CN113941384A - Capsule type secondary centrifuge tube capable of being applied to rapid nondestructive analysis - Google Patents

Capsule type secondary centrifuge tube capable of being applied to rapid nondestructive analysis Download PDF

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Publication number
CN113941384A
CN113941384A CN202111381378.7A CN202111381378A CN113941384A CN 113941384 A CN113941384 A CN 113941384A CN 202111381378 A CN202111381378 A CN 202111381378A CN 113941384 A CN113941384 A CN 113941384A
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China
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solid
centrifugal
solid bottom
column body
centrifuge tube
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CN202111381378.7A
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CN113941384B (en
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朱文文
郁川
柴骏
孙风俭
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Luoyang Vocational and Technical College
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Luoyang Vocational and Technical College
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01LCHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
    • B01L3/00Containers or dishes for laboratory use, e.g. laboratory glassware; Droppers
    • B01L3/50Containers for the purpose of retaining a material to be analysed, e.g. test tubes
    • B01L3/502Containers for the purpose of retaining a material to be analysed, e.g. test tubes with fluid transport, e.g. in multi-compartment structures
    • B01L3/5021Test tubes specially adapted for centrifugation purposes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01LCHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
    • B01L2200/00Solutions for specific problems relating to chemical or physical laboratory apparatus
    • B01L2200/06Fluid handling related problems
    • B01L2200/0631Purification arrangements, e.g. solid phase extraction [SPE]

Abstract

The invention discloses a capsule type secondary centrifuge tube applicable to rapid nondestructive analysis, which comprises a columnar tube body, wherein a hollow bottom joint for sealing the columnar tube body is arranged outside the columnar tube body, a solid bottom joint for sealing the columnar tube body together with the hollow bottom joint is arranged outside the columnar tube body, external threads are arranged on one side of the columnar tube body, internal threads matched with the external threads are arranged inside the solid bottom joint and the hollow bottom joint, a solid bottom is arranged inside the solid bottom joint, and a filter membrane for filtering heavy metals in water body solution inside the columnar tube body and heavy metals in suspended particles is arranged on one side of the solid bottom. The method is simple to operate, does not need complex technical procedures, effectively saves the field emergency detection and analysis time of a large number of samples, and improves the working efficiency.

Description

Capsule type secondary centrifuge tube capable of being applied to rapid nondestructive analysis
Technical Field
The invention relates to the technical field of laboratory rapid analysis, in particular to a capsule type secondary centrifugal tube capable of being applied to rapid nondestructive analysis.
Background
The centrifugation method is one of the most common sample pretreatment methods in laboratories, is commonly used in chemical laboratories, biological laboratories and life science laboratories, and is used as one of the technical means for sample separation, enrichment, preparation and the like. The centrifugal technology mainly depends on different sedimentation coefficients of different substances, and achieves the purpose of substance separation under the action of a certain centrifugal force, and the most common application is sample solid-liquid separation operation. Compared with solid-liquid separation operations such as filtration and standing, the centrifugal method is widely applied to scientific research and production in industries such as biology, medicine, agriculture, bioengineering, biopharmaceutical and the like, especially in the fields of chemical analysis and pharmaceutical analysis due to convenient and rapid operation, good separation effect and convenient and easily-obtained required equipment.
In actual scientific research work, with increasingly prominent environmental problems, in order to deal with sudden heavy metal pollution events, a rapid quantitative analysis technology for on-site heavy metals needs to be developed. For a solid sample with a smooth surface, a handheld X-ray fluorescence spectrometer can complete signal response determination within 1 minute, and synchronous quantitative analysis of multiple metal parameters is realized, so that the device is widely applied to the fields of smelting, metal manufacturing, machining manufacturing, mineral deposit detection and the like. For collected environmental water samples, the content of heavy metals in a solution needs to be measured and the content information of the heavy metals in suspended particles needs to be known. If the X-ray fluorescence spectrometer is used for realizing the determination requirements, in the conventional operation, a fixed volume of an acquired environmental water sample is generally taken for field filtration, suspended particulate matters are intercepted on a filter membrane, and the filter membrane is taken for analysis by using the handheld X-ray fluorescence spectrometer, so that the content of heavy metals in the suspended particulate matters can be determined; meanwhile, adding an alkaline solution into the filtered water sample to enable metal in the solution to react with alkali to generate precipitate, filtering again, and analyzing by using a handheld X-ray fluorescence spectrometer to obtain the content of heavy metal in the water body. Although this operation can realize the detection target, when filtering turbid environment water sample, because the great water sample filtration speed of turbidity is very slow, and whole operation need carry out twice filtration, under the more condition of sample size, needs longer analysis time. Compared with filtration, centrifugation has the advantages of convenience, rapidness, good separation effect and the like. If the centrifugal method can be used for replacing filtration, the time for analyzing the sample can be greatly saved, and the working efficiency is improved.
The centrifugal tube is used as a common experimental consumable in a laboratory, has more types of commercialized centrifugal tubes, and can be divided into a large-volume centrifugal tube, a macro centrifugal tube and a micro centrifugal tube according to the capacity; according to the shape of the bottom of the centrifugal tube, the centrifugal tube can be divided into a pointed-bottom centrifugal tube, a flat-bottom centrifugal tube and a round-bottom centrifugal tube; according to the closing mode of the centrifugal tube cover, the centrifugal tube cover is divided into a gland type and a spiral type; and can be divided into plastic centrifuge tubes, stainless steel centrifuge tubes, etc. according to the material. However, in the above-mentioned analysis of the turbid environment water sample, a solid-liquid separation operation is performed using a currently commercially available centrifuge tube, and after centrifugation, the clear liquid is located at the upper part, and the suspended particles settle at the bottom of the centrifuge tube. After the supernatant is poured out, the solid at the bottom of the centrifugal tube is difficult to take out, the conditions that the sample is damaged and polluted are inevitable in the taking-out process, and even if the solid is taken out smoothly, the taken-out solid cannot be analyzed and measured by using an X-ray fluorescence spectrometer because the surface of the taken-out solid is uneven. And after alkaline solution is added into the poured supernatant to enable the metal in the solution to react with alkali to generate precipitate, the precipitate still needs to be filtered, and then can be analyzed by using a handheld X-ray fluorescence spectrometer. By doing so, the analysis operation time cannot be saved, but an unpredictable pollution risk is introduced to the analysis operation. Therefore, the centrifugal tube which can be applied to rapid nondestructive analysis is urgently needed to be designed, and the working efficiency is improved.
Disclosure of Invention
The invention aims to provide a capsule type secondary centrifugal tube applicable to rapid nondestructive analysis, so as to solve the problems in the background technology.
In order to achieve the purpose, the invention provides the following technical scheme: the utility model provides a can be applied to quick nondestructive analysis's capsule type secondary centrifuging tube, includes the column body, the outside of column body is equipped with the hollow bottom head that is used for sealed column body, the outside of column body is equipped with and carries out the solid bottom head that seals with hollow bottom head jointly to the column body, one side of column body is equipped with the external screw thread, solid bottom head all is equipped with the internal thread identical with the external screw thread with the inside of hollow bottom head, the inside of solid bottom head is equipped with at the bottom of the solid, one side at the bottom of the solid is equipped with the filter membrane that is arranged in filtering heavy metal in the inside water solution of column body and the heavy metal in the suspended particles thing.
Preferably, the outside of column body is equipped with the centrifugal sleeve that is used for loading the centrifuging tube in the centrifuge, centrifugal sleeve's inside is equipped with carries out extruded spacing subassembly to column body surface, spacing subassembly is including being located the inside turning block of centrifugal sleeve, centrifugal sleeve's inside is equipped with the confession turning block pivoted spacing groove, the inside of turning block is equipped with pivot one, the turning block includes inclined plane portion.
Preferably, one side of inclined plane portion is equipped with the centrifuging tube that carries out the lifting to the inside centrifugal sleeve and pops out the subassembly, pop out the subassembly including being located the inside stripper plate of centrifugal sleeve, one side of stripper plate is equipped with the supplementary piece that supplementary stripper plate pressed, the stripper plate can freely slide from top to bottom in the inside of centrifugal sleeve, one side of stripper plate is equipped with the connecting block, the inside of connecting block is equipped with pivot two, the outside of pivot two is equipped with the rotor plate, the inside of rotor plate is equipped with pivot three, one side of rotor plate is equipped with the connecting plate, one side of connecting plate is equipped with carries out the cambered plate that supports solid bottom end joint bottom.
Preferably, one side of the rotating block is shaped like an arc, and in the process that the cylindrical pipe body is inserted into the centrifugal sleeve, the arc part of the rotating block is in contact with the cylindrical pipe body.
Preferably, the cambered surface of the cambered plate is matched with the bottom cambered surface of the solid bottom joint.
Preferably, the solid bottom comprises a convex part, the filter membrane comprises a concave part, and one side of the convex part of the solid bottom is shaped to be matched with the shape of the concave part of the filter membrane.
Preferably, the columnar pipe body, the hollow bottom joint and the solid bottom joint are all made of polytetrafluoroethylene or polypropylene.
The invention has at least the following beneficial effects:
the invention provides a capsule type secondary centrifugal tube capable of being applied to rapid nondestructive analysis. And the operation is simple, and complex technical procedures are not needed. The device can be applied to the research of the water environment heavy metal emergency rapid monitoring and analyzing method combining centrifugation and a handheld X-ray fluorescence spectrometer, a solid sample with a flat surface is rapidly obtained through centrifugation operation, nondestructive analysis is carried out by using the handheld X-ray fluorescence spectrometer, and the rapid determination of the content of heavy metals in the environment water solution and the content of heavy metals in suspended particles is realized. The on-site emergency detection and analysis time of a large number of samples is effectively saved, and the working efficiency is improved. Provides technical support for rapid detection of sudden water body heavy metal pollution.
Drawings
FIG. 1 is a partial schematic view of the structure of the present invention;
FIG. 2 is a partial sectional view of the present invention;
FIG. 3 is a partial sectional view of the present invention;
FIG. 4 is a schematic structural view of the present invention;
FIG. 5 is a cross-sectional view of the pop-up assembly of the present invention;
FIG. 6 is a cross-sectional view of the pop-up assembly of the present invention;
FIG. 7 is an enlarged view of the structure of area A of FIG. 5 according to the present invention;
FIG. 8 is an enlarged view of the structure of the area B in FIG. 6 according to the present invention.
In the figure: 1-a columnar pipe body; 2-hollow bottom joint; 3-solid bottom joint; 4-solid bottom; 5-a filter membrane; 6-external thread; 7-internal threads; 8-a limiting component; 9-a pop-up assembly; 10-a centrifugal sleeve; 41-a boss; 51-a recess; 81-limiting groove; 82, a first rotating shaft; 83-turning block; 831-inclined plane part; 91-extruding a plate; 92-a connecting block; 93-a second rotating shaft; 94-a rotating plate; 95-rotating shaft III; 96-connecting plate; 97-arc panel; 98-auxiliary block.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Referring to fig. 1-8, the present invention provides a technical solution: a capsule type secondary centrifuge tube applicable to rapid nondestructive analysis comprises a columnar tube body 1, a hollow bottom connector 2 for sealing the columnar tube body 1 is arranged outside the columnar tube body 1, the outer part of the columnar pipe body 1 is provided with a solid bottom joint 3 which seals the columnar pipe body 1 together with the hollow bottom joint 2, an external thread 6 is arranged on one side of the columnar pipe body 1, internal threads 7 matched with the external thread 6 are arranged inside the solid bottom joint 3 and the hollow bottom joint 2, the solid bottom joint 3 and the hollow bottom joint 2 are respectively positioned at two ends of the columnar pipe body 1, and are all connected with the columnar pipe body 1 by screw thread, a solid bottom 4 is arranged inside the solid bottom joint 3, one side of the solid bottom 4 is fixedly connected with the solid bottom joint 3, and one side of the solid bottom 4 is provided with a filter membrane 5 for filtering heavy metals in the water solution and suspended particles in the columnar pipe body 1.
Before centrifugal operation, the hollow bottom connector 2 and one end of the columnar tube body 1 of the centrifugal device are quickly connected through threads, and the shape of the connected hollow bottom connector is consistent with that of a common centrifugal tube. And (4) adding the collected environmental water sample into the connected centrifugal tube in a fixed volume. A filter membrane 5 with a diameter of 25mm is placed at the platform of the inner solid bottom 4 of the solid bottom joint 3 in the device. And then the solid bottom connector 3 is quickly connected with the other end of the columnar pipe body 1. The solid bottom adapter 3 here functions similarly to the cap of a conventional centrifuge tube.
After the connection is completed, the centrifuge tube is placed in a centrifuge upside down, namely the solid bottom connector 3 is positioned at the bottom of the centrifuge tube, the hollow bottom connector 2 is positioned at the top of the centrifuge tube, and the hollow bottom connector 2 has a function similar to that of a tube cover of a common centrifuge tube. The benefit of preceding two-step operation is because the inside of solid end fitting 3 is solid, leads to the whole inside volume of centrifuging tube to diminish, so the operation then can avoid the inside volume that leads to diminishes owing to solid end fitting 3, effectively guarantees the volume of centrifugation sample.
And (3) starting the centrifugal machine to carry out centrifugal operation, completing solid-liquid separation of suspended particles in the water body sample under the action of centrifugal force, and storing the suspended particles on a built-in filter membrane 5 of a platform at the bottom of the solid bottom joint 3. At the moment, the centrifugal tube is taken out, the solid bottom connector 3 is turned upside down again, the solid bottom connector 3 is unscrewed, the built-in filter membrane 5 is taken out, the filter membrane 5 already contains suspended particles and is flat in surface, and the content information of the heavy metals in the suspended particles can be obtained by directly irradiating the filter membrane by using the handheld X-ray fluorescence spectrometer. And the sample is not destroyed and can be stored for other parameter analysis.
A new filter membrane 5 with a diameter of 25mm is taken and placed on the solid bottom 4 platform of the solid bottom joint 3. And adding a certain volume of alkaline solution into the centrifuged solution, wherein the alkaline solution reacts with metal ions in the centrifuged sample to generate flocculent precipitate. Then the solid bottom joint 3 with the new filter membrane 5 is quickly connected with the other end of the columnar pipe body 1.
After the connection is completed, the centrifuge tube is placed in the centrifuge upside down again, i.e. the solid bottom sub 3 is located at the bottom of the centrifuge tube and the hollow bottom sub 2 is located at the top of the centrifuge tube.
And (4) starting the centrifuge again to carry out secondary centrifugal operation, completing solid-liquid separation on the flocculation precipitate generated by the reaction of the metal ions in the water sample and the alkaline solution under the action of centrifugal force, and storing the flocculation precipitate on the built-in filter membrane 5 of the platform at the bottom of the solid bottom joint 3. The foregoing operation steps are repeated. Taking out the centrifuge tube, turning upside down again to make the solid bottom joint 3 face upwards, unscrewing the solid bottom joint 3, taking out the built-in filter membrane 5, obtaining the content information of the heavy metal in the flocculation precipitation by directly using the irradiation of the handheld X-ray fluorescence spectrometer, and obtaining the content of the heavy metal in the solution by volume conversion.
Through the operation, the content information of the heavy metals in the environmental water sample solution and the heavy metals in the suspended particles can be quickly obtained, and the quick monitoring and analysis of the emergency property of the heavy metals in the water environment can be realized. The whole operation process is short in time consumption, simple to operate and good in separation effect, the field emergency detection and analysis time of a large number of samples can be effectively saved, and the working efficiency is improved. Provides technical support for rapid detection of sudden water body heavy metal pollution.
The outside of column body 1 is equipped with the centrifugal sleeve 10 that is used for loading the centrifuging tube in the centrifuge, the inside of centrifugal sleeve 10 is equipped with carries out extruded spacing subassembly 8 to column body 1 surface, spacing subassembly 8 is including the turning block 83 that a plurality of intervals that are located centrifugal sleeve 10 inside equal, the inside of centrifugal sleeve 10 is equipped with a plurality of confessions turning block 83 pivoted spacing groove 81, the inside of turning block 83 is equipped with pivot 82, the both ends of pivot 82 all with centrifugal sleeve 10 fixed connection, turning block 83 rotates with pivot 82 to be connected, turning block 83 includes inclined plane portion 831, and the self material of turning block 83 is for having certain elastic rubber, inserts centrifugal sleeve 10's in-process at the centrifuging tube that the experimenter will be equipped with the water sample detection, and one side of solid bottom joint 3 will contact with turning block 83 earlier, under the elastic action of turning block 83 self, the turning block 83 will contract to the inside of spacing groove 81, until the turning block 83 crosses solid bottom head 3 completely, the turning block 83 at this moment will kick-back and extrude each direction of columnar body 1, when solid bottom head 3 slides to the bottom of centrifugation sleeve 10, the turning block 83 that every corresponds carries out spacing extrusion to columnar body 1 simultaneously, further to having increased the inside pivoted stability of centrifuging tube at centrifuge.
One side of inclined plane portion 831 is equipped with and carries out the pop-up subassembly 9 that lifts to the inside centrifuging tube of centrifugal sleeve 10, pop-up subassembly 9 is including being located the inside stripper plate 91 of centrifugal sleeve 10, one side of stripper plate 91 is equipped with the supplementary piece 98 that supplementary stripper plate 91 pressed, one side and stripper plate 91 fixed connection of supplementary piece 98, stripper plate 91 can freely slide from top to bottom in centrifugal sleeve 10 is inside, one side of stripper plate 91 is equipped with connecting block 92, one side and stripper plate 91 fixed connection of connecting block 92, the inside of connecting block 92 is equipped with two pivots 93, and the both ends of two pivots 93 all with centrifugal sleeve 10 fixed connection, the outside of two pivots 93 is equipped with rotor plate 94, and rotor plate 94 rotates with two pivots 93 to be connected, the inside of rotor plate 94 is equipped with three pivots 95, and three pivots 95 rotate to be connected, and the both ends of three pivots 95 all with the inner wall fixed connection of centrifugal sleeve 10, one side of the rotating plate 94 is provided with a connecting plate 96, one side of the connecting plate 96 is fixedly connected with the rotating plate 94, one side of the connecting plate 96 is provided with an arc panel 97 for supporting the bottom of the solid bottom connector 3, one side of the arc panel 97 is fixedly connected with the connecting plate 96, when a centrifuge tube needs to be taken out, the auxiliary block 98 can be pressed towards the bottom of the centrifuge sleeve 10, furthermore, one side of the extrusion plate 91 is abutted against the inclined plane part 831 of the rotating block 83, under the action of extrusion force, the rotating block 83 rotates upwards and enters the limiting groove 81, so that the limiting effect of the rotating block 83 on the columnar tube body 1 is eliminated, meanwhile, the extrusion plate 91 also drives the rotating plate 94 to move downwards, due to the lever principle, the connecting plate 96 on one side of the rotating shaft three 95 drives the arc panel 97 to lift upwards, so as to smoothly eject the centrifuge tube out of the centrifuge sleeve 10, thereby being more convenient for a worker to take out the centrifuge tube, the time of taking the centrifuge tube is saved, and the working efficiency is improved.
One side of the rotating block 83 is shaped like an arc, in the process that the cylindrical pipe body 1 is inserted into the centrifugal sleeve 10, the arc surface part of the rotating block 83 is in contact with the cylindrical pipe body 1, and the arc surface part of the rotating block 83 is more beneficial to inserting the solid bottom joint 3 at one end of the cylindrical pipe body 1 into the centrifugal sleeve 10.
The solid bottom 4 comprises the convex part 41, the filter membrane 5 comprises the concave part 51, one side of the convex part 41 of the solid bottom 4 is matched with the concave part 51 of the filter membrane 5 in shape, when the filter membrane 5 is replaced, the solid bottom connector 3 can be placed on a flat fixed base firstly, so that the solid bottom connector is in a vertical state with a horizontal line, the concave part 51 of the filter membrane 5 is clamped by tweezers and then vertically fed into the solid bottom connector 3 until the concave part 51 is matched with the convex part 41 of the solid bottom 4, the filter membrane 5 at the moment is positioned at the central position of the surface of the solid bottom 4, the phenomenon that the side edge of the filter membrane 5 is bent when the filter membrane 5 is replaced is reduced, the time for replacing the filter membrane 5 is further reduced, and the working efficiency is improved.
The columnar tube body 1, the hollow bottom joint 2 and the solid bottom joint 3 are all made of polytetrafluoroethylene or polypropylene, and the polytetrafluoroethylene and the polypropylene have the characteristics of acid resistance, alkali resistance, various organic solvents resistance and high temperature resistance, so that the quality of the tube body of the centrifugal tube is ensured.
It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims (7)

1. The utility model provides a can be applied to quick nondestructive analysis's capsule formula secondary centrifuging tube, includes column body (1), its characterized in that: the outside of column body (1) is equipped with hollow bottom head (2) that is arranged in sealed column body (1), the outside of column body (1) is equipped with and carries out sealed solid bottom head (3) jointly to column body (1) with hollow bottom head (2), one side of column body (1) is equipped with external screw thread (6), solid bottom head (3) all are equipped with internal thread (7) identical with external screw thread (6) with the inside of hollow bottom head (2), the inside of solid bottom head (3) is equipped with at the bottom of the solid (4), one side at the bottom of the solid (4) is equipped with filter membrane (5) that are arranged in filtering heavy metal in column body (1) inside water solution and the heavy metal in the suspended particles thing.
2. The capsule type secondary centrifuge tube applicable to rapid nondestructive analysis according to claim 1, wherein: the outside of column body (1) is equipped with centrifugal sleeve (10) that is used for loading the centrifuging tube in the centrifuge, the inside of centrifugal sleeve (10) is equipped with carries out extruded spacing subassembly (8) to column body (1) surface, spacing subassembly (8) are including being located inside turning block (83) of centrifugal sleeve (10), the inside of centrifugal sleeve (10) is equipped with the confession turning block (83) pivoted spacing groove (81), the inside of turning block (83) is equipped with pivot (82), turning block (83) are including inclined plane portion (831).
3. The capsule type secondary centrifuge tube applicable to rapid nondestructive analysis according to claim 2, wherein: one side of the inclined plane part (831) is provided with an ejection assembly (9) for lifting the centrifugal tube in the centrifugal sleeve (10), the ejection assembly (9) comprises a pressing plate (91) located inside the centrifugal sleeve (10), one side of the extrusion plate (91) is provided with an auxiliary block (98) for assisting the extrusion plate (91) to press, the extrusion plate (91) can freely slide up and down in the centrifugal sleeve (10), a connecting block (92) is arranged on one side of the extrusion plate (91), a second rotating shaft (93) is arranged inside the connecting block (92), a rotating plate (94) is arranged outside the second rotating shaft (93), a third rotating shaft (95) is arranged inside the rotating plate (94), one side of the rotating plate (94) is provided with a connecting plate (96), and one side of the connecting plate (96) is provided with an arc panel (97) for supporting the bottom of the solid bottom joint (3).
4. The capsule type secondary centrifuge tube applicable to rapid nondestructive analysis according to claim 2, wherein: one side of the rotating block (83) is arc-shaped, and in the process that the cylindrical pipe body (1) is inserted into the centrifugal sleeve (10), the arc-shaped part of the rotating block (83) is in contact with the cylindrical pipe body (1).
5. The capsule type secondary centrifuge tube applicable to rapid nondestructive analysis according to claim 3, wherein: the cambered surface of the cambered plate (97) is matched with the bottom cambered surface of the solid bottom joint (3).
6. The capsule type secondary centrifuge tube applicable to rapid nondestructive analysis according to claim 1, wherein: the solid bottom (4) comprises a convex part (41), the filter membrane (5) comprises a concave part (51), and the shape of one side of the convex part (41) of the solid bottom (4) is matched with the shape of the concave part (51) of the filter membrane (5).
7. The capsule type secondary centrifuge tube applicable to rapid nondestructive analysis according to claim 1, wherein: the columnar pipe body (1), the hollow bottom joint (2) and the solid bottom joint (3) are all made of polytetrafluoroethylene or polypropylene.
CN202111381378.7A 2021-11-21 2021-11-21 Capsule type secondary centrifuge tube capable of being applied to rapid nondestructive analysis Active CN113941384B (en)

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