CN114177642A - Simultaneous distillation and extraction device - Google Patents
Simultaneous distillation and extraction device Download PDFInfo
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- CN114177642A CN114177642A CN202111537417.8A CN202111537417A CN114177642A CN 114177642 A CN114177642 A CN 114177642A CN 202111537417 A CN202111537417 A CN 202111537417A CN 114177642 A CN114177642 A CN 114177642A
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- 238000004821 distillation Methods 0.000 title claims abstract description 60
- 238000000605 extraction Methods 0.000 title claims abstract description 42
- 238000010438 heat treatment Methods 0.000 claims abstract description 75
- 238000002156 mixing Methods 0.000 claims abstract description 29
- 238000009833 condensation Methods 0.000 claims abstract description 22
- 230000005494 condensation Effects 0.000 claims abstract description 22
- 238000001816 cooling Methods 0.000 claims abstract description 19
- 239000000463 material Substances 0.000 claims abstract description 16
- 239000002826 coolant Substances 0.000 claims abstract description 5
- 238000003860 storage Methods 0.000 claims abstract description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 55
- 239000000498 cooling water Substances 0.000 claims description 24
- 238000002474 experimental method Methods 0.000 claims description 9
- 238000005057 refrigeration Methods 0.000 claims description 7
- 238000010521 absorption reaction Methods 0.000 claims description 2
- 230000008878 coupling Effects 0.000 claims description 2
- 238000010168 coupling process Methods 0.000 claims description 2
- 238000005859 coupling reaction Methods 0.000 claims description 2
- 230000000694 effects Effects 0.000 abstract description 6
- 238000007599 discharging Methods 0.000 abstract description 4
- 239000007788 liquid Substances 0.000 abstract description 2
- 239000003153 chemical reaction reagent Substances 0.000 description 7
- 239000002904 solvent Substances 0.000 description 6
- 239000000203 mixture Substances 0.000 description 4
- 150000001875 compounds Chemical class 0.000 description 3
- 239000000110 cooling liquid Substances 0.000 description 3
- 238000009434 installation Methods 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 230000017525 heat dissipation Effects 0.000 description 2
- 238000007789 sealing Methods 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 239000010425 asbestos Substances 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 238000000895 extractive distillation Methods 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000000149 penetrating effect Effects 0.000 description 1
- 229910052895 riebeckite Inorganic materials 0.000 description 1
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
- B01D3/40—Extractive distillation
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/04—Solvent extraction of solutions which are liquid
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01L—CHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
- B01L7/00—Heating or cooling apparatus; Heat insulating devices
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01L—CHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
- B01L9/00—Supporting devices; Holding devices
- B01L9/02—Laboratory benches or tables; Fittings therefor
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Clinical Laboratory Science (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The invention discloses a simultaneous distillation and extraction device, which comprises a test bench, a heating assembly and a cooling assembly, wherein the upper end of the test bench is fixedly connected with a support frame, the upper end of a distillation flask is communicated with a first connecting pipe, the heating assembly is arranged on one side of the support frame, the cooling assembly comprises a condensing pipe, a material conveying pipe penetrates through the interior of the condensing pipe, one end of the material conveying pipe is communicated with a mixing tank, the lower end of the mixing tank is communicated with a second connecting pipe, the upper end of the test bench is provided with an extraction tank, one side of the mixing tank is communicated with a material discharging pipe, and one end of the material discharging pipe is communicated with a storage tank. Can cool down the coolant liquid fast for the condensation effect is better.
Description
Technical Field
The invention belongs to the technical field of distillation and extraction equipment, and particularly relates to a simultaneous distillation and extraction device.
Background
The extraction distillation is a common experimental method for separating liquid mixture in chemistry, and the principle is that the compound is transferred from one solvent to another solvent by using the difference of solubility or distribution coefficient of the compound in two mutually insoluble (or slightly soluble) solvents, most of the compound is extracted by repeated extraction, instruments used for the extraction distillation include alcohol lamps, iron stand tables, asbestos meshes, conical flasks, ox horn tubes, beakers, condensers and other common laboratory instruments, and the extraction and distillation are widely applied to daily life and industrial production.
Extractive distillation, which is distillation in the presence of a readily soluble, high boiling and non-volatile component, which does not form an azeotrope with the other components of the mixture, is generally used to separate systems having very low or even equal relative volatilities, since the volatilities of the two components in the mixture are nearly equal, so that they evaporate at nearly the same temperature and to a similar extent, making separation difficult.
An important part of this distillation process is the choice of solvent, which plays an important role in the separation of the two components, notably the solvent which needs to be chosen so as to change its relative volatility significantly, which would otherwise be a futile attempt, as well as the economics of the solvent, which is easy to separate in the column and which does not react chemically with the components or the mixture, nor cause corrosion in the equipment.
Traditional when carrying out the distillation extraction experiment, the majority is utilizing the alcohol burner directly to heat the bottom of retort, is not convenient for control heating temperature according to the nature of target object itself, if heating temperature can't reach the expectation, reduces the efficiency of distillation extraction to a certain extent, if heating temperature is higher, can cause the damage to the target object again to current cooling module condensation effect is general, for this reason we propose a distillation extraction device simultaneously and solve the problem that exists among the prior art.
Disclosure of Invention
The invention aims to provide a simultaneous distillation and extraction device, which is provided with a movable heating box, a plurality of groups of heating rings are arranged in the heating box, the heating box is moved to enable a distillation flask to be positioned in different heating rings, the heating temperature can be controlled, and a cooling water tank is provided with radiating fins and refrigerating fins, so that cooling liquid can be rapidly cooled, the condensation effect is good, and the problems in the background art are solved.
In order to achieve the purpose, the invention adopts the following technical scheme: a simultaneous distillation and extraction device comprises an experiment table, a heating assembly and a cooling assembly, wherein the upper end of the experiment table is fixedly connected with a support frame, one side of the support frame is fixedly connected with an L-shaped fixing plate, a distillation flask is fixedly clamped on the L-shaped fixing plate, the upper end of the distillation flask is communicated with a first connecting pipe, the heating assembly is arranged on one side of the support frame, and the cooling assembly is arranged at the lower end of the support frame;
the heating assembly comprises a heating box, the heating box is arranged on one side of the supporting frame in a lifting manner, a plurality of groups of heating rings for heating the distillation bottles are arranged in the heating box, and the inner diameters of the heating rings in the heating box are sequentially reduced from top to bottom;
the cooling assembly comprises a condensation pipe, a material conveying pipe penetrates through the interior of the condensation pipe, one end of the first connecting pipe is communicated with one end of the material conveying pipe, a water inlet and a water outlet are formed in the condensation pipe, a water inlet pipe is communicated with the water inlet of the condensation pipe, and a water outlet pipe is communicated with the water outlet of the condensation pipe;
the one end intercommunication of conveying pipeline has the blending tank, the lower extreme intercommunication of blending tank has the second connecting pipe, the upper end of laboratory bench is provided with the extraction jar, the one end of second connecting pipe is located the inside of extraction jar, one side intercommunication of blending tank has row material pipe, the one end intercommunication of arranging the material pipe has the holding vessel.
Preferably, the L-shaped fixing plate comprises a transverse plate and a vertical plate, the upper end of the vertical plate of the L-shaped fixing plate is fixedly connected to one side of the supporting frame, a mounting groove is formed in one side of the transverse plate of the L-shaped fixing plate, and the distillation flask is clamped and fixed inside the mounting groove.
Preferably, one side fixed mounting of support frame has electronic slip table, fixedly connected with connecting rod on electronic slip table's the sliding block, one side of heating cabinet is in the one end fixed connection of connecting rod.
Preferably, the notch has been seted up to the upper end of heating cabinet, the notch is located the retort under, and the internal diameter of notch is greater than the external diameter of retort, fixedly connected with dead lever on the inner wall of heating cabinet, and the dead lever sets up to high temperature resistance dead lever, the heating collar passes through dead lever fixed mounting in the inside of heating cabinet.
Preferably, one side fixedly connected with bracing piece of support frame, the one end fixed connection of bracing piece is on the outer wall of condenser pipe, the condenser pipe is the slope setting.
Preferably, a cooling water tank is fixedly mounted at the top of the support frame, cooling fins are arranged inside the cooling water tank, the upper ends of the cooling fins penetrate through the cooling water tank and extend to the outside of the cooling water tank, refrigeration sheets are arranged on one sides of the cooling fins, and heat absorbing surfaces of the refrigeration sheets are attached to one sides of the cooling fins.
Preferably, the one end of outlet pipe and one side intercommunication of coolant tank, one side intercommunication of coolant tank has the water pipe, the upper end fixed mounting of support frame has the water pump, the one end of water pipe communicates in the end of intaking of water pump, the play water end of water pump communicates with the one end of inlet tube.
Preferably, the upper end fixed mounting of blending tank has micro motor, the inside that the one end of micro motor output shaft runs through the top of blending tank and extends to the blending tank, the top of blending tank inlays the dress and is fixed with the bearing, the fixed inner circle of pegging graft in the bearing of one end of micro motor output shaft, the one end of micro motor output shaft passes through shaft coupling fixedly connected with puddler.
Preferably, one side of extraction jar is sealed the intercommunication and is had the inlet pipe, one side of holding vessel is sealed the intercommunication and is had the discharging pipe, all be provided with the valve on the outer wall of second connecting pipe, inlet pipe, row's material pipe and discharging pipe.
The invention has the technical effects and advantages that: compared with the prior art, the simultaneous distillation and extraction device provided by the invention has the following advantages:
1. according to the invention, through the design of the structures such as the electric push rod, the heating box, the notch and the multiple groups of heating rings with sequentially reduced inner diameters, when the chemical reagent in the distillation flask needs to be distilled, the electric sliding table is utilized to drive the heating box to move upwards, and then the distillation flask is positioned in the specified heating ring according to the property of the chemical reagent, so that the control of the heating temperature is realized, the phenomenon that the heating temperature cannot reach the expected value because the heating temperature is suddenly high or low is avoided, the efficiency of distillation and extraction is reduced to a certain extent, and the heating temperature is higher, so that the target object can be damaged possibly is avoided;
2. according to the invention, through the structural design of the cooling water tank, the radiating fins, the refrigerating fins, the water pump, the water pipe, the water inlet pipe, the water outlet pipe and the like, one side of the cooling water tank is communicated with the water inlet pipe through the water pipe and the water pump, one end of the water inlet pipe is communicated with the water inlet of the condensing pipe, the water outlet of the condensing pipe is communicated with one end of the water outlet pipe, one end of each water outlet pipe is communicated with one side of the cooling water tank, one end of each radiating fin is arranged in the cooling water tank, the refrigerating fins are arranged on one side of the radiating fins, and the cooling liquid in the cooling water tank can be rapidly cooled by utilizing the radiating fins and the refrigerating fins, so that the cooling water tank has a better condensing effect compared with the traditional condensing pipe and is very convenient to use.
Drawings
FIG. 1 is a schematic structural view of the present invention;
FIG. 2 is a schematic axial view of the L-shaped fixing plate of the present invention;
FIG. 3 is a schematic sectional view of the heating cabinet of the present invention;
FIG. 4 is a schematic sectional view of the cooling water tank of the present invention;
fig. 5 is a schematic sectional structure view of the mixing tank of the present invention.
In the figure: 1. a laboratory bench; 2. a support frame; 3. an L-shaped fixing plate; 4. a distillation flask; 5. mounting grooves; 6. a heating box; 7. an electric sliding table; 8. a connecting rod; 9. a notch; 10. heating a ring; 11. fixing the rod; 12. a first connecting pipe; 13. a condenser tube; 14. a delivery pipe; 15. a support bar; 16. a water inlet pipe; 17. a water outlet pipe; 18. a cooling water tank; 19. a heat dissipating fin; 20. a refrigeration plate; 21. a water pipe; 22. a water pump; 23. a mixing tank; 24. a micro motor; 25. a stirring rod; 26. a second connecting pipe; 27. an extraction tank; 28. a discharge pipe; 29. a storage tank.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. The specific embodiments described herein are merely illustrative of the invention and do not delimit the invention. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The invention provides a simultaneous distillation and extraction device as shown in figures 1-5, which comprises an experiment table 1, a heating assembly and a cooling assembly, wherein the upper end of the experiment table 1 is fixedly connected with a support frame 2, one side of the support frame 2 is fixedly connected with an L-shaped fixing plate 3, a distillation flask 4 is fixedly clamped on the L-shaped fixing plate 3, the L-shaped fixing plate 3 comprises a transverse plate and a vertical plate, the upper end of the vertical plate of the L-shaped fixing plate 3 is fixedly connected to one side of the support frame 2, one side of the transverse plate of the L-shaped fixing plate 3 is provided with an installation groove 5, the distillation flask 4 is fixedly clamped in the installation groove 5, and the installation groove 5 is used for clamping and fixing the distillation flask 4;
the heating assembly is arranged on one side of the support frame 2, the heating assembly comprises a heating box 6, the heating box 6 is arranged on one side of the support frame 2 in a lifting way, a plurality of groups of heating rings 10 used for heating the distillation bottles 4 are arranged in the heating box 6, the inner diameters of the heating rings 10 in the heating box 6 are sequentially reduced from top to bottom, an electric sliding table 7 is fixedly arranged on one side of the support frame 2, a connecting rod 8 is fixedly connected onto a sliding block of the electric sliding table 7, one side of the heating box 6 is fixedly connected with one end of the connecting rod 8, a notch 9 is formed in the upper end of the heating box 6, the notch 9 is positioned under the distillation bottles 4, the inner diameter of the notch 9 is larger than the outer diameter of the distillation bottles 4, a fixing rod 11 is fixedly connected onto the inner wall of the heating box 6, the fixing rod 11 is set to be a high-temperature-resistant fixing rod, the heating rings 10 are fixedly arranged in the heating box 6 through the fixing rod 11, the electric sliding table 7 is utilized to drive the heating box 6 to move upwards, then according to the property of the chemical reagent, the distillation flask 4 is positioned in the specified heating ring 10, and then the heating ring 10 is used for heating the distillation flask 4, so that the distillation of the chemical reagent in the distillation flask 4 is realized, and the distillation temperature is also controlled;
a first connecting pipe 12 is communicated with the upper end of the distillation flask 4, a cooling assembly is arranged at the lower end of the support frame 2, the cooling assembly comprises a condensation pipe 13, a feed delivery pipe 14 is arranged inside the condensation pipe 13 in a penetrating manner, one end of the first connecting pipe 12 is communicated with one end of the feed delivery pipe 14, a support rod 15 is fixedly connected to one side of the support frame 2, one end of the support rod 15 is fixedly connected to the outer wall of the condensation pipe 13, the condensation pipe 13 is obliquely arranged, a water inlet and a water outlet are arranged on the condensation pipe 13, a water inlet pipe 16 is communicated with the water inlet of the condensation pipe 13, a water outlet pipe 17 is communicated with the water outlet of the condensation pipe 13, a cooling water tank 18 is fixedly arranged at the top of the support frame 2, a cooling fin 19 is arranged inside the cooling water tank 18, the upper end of the cooling fin 19 penetrates through the cooling water tank 18 and extends to the outside of the cooling water tank 18, and a refrigerating sheet 20 is arranged at one side of the cooling fin 19, the heat absorption surface of the refrigeration sheet 20 is pasted on one side of the heat dissipation fin 19, one end of the water outlet pipe 17 is communicated with one side of the cooling water tank 18, one side of the cooling water tank 18 is communicated with a water pipe 21, a water pump 22 is fixedly mounted at the upper end of the support frame 2, one end of the water pipe 21 is communicated with the water inlet end of the water pump 22, the water outlet end of the water pump 22 is communicated with one end of the water inlet pipe 16, and the cooling liquid in the cooling water tank 18 can be rapidly cooled by utilizing the heat dissipation fin 19 and the refrigeration sheet 20, so that the invention has better condensation effect compared with the traditional condensation pipe;
one end of the feed delivery pipe 14 is communicated with a mixing tank 23, the upper end of the mixing tank 23 is fixedly provided with a micro motor 24, one end of an output shaft of the micro motor 24 penetrates through the top of the mixing tank 23 and extends into the mixing tank 23, the top of the mixing tank 23 is embedded and fixed with a bearing, one end of an output shaft of the micro motor 24 is fixedly inserted into an inner ring of the bearing, one end of the output shaft of the micro motor 24 is fixedly connected with a stirring rod 25 through a coupler, the lower end of the mixing tank 23 is communicated with a second connecting pipe 26, the upper end of the experiment table 1 is provided with an extraction tank 27, one end of the second connecting pipe 26 is positioned in the extraction tank 27, one side of the mixing tank 23 is communicated with a discharge pipe 28, one end of the discharge pipe 28 is communicated with a storage tank 29, one side of the extraction tank 27 is communicated with a feed pipe in a sealing manner, one side of the storage tank 29 is communicated with a discharge pipe in a sealing manner, and valves are arranged on the outer walls of the second connecting pipe 26, the feed pipe, the discharge pipe 28 and the discharge pipe, utilize micro motor 24 to drive puddler 25 and rotate, can make the target carry out better distillation back extraction, carry final target through arranging material pipe 28 and store in carrying fat holding vessel 29, realized distilling the extraction simultaneously.
The working principle is as follows: when the device is used for carrying out distillation and extraction experiments, firstly, a chemical reagent to be distilled is placed in a distillation flask 4, an L-shaped fixing plate 3 is arranged at the lower end of a support frame 2, the distillation flask 4 is clamped and fixed on the L-shaped fixing plate 3, and a first connecting pipe 12 is communicated with a material conveying pipe 14;
then, according to the nature of the chemical reagent, the electric sliding table 7 is opened, the heating box 6 is driven to move upwards by the electric sliding table 7, so that the distillation flask 4 is positioned in the heating box 6, the distillation flask 4 is positioned at a specified position in the heating box 6, and then the distillation flask 4 is heated by the heating ring 10, so that the distillation of the chemical reagent in the distillation flask 4 is realized;
the distilled target object is conveyed to the interior of the conveying pipe 14 through the first connecting pipe 12, and as the condensing pipe 13 is arranged outside the conveying pipe 14, the target object in the conveying pipe 14 can be rapidly condensed by the condensing pipe 13, and then the condensed target object is conveyed to the mixing tank 23;
because blending tank 23 and extraction jar 27 communicate through second connecting pipe 26 to can extract the work to the target object, and when extracting, open micro motor 24, utilize micro motor 24 to drive puddler 25 and rotate, can make the target object carry out better distillation back extraction, carry final target object through arranging material pipe 28 at last and store in the fat holding vessel 29, realized distilling simultaneously and extracted.
Finally, it should be noted that: although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that modifications may be made to the embodiments or portions thereof without departing from the spirit and scope of the invention.
Claims (9)
1. The utility model provides a distill extraction device simultaneously, includes laboratory bench (1), heating element and cooling module, its characterized in that: the upper end of the experiment table (1) is fixedly connected with a support frame (2), one side of the support frame (2) is fixedly connected with an L-shaped fixing plate (3), the L-shaped fixing plate (3) is fixedly clamped with a distillation flask (4), the upper end of the distillation flask (4) is communicated with a first connecting pipe (12), the heating assembly is arranged on one side of the support frame (2), and the cooling assembly is arranged at the lower end of the support frame (2);
the heating assembly comprises a heating box (6), the heating box (6) is arranged on one side of the support frame (2) in a lifting mode, a plurality of groups of heating rings (10) used for heating the distillation bottles (4) are arranged inside the heating box (6), and the inner diameters of the heating rings (10) in the heating box (6) are sequentially reduced from top to bottom;
the cooling assembly comprises a condensation pipe (13), a material conveying pipe (14) penetrates through the condensation pipe (13), one end of the first connecting pipe (12) is communicated with one end of the material conveying pipe (14), a water inlet and a water outlet are formed in the condensation pipe (13), a water inlet pipe (16) is communicated with the water inlet of the condensation pipe (13), and a water outlet pipe (17) is communicated with the water outlet of the condensation pipe (13);
the one end intercommunication of conveying pipeline (14) has blending tank (23), the lower extreme intercommunication of blending tank (23) has second connecting pipe (26), the upper end of laboratory bench (1) is provided with extraction jar (27), the one end of second connecting pipe (26) is located the inside of extraction jar (27), one side intercommunication of blending tank (23) has row material pipe (28), the one end intercommunication of arranging material pipe (28) has holding vessel (29).
2. A simultaneous distillation extraction plant according to claim 1, characterized in that: l shape fixed plate (3) are including diaphragm and riser, the upper end fixed connection of L shape fixed plate (3) riser is in one side of support frame (2), mounting groove (5) have been seted up to one side of L shape fixed plate (3) diaphragm, retort (4) joint is fixed in the inside of mounting groove (5).
3. A simultaneous distillation extraction plant according to claim 1, characterized in that: one side fixed mounting of support frame (2) has electronic slip table (7), fixedly connected with connecting rod (8) on the sliding block of electronic slip table (7), one side of heating cabinet (6) in the one end fixed connection of connecting rod (8).
4. A simultaneous distillation extraction plant according to claim 1, characterized in that: notch (9) have been seted up to the upper end of heating cabinet (6), notch (9) are located retort (4) under, and the internal diameter of notch (9) is greater than the external diameter of retort (4), fixedly connected with dead lever (11) on the inner wall of heating cabinet (6), and dead lever (11) set up to high temperature resistance dead lever, heating collar (10) are through the inside of dead lever (11) fixed mounting in heating cabinet (6).
5. A simultaneous distillation extraction plant according to claim 1, characterized in that: one side fixedly connected with bracing piece (15) of support frame (2), the one end fixed connection of bracing piece (15) is on the outer wall of condenser pipe (13), condenser pipe (13) are the slope setting.
6. A simultaneous distillation extraction plant according to claim 1, characterized in that: the top fixed mounting of support frame (2) has cooling water tank (18), the inside of cooling water tank (18) is provided with radiating fin (19), and the upper end of radiating fin (19) runs through cooling water tank (18) and extends to the outside of cooling water tank (18), one side of radiating fin (19) is provided with refrigeration piece (20), the heat absorption face subsides of refrigeration piece (20) are applied in one side of radiating fin (19).
7. A simultaneous distillation extraction unit according to claim 6, characterized in that: the one end of outlet pipe (17) and one side intercommunication of coolant tank (18), one side intercommunication of coolant tank (18) has water pipe (21), the upper end fixed mounting of support frame (2) has water pump (22), the one end of water pipe (21) communicates in the end of intaking of water pump (22), the play water end of water pump (22) communicates with the one end of inlet tube (16).
8. A simultaneous distillation extraction plant according to claim 1, characterized in that: the utility model discloses a mixing tank, including mixing tank (23), the top of mixing tank (23) is run through to the one end of micro motor (24) output shaft, micro motor (24) upper end fixed mounting has micro motor (24), the inside of mixing tank (23) is extended to the top of micro motor (24) output shaft, the top of mixing tank (23) is inlayed and is equipped with the bearing fixedly, the fixed inner circle of pegging graft in the bearing of one end of micro motor (24) output shaft, shaft coupling fixedly connected with puddler (25) is passed through to the one end of micro motor (24) output shaft.
9. A simultaneous distillation extraction plant according to claim 1, characterized in that: one side of the extraction tank (27) is hermetically communicated with a feed pipe, one side of the storage tank (29) is hermetically communicated with a discharge pipe, and valves are arranged on the outer walls of the second connecting pipe (26), the feed pipe, the discharge pipe (28) and the discharge pipe.
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| CN202111537417.8A CN114177642A (en) | 2021-12-15 | 2021-12-15 | Simultaneous distillation and extraction device |
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| CN202111537417.8A CN114177642A (en) | 2021-12-15 | 2021-12-15 | Simultaneous distillation and extraction device |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115200213A (en) * | 2022-08-03 | 2022-10-18 | 湖南禾益元生物科技有限公司 | Heating device in phytosterol ester extraction process |
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| US20190083902A1 (en) * | 2017-09-21 | 2019-03-21 | Louis Phillip Nevitt | Plant Matter Fractional Distillation System Using Heated Air Induction into Precisely Heated Chamber to Extract a Plant's Organic Compounds Without Use of Solvents |
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