CN113862092A - Detergent composition, detergent and preparation method - Google Patents

Detergent composition, detergent and preparation method Download PDF

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Publication number
CN113862092A
CN113862092A CN202110905298.0A CN202110905298A CN113862092A CN 113862092 A CN113862092 A CN 113862092A CN 202110905298 A CN202110905298 A CN 202110905298A CN 113862092 A CN113862092 A CN 113862092A
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CN
China
Prior art keywords
powder
small
cleaning agent
chenopodium quinoa
millet
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202110905298.0A
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Chinese (zh)
Inventor
李萍花
刘劲岩
刘晓阳
贺晓
呼丽霞
陈芳飞
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shenmu Hede Ecological Agriculture Co ltd
Original Assignee
Shenmu Hede Ecological Agriculture Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shenmu Hede Ecological Agriculture Co ltd filed Critical Shenmu Hede Ecological Agriculture Co ltd
Priority to CN202110905298.0A priority Critical patent/CN113862092A/en
Publication of CN113862092A publication Critical patent/CN113862092A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D7/00Compositions of detergents based essentially on non-surface-active compounds
    • C11D7/22Organic compounds
    • C11D7/40Products in which the composition is not well defined
    • C11D7/44Vegetable products

Abstract

The application discloses a cleaning agent composition, a cleaning agent and a preparation method, wherein the cleaning agent composition comprises the following components in percentage by weight: 30-70% of chenopodium quinoa powder and 30-70% of millet rice powder. The cleaning agent composition adopts pure plant components, and the components have synergistic effect under a specific ratio, so that the cleaning agent composition has the advantages of good decontamination effect, no chemical residue, no damage to skin, environmental friendliness and the like.

Description

Detergent composition, detergent and preparation method
Technical Field
The application relates to the technical field of cleaning, in particular to a cleaning agent composition, a cleaning agent and a preparation method.
Background
Most of the existing cleaning agents are chemically synthesized, although the cleaning capacity is strong, chemical substances in the cleaning agents can be remained on tableware or vegetables and fruits and are difficult to completely remove, the cleaning agents are easy to cause harm to human bodies after long-term use, and chemically synthesized products are not easy to degrade and can cause adverse effects on the environment.
Disclosure of Invention
In view of the above-mentioned drawbacks or deficiencies in the prior art, it is desirable to provide a detergent composition, a detergent and a preparation method, wherein the components contained in the detergent composition are natural raw materials, are natural and environment-friendly, and have a good decontamination effect.
As a first aspect of the present application, the present application provides a detergent composition.
Preferably, the detergent composition comprises the following components in percentage by weight:
30-70% of chenopodium quinoa powder and 30-70% of millet rice powder.
Preferably, the chenopodium quinoa powder is prepared by the following steps:
cleaning the overground part of the small gooseberry, cutting into sections, and deactivating enzyme for 5-10 min;
and (3) dehydrating, frying, drying, crushing and sieving the de-enzymed small gooseberries in sequence to obtain the small gooseberry powder.
Preferably, the particle size of the chenopodium quinoa powder is 50-100 meshes.
Preferably, the particle size of the millet rice flour is 30-80 meshes.
As a second aspect of the present application, there is provided a cleaning agent.
Preferably, the detergent comprises the detergent composition of the first aspect.
Preferably, the cleaning agent is a powder.
Preferably, the detergent is a kitchen ware, tableware and fruit and vegetable detergent.
As a third aspect of the present application, there is provided a process for the preparation of a cleaning agent as described in the second aspect.
Preferably, the preparation method comprises the following steps:
the cleaning agent is prepared by uniformly mixing the chenopodium quinoa powder and the husked millet powder and sterilizing.
Preferably, the chenopodium quinoa powder is prepared by the following steps:
cleaning the overground part of the small gooseberry, cutting into sections, and deactivating enzyme for 5-10 min;
and (3) dehydrating, frying, drying, crushing and sieving the de-enzymed small gooseberries in sequence to obtain the small gooseberry powder.
The beneficial effect of this application:
the cleaning agent composition adopts pure plant components, and the components have synergistic effect under a specific ratio, so that the cleaning agent composition has the advantages of good decontamination effect, no chemical residue, no damage to skin, environmental friendliness and the like.
Detailed Description
The present application will be described in further detail with reference to examples. It is to be understood that the specific embodiments described herein are merely illustrative of the relevant invention and not restrictive of the invention.
It should be noted that the embodiments and features of the embodiments in the present application may be combined with each other without conflict. It is noted that the endpoints of the ranges and any values disclosed herein are not limited to the precise range or value, and that such ranges or values are understood to encompass values close to those ranges or values. For ranges of values, between the endpoints of each of the ranges and the individual points, and between the individual points may be combined with each other to give one or more new ranges of values, and these ranges of values should be considered as specifically disclosed herein.
It should be noted that the raw material referred to in this application is from shenmuu county, elm city, shanxi province.
According to a first aspect of the present application, there is provided a detergent composition comprising 30-70% by weight of chenopodium quinoa powder and 30-70% by weight of millet flour.
Wherein, the small gooseberry powder is the powder of the crushed small gooseberry plant, the small gooseberry is called bitter Chenopodium album L, is an annual herbaceous plant, contains multiple natural effective components such as chenopodium album and polysaccharide, and has multiple functions of antibiosis, antioxidation, dehumidification, detoxification, free radical removal and the like; the application surprisingly discovers that the powder obtained by crushing the chenopodium quinoa plant, namely chenopodium quinoa powder, has excellent effects of removing dirt and oil and can remove various stains including oil-soluble stains;
wherein the millet flour is powder of pulverized millet, the millet is product of husking millet seed, and the millet is annual herbaceous cultivation grain of Gramineae Panicum, and is widely distributed in northwest, north China, south China, inner Mongolia, etc.; the application unexpectedly finds that the broomcorn millet powder has enough adhesive force and friction force, on one hand, the broomcorn millet powder is easy to adsorb on the surface of dirt, prolongs the action time of detergent components and the dirt, and is beneficial to wetting the object to be cleaned, and on the other hand, the broomcorn millet powder can promote stains to be separated from the surface of the object to be cleaned through friction, so that the cleaning and deoiling efficacy of the chenopodium quinoa powder is improved in an auxiliary manner;
in the application, the chenopodium quinoa powder is used as a main effective component of the detergent composition, and the husked millet powder is used as an auxiliary component of the detergent composition, so that the composition has excellent dirt-removing capability and can effectively remove various stains, such as oil-soluble stains such as vegetable oil and animal oil, water-soluble stains such as urine stain and fruit juice, and solid stains such as lime; among them, the content of chenopodium quinoa powder less than 30% results in poor cleaning effect, and the content of chenopodium quinoa powder more than 70% results in reduced adhesion to dirt.
Further, in some preferred embodiments of the present application, the chenopodium quinoa powder is prepared by the steps of:
cleaning the overground part of the small gooseberry, cutting into sections, and deactivating enzyme for 5-10 min;
and (3) dehydrating, frying, drying, crushing and sieving the de-enzymed small gooseberries in sequence to obtain the small gooseberry powder.
Specifically, the method comprises the following steps:
harvesting overground parts of the chenopodium quinoa plants when the chenopodium quinoa plants grow to 30-70 cm;
washing stems and leaves of the small gooseberries by using tap water, and draining;
cutting cleaned Chenopodium quinoa plants into segments with the length of about 10cm, and deactivating enzyme for 5-10min, preferably for 7min, to prevent the Chenopodium quinoa plants from deteriorating due to respiration consumption, enzymatic browning and microbial decay;
dehydrating the de-enzymed small gooseberries and frying the small gooseberries until the water content is 50-60%;
drying the fried small gooseberries until the water content is 8-11%, crushing the small gooseberries to a proper granularity, and sieving the small gooseberries to obtain the small gooseberry powder.
In the embodiment of the present application, the water-removing may be performed by steam water-removing at 100-120 ℃, or microwave water-removing, or intermittent steam microwave water-removing, and the present application is not limited thereto. Steam deactivation is preferably used.
In the embodiments of the present application, the drying may be natural shade drying or vacuum drying or freeze drying, and the present application is not limited thereto.
In the embodiment of the present application, pulverization is performed using a grinder or a pulverizer, and sieving is performed to obtain chenopodium quinoa powder of an appropriate particle size. Wherein, a sieve with 50-100 meshes is adopted for sieving to obtain the chenopodium quinoa powder with the granularity of 50-100 meshes.
The chenopodium quinoa powder obtained by the preparation method greatly preserves the functional substances contained in the chenopodium quinoa powder, is easy to preserve and cannot deteriorate.
Further, in some preferred embodiments herein, the millet flour is prepared by the steps of:
sequentially husking millet, crushing and sieving to obtain the millet rice flour.
Wherein, a 30-80 mesh screen is adopted for sieving to obtain the millet rice flour with the granularity of 30-80 meshes.
Further, the obtained quinoa powder and the millet powder are uniformly mixed to obtain the detergent composition, wherein the content of the quinoa powder is 30-70% and the content of the millet powder is 30-70% in percentage by weight of the detergent composition.
In the embodiment of the present application, the mixing time is not particularly limited, and the components can be uniformly mixed, for example, 8 to 10 minutes. The mixing process may be carried out in a dry powder mixer.
Further, in some preferred embodiments of the present application, the average particle size of the chenopodium quinoa powder (i.e., D)50) Is 50 to 100 mesh, preferably 60 to 80 mesh, and more preferably 70 mesh.
Further, in some preferred embodiments herein, the millet flour has an average particle size of 30 to 80 mesh, preferably 40 to 70 mesh, and more preferably 50 mesh.
The detergent composition of the present application can be formulated into any formulation of detergent conventionally prepared in the art for cleaning of kitchenware, tableware, furniture, fruits and vegetables, clothes and the like. For example, it may be formulated into a suspension, emulsion, paste, gel, powder, etc., and preferably the detergent composition of the present application is prepared as a powder.
According to a second aspect of the present application, there is provided a detergent comprising the detergent composition of the first aspect.
In a more preferred embodiment herein, the cleanser consists of the cleanser composition of the first aspect, i.e., the cleanser consists of 30 to 70% Chenopodium quinoa powder and 30 to 70% husked millet powder by weight percent of the cleanser.
The cleaning agent of the embodiment is simple in components, contains natural raw materials, is green, safe and non-irritant, and cannot cause adverse effects on objects to be cleaned and the environment.
Further, in some preferred embodiments of the present application, the cleaning agent is a powder.
Further, in some preferred embodiments of the present application, the detergent is a kitchen ware, tableware and fruit and vegetable detergent.
The cleaning agent does not contain chemical substances, does not cause chemical residues on the surfaces of kitchen utensils, tableware, fruits and vegetables, and effectively avoids potential harm to human bodies caused by chemical substance residues.
According to a third aspect of the present application, there is provided a process for the preparation of a cleaning agent according to the second aspect, in particular a powder formulation, comprising:
the cleaning agent is prepared by uniformly mixing the chenopodium quinoa powder and the husked millet powder and sterilizing.
In the embodiment of the present application, the mixing time is not particularly limited, and it is sufficient to achieve uniform mixing of the components, for example, 8 to 10 minutes. The mixing process may be carried out in a dry powder mixer.
In the embodiments of the present application, the sterilization mode is not limited, and preferably radiation sterilization, for example, radiation sterilization using ultraviolet rays, infrared rays, microwaves, etc., and the sterilization method is safe and reliable without affecting the quality of the detergent.
In an embodiment of the present application, the detergent is dispensed after sterilization.
Further, in some preferred embodiments of the present application, the chenopodium quinoa powder is prepared by the steps of:
cleaning aerial part of Chenopodium quinoa, cutting, and deactivating enzyme for 5-10 min;
and (3) dehydrating, frying, drying, crushing and sieving the de-enzymed small gooseberries in sequence to obtain the small gooseberry powder.
Specifically, the method comprises the following steps:
harvesting overground parts of the chenopodium quinoa plants when the chenopodium quinoa plants grow to 30-70 cm;
washing stems and leaves of the small gooseberries by using tap water, and draining;
cutting cleaned Chenopodium quinoa plants into segments with the length of about 10cm, and deactivating enzyme for 5-10min, preferably for 7min, to prevent the Chenopodium quinoa plants from deteriorating due to respiration consumption, enzymatic browning and microbial decay;
dehydrating the de-enzymed small gooseberries and frying the small gooseberries until the water content is 50-60%;
drying the fried small gooseberries until the water content is 8-11%, crushing the small gooseberries to a proper granularity, and sieving the small gooseberries to obtain the small gooseberry powder. Wherein, a sieve with 50-100 meshes is adopted for sieving to obtain the chenopodium quinoa powder with the granularity of 50-100 meshes.
Further, in some preferred embodiments herein, the millet flour is prepared by the steps of:
sequentially husking millet, crushing and sieving to obtain the millet rice flour.
Wherein, a 30-80 mesh screen is adopted for sieving to obtain the millet rice flour with the granularity of 30-80 meshes.
The preparation method is simple and easy to operate, industrial production is easy to realize, and the prepared detergent is natural and environment-friendly and has a good decontamination effect.
In the embodiments of the present application, the detergent may be used according to a conventional use method, as specifically described below:
the proper amount of the cleaning agent is directly sprayed on the surface of wet kitchen ware, tableware or fruits and vegetables, and the cleaning agent is washed by clean water after being fully rubbed.
Or 10-20 g of the cleaning agent can be put into 1000mL of water, 250 g of vegetables or fruits are put into the water for soaking for 5-30 minutes, and then the vegetables or fruits are taken out and washed for 1-3 minutes by using clean water.
To further illustrate the present invention, the detergent compositions and detergents provided herein are described in detail in conjunction with the following examples, but it is to be understood that these examples are presented to illustrate the principles of the present invention and that the detailed embodiments and specific procedures are given to further illustrate the features and advantages of the present invention, not to limit the claims of the present invention, and the scope of the present invention is not limited to the following examples.
Example 1
Collecting the overground part of the small gooseberry with the plant height of about 60cm, fully cleaning the small gooseberry with tap water and draining the water; cutting the cleaned aerial part of Chenopodium quinoa L into segments with length of 10cm, and deactivating enzyme with steam at 100 deg.C for 7 min; dewatering the de-enzymed small gooseberry, and parching until the water content is 50%; drying the fried small gooseberries by a freeze dryer until the water content is 8%, then putting the dried small gooseberries into a double-roller mill for crushing and sieving to obtain 50-mesh small gooseberry powder;
selecting husked millet without worm damage and mildew, pulverizing in a double-roller mill, and sieving to obtain 30 mesh husked millet powder;
mixing the chenopodium quinoa powder and the husked millet powder according to the mass percent of 7: 3 to obtain the detergent composition.
Example 2
Collecting the overground part of the small gooseberry with the plant height of about 60cm, fully cleaning the small gooseberry with tap water and draining the water; cutting the cleaned aerial part of Chenopodium quinoa L into segments with length of 10cm, and deactivating enzyme with steam at 110 deg.C for 10 min; dewatering the de-enzymed small gooseberry, and parching to water content of 60%; drying the fried small gooseberries by a freeze dryer until the water content is 9%, then putting the dried small gooseberries into a double-roller mill for crushing and sieving to obtain 70-mesh small gooseberry powder;
selecting worm-eaten-free and mildew-free husked millet, putting the husked millet into a double-roller mill, crushing and sieving to obtain 50-mesh husked millet flour;
mixing the chenopodium quinoa powder and the husked millet powder according to the mass percentage of 5: 5 to obtain the detergent composition.
Example 3
Collecting the overground part of the small gooseberry with the plant height of about 60cm, fully cleaning the small gooseberry with tap water and draining the water; cutting the cleaned overground part of the small gooseberry into segments with the length of 10cm, and performing steam deactivation for 5min at 120 ℃; dewatering the de-enzymed small gooseberry, and parching to water content of 55%; drying the fried small gooseberries by a freeze dryer until the water content is 11%, then putting the dried small gooseberries into a double-roller mill for crushing and sieving to obtain 100-mesh small gooseberry powder;
selecting worm-eaten-free and mildew-free millet, putting into a double-roller mill, grinding, and sieving to obtain 80-mesh millet rice flour;
mixing the chenopodium quinoa powder and the husked millet powder according to the mass percentage of 3: 7 to obtain the detergent composition.
Comparative example 1
A detergent composition was prepared by referring to the method of example 1 except that millet flour was not contained.
Comparative example 2
A detergent composition was prepared by referring to the method of example 1, except that the average particle size of the Chenopodium quinoa powder was 30 mesh, and the mass percentage of the Chenopodium quinoa powder to the millet rice powder was 2: 8.
Comparative example 3
Collecting the overground part of the small goosebeery with the plant height of about 60cm, fully cleaning the overground part of the small goosebeery with tap water, draining the water, and burning the small goosebeery into ash;
selecting husked millet without worm damage and mildew, pulverizing in a double-roller mill, and sieving to obtain 30 mesh husked millet powder;
mixing the chenopodium quinoa ash and the husked millet powder according to the mass percentage of 7: 3 to obtain the detergent composition.
Comparative example 4
Collecting aerial parts of Chenopodium quinoa with plant height of about 60cm, cleaning with tap water, draining, cutting, and squeezing to obtain juice;
husking husked millet without worm damage and mildew, putting into a double-roller type flour mill, crushing, and sieving to obtain 30-mesh husked millet flour;
mixing the chenopodium quinoa juice and the husked millet powder according to the mass percentage of 7: 3 to obtain the detergent composition.
The detergent compositions of examples 1-3 and comparative examples 1-4 were tested for detergency according to the detergency test method in QB/T4348 kitchen grease stain cleaners, as follows:
50g of the detergent compositions of examples 1 to 3 and comparative examples 1 to 4 were taken, 150g of water was added to prepare a cleaning suspension, and the prepared soil pieces were respectively placed in the cleaning suspension for cleaning, dried, weighed, and the detergency was calculated according to the following formula:
f=(m1-m2)/(m1-m0) X 100%, wherein m0Is the mass of the test piece, m1M is mass of the smear before cleaning2The results are shown in the following table for the mass of the soiled sheet after cleaning:
example 1 Example 2 Example 3 Comparative example 1 Comparative example 2 Comparative example 3 Comparative example 4
Detergency 92.3% 95.8% 93.0% 75.4% 81.8% 56.4% 72.9%
The detergent composition has remarkable decontamination capability, the effect is obviously higher than that of the detergent composition only containing the chenopodium quinoa powder, the chenopodium quinoa powder and the husked millet powder are cooperatively matched, the decontamination capability of the chenopodium quinoa powder is improved, and the content and the average granularity of the chenopodium quinoa powder influence the decontamination effect of the chenopodium quinoa powder.
As can be seen from comparison of example 1 with comparative example 3 and comparative example 4, the chenopodium quinoa powder prepared by the method of the present application has a significantly better decontamination effect than the chenopodium quinoa is burnt into ash and is better than the chenopodium quinoa is squeezed, which indicates that the process affects the efficacy of chenopodium quinoa, and on one hand, the content of functional substances, such as saponin substances, may be destroyed by the chenopodium quinoa burnt into ash and the squeezing thereof, so that the decontamination effect is reduced; on the other hand, the small goosebeery is made into powder which can play a certain role of an abrasive agent, thereby having better decontamination effect.
The detergent composition and the detergent provided by the application have excellent decontamination effect, the oil and stain removal capacity is equivalent to that of a commercially available detergent, and the detergent composition does not contain chemical substances, does not cause chemical residues on kitchen ware, tableware, fruits and vegetables, is green and healthy, and has no irritation to skin.
The above description is only a preferred embodiment of the application and is illustrative of the principles of the technology employed. It will be appreciated by a person skilled in the art that the scope of the invention as referred to in the present application is not limited to the embodiments with a specific combination of the above-mentioned features, but also covers other embodiments with any combination of the above-mentioned features or their equivalents without departing from the inventive concept. For example, the above features may be replaced with (but not limited to) features having similar functions disclosed in the present application.

Claims (9)

1. The detergent composition is characterized by comprising the following components in percentage by weight:
30-70% of chenopodium quinoa powder and 30-70% of millet rice powder.
2. The detergent composition as claimed in claim 1, wherein said Chenopodium quinoa powder is prepared by the steps of:
cleaning the overground part of the small gooseberry, cutting into sections, and deactivating enzyme for 5-10 min;
and (3) dehydrating, frying, drying, crushing and sieving the de-enzymed small gooseberries in sequence to obtain the small gooseberry powder.
3. The detergent composition as claimed in claim 1, wherein said chenopodium quinoa powder has a particle size of 50 to 100 mesh.
4. The detergent composition of claim 1, wherein the millet flour has a particle size of 30 to 80 mesh.
5. A detergent comprising the detergent composition according to any one of claims 1 to 4.
6. The cleaning agent according to claim 5, wherein the cleaning agent is a powder.
7. The cleaning agent of claim 5, wherein the cleaning agent is a kitchen ware, tableware and fruit and vegetable cleaning agent.
8. A process for preparing a cleaning agent according to any one of claims 5 to 7, comprising:
the cleaning agent is prepared by uniformly mixing the chenopodium quinoa powder and the husked millet powder and sterilizing.
9. The method of claim 8, wherein said chenopodium quinoa powder is prepared by the steps of:
cleaning the overground part of the small gooseberry, cutting into sections, and deactivating enzyme for 5-10 min;
and (3) dehydrating, frying, drying, crushing and sieving the de-enzymed small gooseberries in sequence to obtain the small gooseberry powder.
CN202110905298.0A 2021-07-30 2021-07-30 Detergent composition, detergent and preparation method Pending CN113862092A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202110905298.0A CN113862092A (en) 2021-07-30 2021-07-30 Detergent composition, detergent and preparation method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202110905298.0A CN113862092A (en) 2021-07-30 2021-07-30 Detergent composition, detergent and preparation method

Publications (1)

Publication Number Publication Date
CN113862092A true CN113862092A (en) 2021-12-31

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1733783A (en) * 2005-06-20 2006-02-15 西安交通大学 Method for extracting general saponin from chenopodium album
CN101260347A (en) * 2008-04-24 2008-09-10 杨宝侠 Green tableware detergent
CN103013712A (en) * 2012-12-22 2013-04-03 张宗山 Oil stain remover and oil stain removal method

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1733783A (en) * 2005-06-20 2006-02-15 西安交通大学 Method for extracting general saponin from chenopodium album
CN101260347A (en) * 2008-04-24 2008-09-10 杨宝侠 Green tableware detergent
CN103013712A (en) * 2012-12-22 2013-04-03 张宗山 Oil stain remover and oil stain removal method

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
朱华 等: "《中国壮药图鉴(上)》", 广西科学技术出版社 *

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Application publication date: 20211231