CN113667547A - Edible cleaning emulsion and preparation method and application thereof - Google Patents

Edible cleaning emulsion and preparation method and application thereof Download PDF

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Publication number
CN113667547A
CN113667547A CN202110998441.5A CN202110998441A CN113667547A CN 113667547 A CN113667547 A CN 113667547A CN 202110998441 A CN202110998441 A CN 202110998441A CN 113667547 A CN113667547 A CN 113667547A
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parts
edible
cleaning
cleaning emulsion
surfactant
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程绍禹
叶自溢
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Guangzhou Aijia Youfang Daily Necessities Co ltd
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Guangzhou Aijia Youfang Daily Necessities Co ltd
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66Non-ionic compounds
    • C11D1/662Carbohydrates or derivatives
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66Non-ionic compounds
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/20Organic compounds containing oxygen
    • C11D3/2003Alcohols; Phenols
    • C11D3/2006Monohydric alcohols
    • C11D3/201Monohydric alcohols linear
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/20Organic compounds containing oxygen
    • C11D3/2003Alcohols; Phenols
    • C11D3/2041Dihydric alcohols
    • C11D3/2044Dihydric alcohols linear
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/20Organic compounds containing oxygen
    • C11D3/2003Alcohols; Phenols
    • C11D3/2065Polyhydric alcohols
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/20Organic compounds containing oxygen
    • C11D3/22Carbohydrates or derivatives thereof
    • C11D3/222Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/38Products with no well-defined composition, e.g. natural products
    • C11D3/382Vegetable products, e.g. soya meal, wood flour, sawdust
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/38Products with no well-defined composition, e.g. natural products
    • C11D3/386Preparations containing enzymes, e.g. protease or amylase
    • C11D3/38618Protease or amylase in liquid compositions only
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/38Products with no well-defined composition, e.g. natural products
    • C11D3/386Preparations containing enzymes, e.g. protease or amylase
    • C11D3/38627Preparations containing enzymes, e.g. protease or amylase containing lipase
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/38Products with no well-defined composition, e.g. natural products
    • C11D3/386Preparations containing enzymes, e.g. protease or amylase
    • C11D3/38636Preparations containing enzymes, e.g. protease or amylase containing enzymes other than protease, amylase, lipase, cellulase, oxidase or reductase
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/38Products with no well-defined composition, e.g. natural products
    • C11D3/386Preparations containing enzymes, e.g. protease or amylase
    • C11D3/38645Preparations containing enzymes, e.g. protease or amylase containing cellulase
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/38Products with no well-defined composition, e.g. natural products
    • C11D3/386Preparations containing enzymes, e.g. protease or amylase
    • C11D3/38654Preparations containing enzymes, e.g. protease or amylase containing oxidase or reductase
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/48Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Wood Science & Technology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Emergency Medicine (AREA)
  • Molecular Biology (AREA)
  • Detergent Compositions (AREA)

Abstract

An edible cleaning emulsion and its preparation method and application are provided. The invention provides edible cleaning emulsion which comprises the following preparation raw materials in parts by weight: 10-50 parts of solvent, 2-20 parts of surfactant, 20-50 parts of filler, 0.1-5 parts of bactericide and 0.5-5 parts of enzyme composition. The edible cleaning emulsion provided by the invention is reasonably matched, so that the excellent decontamination and antibacterial performance is realized, the dosage of the surfactant is obviously reduced, the provided cleaning emulsion is safe and edible, the performance is stable, the decontamination, antibacterial and safety performances are realized, the harm caused by the mistaken eating of children and pets can be effectively avoided, and the edible cleaning emulsion can be widely applied to cleaning of clothes, kitchenware, tableware, toys and the like.

Description

Edible cleaning emulsion and preparation method and application thereof
Technical Field
The invention belongs to the technical field of daily chemical articles, and particularly relates to edible cleaning emulsion and a preparation method thereof.
Background
The cleaning agent is a general name of cleaning products used for washing clothes, cleaning tools, cleaning furniture and the like, and becomes an indispensable daily chemical product in daily life. In order to ensure good cleaning effect, the cleaning agent used in daily life usually contains inedible components, the content of the surfactant is high, part of chemical components contained in the cleaning agent are easy to generate irritation to human skin and the like, the biodegradation degree of the cleaning agent is low, and environmental pollution is easy to cause. The safety of the existing daily chemical cleaning agent is not ideal enough, and if people or animals eat the cleaning agent by mistake, the health of the people or animals can be affected, and even the personal safety is harmed. There are reports of health accidents caused by children eating detergents by mistake without the effective supervision of guardians.
The biosurfactant is a metabolite with certain surface activity secreted by microorganisms in a metabolic process under certain conditions, such as glycolipid, polysaccharide lipid, lipopeptide or neutral lipid derivative. Although the biosurfactant product has the advantages of good performance, safety, environmental protection and easy degradation, the industrial production of the biosurfactant product is still in the initial stage, the production cost and the application cost are higher, the global dosage of the biosurfactant is less than 2 percent of the global dosage of all the biosurfactants, and the industrial application of the biosurfactant product in the daily chemical field is limited to a certain extent.
Therefore, it would be of great interest to provide an edible cleansing emulsion having a low biosurfactant content.
Disclosure of Invention
In order to solve the problems in the prior art, the inventor screens and compounds raw materials for preparing the cleaning agent through a large number of tests to screen safe and stable raw materials, and reasonably collocates the raw materials, so that the excellent decontamination and antibacterial performance is realized, the dosage of the surfactant is obviously reduced, the provided cleaning emulsion is safe, edible and stable in performance, the consideration of decontamination, bacteriostasis and safety performance is realized, the harm caused by the mistaken eating of children and pets can be effectively avoided, and the cleaning emulsion can be widely applied to cleaning clothes, tableware, toys and the like. The present invention has been completed based on the above findings.
The objects of the invention will be further apparent and elucidated by the following detailed description.
The invention provides edible cleaning emulsion which comprises the following preparation raw materials in parts by weight: 10-50 parts of solvent, 2-20 parts of surfactant, 20-50 parts of filler, 0.1-5 parts of bactericide and 0.5-5 parts of enzyme composition.
The combination and the parts by weight of the raw materials for preparation are determined by a large number of experiments, and the edible cleaning emulsion provided by the invention has excellent decontamination, bacteriostasis and safety performance.
Preferably, the edible cleaning emulsion comprises the following preparation raw materials in parts by weight: 30-50 parts of solvent, 5-10 parts of surfactant, 25-40 parts of filler, 0.2-4 parts of bactericide and 1-3 parts of enzyme composition.
Preferably, the surfactant is a biological surfactant selected from one or more of rhamnolipid, sophorolipid, algal glycolipid, phospholipid, neutral lipid, SD100 and 10075.
Preferably, the enzyme composition comprises amylase, protease, cellulase, lipase, superoxide dismutase, pectinase and lysozyme, and the mass ratio of the amylase to the protease is 0.5-2: 1-3: 1-5: 0.5-2: 0.1-1.
More preferably, the enzyme composition consists of amylase, protease, cellulase, lipase, superoxide dismutase, pectinase and lysozyme in a mass ratio of 1:2:4:1:0.5:0.5: 0.5.
The filler is selected from one or more of glucose, sodium gluconate, xylitol, maltose, lactose and pregelatinized starch.
The solvent is selected from one or more of ethanol, propylene glycol, glycerol and water. The inventor finds that the cleaning emulsion provided by the invention can exert the performance more favorably and obviously enhance the stability under the condition that the solvent contains glycerol and the filler contains sodium gluconate through a large number of experiments.
The bactericide is one or more selected from Eucalyptus oil, tea tree oil, lemon oil and herba Menthae oil.
In addition, the present invention also provides a method of preparing an edible cleansing emulsion comprising the steps of:
1) adding a solvent and a filler into an emulsifying pot, homogenizing and shearing for 20-50 min to obtain a first mixture;
2) adding a surfactant and an enzyme composition into the first mixture, and homogenizing and shearing for 10-30 min to obtain a second mixture;
3) and adding a bactericide into the second mixture, homogenizing and shearing for 5-20 min, and uniformly stirring to obtain the edible cleaning emulsion.
In addition, the invention also provides the application of the edible cleaning emulsion in cleaning clothes, cleaning kitchenware, cleaning tableware and cleaning toys.
Compared with the prior art, the invention has the beneficial effects that: the raw materials used in the invention are natural, safe, nontoxic and nonirritating, and by combining the active ingredients of the surfactant, the ferment composition and the bactericide, the edible cleaning emulsion provided by the invention realizes excellent decontamination and bacteriostasis performance, simultaneously obviously reduces the dosage of the surfactant, is safe and edible, has stable performance, realizes the consideration of decontamination, bacteriostasis and safety performance, can effectively avoid the harm brought by the mistaken eating of children and pets, and can be widely applied to the cleaning of clothes, tableware, toys and the like. The preparation method of the edible cleaning emulsion provided by the invention is simple, and the prepared edible cleaning emulsion has stable quality. In addition, the invention also provides the application of the edible cleaning emulsion in cleaning clothes, cleaning kitchenware, cleaning tableware and cleaning toys.
Detailed Description
The present invention will be described in further detail with reference to specific examples.
In the present invention, all the preparation raw materials are commercially available products, or can be obtained by means of conventional techniques in the field. For example: rhamnolipid is purchased from Shanghai Yingchuang chemical Co., Ltd, sophorolipid is purchased from Shanghai Yichuang chemical Co., Ltd, SD100 is purchased from Guangzhou Tunxin chemical engineering science and technology Co., Ltd, 10075 is purchased from Guangzhou Tunxin chemical engineering science and technology Co., Ltd, cellulase is purchased from Novicin Biotechnology Co., Ltd, Eucalyptus essential oil is purchased from Jiangxi Zhongxiang Co., Ltd, and tea tree essential oil is purchased from Jiangxi Zhongxiang Co., Ltd.
Example an edible cleansing emulsion
The edible cleaning emulsion comprises the following preparation raw materials in parts by weight: 48 parts of solvent, 15 parts of surfactant, 35 parts of filler, 1 part of bactericide and 1 part of enzyme composition; the more specific components and parts by weight are as follows: SD 1007 parts, 100758 parts, propylene glycol 35 parts, ethanol 5 parts, glycerol 8 parts, glucose 20 parts, maltodextrin 15 parts, eucalyptus essential oil 1 part and enzyme composition 1 part. The enzyme composition comprises amylase, protease, cellulase, lipase, superoxide dismutase, pectinase and lysozyme, and the mass ratio of the amylase to the protease to the cellulase to the lipase is 1:2:4:1:0.5:0.5: 0.5.
A method of preparing an edible cleansing emulsion comprising the steps of: adding a solvent and a filler into an emulsifying pot, homogenizing and shearing for 30min to obtain a first mixture; adding a surfactant and an enzyme composition into the first mixture, and homogenizing and shearing for 15min to obtain a second mixture; adding a bactericide into the second mixture, homogenizing and shearing for 10min, uniformly stirring to obtain the edible cleaning emulsion, and filling after the edible cleaning emulsion is detected to be qualified.
EXAMPLE two edible cleaning emulsions
The edible cleaning emulsion comprises the following preparation raw materials in parts by weight: 48 parts of solvent, 10 parts of surfactant, 40 parts of filler, 1 part of bactericide and 1 part of enzyme composition; the more specific components and parts by weight are as follows: 5 parts of rhamnolipid, 100755 parts of propylene glycol, 10 parts of ethanol, 8 parts of glycerol, 25 parts of sodium gluconate, 15 parts of maltodextrin, 1 part of tea tree essential oil and 1 part of an enzyme composition. The enzyme composition comprises amylase, protease, cellulase, lipase and lysozyme in a mass ratio of 1.5:2:3:1:1:0.5: 0.5.
A method of preparing an edible cleansing emulsion comprising the steps of: adding a solvent and a filler into an emulsifying pot, homogenizing and shearing for 35min to obtain a first mixture; adding a surfactant and an enzyme composition into the first mixture, and homogenizing and shearing for 15min to obtain a second mixture; adding a bactericide into the second mixture, homogenizing and shearing for 8min, uniformly stirring to obtain the edible clean emulsion, and filling after the edible clean emulsion is detected to be qualified.
EXAMPLE III edible cleaning emulsions
The edible cleaning emulsion comprises the following preparation raw materials in parts by weight: 45 parts of solvent, 10 parts of surfactant, 43 parts of filler, 1 part of bactericide and 1 part of enzyme composition; the more specific components and parts by weight are as follows: 5 parts of trehalose glycolipid, 100755 parts of propylene glycol, 30 parts of ethanol, 5 parts of glycerol, 25 parts of glucose, 18 parts of maltodextrin, 1 part of tea tree essential oil and 1 part of enzyme composition. The enzyme composition comprises amylase, protease, cellulase, lipase and lysozyme in a mass ratio of 1:2:4:1:1:0.5: 0.5.
A method of preparing an edible cleansing emulsion comprising the steps of: adding solvent and filler into emulsifying pot, homogenizing and shearing for 40min to obtain first mixture; adding a surfactant and an enzyme composition into the first mixture, and homogenizing and shearing for 15min to obtain a second mixture; adding a bactericide into the second mixture, homogenizing and shearing for 8min, uniformly stirring to obtain the edible clean emulsion, and filling after the edible clean emulsion is detected to be qualified.
Example four edible cleaning emulsions
The edible cleaning emulsion comprises the following preparation raw materials in parts by weight: 46 parts of solvent, 15 parts of surfactant, 37 parts of filler, 1 part of bactericide and 1 part of enzyme composition; the more specific components and parts by weight are as follows: 5 parts of trehalose glycolipid, 10 parts of SD 10010 parts of ethanol, 40 parts of glycerol, 20 parts of glucose, 17 parts of maltodextrin, 1 part of lemon essential oil and 1 part of enzyme composition. The enzyme composition comprises amylase, protease, cellulase, lipase and lysozyme in a mass ratio of 1:2:4:1:1:0.5: 1.
A method of preparing an edible cleansing emulsion comprising the steps of: adding solvent and filler into emulsifying pot, homogenizing and shearing for 40min to obtain first mixture; adding a surfactant and an enzyme composition into the first mixture, and homogenizing and shearing for 15min to obtain a second mixture; adding a bactericide into the second mixture, homogenizing and shearing for 8min, uniformly stirring to obtain the edible clean emulsion, and filling after the edible clean emulsion is detected to be qualified.
Safety test example:
get the original hair separatelyThe edible cleaning emulsions provided in the first to fourth working examples were subjected to toxicological tests according to GB15193.1-2014 "food safety toxicological evaluation procedure", using a maximum tolerance dosing test method, at a dose of 15000mg/kg BW, using 30 kunming mice randomly divided into 4 groups, male and female halves. Animals were fasted for 16h before the test, without any restriction on water. The animals were dosed with 800mg/mL samples using a gavage regimen of 0.2mL/10g body weight. Observing the behavior of the mice after gastric lavage, weighing 1 time per week, observing 14d, and calculating LD50The results are shown in Table 1.
Table 1 LD of edible cleansing emulsions provided herein50
Figure BDA0003234629190000061
As can be seen from the data of the implementation cases, the data disclosed so far are represented by the ethanol mouse LD 50: 5628mg/kg is standard, and the main raw material added in the patent is LD 50: 21000-32200 mg/kg; while the average result of LD50 of the patent is more than 28000mg/kg, the amount shows that the product is safe and has no toxicity after eating.
Antibacterial performance test example:
the edible cleaning emulsions provided in the first to fourth examples of the present invention and the commercial detergent were respectively used to perform the bacteriostatic performance test according to the method of GB 9985-.
Table 2 bacteriostatic test results for edible cleaning emulsions provided by the invention
Embodiment 1 Example II Example three Example four Commercial detergent
Staphylococcus aureus 99.3% 99.0% 99.4% 99.0% 96.8%
Candida albicans 98.6% 98.5% 98.5% 98.6% 96.2%
Escherichia coli 99.5% 99.2% 99.0% 99.0% 97.3%
Hard object surface oil stain removal performance test example:
the edible cleaning emulsions provided in the first to fourth examples of the present invention and commercially available detergents were respectively used to perform a greasy dirt removal performance test. Using a 10cm × 10cm glass plate as a mold hard object surface before useAll glass plates were washed with chloroform and thoroughly dried, and their initial mass (m) was recorded0) About 0.1g of oil stain (to the nearest 0.0001g) was applied and used after aging in an oven at 60 ℃ overnight. Drying at room temperature for 4h, recording the weight as m1. Washing treatment: in a decontamination machine, 15 groups of washing water (tap water, containing 0.1% detergent) were prepared, one group of washing water was soaked in a group of glass plates at 30 ℃ for 1min, and after washing for 2.5min, the dishes were taken out, air dried for 4h, and the recorded weight was m2. The average stain removal per group was calculated: the removal efficiency of the oil stain was calculated by the following formula, and the results are shown in Table 3.
Figure BDA0003234629190000071
Table 3 oil stain removal test results for edible cleaning emulsions provided by the invention
Embodiment 1 Example II Example three Example four Commercial detergent
Oil removal rate 99.5% 99.0% 98.7% 99.0% 98.1%
The test examples show that the edible cleaning emulsion provided by the invention has excellent safety, bacteriostasis and cleaning performance, the overall performance of the edible cleaning emulsion is superior to that of a commercial detergent, and the edible cleaning emulsion can meet the use requirements of cleaning clothes, cleaning kitchenware, cleaning tableware and cleaning toys in daily life.
The foregoing is a more detailed description of the invention in connection with specific preferred embodiments and it is not intended that the invention be limited to these specific details. For those skilled in the art to which the invention pertains, several simple deductions or substitutions can be made without departing from the spirit of the invention, and all shall be considered as belonging to the protection scope of the invention.

Claims (10)

1. An edible cleansing emulsion characterized by: the preparation method comprises the following preparation raw materials in parts by weight: 10-50 parts of solvent, 2-20 parts of surfactant, 20-50 parts of filler, 0.1-5 parts of bactericide and 0.5-5 parts of enzyme composition.
2. The edible cleaning emulsion of claim 1, wherein: the preparation method comprises the following preparation raw materials in parts by weight: 30-50 parts of solvent, 5-10 parts of surfactant, 25-40 parts of filler, 0.2-4 parts of bactericide and 1-3 parts of enzyme composition.
3. An edible cleaning emulsion according to claim 1 or 2 characterized in that: the surfactant is a biological surfactant, and is selected from one or more of rhamnolipid, sophorolipid, algal glycolipid, phospholipid, neutral lipid, SD100 and 10075.
4. An edible cleaning emulsion according to claim 1 or 2 characterized in that: the enzyme composition comprises amylase, protease, cellulase, lipase, superoxide dismutase, pectinase and lysozyme, and the mass ratio of the amylase to the protease is 0.5-2: 1-3: 1-5: 0.5-2: 0.1-1.
5. The edible cleaning emulsion of claim 4, wherein: the enzyme composition comprises amylase, protease, cellulase, lipase, superoxide dismutase, pectinase and lysozyme in a mass ratio of 1:2:4:1:0.5:0.5: 0.5.
6. An edible cleaning emulsion according to claim 1 or 2 characterized in that: the filler is selected from one or more of glucose, sodium gluconate, xylitol, maltose, lactose and pregelatinized starch.
7. An edible cleaning emulsion according to claim 1 or 2 characterized in that: the solvent is selected from one or more of ethanol, propylene glycol, glycerol and water.
8. An edible cleaning emulsion according to claim 1 or 2 characterized in that: the bactericide is one or more selected from Eucalyptus oil, tea tree oil, lemon oil and herba Menthae oil.
9. A process for preparing an edible cleaning emulsion according to claim 1, characterized in that: the method comprises the following steps:
1) adding a solvent and a filler into an emulsifying pot, homogenizing and shearing for 20-50 min to obtain a first mixture;
2) adding a surfactant and an enzyme composition into the first mixture, and homogenizing and shearing for 10-30 min to obtain a second mixture;
3) and adding a bactericide into the second mixture, homogenizing and shearing for 5-20 min, and uniformly stirring to obtain the edible cleaning emulsion.
10. Use of an edible cleaning emulsion according to claim 1 for cleaning laundry, cleaning kitchen ware, cleaning dishware and cleaning toys.
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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101448399A (en) * 2006-04-21 2009-06-03 花王株式会社 Composition of biofilm control agent
CN103025856A (en) * 2010-07-22 2013-04-03 荷兰联合利华有限公司 Detergent compositions comprising biosurfactant and enzyme
CN107929104A (en) * 2017-12-25 2018-04-20 深圳市芭格美生物科技有限公司 A kind of three-in-one wash and maintenance liquid of biology enzyme and preparation method thereof
CN109135946A (en) * 2018-10-10 2019-01-04 江南大学 A kind of edible detergent and preparation method thereof
EP3686265A1 (en) * 2019-01-23 2020-07-29 BlueSun Consumer Brands, S.L. Detergent composition with sophorolipids
CN113214912A (en) * 2021-03-24 2021-08-06 广州市爱家有方日用品有限公司 Pollution-free environment-friendly cleaning effervescent tablet and preparation method thereof

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101448399A (en) * 2006-04-21 2009-06-03 花王株式会社 Composition of biofilm control agent
CN103025856A (en) * 2010-07-22 2013-04-03 荷兰联合利华有限公司 Detergent compositions comprising biosurfactant and enzyme
CN107929104A (en) * 2017-12-25 2018-04-20 深圳市芭格美生物科技有限公司 A kind of three-in-one wash and maintenance liquid of biology enzyme and preparation method thereof
CN109135946A (en) * 2018-10-10 2019-01-04 江南大学 A kind of edible detergent and preparation method thereof
EP3686265A1 (en) * 2019-01-23 2020-07-29 BlueSun Consumer Brands, S.L. Detergent composition with sophorolipids
CN113214912A (en) * 2021-03-24 2021-08-06 广州市爱家有方日用品有限公司 Pollution-free environment-friendly cleaning effervescent tablet and preparation method thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
谢宇: "《变化莫测的分子王国—化学工业》", 百花洲文艺出版社, pages: 138 *

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