CN114010544B - 一种涂抹型面膜及其制备方法 - Google Patents
一种涂抹型面膜及其制备方法 Download PDFInfo
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Abstract
本发明提供一种涂抹型面膜及其制备方法,所述涂抹型面膜包括水相、油相和增稠剂;以所述涂抹型面膜的总质量为基准计,所述水相的含量为60~84.9wt%、所述油相的含量为15~39.9wt%和所述增稠剂的含量为0.1~2wt%。其通过调节油相和水相的比例,使得面膜在涂敷至皮肤表面后,10~15分钟内从乳白色膏状变成透明,并且洗去的时候又可以二次乳化,易于清洗,从而达到清洁肌肤的作用。
Description
技术领域
本发明涉及护肤品领域,特别是涉及一种涂抹型面膜及其制备方法。
背景技术
涂抹面膜可分为:睡眠面膜、泥类面膜、霜状类面膜等。
涂抹面膜是近年来增长速度非常快的个人护肤单品之一。尤其是疫情之后,宅家精细化美容的兴起,让涂抹面膜越来越受年轻消费者的喜爱。数据显示,2020年1到7月,天猫国际平台上涂抹面膜销售同比增长超400%,成交占面膜品类超三分之一。
如今,随着电子商务的蒸蒸日上,主要的推广渠道为网络直播、短视频,这些渠道对产品的要求的最大特点是,可视化,有趣味,简单逻辑。一般的涂抹面膜是取料体厚涂在脸部,15分钟后洗去,这个过程在宏观视觉效果上几乎是没有任何变化的,无法引起消费者对产品的兴趣。
发明内容
鉴于以上所述现有技术的缺点,本发明的目的在于提供一种涂抹型面膜及其制备方法,其在涂敷至面部后,15分钟内由乳白色渐变成透明的油膜状,用于解决现有技术中的问题。
为实现上述目的及其他相关目的,本发明是通过以下技术方案获得的。
本发明提供一种涂抹型面膜,包括水相、油相和增稠剂;以所述涂抹型面膜的总质量为基准计,所述水相的含量为60~84.9wt%、所述油相的含量为15~39.9wt%和所述增稠剂的含量为0.1~2wt%。
优选地,所述涂抹型面膜在使用时15分钟内由乳白色变成透明色,且洗去时可以二次乳化。
优选地,所述增稠剂的含量为0.25wt%~0.55wt%。此时,所述水相的含量为60~84.75wt%,所述油相的含量为15~39.75wt%。
如,所述水相的含量可以为60wt%、61wt%、62wt%、63wt%、64wt%、65wt%、66wt%、67wt%、68wt%、69wt%、70wt%、71wt%、72wt%、73wt%、74wt%、75wt%、76wt%、77wt%、78wt%、79wt%、80wt%、81wt%、82wt%、83wt%或84wt%。
再如,所述油相的含量为15wt%、16wt%、17wt%、18wt%、19wt%、20wt%、21wt%、22wt%、23wt%、24wt%、25wt%、26wt%、27wt%、28wt%、29wt%、30wt%、31wt%、32wt%、33wt%、34wt%、35wt%、36wt%、37wt%、38wt%或39wt%。
再如,所述增稠剂的含量可以为0.25wt%、0.26wt%、0.27wt%、0.28wt%、0.29wt%、0.30wt%、0.31wt%、0.32wt%、0.33wt%、0.34wt%、0.35wt%、0.36wt%、0.37wt%、0.38wt%、0.39wt%、0.40wt%、0.41wt%、0.42wt%、0.43wt%、0.44wt%、0.45wt%、0.46wt%、0.47wt%、0.48wt%、0.49wt%、0.50wt%、0.51wt%、0.52wt%、0.53wt%、0.54wt%或0.55wt%。
优选地,所述水相至少包括多元醇、防腐剂和亲水性乳化剂。更优选地,所述水相还包括选自保湿剂和螯合剂中的一种或两种。
优选地,所述油相至少包括合成油和亲油乳化剂。更优选地,所述油相还包括选自矿物油、植物油和抗氧剂中的一种或多种。
优选地,所述增稠剂选自卡波姆、聚丙烯酸类和黄原胶中的一种或多种。优选地,所述聚丙烯酸类选自聚丙烯酸钠、丙烯酸(酯)类/C10-30烷醇丙烯酸酯交联聚合物中的一种或两种。
优选地,所述水相中含有5~15重量份的多元醇、0.5~3重量份的防腐剂、1~5重量份的亲水乳化剂和50~75重量份的水。更优选地,所述多元醇为8~12重量份。更优选地,所述水为55~70重量份。
如,所述水相中多元醇的含量为8重量份、9重量份、10重量份、11重量份或12重量份。
如,所述水相中防腐剂的含量为0.5重量份、1重量份、1.5重量份、2重量份、2.5重量份或3重量份。
如,所述水相中亲水乳化剂的含量为1重量份、2重量份、3重量份、4重量份或5重量份。
如,所述水相中水的含量为55重量份、56重量份、57重量份、58重量份、59重量份、60重量份、61重量份、62重量份、63重量份、64重量份、65重量份、66重量份、67重量份、68重量份、69重量份或70重量份。
优选地,所述油相中含有5~30重量份的合成油和5~10重量份的亲油乳化剂。更优选地,所述合成油的含量为8~15重量份。
如,所述油相中合成油的含量为8重量份、9重量份、10重量份、11重量份、12重量份、13重量份、14重量份或15重量份。
再如,所述油相中亲油乳化剂的含量为5重量份、6重量份、7重量份、8重量份、9重量份或10重量份。
优选地,所述多元醇选自甘油、丁二醇、丙二醇、戊二醇和己二醇中的一种或多种。
优选地,所述保湿剂选自植物多糖、甜菜碱和尿素中的一种或多种。更优选地,所述植物多糖选自海藻多糖、银耳多糖和黄芪多糖中的一种或两种。优选地,以所述涂抹型面膜的总质量为基准计,所述保湿剂为1~3wt%。
优选地,所述防腐剂为水溶性防腐剂。更优选地,所述防腐剂为选自苯氧乙醇和乙基己基甘油中的一种或两种。优选地,以所述涂抹型面膜的总质量为基准计,所述防腐剂为0.1~3wt%。更优选地,以所述涂抹型面膜的总质量为基准计,所述防腐剂为0.2~0.5wt%,如可以为0.2wt%、0.3wt%、0.4wt%或0.5wt%。
优选地,所述螯合剂为EDTA盐和对羟基苯乙酮中的一种或两种。优选地,以所述涂抹型面膜的总质量为基准计,所述螯合剂为0.2~0.6wt%,如可以为0.2wt%、0.3wt%、0.4wt%、0.5wt%或0.6wt%。
优选地,所述亲水性乳化剂选自聚醚类乳化剂、聚山梨醇类乳化剂和阴离子乳化剂中的一种或多种。更优选地,所述聚醚类乳化剂选自鲸蜡硬脂醇聚醚-20和鲸蜡醇聚醚-21中的一种或两种。更优选地,所述聚山梨醇类乳化剂选自聚山梨醇-20、聚山梨醇-60和聚山梨醇-80中的一种或多种。
优选地,所述矿物油选自白油和凡士林中的一种或多种。优选地,以所述涂抹型面膜的总质量为基准计,所述矿物油不超过5wt%,如可以为1wt%、1.5wt%、2wt%、2.5wt%、3wt%、3.5wt%、4wt%、4.5wt%或5wt%。
优选地,所述植物油选自橄榄油和霍霍巴油中的一种或两种。优选地,以所述涂抹型面膜的总质量为基准计,所述植物油为4~8wt%,如可以为4wt%、5wt%、6wt%、7wt%或8wt%。
优选地,所述合成油选自辛酸/癸酸甘油三酯和聚二甲基硅氧烷中的一种或两种。
优选地,所述亲油乳化剂选自甘油硬脂酸脂、硬脂醇、山嵛醇、棕榈醇和鲸蜡硬脂醇中的一种或多种。
优选地,所述抗氧剂选自维生素E或维生素E醋酸酯。优选地,以所述涂抹型面膜的总质量为基准计,抗氧剂为0.1wt%~0.5wt%,如可以为0.1wt%、0.2wt%、0.3wt%、0.4wt%或0.5wt%。
本发明还公开了如上述所述的涂抹型面膜的制备方法,包括如下步骤:将各组分混合。
优选地,先将水相和油相分别混合,再将水相和油相混合,然后加入增稠剂混合。优选地,水相和油相的混合为在70~80℃下进行。
优选地,加入增稠剂混合的温度为45~55℃。
优选地,加入增稠剂混合完成后降温至室温。
本发明上述技术方案的技术效果:
本发明上述技术方案形成的涂抹型面膜,其通过调节油相和水相的比例,使得面膜在涂敷至皮肤表面后,10~15分钟内从乳白色膏状变成透明,并且洗去的时候又可以二次乳化,易于清洗,从而达到清洁肌肤的作用。进一步地,这种涂敷后变色特性非常有商业价值和实际的使用价值。从商业角度来说,这一性能能增加产品的可视化和趣味性,与目前的短视频和直播营销方式更加契合,吸引消费者的关注度,更加直观的理解产品的功效,比如吸收,吸附,提亮等;从实际使用角度来说,增加了体验感,使得消费者不用计时或者看时间,而仅仅通过面膜是否变成透明的状态就可以判断是否已经到洗去时间,增加了衡量时间的维度,特别适合不方便或者容易忘记计时的消费者使用,从而通过适合的涂敷时间发挥面膜应用的最佳功效。
具体实施方式
在进一步描述本发明具体实施方式之前,应理解,本发明的保护范围不局限于下述特定的具体实施方案;还应当理解,本发明实施例中使用的术语是为了描述特定的具体实施方案,而不是为了限制本发明的保护范围。下列实施例中未注明具体条件的试验方法,通常按照常规条件,或者按照各制造商所建议的条件。
当实施例给出数值范围时,应理解,除非本发明另有说明,每个数值范围的两个端点以及两个端点之间任何一个数值均可选用。除非另外定义,本发明中使用的所有技术和科学术语与本技术领域技术人员通常理解的意义相同。除实施例中使用的具体方法、设备、材料外,根据本技术领域的技术人员对现有技术的掌握及本发明的记载,还可以使用与本发明实施例中所述的方法、设备、材料相似或等同的现有技术的任何方法、设备和材料来实现本发明。
本申请中提供的涂抹型面膜在在使用时15分钟内由乳白色变成透明色,且洗去时可以二次乳化。在使用时,在皮肤表面的涂抹量可以为0.1~5g/cm2,在下述实施例和对比例中,涂抹量均采用2g/cm2。
对比例1
本实施例中涂抹型面膜的配方如下:
制备方法包括如下步骤:
1)将油相混合、水相混合,分别加热到75~80℃,待用;
2)将油相和水相混合以乳化,均质速度1000转/分钟,均质5分钟;
3)50℃加入增稠剂,均质均匀;
4)低温冷却至35℃,出料检验。
本实施例中获得的涂抹型面膜,经进行实验,其能够完成乳化,也能够形成霜状类的涂抹面膜,但是在15分钟内,无法由乳白色变成透明。
对比例2
本实施例中涂抹型面膜的配方如下:
本实施例中涂抹型面膜的制备方法包括如下步骤:
1)将油相混合、水相混合,然后分别加热到75℃,待用;
2)将油相和水相混合以乳化,均质速度2000转/分钟,均质5分钟;
3)50℃加入增稠剂,均质均匀;
4)低温冷却至35℃,出料检验。
本实施例中涂抹型面膜的经实验,其能够能完成部分乳化,能形成霜状类的涂抹面膜;但是在15分钟内,无法由乳白变透明。且油膜感非常强,外观上有透明感,在洗去过程中无法二次乳化。
实施例1
本实施例中涂抹型面膜的配方如下:
本实施例中制备方法包括如下步骤:
1)将油相混合、水相混合,并分别加热到75~80℃,待用;
2)将油相和水相混合以乳化,均质速度1000~2000转/分钟,均质3~5分钟;
3)50℃加入增稠剂,均质均匀;
4)低温冷却至35℃,出料检验。
本实施例中获得的涂抹型面膜的实验效果如下:其能够完成部分乳化,能形成霜状类的涂抹面膜,可在15分钟内,由乳白变透明。并且洗去的时候又可以二次乳化,易于清洗,从而达到清洁肌肤的作用。
实施例2
本实施例中涂抹型面膜的配方如下:
本实施例中制备方法包括如下步骤:
1)将油相混合、水相混合,并分别加热到75℃,待用;
2)将油相和水相混合以乳化,均质速度2000转/分钟,均质5分钟;
3)50℃加入增稠剂,均质均匀;
4)低温冷却至35℃,出料检验。
本实施例中获得的涂抹型面膜的实验效果如下:其能够完成部分乳化,能形成霜状类的涂抹面膜,可在15分钟内,由乳白变透明。并且洗去的时候又可以二次乳化,易于清洗,从而达到清洁肌肤的作用。
实施例3
本实施例中涂抹型面膜的配方如下:
本实施例中制备方法包括如下步骤:
1)将油相混合、水相混合,并分别加热到80℃,待用;
2)将油相和水相混合以乳化,均质速度2000转/分钟,均质5分钟;
3)50℃加入增稠剂,均质均匀;
4)低温冷却至35℃,出料检验。
本实施例中获得的涂抹型面膜的实验效果如下:其能够完成部分乳化,能形成霜状类的涂抹面膜,可在15分钟内,由乳白变透明。并且洗去的时候又可以二次乳化,易于清洗,从而达到清洁肌肤的作用。
上述实施例仅例示性说明本发明的原理及其功效,而非用于限制本发明。任何熟悉此技术的人士皆可在不违背本发明的精神及范畴下,对上述实施例进行修饰或改变。因此,举凡所属技术领域中具有通常知识者在未脱离本发明所揭示的精神与技术思想下所完成的一切等效修饰或改变,仍应由本发明的权利要求所涵盖。
Claims (8)
1.一种涂抹型面膜,其特征在于,包括水相、油相和增稠剂;以所述涂抹型面膜的总质量为基准计,所述水相的含量为60~84.9wt%、所述油相的含量为15~39.9wt%和所述增稠剂的含量为0.1~2wt%;所述水相包括多元醇、防腐剂和亲水性乳化剂;所述油相包括合成油和亲油乳化剂;所述油相还包括选自矿物油、植物油和抗氧剂中的一种或多种;所述水相中含有5~15重量份的多元醇、0.5~3重量份的防腐剂、1~5重量份的亲水乳化剂和50~75重量份的水;所述油相中含有5~30重量份的合成油和5~10重量份的亲油乳化剂;所述合成油选自辛酸/癸酸甘油三酯和聚二甲基硅氧烷中的一种或两种;所述亲油乳化剂选自甘油硬脂酸脂、硬脂醇、山嵛醇、棕榈醇和鲸蜡硬脂醇中的一种或多种;所述亲水性乳化剂选自聚醚类乳化剂和聚山梨醇类乳化剂中的一种或两种;所述涂抹型面膜在使用时15分钟内由乳白色变成透明色,且洗去时可以二次乳化。
2.根据权利要求1所述的涂抹型面膜,其特征在于,所述增稠剂选自卡波姆、聚丙烯酸类和黄原胶中的一种或多种;
和/或,所述多元醇选自甘油、丁二醇、丙二醇、戊二醇和己二醇中的一种或多种;
和/或,所述水相还包括保湿剂和螯合剂中的一种或两种;
和/或,所述防腐剂为水溶性防腐剂。
3.根据权利要求2所述的涂抹型面膜,其特征在于,所述聚丙烯酸类选自聚丙烯酸钠和丙烯酸(酯)类/C10-30 烷醇丙烯酸酯交联聚合物中的一种或两种。
4.根据权利要求2所述的涂抹型面膜,其特征在于,所述防腐剂为选自苯氧乙醇和乙基己基甘油中的一种或两种;
和/或,所述保湿剂选自植物多糖、甜菜碱和尿素中的一种或多种;
和/或,所述螯合剂为EDTA盐和对羟基苯乙酮中的一种或两种。
5.根据权利要求1所述的涂抹型面膜,其特征在于,所述矿物油选自己二醇和凡士林中的一种或多种;
和/或,所述植物油选自橄榄油和霍霍巴油中的一种或两种;
和/或,所述抗氧剂选自维生素E或维生素E醋酸酯。
6.一种如权利要求1~5任一项所述的涂抹型面膜的制备方法,其特征在于,将各组分混合均匀。
7.根据权利要求6所述的制备方法,其特征在于,先将水相和油相分别混合,再将水相和油相混合,然后加入增稠剂混合。
8.根据权利要求6所述的制备方法,其特征在于,水相和油相的混合为在70~80℃下进行;
和/或,加入增稠剂混合的温度为45~55℃;和/或,加入增稠剂混合完成后降温至室温。
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