CN113499291A - Pseudo-ginseng freckle removing mask and preparation method thereof - Google Patents
Pseudo-ginseng freckle removing mask and preparation method thereof Download PDFInfo
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
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Abstract
The invention discloses a pseudo-ginseng freckle-removing mask and a preparation method thereof, belonging to the technical field of skin care products, wherein the mask comprises the following raw materials: notoginseng radix, fructus Hippophae, folium Allii tuberosi, radix Rhodiolae, radix Dauci Sativae, fructus Luffae, fructus Hordei Germinatus, radix Puerariae, herba Menthae and herba plantaginis; the preparation method comprises the following steps: weighing and crushing the raw materials, carrying out infrared irradiation treatment on the pseudo-ginseng, the malt and the plantain, then adding dried sea buckthorn fruits, Chinese chives, rhodiola rosea, towel gourds, kudzu roots, mint and carrots, adding water, stirring, carrying out ultrasonic treatment and standing, then centrifuging, and infiltrating facial mask cloth with the obtained filtrate; the pseudo-ginseng freckle-removing mask disclosed by the invention can not only break away generated melanin, but also fundamentally inhibit the synthesis of the melanin, so that the effects of removing skin spots and preventing skin from rebounding are achieved; according to the invention, by controlling the preparation process, all the finally obtained water-soluble components are obtained, and the problems of poor experience feeling and other skin problems caused by the poor experience feeling due to the fat-soluble components contained in the existing freckle-removing facial mask are avoided.
Description
Technical Field
The invention belongs to the technical field of skin care products, and particularly relates to a pseudo-ginseng freckle removing mask and a preparation method thereof.
Background
As modern people have fast pace of life, high pressure, irregular diet and sleep, sunburn radiation, electromagnetic radiation and the like, spots such as color spots, freckles, sunburn, chloasma, senile spots, cyasma, radiation spots and the like appear on the skin of many people, skin spots are mainly caused by hyperpigmentation, and after the skin is stimulated to become sensitive, a human body can be in a self-protection state in order to protect the skin and resist external invasion, at the moment, melanocytes existing in the human body can secrete melanin, and the pigment can move layer by layer through cell metabolism to form freckles, sunburn and the like on the skin epidermis. According to the theory of traditional Chinese medicine, the problems of the skin are actually the expression of 'blood stasis obstruction', the spots are really and thoroughly removed, the skin can be solved from the deep layer of the skin, the skin needs to go deep into the bottom layer of the skin to block the synthesis of melanin, and the accumulated and precipitated melanin is scattered to improve the metabolism function of the skin. The existing spot-removing products often have the problem of temporary solution and permanent solution, spots are obviously improved in the using process of the products, and the spots rebound once the products are stopped. Therefore, there is a need to develop a product that can remove freckles fundamentally to eliminate the trouble of skin spotting.
Some traditional Chinese medicine components have good effects on removing freckles, and a large number of traditional Chinese medicine component-added freckle-removing facial masks are available at present, but various essential oil components are usually added into raw materials of the traditional Chinese medicine freckle-removing facial mask, or water-soluble components and fat-soluble components in the traditional Chinese medicine raw materials are extracted by high-temperature decoction to serve as effective components of the facial mask, so that the traditional Chinese medicine freckle-removing facial mask is high in oiliness, when the traditional Chinese medicine freckle-removing facial mask is directly applied to the face or applied to the face in a facial mask paper mode, the contacted hair is easily greasy, so that a great deal of inconvenience is brought, poor experience is caused, facial pores are blocked in the using process, and other skin problems such as acne growing and the like are easily caused while people feel uncomfortable.
Disclosure of Invention
In order to solve the problems in the prior art, the invention provides a pseudo-ginseng freckle-removing mask and a preparation method thereof.
In order to achieve the purpose, the invention provides the following technical scheme:
the invention provides a pseudo-ginseng freckle removing mask which comprises the following raw materials in parts by weight: 50-60 parts of pseudo-ginseng, 20-30 parts of dried sea buckthorn, 5-8 parts of Chinese chives, 10-30 parts of rhodiola rosea, 10-15 parts of carrots, 20-25 parts of towel gourds, 5-10 parts of malt, 10-20 parts of kudzu roots, 5-10 parts of mint and 20-30 parts of plantain seeds.
Preferably, the raw materials comprise the following components in parts by weight: 55 parts of pseudo-ginseng, 25 parts of dried sea-buckthorn fruit, 6 parts of Chinese chives, 20 parts of rhodiola rosea, 12 parts of carrots, 23 parts of towel gourds, 8 parts of malt, 15 parts of kudzu roots, 8 parts of mint and 25 parts of plantain.
The invention also provides a preparation method of the pseudo-ginseng freckle-removing mask, which comprises the following steps: weighing the raw materials according to the weight parts, crushing, carrying out infrared irradiation treatment on the crushed panax notoginseng, the crushed malt and the crushed plantain, then adding the crushed dried hippophae rhamnoides, the crushed Chinese chives, the crushed rhodiola rosea, the crushed towel gourd, the crushed kudzu root, the crushed mint and the crushed carrot, adding water, stirring, carrying out ultrasonic treatment and standing, then carrying out centrifugation, and infiltrating a mask cloth with the obtained filtrate to obtain the panax notoginseng freckle removing mask.
Preferably, the crushing is carried out until the particle size is 1-3 mm.
Preferably, the infrared ray is short-wave infrared ray with the wavelength of 1-1.5 mu m.
Preferably, the irradiation distance is 15-20 cm, and the irradiation time is 50-60 s.
Preferably, the water adding amount is 3-5 times of the total weight of the raw materials.
Preferably, the power of ultrasonic treatment is 400-500W, the frequency is 20-30 KHz, and the time is 1-2 min.
Preferably, the pressure intensity during ultrasonic treatment is 5-8 MPa.
Preferably, the standing time is 10-12 h, and the standing is carried out at 4 ℃.
Compared with the prior art, the invention has the following beneficial effects:
the invention adopts the pseudo-ginseng with the functions of promoting blood circulation to remove blood stasis, benefiting qi and nourishing blood as a main raw material, and matches dried sea-buckthorn fruit, Chinese chives, rhodiola rosea, carrots, luffa, malt, kudzu roots, plantain and the like, and the components in the pseudo-ginseng, the malt and the plantain are changed by carrying out infrared irradiation treatment, so that more water-soluble components with the freckle removing effect are obtained by subsequent normal-temperature water extraction; the raw materials are subjected to ultrasonic treatment and standing extraction, so that water-soluble components in the raw materials are fully extracted, and under the combined action of effective components extracted from the raw materials, the pseudo-ginseng freckle removing mask disclosed by the invention can not only disperse generated melanin, but also fundamentally inhibit the synthesis of the melanin, so that the effects of removing skin spots and preventing skin from rebounding are achieved.
According to the invention, by controlling the preparation process, all the finally obtained water-soluble components are obtained, and the problems of poor experience feeling and other skin problems caused by the poor experience feeling due to the fat-soluble components contained in the existing freckle-removing facial mask are avoided.
Detailed Description
Reference will now be made in detail to various exemplary embodiments of the invention, the detailed description should not be construed as limiting the invention but as a more detailed description of certain aspects, features and embodiments of the invention.
It is to be understood that the terminology used herein is for the purpose of describing particular embodiments only and is not intended to be limiting of the invention.
Further, for numerical ranges in this disclosure, it is understood that each intervening value, between the upper and lower limit of that range, is also specifically disclosed. Every smaller range between any stated value or intervening value in a stated range and any other stated or intervening value in a stated range is encompassed within the invention. The upper and lower limits of these smaller ranges may independently be included or excluded in the range.
Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs. Although only preferred methods and materials are described herein, any methods and materials similar or equivalent to those described herein can be used in the practice or testing of the present invention. All documents mentioned in this specification are incorporated by reference herein for the purpose of disclosing and describing the methods and/or materials associated with the documents. In case of conflict with any incorporated document, the present specification will control.
It will be apparent to those skilled in the art that various modifications and variations can be made in the specific embodiments of the present disclosure without departing from the scope or spirit of the disclosure. Other embodiments will be apparent to those skilled in the art from consideration of the specification. The description and examples are intended to be illustrative only.
As used herein, the terms "comprising," "including," "having," "containing," and the like are open-ended terms that mean including, but not limited to.
The "parts" in the present invention are in parts by weight unless otherwise specified.
Example 1
The preparation method of the pseudo-ginseng freckle-removing mask comprises the following steps:
(1) weighing 55 parts of pseudo-ginseng, 25 parts of dried sea buckthorn fruit, 6 parts of Chinese chives, 20 parts of rhodiola rosea, 12 parts of carrots, 23 parts of towel gourds, 8 parts of malt, 15 parts of kudzuvine roots, 8 parts of mint and 25 parts of plantain seeds;
(2) crushing the raw materials, and sieving the crushed raw materials with a 10-mesh sieve to obtain the raw materials with the particle size of 1.7 mm;
(3) mixing pulverized Notoginseng radix, fructus Hordei Germinatus and Plantago Ovata, and irradiating with infrared ray of 1 μm for 60s at a distance of 15 cm;
(4) adding crushed dried sea buckthorn fruits, Chinese chives, rhodiola rosea, loofah, kudzu roots, mint and carrots into the raw materials subjected to infrared irradiation treatment in the step (3), adding deionized water 4 times of the total weight of all the raw materials, uniformly stirring, performing ultrasonic treatment under the pressure of 8Mpa, wherein the ultrasonic treatment power is 500W, the frequency is 25KHz, the time is 2min, standing and extracting for 12h at the temperature of 4 ℃ after the ultrasonic treatment is finished, centrifuging, standing the obtained filtrate for 15d, observing that no layering occurs, and infiltrating facial mask cloth with the obtained filtrate to obtain the pseudo-ginseng freckle removing facial mask.
Example 2
The preparation method of the pseudo-ginseng freckle-removing mask comprises the following steps:
(1) weighing 50 parts of pseudo-ginseng, 20 parts of dried sea buckthorn fruit, 8 parts of Chinese chives, 30 parts of rhodiola rosea, 10 parts of carrots, 20 parts of towel gourds, 10 parts of malt, 10 parts of kudzuvine roots, 5 parts of mint and 30 parts of plantain seeds;
(2) crushing the raw materials, and sieving the crushed raw materials with a 10-mesh sieve to obtain the raw materials with the particle size of 1.7 mm;
(3) performing infrared irradiation treatment on pulverized Notoginseng radix, fructus Hordei Germinatus and herba plantaginis of Longipedunn, wherein the infrared wavelength is 1.5 μm, the irradiation distance is 20cm, and the irradiation time is 50 s;
(4) adding the crushed dried sea buckthorn fruits, the leeks, the rhodiola rosea, the loofah, the radix puerariae, the mint and the carrots into the raw materials subjected to the infrared irradiation treatment in the step (3), adding deionized water which is 3 times of the total weight of all the raw materials, uniformly stirring, carrying out ultrasonic treatment under the pressure of 5Mpa, wherein the power of ultrasonic treatment is 400W, the frequency is 20KHz, the time is 2min, standing and extracting for 10h at the temperature of 4 ℃ after the ultrasonic treatment is finished, centrifuging, standing the obtained filtrate for 15d, observing that no layering occurs, and infiltrating a mask cloth with the obtained filtrate to obtain the pseudo-ginseng freckle removing mask.
Example 3
The preparation method of the pseudo-ginseng freckle-removing mask comprises the following steps:
(1) weighing 60 parts of pseudo-ginseng, 30 parts of dried sea buckthorn fruit, 5 parts of Chinese chives, 10 parts of rhodiola rosea, 15 parts of carrots, 25 parts of towel gourd, 5 parts of malt, 20 parts of kudzuvine roots, 10 parts of mint and 20 parts of plantain seeds;
(2) crushing the raw materials, and sieving the crushed raw materials with a 10-mesh sieve to obtain the raw materials with the particle size of 1.7 mm;
(3) performing infrared irradiation treatment on pulverized Notoginseng radix, fructus Hordei Germinatus and herba plantaginis of Longipedunn, wherein the infrared wavelength is 1 μm, the irradiation distance is 15cm, and the irradiation time is 60 s;
(4) adding the crushed dried sea buckthorn fruits, the leeks, the rhodiola rosea, the loofah, the radix puerariae, the mint and the carrots into the raw materials subjected to the infrared irradiation treatment in the step (3), adding deionized water which is 5 times of the total weight of all the raw materials, uniformly stirring, performing ultrasonic treatment under the pressure of 7Mpa, wherein the power of the ultrasonic treatment is 450W, the frequency is 30KHz, the time is 1min, standing and extracting for 12h at the temperature of 4 ℃ after the ultrasonic treatment is finished, centrifuging, standing the obtained filtrate for 15d, observing that no layering occurs, and infiltrating a facial mask cloth with the obtained filtrate to obtain the pseudo-ginseng freckle removing facial mask.
Example 4
The preparation method of the pseudo-ginseng freckle-removing mask comprises the following steps:
(1) weighing 55 parts of pseudo-ginseng, 25 parts of dried sea buckthorn fruit, 6 parts of Chinese chives, 20 parts of rhodiola rosea, 12 parts of carrots, 23 parts of towel gourds, 8 parts of malt, 15 parts of kudzuvine roots, 8 parts of mint and 25 parts of plantain seeds;
(2) crushing the raw materials, and sieving the crushed raw materials with a 10-mesh sieve to obtain the raw materials with the particle size of 1.7 mm;
(3) mixing pulverized Notoginseng radix, fructus Hordei Germinatus and Plantago Ovata, and irradiating with infrared ray of 1 μm for 60s at a distance of 15 cm;
(4) adding crushed dried sea buckthorn fruits, Chinese chives, rhodiola rosea, towel gourds, kudzu roots, mint and carrots into the raw materials subjected to infrared irradiation treatment in the step (3), adding deionized water 4 times of the total weight of all the raw materials, uniformly stirring, performing ultrasonic treatment under the pressure of 8Mpa, performing ultrasonic treatment at the power of 500W and the frequency of 25KHz for 1min, performing intermittent treatment for 1min, performing ultrasonic treatment for 1min, standing and extracting for 12h at the temperature of 4 ℃, centrifuging, standing the obtained filtrate for 15d, observing no layering, and infiltrating facial mask cloth with the obtained filtrate to obtain the pseudo-ginseng freckle removing facial mask.
Example 5
The preparation method of the pseudo-ginseng freckle-removing mask comprises the following steps:
(1) weighing 55 parts of pseudo-ginseng, 25 parts of dried sea buckthorn fruit, 6 parts of Chinese chives, 20 parts of rhodiola rosea, 12 parts of carrots, 23 parts of towel gourds, 8 parts of malt, 15 parts of kudzuvine roots, 8 parts of mint and 25 parts of plantain seeds;
(2) crushing the raw materials, and sieving the crushed raw materials with a 10-mesh sieve to obtain the raw materials with the particle size of 1.7 mm;
(3) mixing pulverized Notoginseng radix, fructus Hordei Germinatus and Plantago Ovata, and irradiating with infrared ray of 1 μm for 60s at a distance of 15 cm;
(4) adding crushed dried sea buckthorn fruits, Chinese chives, rhodiola rosea, loofah, kudzu roots, mint and carrots into the raw materials subjected to infrared irradiation treatment in the step (3), adding deionized water 4 times of the total weight of all the raw materials, uniformly stirring, performing ultrasonic treatment under the pressure of 8Mpa, wherein the ultrasonic treatment power is 500W, the frequency is 25KHz, the time is 2min, standing and extracting for 12h at the temperature of 4 ℃ after the ultrasonic treatment is finished, centrifuging, adding 3 parts of nano tourmaline powder into the obtained filtrate, uniformly stirring, and infiltrating facial mask cloth with the obtained liquid to obtain the pseudo-ginseng freckle removing facial mask.
Example 6
The preparation method of the pseudo-ginseng freckle-removing mask comprises the following steps:
(1) weighing 55 parts of pseudo-ginseng, 25 parts of dried sea buckthorn fruit, 6 parts of Chinese chives, 20 parts of rhodiola rosea, 12 parts of carrots, 23 parts of towel gourds, 8 parts of malt, 15 parts of kudzuvine roots, 8 parts of mint and 25 parts of plantain seeds;
(2) crushing the raw materials, and sieving the crushed raw materials with a 10-mesh sieve to obtain the raw materials with the particle size of 1.7 mm;
(3) freezing the pulverized raw materials at-20 deg.C for 10h, mixing Notoginseng radix, fructus Hordei Germinatus and herba plantaginis, and irradiating with infrared ray at wavelength of 1 μm and irradiation distance of 15cm for 60 s;
(4) adding crushed dried sea buckthorn fruits, Chinese chives, rhodiola rosea, loofah, kudzu roots, mint and carrots into the raw materials subjected to infrared irradiation treatment in the step (3), adding deionized water 4 times of the total weight of all the raw materials, uniformly stirring, performing ultrasonic treatment under the pressure of 8Mpa, wherein the ultrasonic treatment power is 500W, the frequency is 25KHz, the time is 2min, standing and extracting for 12h at the temperature of 4 ℃ after the ultrasonic treatment is finished, centrifuging, standing the obtained filtrate for 15d, observing that no layering occurs, and infiltrating facial mask cloth with the obtained filtrate to obtain the pseudo-ginseng freckle removing facial mask.
Comparative example 1
The difference from example 1 is that no Plantago asiatica is added in step (1).
Comparative example 2
The difference from example 1 is that step (3) is not included, i.e., the infrared irradiation treatment is not performed on notoginseng, malt and plantain.
Comparative example 3
The difference from example 1 is that the sonication in step (4) is carried out at atmospheric pressure.
Effect verification
135 patients with different types and different degrees of spots (not including white spots) on the face are selected and randomly divided into 9 groups, 15 patients in each group are applied with the pseudo-ginseng spot-removing facial masks prepared in the examples 1 to 6 and the comparative examples 1 to 3 respectively, each group of patients is applied for 3 times per week for 15min each time, and after 2 months, the using effect is observed and evaluated, if the spots disappear, the effect is marked as obvious effect: the spots faded as effective; the spot fading was not noticeable or was darker or more numerous than before use, and the total effective rate (%) was (number of effects + number of effects)/15 × 100%, and the evaluation results of each group are shown in table 1:
TABLE 1
Group of | Show effect | Is effective | Invalidation | Total effective rate/%) |
Example 1 | 9 | 5 | 1 | 93.3 |
Example 2 | 7 | 6 | 2 | 86.7 |
Example 3 | 8 | 6 | 1 | 93.3 |
Example 4 | 9 | 6 | 0 | 100 |
Example 5 | 12 | 3 | 0 | 100 |
Example 6 | 10 | 5 | 0 | 100 |
Comparative example 1 | 3 | 5 | 7 | 53.3 |
Comparative example 2 | 4 | 5 | 6 | 60.0 |
Comparative example 3 | 3 | 6 | 6 | 60.0 |
As can be seen from table 1, the pseudo-ginseng spot-removing mask prepared by the invention can effectively remove various spots on the skin, and as can be seen from the comparison of the examples 1, 4 and 6, the spot-removing effect of the finally obtained mask can be improved by setting the ultrasonic treatment to be an intermittent mode or performing the freezing treatment on the raw materials in advance, which is probably because the extraction rate of water-soluble active ingredients in the raw materials can be improved by performing the intermittent ultrasonic treatment and performing the freezing treatment on the raw materials in advance; as can be seen from the comparison between example 1 and example 5, the addition of nano tourmaline powder to the obtained filtrate can also improve the freckle-removing effect, which is probably because the nano tourmaline powder can promote skin metabolism and better promote the dispersion and elimination of melanin after contacting the skin.
After 3 months, each group of patients are followed up, and the patients applying the pseudo-ginseng freckle removing mask prepared in the examples 1-6 are found to have no longer freckles, namely no rebound occurs, so that the pseudo-ginseng freckle removing mask disclosed by the invention can fundamentally inhibit the synthesis of melanin and achieve the effect of removing freckles for a long time.
The above description is only for the preferred embodiment of the present invention, and the protection scope of the present invention is not limited thereto, and any person skilled in the art should be able to cover the technical scope of the present invention, the technical solution and the inventive concept of the present invention equivalent or change within the technical scope of the present invention.
Claims (10)
1. The pseudo-ginseng freckle removing mask is characterized by comprising the following raw materials in parts by weight: 50-60 parts of pseudo-ginseng, 20-30 parts of dried sea buckthorn, 5-8 parts of Chinese chives, 10-30 parts of rhodiola rosea, 10-15 parts of carrots, 20-25 parts of towel gourds, 5-10 parts of malt, 10-20 parts of kudzu roots, 5-10 parts of mint and 20-30 parts of plantain seeds.
2. The pseudo-ginseng spot removing mask according to claim 1, which is characterized by comprising the following raw materials in parts by weight: 55 parts of pseudo-ginseng, 25 parts of dried sea-buckthorn fruit, 6 parts of Chinese chives, 20 parts of rhodiola rosea, 12 parts of carrots, 23 parts of towel gourds, 8 parts of malt, 15 parts of kudzu roots, 8 parts of mint and 25 parts of plantain.
3. A preparation method of the pseudo-ginseng freckle removing mask as claimed in any one of claims 1 to 2, which is characterized by comprising the following steps: weighing the raw materials according to the weight parts, crushing, carrying out infrared irradiation treatment on the crushed panax notoginseng, the crushed malt and the crushed plantain, then adding the crushed dried hippophae rhamnoides, the crushed Chinese chives, the crushed rhodiola rosea, the crushed towel gourd, the crushed kudzu root, the crushed mint and the crushed carrot, adding water, stirring, carrying out ultrasonic treatment and standing, then carrying out centrifugation, and infiltrating a mask cloth with the obtained filtrate to obtain the panax notoginseng freckle removing mask.
4. The method according to claim 3, wherein the pulverization is carried out to a particle size of 1 to 3 mm.
5. The method according to claim 3, wherein the infrared ray is a short-wave infrared ray having a wavelength of 1 to 1.5 μm.
6. The method according to claim 3, wherein the irradiation distance is 15 to 20cm, and the irradiation time is 50 to 60 seconds.
7. The preparation method according to claim 3, wherein the amount of water added is 3 to 5 times of the total weight of the raw materials.
8. The preparation method according to claim 3, wherein the ultrasonic treatment is performed at a power of 400-500W, a frequency of 20-30 KHz and a time of 1-2 min.
9. The production method according to claim 3, wherein the pressure at the time of the ultrasonic treatment is 5 to 8 MPa.
10. The preparation method according to claim 3, wherein the standing time is 10 to 12 hours, and the standing is performed at 4 ℃.
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