CN113633581A - Phycobiliprotein lipstick and lip-moistening product and preparation method thereof - Google Patents
Phycobiliprotein lipstick and lip-moistening product and preparation method thereof Download PDFInfo
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- CN113633581A CN113633581A CN202111005972.6A CN202111005972A CN113633581A CN 113633581 A CN113633581 A CN 113633581A CN 202111005972 A CN202111005972 A CN 202111005972A CN 113633581 A CN113633581 A CN 113633581A
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- phycobiliprotein
- lipstick
- lip
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- white beeswax
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/927—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of insects, e.g. shellac
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/04—Preparations containing skin colorants, e.g. pigments for lips
- A61Q1/06—Lipsticks
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/001—Preparations for care of the lips
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Dermatology (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Insects & Arthropods (AREA)
- Zoology (AREA)
- Cosmetics (AREA)
Abstract
The invention relates to a natural marine phycobiliprotein lipstick and lip-moistening cosmetic and a preparation method thereof, and the preparation method comprises the following steps of (1) extracting food-grade phycobiliprotein; (2) mixing oleum Olivarum and oleum Simmondsia chinensis uniformly; (3) grinding and mixing vitamin E, octyl dodecanol, cetyl polyethylene glycol and phycobiliprotein in a mortar; (4) melting the white beewax in water bath; (5) adding the mixture obtained in the steps (2) and (3) and propylparaben into the melted white beeswax in several times, and quickly and uniformly mixing; (6) and (5) pouring the mixed material in the step (5) into a lipstick mould while the mixed material is hot, and cooling and demoulding. The lipstick adopts phycobiliprotein as a coloring agent, and can be mixed with carmine according to different proportions to prepare different colors such as scarlet, orange red, purple red and the like.
Description
Technical Field
The invention relates to the technical field of cosmetic preparation, in particular to a natural marine phycobiliprotein lipstick and lip gloss product and a preparation method thereof.
Background
Lipstick and lip balm products are relatively common beauty products in female life. The lipstick shows different colours through different pigment additions, can let painter's lip demonstrate different color and luster and gloss, can reach and decorate the lip profile, reinforcing facial aesthetic feeling promotes the effect of individual temperament. The lip balm prevents lip chapping through substances rich in grease, has the effects of moisturizing, moistening lips and improving the glossiness of the lips, and is a product which is commonly used in daily life. The main components of lipstick and lip gloss products comprise grease, wax, colorant, antioxidant, preservative and the like, the commercially available lipstick and lip gloss products mainly comprise ceresin, paraffin and lanolin, and the mineral wax and the lanolin are low in price but poor in texture and can generate sticky feeling. Lanolin and wax have complex components, are easy to cause allergy, red swelling and chapping reaction on fragile lip skin, and can cause damage to the lip skin even if the original effect of moisturizing the lips is not achieved. The color of the lipstick is mostly prepared by mixing inedible chemical pigments with different proportions, the pigments contain partial heavy metal ions, and the lipstick is smeared on the lips, so that the lipstick can be inevitably taken into the body through speaking, drinking and eating, is accumulated day by month, and causes heavy metal poisoning and even more serious harm to the body.
There are over 100 million animals and plants and hundreds of millions of microorganisms in the ocean, and the total amount of organisms accounts for 87% of the total biomass of the earth. Because of the special living environment of the sea, marine organisms can synthesize molecules with peculiar and novel chemical structures, which are different from terrestrial organisms, and 3.5 ten thousand marine natural products, half of which have various biological activities, have been found. The marine organisms have a unique gene system different from terrestrial organisms, and provide unique marine resources for related product development. The "seaweed" is a generic name of marine algae such as kelp, laver, undaria pinnatifida, gelidium amansii, etc., which is an algae growing in the sea. Algae contains a unique protein substance, phycobiliprotein, which is a natural water-soluble pigment protein with fluorescence and is mainly divided into four types of phycoerythrin, phycocyanin, allophycocyanin and phycoerythrocyanin. Phycoerythrin and phycocyanin are generally common, phycoerythrin appears red, and phycocyanin appears blue. Phycobiliprotein is classified into food grade, pharmaceutical grade and reagent grade according to purity, and the value is gradually improved along with the improvement of the purity. The application of the food-grade phycobiliprotein mainly comprises the following steps: (1) as a food additive, the compound tablet candy is added into products such as yoghourt, ice cream, hard candy, biscuits, sponge cakes, cans and the like, enriches the color of the food, and is a compound tablet candy with the function of regulating fatigue and the like and a preparation method thereof. (2) The antioxidant is used in facial mask and moisturizing cream. The food-grade phycobiliprotein is used in the fields of food and cosmetics, and mainly utilizes the color and the antioxidation effect of the phycobiliprotein.
Although there are many lipstick products on the market, the mature products of lipstick prepared by natural pigments are rare at present. Phycoerythrin is water-soluble, can produce a very obvious and nice reddish orange color only by a little, and can prepare more different colors by utilizing different proportions of the phycoerythrin and other pigments. And the phycoerythrin has natural source and antioxidant activity, and can not cause anaphylactic reaction and heavy metal hazard of common lipstick, so that the safe and nontoxic phycobiliprotein is used for preparing the lipstick, the beauty is kept, the body is not damaged, and the antioxidant effect is generated on the lip skin.
The phycobiliprotein lipstick and lip balm products provided by the invention are not reported in the prior art, so that the phycobiliprotein lipstick and lip balm functional cosmetics are developed by combining the color and the antioxidation of phycobiliprotein in cosmetics such as a lipstick and a lip balm prepared from marine natural seaweed protein, and have wide market prospect.
Disclosure of Invention
The invention aims at the problems and provides a lipstick and lip-moistening product containing phycobiliprotein and a preparation method thereof, wherein the phycobiliprotein is used as a pigment, the prepared lipstick has the characteristics of moistening, moisturizing, coloring, nature and safety, does not generate side effects on a body, and the antioxidant capacity of the phycobiliprotein enables the lipstick to have the characteristics of oxidation resistance and aging resistance.
In order to achieve the purpose, the technical scheme adopted by the invention is as follows:
a lipstick and lip-moistening product containing phycobiliprotein is prepared from the following components in parts by weight: 4-7 parts of white beeswax, 4-8 parts of olive oil, 1-4 parts of jojoba oil, 0.5-2 parts of vitamin E, 0.5-2 parts of phycoerythrin, 0.5-2 parts of carmine (lipstick does not need to be added), 0.05-0.2 part of octyl dodecanol, 0.8-3 parts of cetyl polyethylene glycol and 0.01-0.05 part of propyl paraben.
A lipstick and lip-moistening product containing phycobiliprotein and a preparation method thereof, the method comprises the following steps:
(1) breaking cell wall of Sargassum with deionized water, pulverizing, freezing and thawing in refrigerator at-20 deg.C for 3-5 times, adding 70% ammonium sulfate according to the volume of the crude extractive solution, salting out, dialyzing the precipitate, ultrafiltering the dialyzed solution in a centrifuge at 5000-6000 rpm and 4 deg.C for 20-30 min, and vacuum freeze drying the ultrafiltered solution to obtain phycobiliprotein with purity of food grade.
(2) Mixing oleum Olivarum and oleum Simmondsia chinensis uniformly;
(3) grinding vitamin E, octyldodecanol, cetyl polyethylene glycol, phycobiliprotein, and carmine (lipstick is not required to be added) with mortar, and mixing for 5-10min until no granule exists;
(4) melting the white beeswax in water bath at 65-100 ℃;
(5) after the white beeswax is melted, cooling to 62-65 ℃, adding the mixture of (2) and (3) and propylparaben into the melted white beeswax in several times, and quickly mixing uniformly for 1-2min (preferably 1 min);
(6) and (5) pouring the mixed material in the lipstick mold while the mixed material is hot, cooling for 30-50min, demolding, sealing and storing.
The raw materials in the invention are all food grade, and the components of the invention are explained as follows:
the olive oil is prepared by directly cold pressing olive fruits, does not undergo heating and chemical treatment, has natural health care and beauty treatment effects, has a moistening effect in the invention, and enables the ointment to be soft enough and easy to apply.
Compared with mineral wax, the white beeswax is a fatty substance secreted by worker bees, is smooth, has the fragrance of bees, contains acids, carotenoid, vitamin A and other components, and has a shape-fixing effect to moisten the paste.
The food-grade phycobiliprotein is prepared from seaweed containing phycobiliprotein such as thallus Porphyrae, thallus Gracilariae, Polysiphonia nodosa, herba Gelidonii, Gelidium amansii, Mycena furcata, Gracilaria, Laurencia acuminata, Corallium japonicum Kishinouye, and Grateloupia filicina by crushing, freeze thawing, salting out, dialyzing, and vacuum freeze drying. Phycoerythrin is red and phycocyanin is blue, and is a natural pigment in the present invention.
The jojoba oil has a structure similar to that of human skin lipid, has high skin affinity, has moistening and moisturizing effects, and can make lip skin elastic and reduce wrinkles.
Vitamin E, a fat-soluble vitamin, also known as tocopherol, is one of the major antioxidants. The antioxidant is easily soluble in organic solvents such as fat and ethanol, is stable to heat and acid, is unstable to alkali and is insensitive to heat, and has an antioxidant effect.
Compared with the prior art, the invention has the beneficial technical effects that:
1. the lipstick in the market at present mostly contains some raw materials which have side effects on human bodies, and part of pigments contain heavy metal ions.
2. The lipstick can be made into scarlet, orange red, purple red and other colors by using different proportions of food-grade phycobiliprotein and carmine.
3. The lipstick prepared by taking the food-grade phycobiliprotein as the pigment has the advantages of low cost and convenient preparation process, and the phycobiliprotein raw material is wide and easy to obtain and is easy to realize batch production.
The invention develops related functional cosmetics by using specific marine natural pigment protein with oxidation resistance and ultraviolet resistance, and has huge market potential and wide prospect; different from the lipstick applying chemical pigments on the market, the phycobiliprotein of the pigment of the lipstick and lip gloss prepared by the invention is extracted from natural seaweed, is safe and natural, has no side effect on human body, and has the efficacy of moisturizing and resisting oxidation on skin around lips.
Drawings
FIG. 1 is a process flow chart of the present invention for producing lipstick and lip gloss containing phycobiliprotein.
FIG. 2 is a diagram of lipstick body and smearing effect with different ratios of phycobiliprotein content;
FIG. 3 is a diagram of lip balm with different ratios of phycobiliprotein content;
FIG. 4 is a diagram of the final product of comparative example 1;
FIG. 5 shows the final product of comparative example 2.
Detailed Description
In order to better understand the essence of the present invention, the following examples are provided to illustrate the preparation method of the phycobiliprotein lipstick and lip gloss product of the present invention, but the present invention is not limited by these examples.
Example 1: preparation of lipstick containing phycobiliprotein
The preparation method comprises the following steps:
(1) breaking cell wall of thallus Porphyrae with deionized water, pulverizing, freezing and thawing in refrigerator at-20 deg.C for 3 times, filtering the crude extractive solution, adding 70% ammonium sulfate, salting out, dialyzing the precipitate, ultrafiltering at 6000rpm and 4 deg.C for 20min, and vacuum freeze drying to obtain phycobiliprotein with food grade purity;
(2) weighing 2.35g of olive oil and 0.47g of jojoba oil, and uniformly mixing;
(3) weighing 0.18g of vitamin E, 0.2g of food-grade phycobiliprotein prepared in the step (1), 0.3g of carmine, 0.03g of octyldodecanol and 0.21g of cetyl polyethylene glycol, and grinding and mixing uniformly by using a mortar for 5-10min until no particles exist;
(4) weighing 1.1g of white beeswax, and melting in a water bath at 75 ℃;
(5) after the white beeswax is melted, cooling to 65 ℃, adding the mixture of (2) and (3) and 0.01g of propyl hydroxybenzoate weighed into the melted white beeswax in portions, and quickly mixing uniformly for 1 min;
(6) and (5) pouring the mixed material in the step (5) into a lipstick mould while the mixed material is hot, cooling for 30min, demoulding, and sealing for storage.
The obtained lipstick body is date red, and has orange red color, as shown in figure 2 b. The paste is smooth, glossy, moderate in hardness, good in mouth and lip moistening degree and has an antioxidant function.
Example 2: preparation of lip balm containing phycobiliprotein
The preparation method comprises the following steps:
(1) breaking cell wall of thallus Porphyrae with deionized water, pulverizing, freezing and thawing in refrigerator at-20 deg.C for 3 times, filtering the crude extractive solution, adding 70% ammonium sulfate, salting out, dialyzing the precipitate, ultrafiltering at 6000rpm and 4 deg.C for 20min, and vacuum freeze drying to obtain phycobiliprotein with food grade purity;
(2) weighing 2.71g of olive oil and 0.54g of jojoba oil, and mixing uniformly;
(3) weighing 0.18g of vitamin E, 0.42g of food-grade phycobiliprotein prepared in the step (1), 0.03g of octyldodecanol and 0.21g of cetyl polyethylene glycol, and grinding and mixing uniformly for 5-10min by using a mortar until no particles exist;
(4) weighing 1.2g of white beeswax, and melting in a water bath at 75 ℃;
(5) after the white beeswax is melted, cooling to 63 ℃, adding the mixture of (2) and (3) and 0.01g of propyl hydroxybenzoate weighed into the melted white beeswax in portions, and quickly mixing uniformly for 1 min;
(6) and (5) pouring the mixed material in the step (5) into a lipstick mould while the mixed material is hot, cooling for 30min, demoulding, and sealing for storage.
The obtained lip balm is bluish purple, has light blue smearing effect, and has smooth and glossy appearance, moderate hardness, good moistening effect on mouth and lips, and antioxidant effect as shown in figure 3 d.
Example 3: preparation of lipstick containing phycobiliprotein
The preparation method comprises the following steps:
(1) adding deionized water into Eucheuma Gelatinosum, breaking cell wall, pulverizing, freezing and thawing in refrigerator at-20 deg.C for 3 times, filtering the crude extractive solution, adding 70% ammonium sulfate, salting out, collecting precipitate, dialyzing, ultrafiltering at 6000rpm and 4 deg.C for 20min, and vacuum freeze drying to obtain phycobiliprotein with food grade purity;
(2) weighing 2.35g of olive oil and 0.47g of jojoba oil, and uniformly mixing;
(3) weighing 0.18g of vitamin E, 0.3g of food-grade phycobiliprotein prepared in the step (1), 0.35g of carmine, 0.03g of octyldodecanol and 0.21g of cetyl polyethylene glycol, and grinding and mixing the components uniformly for 5-10min by using a mortar until no particles exist;
(4) weighing 1.1g of white beeswax, and melting in a water bath at 75 ℃;
(5) after the white beeswax is melted, cooling to 62 ℃, adding the mixture of (2) and (3) and 0.01g of propyl hydroxybenzoate weighed into the melted white beeswax in portions, and quickly mixing uniformly for 1 min;
(6) and (5) pouring the mixed material in the step (5) into a lipstick mould while the mixed material is hot, cooling for 30min, demoulding, and sealing for storage.
The obtained lipstick body is purple red, and has red smearing effect, as shown in figure 2a, the lipstick body is smooth, glossy, moderate in hardness, good in mouth and lip moistening degree, and has antioxidant function.
Example 4: preparation of lip balm containing phycobiliprotein
The preparation method comprises the following steps:
(1) adding deionized water into Eucheuma Gelatinosum, breaking cell wall, pulverizing, freezing and thawing in refrigerator at-20 deg.C for 3 times, filtering the crude extractive solution, adding 70% ammonium sulfate, salting out, collecting precipitate, dialyzing, ultrafiltering at 6000rpm and 4 deg.C for 20min, and vacuum freeze drying to obtain phycobiliprotein with food grade purity;
(2) weighing 2.71g of olive oil and 0.54g of jojoba oil, and mixing uniformly;
(3) weighing 0.18g of vitamin E, 0.36g of food-grade phycobiliprotein prepared in the step (1), 0.03g of octyldodecanol and 0.21g of cetyl polyethylene glycol, and grinding and mixing uniformly for 5-10min by using a mortar until no particles exist;
(4) weighing 1.2g of white beeswax, and melting in a water bath at 75 ℃;
(5) after the white beeswax is melted, cooling to 64 ℃, adding the mixture of (2) and (3) and 0.01g of propyl hydroxybenzoate weighed into the melted white beeswax in portions, and quickly mixing uniformly for 1 min;
(6) pouring the mixed material in the step (5) into a lipstick mould while the mixed material is hot, cooling for 30min, demoulding, sealing and storing;
the obtained lip balm is bluish purple, has light blue smearing effect, and has smooth and glossy ointment body, moderate hardness, good moistening degree for mouth and lip, and antioxidant effect as shown in figure 3 c.
Example 5: preparation of phycobiliprotein lipstick with different proportions
The preparation method comprises the following steps:
(1) the preparation method of lipstick containing phycobiliprotein in different proportions is as in example 1, and lipsticks with different colors are prepared by changing the proportion of phycobiliprotein and carmine, as shown in figure 2.
(2) 4 pieces of phycobiliprotein lipstick with different mixture ratios are prepared, wherein a and b are respectively embodiment 3 and embodiment 1. In the step c, the content of phycobiliprotein is 0.2g, the content of carmine is 0.25g, the obtained lipstick body is bright red, the smearing effect is tomato red, the lipstick body is smooth and glossy, has moderate hardness, has good moistening degree for the mouth and lips, and has an antioxidant function; d, the content of phycobiliprotein is 0.18g, the content of carmine is 0.2g, the obtained lipstick body is light red, the smearing effect is light red, the lipstick body is smooth and glossy, the hardness is moderate, the moistening degree of the mouth and the lips is good, and the lipstick body has an antioxidant function.
Example 6: preparation of phycobiliprotein lip balm with different proportions
The preparation method comprises the following steps:
(1) the lip balm with different proportions is prepared by the method of example 2, and lip balms with different colors are prepared by changing the adding proportion of the phycobiliprotein, as shown in figure 3.
(2) 4 pieces of phycobiliprotein lip balms with different mixture ratios are prepared, wherein c and d are respectively embodiment 4 and embodiment 2. The content of phycobiliprotein in the lipstick a is 0.24g, the obtained lip balm is gray, the lipstick is smooth and glossy, has moderate hardness, has good moistening degree for the mouth and the lips, and has an antioxidant function; and b, the content of phycobiliprotein is 0.3g, the obtained lip balm paste is light purple, and the lip balm paste is smooth and glossy, has moderate hardness, has good moistening degree for the mouth and the lips, and has an antioxidant function.
Example 7: determination of total oxidation resistance and hydroxyl radical OH removal capacity of natural seaweed phycobiliprotein lipstick and lip-moistening product
The prepared paste is smashed and dissolved to prepare a solution to be tested, and the total antioxidant capacity (T-AOC) and the hydroxyl radical OH scavenging capacity are measured to evaluate the antioxidant and anti-aging capacity of the invention, wherein the measuring method comprises the following steps:
(1) the total antioxidant capacity (T-AOC) measuring kit is used for measuring the total antioxidant capacity of the invention, and the specific operation steps are as follows: adding 5 μ L sample solution into 96 empty plate, and adding 180 μ L FRAP working solution (composed of 0.3mol/L acetate buffer solution, 10mmol/L TPTZ solution, and 20mmol/L FeCl solution)3The solution is prepared according to the volume ratio of 10: 1, and is used as the solution in situ), mixed evenly, reacted for 3-5min at 37 ℃, and the light absorption value is measured at the wavelength of 593 nm. Preparing a standard curve by using the OD values of the standard substance as abscissa and the concentrations of the standard substance corresponding to each OD value as ordinate, and preparing a curve common by using an excel tableSubstituting the OD value measured by the sample into a formula, calculating the result, and obtaining the total oxidation resistance of the measured sample by using FeSO4Standard solution concentration. The total oxidation resistance of the product is 0.528mM by determination;
(2) the hydroxyl radical OH scavenging capacity of the invention is measured by a salicylic acid method, and the specific operation steps are as follows: adding 9mmol/LFeSO into the test tube41mL, 9mmol/L salicylic acid-ethanol 1mL and the solution to be tested 1mL, finally 8.8mmol/L H is added2O21 mL. After 1.5h reaction at 37 ℃ centrifugation at 12000r/min for 10min was performed, followed by absorbance determination at 536nm using double distilled water as a reference. At a ratio of 9mmol/LFeSO41mL, 1mL of 9mmol/L salicylic acid-ethanol, 1mL of the solution to be detected and 1mL of double distilled water are used as the background absorption value of the solution to be detected. Each absorbance was measured 3 times in parallel and averaged. The clearance calculation formula is: clearance (%) ═ a0-(AX-AX0))/A0X 100%, wherein: a. the0The absorbance of the blank control solution; a. theXIs the absorbance after adding the solution to be measured; a. theX0The background absorption value of the solution to be measured. Through determination, the hydroxyl free radical OH clearance of the product is 55.93 percent;
the experimental determination of the total oxidation resistance (T-AOC) and the hydroxyl radical OH clearance rate shows that the lipstick and lip balm of the natural seaweed phycobiliprotein prepared by the invention has strong oxidation resistance and hydroxyl radical OH clearance capacity, and shows that the product prepared by the invention has the functions of oxidation resistance and anti-aging activity.
Comparative example 1
The preparation method comprises the following steps:
(1) breaking cell wall of thallus Porphyrae with deionized water, pulverizing, freezing and thawing in refrigerator at-20 deg.C for 3 times, filtering the crude extractive solution, adding 70% ammonium sulfate, salting out, dialyzing the precipitate, ultrafiltering at 6000rpm and 4 deg.C for 20min, and vacuum freeze drying to obtain phycobiliprotein with food grade purity;
(2) weighing 2.35g of olive oil and 0.47g of jojoba oil, and uniformly mixing;
(3) weighing 0.18g of vitamin E, 0.3g of food-grade phycobiliprotein prepared in the step (1), 0.25g of carmine, 0.03g of octyldodecanol and 0.21g of cetyl polyethylene glycol, and grinding and mixing the components uniformly for 5-10min by using a mortar until no particles exist;
(4) weighing 1.1g of white beeswax, and melting in water bath at 90 ℃;
(5) after the white beeswax is melted, cooling the temperature to 72-75 ℃, adding the mixture of (2) and (3) and 0.01g of propyl hydroxybenzoate weighed into the melted white beeswax in portions, and quickly and uniformly mixing for 3 min;
(6) and (5) pouring the mixed material in the step (5) into a lipstick mould while the mixed material is hot, cooling for 30min, demoulding, and sealing for storage.
The obtained paste is grey white, the color of the phycobiliprotein disappears, and the finished product of the comparative example 1 is shown in figure 4, and the paste is slightly rough in texture, more in surface pores, not glossy and still moist.
Comparative example 2
The preparation method comprises the following steps:
(1) breaking cell wall of thallus Porphyrae with deionized water, pulverizing, freezing and thawing in refrigerator at-20 deg.C for 3 times, filtering the crude extractive solution, adding 70% ammonium sulfate, salting out, dialyzing the precipitate, ultrafiltering at 6000rpm and 4 deg.C for 20min, and vacuum freeze drying to obtain phycobiliprotein with food grade purity;
(2) weighing 2.71g of olive oil and 0.54g of jojoba oil, and mixing uniformly;
(3) weighing 0.18g of vitamin E, 0.4g of food-grade phycobiliprotein prepared in the step (1), 0.03g of octyldodecanol and 0.21g of cetyl polyethylene glycol, and grinding and mixing the components uniformly for 5-10min by using a mortar until no particles exist;
(4) weighing 1.1g of white beeswax, and melting in a water bath at 75 ℃;
(5) after the white beeswax is melted, cooling to 62-65 ℃, adding the mixture of (2) and (3) and 0.01g of propyl hydroxybenzoate weighed into the melted white beeswax in portions, and quickly mixing uniformly for 1 min;
(6) and (5) pouring the mixed material in the step (5) into a lipstick mould while the mixed material is hot, cooling for 30min, demoulding, and sealing for storage.
The obtained paste is bluish purple, the smearing effect is bluish purple, and the finished product of the comparative example 2 is shown in figure 5, the paste is slightly rough in texture, more in surface pores, not glossy, and has moderate moisture and an antioxidant function.
Table 1 evaluation table of products of the present invention and comparative examples
Claims (6)
1. A phycobiliprotein-containing lipstick and lip balm product is characterized by comprising the following raw materials:
phycobiliprotein-containing lipstick:
a matrix system: white beeswax, oleum Olivarum, and jojoba oil
And (3) coloring system: phycobiliprotein, carmine
A moisturizing system: vitamin E
Additive system: octyl dodecanol, cetyl polyethylene glycol, propyl paraben lip gloss:
a matrix system: white beeswax, oleum Olivarum, and jojoba oil
And (3) coloring system: phycobiliprotein
A moisturizing system: vitamin E
Additive system: octyl dodecanol, cetyl polyethylene glycol, propyl p-hydroxybenzoate.
2. The phycobiliprotein-containing lipstick and lip balm according to claim 1, wherein the lipstick comprises the following raw materials in parts by weight: 4-7 parts of white beeswax, 4-10 parts of olive oil, 1-4 parts of jojoba oil, 0.5-2 parts of vitamin E, 0.5-2 parts of phycoerythrin, 0.5-2 parts of carmine (lipstick does not need to be added), 0.05-0.2 part of octyl dodecanol, 0.8-3 parts of cetyl polyethylene glycol and 0.01-0.05 part of propyl paraben.
3. The phycobiliprotein lipstick and lip balm according to claim 1, wherein said phycobiliprotein is prepared by the method comprising the steps of: breaking cell wall of Sargassum with deionized water, pulverizing, freezing and thawing in refrigerator at-20- -30 deg.C for 3-5 times, filtering the crude extractive solution, adding 70% ammonium sulfate, salting out, dialyzing the precipitate, ultrafiltering at 5000-6000 rpm and 4 deg.C for 20-30 min, and vacuum freeze drying to obtain phycobiliprotein with food grade purity.
4. A phycobiliprotein-containing lipstick and lip balm according to claim 3, wherein: the seaweed comprises one or more of thallus Porphyrae, thallus Gracilariae, Polysiphonia urceolata, herba Gelidonii, Gelidium amansii, herba Pteridis Virginianum, Cladosiphon okamuranus, Gracilaria, Laurencia virescens, Corallium japonicum Kishinouye, and Grateloupia filicina.
5. The method for preparing phycobiliprotein lipstick and lip balm according to claim 1, comprising the steps of:
(1) mixing oleum Olivarum and oleum Simmondsia chinensis uniformly;
(2) grinding vitamin E, octyldodecanol, cetyl polyethylene glycol, phycobiliprotein, and carmine (lipstick is not required to be added) with mortar, and mixing for 5-10min until no granule exists;
(3) melting the white beeswax in water bath at 65-100 ℃;
(4) after the white beeswax is melted, cooling to 60-70 ℃, adding the mixture of (1) and (2) and propylparaben into the melted white beeswax in several times, and quickly (1-5min) mixing uniformly;
(5) and (4) pouring the mixed material in the step (4) into a lipstick mould while the mixed material is hot, cooling for 30-50min, and demoulding to finish the preparation.
6. The method for preparing phycobiliprotein lipstick and lip balm as claimed in claim 5, wherein the temperature in step (4) is 62 ℃ to 65 ℃ and the time for rapid mixing is 1 to 2 min.
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