CN114133281A - Humic acid-containing water-soluble fertilizer and production method thereof - Google Patents

Humic acid-containing water-soluble fertilizer and production method thereof Download PDF

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Publication number
CN114133281A
CN114133281A CN202111230192.1A CN202111230192A CN114133281A CN 114133281 A CN114133281 A CN 114133281A CN 202111230192 A CN202111230192 A CN 202111230192A CN 114133281 A CN114133281 A CN 114133281A
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China
Prior art keywords
parts
liquid
soluble fertilizer
humic acid
vegetable
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Pending
Application number
CN202111230192.1A
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Chinese (zh)
Inventor
赵瑛
刘刚
张运晖
王枝祥
陈玉梁
冯守疆
崔明九
曾凡逵
史丽娜
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Weiyuan Lvyin Poultry Breeding Co ltd
Biotechnology Research Institute Gansu Academy Of Agricultural Sciences
Lanzhou Institute of Chemical Physics LICP of CAS
Original Assignee
Weiyuan Lvyin Poultry Breeding Co ltd
Biotechnology Research Institute Gansu Academy Of Agricultural Sciences
Lanzhou Institute of Chemical Physics LICP of CAS
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Application filed by Weiyuan Lvyin Poultry Breeding Co ltd, Biotechnology Research Institute Gansu Academy Of Agricultural Sciences, Lanzhou Institute of Chemical Physics LICP of CAS filed Critical Weiyuan Lvyin Poultry Breeding Co ltd
Priority to CN202111230192.1A priority Critical patent/CN114133281A/en
Publication of CN114133281A publication Critical patent/CN114133281A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05BPHOSPHATIC FERTILISERS
    • C05B7/00Fertilisers based essentially on alkali or ammonium orthophosphates
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/80Soil conditioners
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G5/00Fertilisers characterised by their form
    • C05G5/20Liquid fertilisers
    • C05G5/23Solutions

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Pest Control & Pesticides (AREA)
  • Soil Sciences (AREA)
  • Fertilizers (AREA)

Abstract

The invention belongs to the technical field of agricultural fertilizers, and particularly relates to a humic acid-containing water-soluble fertilizer and a production method thereof, wherein the water-soluble fertilizer is prepared from biogas slurry, potato residue homogeneous liquid, vegetable-tail vegetable fermentation liquid, mushroom polypeptide liquid, microbial polysaccharide, potassium fulvate, urea, monopotassium phosphate and vitamin B complex in parts by weight as follows: 10 parts of biogas slurry, 8 parts of potato residue homogenizing liquid, 5 parts of vegetable tail fermentation liquid, 6 parts of mushroom polypeptide liquid, 2 parts of microbial polysaccharide, 3 parts of potassium fulvate, 12 parts of urea, 22 parts of monopotassium phosphate and 1 part of compound vitamin B. The water-soluble fertilizer is rich in biogas slurry, humic acid, nitrogen, phosphorus, potassium and other major elements, is balanced in nutrition, can improve soil properties, provides comprehensive nutrient elements for crop growth, promotes crop growth, can effectively improve crop yield and quality, can be widely used for cultivation of crops such as sweet sorghum, ryegrass and highland barley, improves yield by 10-25%, and has good popularization and application prospects.

Description

Humic acid-containing water-soluble fertilizer and production method thereof
Technical Field
The invention belongs to the technical field of agricultural fertilizers, and particularly relates to a humic acid-containing water-soluble fertilizer and a production method thereof.
Background
Soil is a loose soil surface layer for crop growth, and fertility is the basic characteristic of soil. The basic soil traits affecting fertility are many, and the main traits are as follows: the thickness of the soil plough layer, the texture and the structure of the plough layer soil, the content of organic matters in the soil, the content of nutrients such as nitrogen, phosphorus and potassium in the soil, the pH value of the soil and the like. In the current domestic cultivated soil, the fertility level is low, the physical and chemical properties of the soil are poor, the saline-alkali hardening condition is serious, and the low-yield soil with low crop yield accounts for about 30 percent. Especially, the crop fertilization is mainly performed by chemical fertilizers, and due to long-term excessive or unreasonable application of the chemical fertilizers, various nutrition proportions in soil are disordered, soil hardening is caused, and the utilization rate of the fertilizers and the quality of agricultural products are reduced.
The humic acid type fertilizer contains two main types of humic acid, namely fulvic acid and fulvic acid, integrates crop nutrition conditioning and soil structure conditioning into one fertilizer, has the effects of improving soil, enhancing fertilizer efficiency, stimulating crop growth and the like, has important effects in the aspects of enhancing crop stress resistance, cultivating seed development, increasing soil field water holding capacity, promoting growth of beneficial microorganisms in soil, inhibiting generation of pathogenic microorganisms, improving soil micro-ecological environment and the like, and is increasingly valued. Therefore, the production method of the humic acid-containing water-soluble fertilizer and the product produced by the same are developed, the low-yield soil is improved, and the method has important significance for realizing balanced yield increase of agriculture and accelerating agricultural modernization.
In the prior art and the water-soluble fertilizer containing humic acid, the humic acid only contains humic acid and trace elements, nitrogen, phosphorus and potassium elements necessary for crop growth are lacked, and the nutrition is incomplete. Compared with patent 1, the production method of the humic acid water-soluble fertilizer (application number CN201811512273.9) has the advantages that calcium, ferrous sulfate, manganese sulfate and the like in the formula are easy to precipitate in the mixing process, so that caking is caused and the fertilizer efficiency is reduced. In comparison with patent 2, a water-soluble fertilizer containing high-concentration humic acid and a preparation method thereof (patent No. 201310357167.9), the formula of the water-soluble fertilizer contains potassium acetate and borax, and the mixture is heated and stirred to obtain a mixed solution which is easy to react after being cooled to cause the loss of effective components.
Disclosure of Invention
Aiming at the problems and the defects in the prior art, the invention provides the humic acid-containing water-soluble fertilizer which is reasonable in preparation, easy to prepare, capable of enhancing the fertilizer efficiency, improving the soil, easy to absorb by crops, stimulating the growth of the crops and improving the quality of agricultural products.
The invention also aims to provide a production method of the humic acid-containing water-soluble fertilizer.
In order to achieve the purpose, the invention provides the following technical scheme:
a water-soluble fertilizer containing humic acid is prepared from biogas slurry, potato residue homogenizing liquid, vegetable-tailed vegetable fermentation liquid, mushroom polypeptide liquid, microbial polysaccharide, potassium fulvate, urea, monopotassium phosphate and vitamin B complex according to the following weight part ratios: 10 parts of biogas slurry, 8 parts of potato residue homogenizing liquid, 5 parts of vegetable tail fermentation liquid, 6 parts of mushroom polypeptide liquid, 2 parts of microbial polysaccharide, 3 parts of potassium fulvate, 12 parts of urea, 22 parts of monopotassium phosphate and 1 part of compound vitamin B.
A production method of a humic acid-containing water-soluble fertilizer comprises the steps of weighing 2 parts of microbial polysaccharide, 3 parts of potassium fulvate, 12 parts of urea, 22 parts of monopotassium phosphate and 1 part of compound vitamin B according to the weight parts, uniformly mixing and crushing the raw materials to obtain a mixture A, automatically quantitatively packaging the mixture A into plastic bottles with the powder content of 40-65% in each bottle, homogenizing a mixed solution of 10 parts of biogas slurry, 8 parts of potato residue homogenized liquid, 5 parts of vegetable tail vegetable fermentation liquid and 6 parts of mushroom polypeptide liquid to obtain a mixture B, filling the mixture B into the plastic bottles with the content of 40-65%, and uniformly mixing to obtain a biogas slurry humic acid water-soluble fertilizer finished product.
Furthermore, the biogas slurry is brown clear liquid formed by fermenting organic substances such as livestock and poultry manure, quinoa straws, sweet sorghum straws and the like through biogas.
Further, the potato residue homogeneous liquid is a slurry obtained by adding pectinase into the waste residue obtained after processing the potato starch to decompose a fermentation product, and homogenizing under high pressure.
Furthermore, the vegetable tail fermentation liquid is a slurry obtained by adding cellulase into vegetable tail for decomposition, performing vacuum filtration on a fermentation product, and homogenizing filtrate under high pressure.
Furthermore, the mushroom polypeptide liquid is a slurry obtained by crushing mushroom sticks of waste agaricus bisporus, tricholoma matsutake and the like, adding protease and cellulase for decomposition, filtering a fermentation product, and filtering the filtrate to homogenize the filtrate under high pressure.
Further, the vitamin B complex is prepared by mixing VB6, VB2 and VB1 in a ratio of 1:2:2 by weight.
Compared with the prior art, the invention has the beneficial effects that:
the water-soluble fertilizer is used by 4-12kg per mu, is uniformly mixed by adding water to form 500-fold liquid spraying of 800-fold, is reasonable in proportion, is dissolved or diluted by water to form the water-soluble fertilizer, is sprayed on leaf surfaces, can improve soil properties, provides comprehensive nutrient elements for crop growth, promotes crop growth, and can effectively improve crop yield and quality.
Detailed Description
The present invention will be described in detail with reference to the following embodiments.
Example 1
A water-soluble fertilizer containing humic acid is prepared from biogas slurry, potato residue homogenizing liquid, vegetable-tailed vegetable fermentation liquid, mushroom polypeptide liquid, microbial polysaccharide, potassium fulvate, urea, monopotassium phosphate and vitamin B complex according to the following weight part ratios: 100 kg of biogas slurry, 80 kg of potato residue homogeneous liquid, 50kg of vegetable tail vegetable fermentation liquid, 60 kg of mushroom polypeptide liquid, 20kg of microbial polysaccharide, 30kg of potassium fulvate, 120kg of urea, 220kg of monopotassium phosphate and 10kg of compound vitamin B.
The production method of the humic acid-containing water-soluble fertilizer comprises the following steps of weighing 20kg of microbial polysaccharide, 30kg of potassium fulvate, 120kg of urea, 220kg of monopotassium phosphate and 10kg of compound vitamin B respectively, mixing, crushing, uniformly stirring to obtain a mixture A, feeding the mixture A into a solid powder quantitative packaging machine for automatic quantitative packaging and filling into plastic bottles, wherein 65% of each bottle is filled in each plastic bottle, then weighing 100 kg of biogas slurry, 80 kg of potato residue homogeneous liquid, 50kg of vegetable tail vegetable fermentation liquid and 60 kg of mushroom polypeptide liquid respectively, mixing uniformly in a homogenizer to form a mixture B, filling the mixture B into the plastic bottles with the loading of 65%, filling and uniformly mixing to obtain a biogas slurry humic acid water-soluble fertilizer finished product.
12kg of the humic acid water-soluble fertilizer produced in the embodiment 1 is used per mu, water is added, the mixture is uniformly stirred to form 800 times of liquid, and the liquid is sprayed, wherein the humic acid water-soluble fertilizer product is used for increasing the yield of sweet sorghum crops by 25.12%, increasing the yield of highland barley by 20.61% and increasing the yield of buckwheat by 15.43%. The yield of the contrast sweet sorghum is increased by 1.35%, the yield of the highland barley is increased by 1.62%, and the yield of the buckwheat is increased by 1.27%.
Example 2
A water-soluble fertilizer containing humic acid is prepared from biogas slurry, potato residue homogenizing liquid, vegetable-tailed vegetable fermentation liquid, mushroom polypeptide liquid, microbial polysaccharide, potassium fulvate, urea, monopotassium phosphate and vitamin B complex according to the following weight part ratios: 100 kg of biogas slurry, 80 kg of potato residue homogeneous liquid, 50kg of vegetable tail vegetable fermentation liquid, 60 kg of mushroom polypeptide liquid, 20kg of microbial polysaccharide, 30kg of potassium fulvate, 120kg of urea, 220kg of monopotassium phosphate and 10kg of compound vitamin B.
The production method of the humic acid-containing water-soluble fertilizer comprises the following steps of weighing 20kg of microbial polysaccharide, 30kg of potassium fulvate, 120kg of urea, 220kg of monopotassium phosphate and 10kg of compound vitamin B respectively, mixing, crushing, uniformly stirring to obtain a mixture A, feeding the mixture A into a solid powder quantitative packaging machine for automatic quantitative packaging and filling into plastic bottles, wherein the content of each plastic bottle is 58%, then weighing 100 kg of biogas slurry, 80 kg of potato residue homogeneous liquid, 50kg of vegetable tail vegetable fermentation liquid and 60 kg of mushroom polypeptide liquid respectively, mixing uniformly in a homogenizer to form a mixture B, filling the mixture B into the plastic bottles with the loading of 58%, filling and uniformly mixing to obtain the biogas slurry humic acid water-soluble fertilizer finished product.
8kg of the humic acid water-soluble fertilizer in the embodiment 2 is added with water and stirred uniformly to form 600 times of liquid for spraying, and the humic acid water-soluble fertilizer is used for increasing the yield of the sweet sorghum crops by 22.13%, the yield of the highland barley by 18.42% and the yield of the buckwheat by 13.63%. The yield of the contrast sweet sorghum is increased by 1.35%, the yield of the highland barley is increased by 1.62%, and the yield of the buckwheat is increased by 1.27%.
Example 3
A water-soluble fertilizer containing humic acid is prepared from biogas slurry, potato residue homogenizing liquid, vegetable-tailed vegetable fermentation liquid, mushroom polypeptide liquid, microbial polysaccharide, potassium fulvate, urea, monopotassium phosphate and vitamin B complex according to the following weight part ratios: 100 kg of biogas slurry, 80 kg of potato residue homogeneous liquid, 50kg of vegetable tail vegetable fermentation liquid, 60 kg of mushroom polypeptide liquid, 20kg of microbial polysaccharide, 30kg of potassium fulvate, 120kg of urea, 220kg of monopotassium phosphate and 10kg of compound vitamin B.
The production method of the humic acid-containing water-soluble fertilizer comprises the following steps of weighing 20kg of microbial polysaccharide, 30kg of potassium fulvate, 120kg of urea, 220kg of monopotassium phosphate and 10kg of compound vitamin B respectively, mixing, crushing, uniformly stirring to obtain a mixture A, feeding the mixture A into a solid powder quantitative packaging machine for automatic quantitative packaging and filling into plastic bottles, wherein 40% of the plastic bottles are filled, then weighing 100 kg of biogas slurry, 80 kg of potato residue homogeneous liquid, 50kg of vegetable tail vegetable fermentation liquid and 60 kg of mushroom polypeptide liquid respectively, mixing uniformly in a homogenizer to form a mixture B, filling the mixture B into the plastic bottles with the filling amount of 40%, filling and uniformly mixing to obtain the finished product of the biogas slurry humic acid water-soluble fertilizer.
4kg of the humic acid water-soluble fertilizer in the embodiment 3 is added with water and stirred uniformly to form 500 times of liquid for spraying, and the humic acid water-soluble fertilizer is used for increasing the yield of the sweet sorghum crops by 20.32%, increasing the yield of the highland barley by 15.24% and increasing the yield of the buckwheat by 10.51%. The yield of the contrast sweet sorghum is increased by 1.35%, the yield of the highland barley is increased by 1.62%, and the yield of the buckwheat is increased by 1.27%.
In the above examples 1-3, the water soluble fertilizer product is used for increasing the yield of the sweet sorghum crop by 20-25%, increasing the yield of the highland barley by 15-20% and increasing the yield of the buckwheat by 10-15%.

Claims (7)

1. The water-soluble fertilizer containing humic acid is characterized by being prepared from biogas slurry, potato residue homogenized liquid, vegetable-tailed vegetable fermentation liquid, mushroom polypeptide liquid, microbial polysaccharide, potassium fulvate, urea, monopotassium phosphate and vitamin B complex in parts by weight as follows: 10 parts of biogas slurry, 8 parts of potato residue homogenizing liquid, 5 parts of vegetable tail fermentation liquid, 6 parts of mushroom polypeptide liquid, 2 parts of microbial polysaccharide, 3 parts of potassium fulvate, 12 parts of urea, 22 parts of monopotassium phosphate and 1 part of compound vitamin B.
2. A production method of a humic acid-containing water-soluble fertilizer is characterized by comprising the steps of weighing 2 parts of microbial polysaccharide, 3 parts of potassium fulvate, 12 parts of urea, 22 parts of monopotassium phosphate and 1 part of compound vitamin B according to the weight parts, uniformly mixing and crushing to obtain a mixture A, automatically quantitatively packaging and filling the mixture A into plastic bottles with the filling amount of 40-65% by weight, homogenizing a mixed solution of 10 parts of biogas slurry, 8 parts of potato residue homogenized solution, 5 parts of vegetable tail vegetable fermentation solution and 6 parts of mushroom polypeptide solution to obtain a mixture B, filling the mixture B into the plastic bottles with the filling amount of 40-65% and uniformly mixing to obtain a biogas slurry humic acid water-soluble fertilizer finished product.
3. The method for producing the humic acid-containing water-soluble fertilizer as claimed in claim 2, wherein the biogas slurry is a brown clear liquid formed by biogas fermentation of organic substances such as livestock and poultry manure, quinoa straw, sweet sorghum straw and the like.
4. The method for producing the humic acid-containing water-soluble fertilizer as claimed in claim 2, wherein the potato residue homogenized liquid is a slurry obtained by adding fermentation products obtained by decomposing the waste residues obtained by processing the potato starch with pectinase and homogenizing the fermentation products under high pressure.
5. The method for producing the humic acid-containing water-soluble fertilizer as claimed in claim 2, wherein the vegetable-tail fermentation liquid is a slurry obtained by vacuum-filtering a fermentation product obtained by decomposing vegetable-tail with cellulase and homogenizing the filtrate under high pressure.
6. The method for producing a humic acid-containing water-soluble fertilizer as claimed in claim 2, wherein the mushroom polypeptide liquid is a slurry obtained by crushing mushroom sticks such as waste agaricus bisporus, tricholoma matsutake and the like, adding a fermentation product obtained by decomposing protease and cellulase, filtering, and homogenizing the filtered juice under high pressure.
7. The production method of the humic acid-containing water-soluble fertilizer as claimed in claim 2, wherein the vitamin B complex is prepared by mixing powder VB6, powder VB2 and powder VB1 in a weight ratio of 1:2: 2.
CN202111230192.1A 2021-10-22 2021-10-22 Humic acid-containing water-soluble fertilizer and production method thereof Pending CN114133281A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116789503A (en) * 2023-07-13 2023-09-22 古浪法麦克斯农业服务有限公司 Special water-soluble fertilizer for topdressing of onions

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101885627A (en) * 2010-06-26 2010-11-17 甘肃省农业科学院生物技术研究所 Method for producing liquid bio-fertilizer from potato cell sap
CN105967798A (en) * 2016-05-06 2016-09-28 南宁绿智环保科技有限公司 Balanced humic acid-containing alkaline liquid fertilizer and preparation method thereof
CN107954798A (en) * 2017-11-25 2018-04-24 贵阳开磷化肥有限公司 A kind of special Water soluble fertilizer containing humic acid of trickle irrigation rice and preparation method thereof
CN108558499A (en) * 2018-04-09 2018-09-21 山东省农业科学院农业资源与环境研究所 A kind of compound formulation for melon crop of the extract containing edible fungi residue
CN113185342A (en) * 2021-03-30 2021-07-30 仲恺农业工程学院 Method and device for producing efficient organic liquid fertilizer by using waste vegetables

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101885627A (en) * 2010-06-26 2010-11-17 甘肃省农业科学院生物技术研究所 Method for producing liquid bio-fertilizer from potato cell sap
CN105967798A (en) * 2016-05-06 2016-09-28 南宁绿智环保科技有限公司 Balanced humic acid-containing alkaline liquid fertilizer and preparation method thereof
CN107954798A (en) * 2017-11-25 2018-04-24 贵阳开磷化肥有限公司 A kind of special Water soluble fertilizer containing humic acid of trickle irrigation rice and preparation method thereof
CN108558499A (en) * 2018-04-09 2018-09-21 山东省农业科学院农业资源与环境研究所 A kind of compound formulation for melon crop of the extract containing edible fungi residue
CN113185342A (en) * 2021-03-30 2021-07-30 仲恺农业工程学院 Method and device for producing efficient organic liquid fertilizer by using waste vegetables

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116789503A (en) * 2023-07-13 2023-09-22 古浪法麦克斯农业服务有限公司 Special water-soluble fertilizer for topdressing of onions

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Application publication date: 20220304