxidant cleansing cream.
It can be seen from the combination of examples 1 to 9 and comparative example 5 and table 5 that, in comparative example 5, the lactobacillus/soybean milk fermentation product filtrate composition was replaced with the same quality of the dileakage yeast fermentation product filtrate composition, so that the oil control ability of the oil control antioxidant cleansing cream was improved, since the dileakage yeast fermentation product filtrate could play the role of oil control.
It can be seen from the combination of examples 1 to 9 and comparative example 6 and table 5 that, in comparative example 6, the oil-controlling ability of the oil-controlling antioxidant cleansing cream was decreased by replacing the split yeast fermentation product filtrate composition with the lactobacillus/soybean milk fermentation product filtrate composition of the same quality, since the split yeast fermentation product filtrate can play the role of oil control.
And (2) test II: moisture retention test
The test conditions are as follows: the test environment temperature is 20-22 ℃, and the relative humidity is 40-60%.
The test method comprises the following steps: selecting 75 healthy women in the same area and age range of 18-45 years as test subjects, randomly dividing the test subjects into 15 groups, marking 5 persons in each group as 1-15 groups of test subjects, cleaning the face of each group of test subjects by using the same facial cleanser, washing the face by using clear water, then sucking the face by using a non-scrap absorbent dry paper towel, sitting still in a test environment, testing the moisture content of the cheek skin of each test subject, and averaging the data obtained in each group to be used as the average initial moisture content of the skin of each group of test subjects; each subject then used the same foundation at 0.1ml/cm2The dosage of the oil-control antioxidant cleansing cream is uniformly applied to cheeks, after 30min, 1-9 groups of the oil-control antioxidant cleansing cream corresponding to examples 1-9 are used, 10-15 groups of the oil-control antioxidant cleansing cream corresponding to comparative examples 1-6 are used, the dosage is 5ml, makeup is removed, the cheeks are cleaned by clear water after being rubbed for 30s, water is sucked dry by a non-scrap water-absorbing dry paper towel, the moisture content of the cheek skin of each subject is tested, and the average value of the data obtained in each group is used as the average final moisture content of the skin of each group of subjects.
And (3) test results: the skin moisture content of the cheeks of the subjects before and after using the oil-control antioxidant makeup remover cream corresponding to examples 1 to 9 and comparative examples 1 to 6 is shown in table 6 below.
TABLE 6 test results of the moisturizing test
Sample (I) Initial skin moisture content (%) Final skin moisture (%)
Example 1 53.4 54.2
Example 2 54.1 54.9
Example 3 54.7 55.4
Example 4 54.5 55.6
Example 5 56.1 56.9
Example 6 55.2 56.2
Example 7 56.7 57.5
Example 8 57.1 58.1
Example 9 55.4 56.6
Comparative example 1 53.8 54.2
Comparative example 2 57.3 57.8
Comparative example 3 56.4 56.8
Comparative example 4 54.5 55.1
Comparative example 5 52.9 53.5
Comparative example 6 56.6 57.3
It can be seen by combining examples 1-9 and tables 5-6 that the skin moisture content of the subjects is increased after makeup removal by using the oil-control antioxidant makeup remover, which indicates that examples 1-9 all have better moisturizing capability, and thus the oil-control antioxidant makeup remover of examples 1-9 not only has excellent oil-control capability, but also has excellent moisturizing efficacy, and is not easy to damage the barrier layer of the skin, and the moisturizing effect of examples 4-9 is slightly better than that of examples 1-3, because the β -glucan is added in examples 4-9, which is beneficial to improving the moisturizing capability of the makeup remover.
As can be seen by combining examples 1-9 and comparative examples 1-3 with Table 6, in comparative examples 1-3, the moisturizing capability of the cleansing cream is greatly influenced due to the adjustment of the amount of each component of the emollient, which indicates that the cleansing cream obtained by compounding the coconut oil alcohol-caprylate/caprate, the cetyl alcohol ethyl hexanoate and the caprylic/capric triglyceride has better moisturizing performance under a specific ratio.
As can be seen by combining examples 1-9 and comparative example 4 with Table 6, the effect of not adding escin on the moisturizing ability of the cleansing cream is small.
It can be seen from the combination of examples 1 to 9 and comparative example 5 and table 6 that, in comparative example 5, the substitution of the lactobacillus/soybean milk fermentation product filtrate composition with the same quality of the bifidus yeast fermentation product filtrate composition has less influence on the moisturizing ability of the oil-controlling antioxidant cleansing cream, since both the lactobacillus/soybean milk fermentation product filtrate and the bifidus yeast fermentation product filtrate can play a role in moisturizing.
As can be seen by combining examples 1-9 and comparative example 6 with Table 6, since both the lactic acid bacteria/soybean milk fermentation product filtrate and the secondary split yeast fermentation product filtrate can play a moisturizing role, in comparative example 6, the lactic acid bacteria/soybean milk fermentation product filtrate composition of the same quality is used instead of the secondary split yeast fermentation product filtrate composition, and the influence on the moisturizing capability of the oil-controlling antioxidant cleansing cream is small.
And (3) test III: makeup removal effect test
The test conditions are as follows: the test environment temperature is 20-22 ℃, and the relative humidity is 40-60%.
The test method comprises the following steps: selecting 75 healthy women in the same area and age range of 18-45 years as testees, randomly dividing the testees into 15 groups, marking each group as 1-15 groups of testees, respectively applying the same type of aqueous eyeliner, aqueous mascara, oily mascara, foundation and lipstick on cleaned skin on the back of hands in equal amount, completely drying the testees, applying oil-controlling antioxidant makeup remover to the washed skin on the back of hands by using the same type of makeup removing cotton, wherein 1-9 groups use the oil-controlling antioxidant makeup remover corresponding to examples 1-9, 10-15 groups use the oil-controlling antioxidant makeup remover corresponding to comparative examples 1-6, respectively rubbing the positions of the backs of hands coated with different cosmetics for 10s, then wiping the positions in the same direction, replacing the makeup removing cotton, repeatedly applying the oil-controlling antioxidant makeup remover and wiping until the makeup removing cotton has no color, recording the wiping times of each tester and the residual situation of the cosmetics, the number of wipes obtained for each group was averaged.
And (3) test results: the number of wipes and the amount of makeup left by the subjects who used the oil-controlling antioxidant cleansing creams according to examples 1 to 9 and comparative examples 1 to 6 are shown in Table 7 below.
TABLE 7 removal of makeup test results
Figure BDA0003492929510000111
Figure BDA0003492929510000121
As can be seen by combining examples 1-9 and tables 5-7, examples 1-9 all have excellent makeup removing capability, so that the oil-control antioxidant makeup remover cream of examples 1-9 has good makeup removing performance, oil-control performance and moisturizing performance, can thoroughly clean cosmetics, is not easy to damage skin, and overcomes the defect that skin is easily damaged due to over-cleaning of oil-control products.
As can be seen by combining examples 1-9 and comparative examples 1-3 with Table 7, in comparative examples 1-3, the makeup removing capability of the makeup removing cream is greatly influenced due to the adjustment of the dosage of each component of the emollient, which shows that the makeup removing cream prepared by the combination of coconut oil alcohol-caprylate/caprate, cetyl ethyl hexanoate and caprylic/capric triglyceride has better makeup removing effect under a specific ratio.
As can be seen by combining examples 1-9 and comparative example 4 with Table 7, the effect of not adding escin on the makeup removing ability of the makeup removing cream is small.
It can be seen from the combination of examples 1-9 and comparative example 5 and from Table 7 that the substitution of the lactobacillus/soymilk fermentation product filtrate composition with an equal mass of the yeast diligen fermentation product filtrate composition had a smaller effect on the makeup removing ability of the oil-controlling antioxidant makeup remover cream.
It can be seen from the combination of examples 1 to 9 and comparative example 6 and from Table 7 that the substitution of the secondary yeast fermentation product filtrate composition with an equal mass of the lactobacillus/soymilk fermentation product filtrate composition had a smaller effect on the makeup removing ability of the oil-controlling antioxidant makeup remover cream.
The above embodiments are preferred embodiments of the present application, and the protection scope of the present application is not limited by the above embodiments, so: all equivalent changes made according to the structure, shape and principle of the present application shall be covered by the protection scope of the present application.

Claims (10)

1. The oil-control antioxidant makeup remover is characterized by comprising the following components in parts by weight:
emollient 500-800 parts
90-300 parts of emulsifier
20-60 parts of thickening agent
1-5 parts of aescin
0.2-3 parts of lactobacillus/soybean milk fermentation product filtrate composition
0.2-3 parts of schizosaccharomyces cerevisiae fermentation product filtrate composition
Wherein the lactobacillus/soy milk fermentation product filtrate composition comprises 0.002-0.03 weight parts of lactobacillus/soy milk fermentation product filtrate, and the yeast for bifidus fermentation product filtrate composition comprises 0.197-2.967 weight parts of yeast for bifidus fermentation product filtrate.
2. The oil-controlling antioxidant makeup remover according to claim 1, wherein the lactobacillus/soy milk fermentation product filtrate composition comprises the following components in percentage by mass:
Lactobacillus/Soybean milk fermentation product filtrate 1%
49.5 percent of water
And 49.5 percent of butanediol.
3. The oil-control antioxidant cleansing cream according to claim 1, wherein the cracked yeast fermentation product filtrate composition comprises the following components in percentage by mass:
98.9 percent of secondary fission yeast fermentation product filtrate
0.8 percent of 1, 2-hexanediol
0.3 percent of p-hydroxyacetophenone.
4. The oil-control antioxidant makeup remover according to claim 1, characterized in that: the oil-control antioxidant makeup remover also comprises 0.2-3 parts by weight of beta-glucan composition, and the beta-glucan composition comprises 0.002-0.033 parts by weight of beta-glucan.
5. The oil-control antioxidant makeup remover according to claim 4, wherein the beta-glucan composition comprises the following components in percentage by mass:
1.1% of beta-glucan
87.9 percent of water
Butanediol 10%
0.5 percent of 1, 2-hexanediol
0.5 percent of p-hydroxyacetophenone.
6. The oil-control antioxidant makeup remover according to claim 1, characterized in that: the oil-control antioxidant cleansing cream also comprises 1-5 parts by weight of vitamin C.
7. The oil-control antioxidant makeup remover according to claim 1, wherein the emollient comprises the following components in parts by weight:
cocoanol-caprylate/caprate 370-500 parts
100 portions of cetyl ethyl hexanoate and 200 portions of
30-100 parts of caprylic/capric triglyceride.
8. The oil-control antioxidant makeup remover according to claim 1, wherein the emulsifier comprises the following components in parts by weight:
30-100 parts of sorbitol polyether-30 tetraoleate
30-100 parts of PEG-12 diisostearate
30-100 parts of PEG-20 glycerol triisostearate.
9. The oil-control antioxidant makeup remover according to claim 1, wherein the thickener comprises the following components in percentage by mass:
80 percent of synthetic wax
Candelilla wax 17%
3% of carnauba wax.
10. The preparation method of the oil-control antioxidant cleansing cream as claimed in any one of claims 1 to 9, which is characterized by comprising the following steps:
s1, weighing the raw materials according to the proportion, mixing the raw materials except the emollient, and stirring to obtain a mixture A;
s2, uniformly stirring the emollient at 75-85 ℃ to obtain the emollient after heating and stirring;
s3, adding the mixture A into the heated and stirred emollient, and stirring uniformly to obtain a mixture B;
and S4, cooling the mixture B to 25 ℃ to obtain the oil-control antioxidant cleansing cream.
CN202210103239.6A 2022-01-27 2022-01-27 Oil-control antioxidant cleansing cream and preparation method thereof Active CN114224820B (en)

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Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112156037A (en) * 2020-11-06 2021-01-01 上海花飞谷品牌管理有限公司 Skin-care soothing composition, makeup removing lotion and preparation method thereof
CN112773761A (en) * 2021-02-22 2021-05-11 广州花出见生物科技有限公司 Cosmetic composition, essence and preparation method thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112156037A (en) * 2020-11-06 2021-01-01 上海花飞谷品牌管理有限公司 Skin-care soothing composition, makeup removing lotion and preparation method thereof
CN112773761A (en) * 2021-02-22 2021-05-11 广州花出见生物科技有限公司 Cosmetic composition, essence and preparation method thereof

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