CN113498816A - Agilawood tea powder and preparation method and application thereof - Google Patents
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F3/00—Tea; Tea substitutes; Preparations thereof
- A23F3/34—Tea substitutes, e.g. matè; Extracts or infusions thereof
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- A—HUMAN NECESSITIES
- A21—BAKING; EDIBLE DOUGHS
- A21D—TREATMENT, e.g. PRESERVATION, OF FLOUR OR DOUGH, e.g. BY ADDITION OF MATERIALS; BAKING; BAKERY PRODUCTS; PRESERVATION THEREOF
- A21D13/00—Finished or partly finished bakery products
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- A—HUMAN NECESSITIES
- A21—BAKING; EDIBLE DOUGHS
- A21D—TREATMENT, e.g. PRESERVATION, OF FLOUR OR DOUGH, e.g. BY ADDITION OF MATERIALS; BAKING; BAKERY PRODUCTS; PRESERVATION THEREOF
- A21D2/00—Treatment of flour or dough by adding materials thereto before or during baking
- A21D2/08—Treatment of flour or dough by adding materials thereto before or during baking by adding organic substances
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Abstract
The invention discloses agilawood tea powder, which is prepared from agilawood seeds. Also discloses a preparation method of the agilawood tea powder and application of the agilawood tea powder in tea drinking and baking. The agilawood tea powder disclosed by the invention can fully utilize agilawood seed resources, reduce resource waste and provide richer raw materials for agilawood tea, and in addition, the agilawood tea powder is prepared by a fermentation method, so that the secondary conversion of microbes to agilawood substances is promoted, and the output of agilawood oil is improved.
Description
Technical Field
The invention relates to the technical field of agilawood processing, and particularly relates to agilawood tea powder and a preparation method and application thereof.
Background
Aquilaria agallocha, also called Aquilaria sinensis (lour.) Gilg, belongs to Aquilaria of Thymelaeaceae, is a tropical and subtropical evergreen tree, and is a unique precious medicinal plant in China. At present, the utilization of the agilawood is mainly concentrated on the production of the agilawood by the branches and the roots, but the agilawood formation period is too long, the trees are greatly damaged after the materials are taken, and the utilization rate of agilawood resources is very low. Generally speaking, eaglewood oil, which is an oily substance with low polarity or volatility and fragrance extracted from eaglewood, is mainly used for utilization of eaglewood. At present, more than 70 sesquiterpene compounds in volatile and semi-volatile components of the agilawood volatile oil are reported, more than 80 2- (2-phenethyl) chromone compounds are found, and more than 30 simple volatile aromatic components are also found. Modern pharmacological research finds that the active sesquiterpene component has the effects of tranquilizing and allaying excitement and invigorating stomach, the phenethyl chromone compound has activities in aspects of antianaphylaxis, neuroprotection and the like in different degrees, and the aromatic component has the effect of relieving cough and the like.
The quantity of seeds produced by the aquilaria sinensis trees every year is rich, but the aquilaria sinensis seeds are easy to rot in tropical and subtropical zones, and most of the aquilaria sinensis seeds are discarded except for a part of the aquilaria sinensis seeds which are used for seedling raising, so that great waste is caused. Along with the enlargement of planting area of aquilaria sinensis trees in recent years, more and more aquilaria sinensis seed resources are provided, but research and utilization of aquilaria sinensis seeds are still in a starting stage, in the prior art, the research on change of physiological and biochemical indexes of aquilaria sinensis seeds in a storage process is found in Zhadong et al, the research on analysis and evaluation of nutritional ingredients of aquilaria sinensis seeds is found in Cheng Wu Jing et al, the research on fat-soluble ingredients and anti-liver cancer activity of aquilaria sinensis seeds is found in Zheng Wei et al, the research on oxidation resistance of aquilaria sinensis seeds is also found, and the aquilaria sinensis seeds not only have rich nutrition, but also have certain health care efficacy. The prior eaglewood tea mostly uses eaglewood containing resin as a raw material, and part of eaglewood leaves are used as the raw material of the eaglewood tea, but the application of the eaglewood seeds in tea drinking and baking needs to be researched.
Disclosure of Invention
Therefore, the invention aims to provide agilawood powder containing agilawood seeds, and the agilawood powder is prepared by a fermentation method so as to improve the utilization value of agilawood resources.
The technical scheme of the invention is realized as follows:
an agilawood tea powder, wherein the raw material of the agilawood tea powder comprises agilawood seeds.
The technical scheme is that the raw materials of the agilawood tea powder also comprise a second raw material, and the second raw material is one or more of agilawood leaves, agilawood flowers and agilawood blocks containing resin which are mixed in any proportion.
The further technical scheme is that the weight ratio of the agilawood seeds to the second raw material is 1: 0.2-0.8.
A preparation method of the agilawood tea powder comprises the following steps of drying, crushing and mixing the raw materials at a low temperature in sequence to prepare mixed powder; fermenting the mixed powder, and drying at constant temperature to obtain agilawood tea powder; the low-temperature drying is to dry the raw materials for 12 to 24 hours at the low temperature of between 10 ℃ below zero and 4 ℃; the constant-temperature drying is constant-temperature drying at the temperature of 40-60 ℃ for 6-12 h.
The further technical proposal is that the fermentation is natural stacking fermentation for 5 to 10 days.
The further technical scheme is that the fermentation is artificial fermentation, and the artificial fermentation is fermentation for 12-48h under the conditions that the temperature is 35-38 ℃ and the humidity is 60-80% after mixing the mixed powder and the zymocyte.
The fermentation bacteria are one or more of the following mixed bacteria in any proportion, i.e. the trichoderma theobromae, the trichoderma chromotrichum, the trichoderma, the fusarium rubrum, the aspergillus, the mucor, the penicillium, the trichoderma, the schizophyllum, the cephalosporium and the fusarium.
The further technical scheme is that the weight ratio of the mixed powder to the zymocyte is as follows: 1:0.015-0.03.
The further technical scheme is that the crushing is ultramicro crushing, and the raw materials are crushed into powder with the granularity of more than 400 meshes.
An application of the above lignum Aquilariae Resinatum tea powder in tea drinking and baking is provided.
Compared with the prior art, the invention has the beneficial effects that:
(1) the agilawood tea has the advantages that agilawood seed resources are fully utilized, the resource waste is reduced, and richer raw materials are provided for agilawood tea.
(2) According to the invention, the agilawood tea powder is prepared by using a fermentation method, so that the secondary conversion of the microbes to agilawood substances is promoted, the output of the agilawood oil is improved, and the utilization rate of agilawood is further improved by fermentation.
(3) The method for preparing the agilawood tea powder by fermenting the agilawood seeds as the raw materials is favorable for improving the comprehensive quality of the agilawood tea powder, and the agilawood tea powder is mainly fine powder and yellow in appearance; the soup color is mainly yellow, bright and has no tea residue; the smell is mellow and thick; has rich taste and sweet aftertaste, and the comprehensive score is over 93 points.
(4) The agilawood tea powder provided by the invention fully exerts the medicinal efficacy of agilawood, increases the types and the purposes of agilawood tea, and meets the standard of NY/T2672-supplement 2015 tea powder.
(5) This application agalloch eaglewood tea powder owing to through superfine grinding, tea powder reaches more than 400 meshes, not only can guarantee that the fragrant and mellow of tea is strong, also can be applied to and bake, increase the flavor and the taste of cake.
Detailed Description
For clear and complete description of the technical solutions in the present invention, it is obvious that the inventor combines the embodiments to describe, but the following embodiments describe only some embodiments of the present invention, not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
An agilawood tea powder, wherein the raw material of the agilawood tea powder is agilawood seeds. The preparation method of the agilawood tea powder comprises the following steps: drying, crushing and mixing the agilawood seeds at low temperature in sequence to prepare agilawood powder; naturally stacking and fermenting the agilawood powder for 10 days, and drying at constant temperature to prepare agilawood tea powder; the low-temperature drying is to dry the raw materials for 24 hours at the low temperature of 4 ℃; the constant-temperature drying is carried out for 12 hours at the temperature of 60 ℃. The pulverization is ultramicro pulverization, and the raw materials are pulverized into 400-mesh powder. The agilawood tea powder is applied to tea drinks.
Example 2
An agilawood tea powder, wherein the raw material of the agilawood tea powder is agilawood seeds. The preparation method of the agilawood tea powder comprises the following steps: drying, crushing and mixing the agilawood seeds at low temperature in sequence to prepare agilawood powder; the agilawood powder is dried at constant temperature after being artificially fermented to prepare the agilawood tea powder; the low-temperature drying is to dry the raw materials for 24 hours at the low temperature of 4 ℃; the constant-temperature drying is carried out for 12 hours at the temperature of 60 ℃. The pulverization is ultramicro pulverization, and the raw materials are pulverized into 400-mesh powder. The agilawood tea powder is applied to tea drinks.
The artificial fermentation is to ferment the mixed powder and the zymophyte for 24 hours under the conditions of the temperature of 35 ℃ and the humidity of 80 percent. The fermentation bacteria are mixture of cacao diplodia, brick red fusarium, trichoderma, schizophyllum, cephalosporium and fusarium in any proportion. The weight ratio of the mixed powder to the zymocyte is as follows: 1:0.01.
Example 3
An agilawood tea powder is prepared from agilawood seeds and agilawood leaves. The weight ratio of the agilawood seeds to the agilawood leaves is 1: 0.5.
A preparation method of the agilawood tea powder comprises the following steps of drying, crushing and mixing the raw materials at a low temperature in sequence to prepare mixed powder; naturally stacking and fermenting the mixed powder for 5 days, and drying at constant temperature to prepare agilawood tea powder; the low-temperature drying is to dry the raw materials for 20 hours at the low temperature of 2 ℃; the constant-temperature drying is carried out for 12 hours at the temperature of 60 ℃. The pulverization is ultramicro pulverization, and the raw materials are pulverized into 650-mesh powder. The application of the agilawood tea powder in baking is provided.
Example 4
An agilawood tea powder is prepared from agilawood seeds and agilawood leaves. The weight ratio of the agilawood seeds to the agilawood leaves is 1: 0.5.
A preparation method of the agilawood tea powder comprises the following steps of drying, crushing and mixing the raw materials at a low temperature in sequence to prepare mixed powder; the mixed powder is dried at constant temperature after being artificially fermented to prepare agilawood tea powder; the low-temperature drying is to dry the raw materials for 20 hours at the low temperature of 2 ℃; the constant-temperature drying is carried out for 12 hours at the temperature of 60 ℃. The artificial fermentation is to mix the mixed powder and zymophyte and ferment for 36h at the temperature of 38 ℃ and the humidity of 80 percent. The fermentation bacteria are the mixture of the tricolor trichoderma theobromae, the chromotrichum, the coco globispora, the brick red fusarium, the aspergillus, the mucor, the penicillium, the trichoderma, the schizophyllum, the cephalosporium and the fusarium in any proportion. The weight ratio of the mixed powder to the zymocyte is as follows: 1:0.01. The pulverization is ultramicro pulverization, and the raw materials are pulverized into 650-mesh powder. The application of the agilawood tea powder in baking is provided.
Example 5
The agilawood tea powder comprises agilawood seeds and a second raw material, wherein the second raw material is agilawood leaves and agilawood blocks containing resin, and the weight ratio of the agilawood seeds to the second raw material is 1:0.2 by mixing the agilawood leaves and the agilawood blocks in a ratio of 1: 2.
A preparation method of the agilawood tea powder comprises the following steps of drying, crushing and mixing the raw materials at a low temperature in sequence to prepare mixed powder; naturally stacking and fermenting the mixed powder for 7 days, and drying at constant temperature to prepare agilawood tea powder; the low-temperature drying is to dry the raw materials for 12 hours at the low temperature of-10 ℃; the constant-temperature drying is constant-temperature drying at the temperature of 40 ℃ for 6 h. The pulverization is ultramicro pulverization, and the raw materials are pulverized into 800-mesh powder. An application of the lignum Aquilariae Resinatum tea powder in tea beverage is provided.
Example 6
The agilawood tea powder comprises agilawood seeds and a second raw material, wherein the second raw material is agilawood leaves and agilawood blocks containing resin, and the weight ratio of the agilawood seeds to the second raw material is 1:0.2 by mixing the agilawood leaves and the agilawood blocks in a ratio of 1: 2.
A preparation method of the agilawood tea powder comprises the following steps of drying, crushing and mixing the raw materials at a low temperature in sequence to prepare mixed powder; the mixed powder is dried at constant temperature after being artificially fermented to prepare agilawood tea powder; the low-temperature drying is to dry the raw materials for 12 hours at the low temperature of-10 ℃; the constant-temperature drying is constant-temperature drying at the temperature of 40 ℃ for 6 h. The artificial fermentation is to ferment the mixed powder and the zymophyte for 24 hours at the temperature of 35 ℃ and the humidity of 70 percent after being mixed. The fermentation bacteria are the mixture of the two-color botrytis cacao, the two-color botrytis mucor, the penicillium, the trichoderma, the schizophyllum, the cephalosporium and the fusarium in any proportion. The weight ratio of the mixed powder to the zymocyte is as follows: 1:0.015. The pulverization is ultramicro pulverization, and the raw materials are pulverized into 800-mesh powder. An application of the lignum Aquilariae Resinatum tea powder in tea beverage is provided.
Example 7
An lignum Aquilariae Resinatum tea powder comprises lignum Aquilariae Resinatum seed and lignum Aquilariae Resinatum flower. The weight ratio of the agilawood seeds to the agilawood flowers is 1: 0.6.
A preparation method of the agilawood tea powder comprises the following steps of drying, crushing and mixing the raw materials at a low temperature in sequence to prepare mixed powder; naturally stacking and fermenting the mixed powder for 5 days, and drying at constant temperature to prepare agilawood tea powder; the low-temperature drying is to dry the raw materials for 20 hours at the low temperature of 2 ℃; the constant-temperature drying is carried out for 12 hours at the temperature of 60 ℃. The pulverization is ultramicro pulverization, and the raw materials are pulverized into 650-mesh powder. The application of the agilawood tea powder in baking is provided.
Example 8
The agilawood tea powder comprises agilawood seeds and a second raw material, wherein the second raw material is agilawood leaves, agilawood flowers and resin-containing agilawood blocks which are mixed in a ratio of 1:1:1, and the weight ratio of the agilawood seeds to the second raw material is 1: 0.8.
A preparation method of the agilawood tea powder comprises the following steps of drying, crushing and mixing the raw materials at a low temperature in sequence to prepare mixed powder; the mixed powder is dried at constant temperature after being artificially fermented to prepare agilawood tea powder; the low-temperature drying is to dry the raw materials for 12 hours at the low temperature of-10 ℃; the constant-temperature drying is constant-temperature drying at the temperature of 40 ℃ for 6 h. The artificial fermentation is to ferment the mixed powder and the zymophyte for 24 hours at the temperature of 35 ℃ and the humidity of 70 percent after being mixed. The fermentation bacteria are the mixture of the two-color botrytis cacao, the two-color botrytis mucor, the penicillium, the trichoderma, the schizophyllum, the cephalosporium and the fusarium in any proportion. The weight ratio of the mixed powder to the zymocyte is as follows: 1:0.015. The pulverization is ultramicro pulverization, and the raw materials are pulverized into 800-mesh powder. An application of the lignum Aquilariae Resinatum tea powder in tea beverage is provided.
Comparative example 1
An agilawood tea powder, wherein agilawood leaves are used as raw materials of the agilawood tea powder. The preparation method of the agilawood powder is the same as that in example 1, and the agilawood leaves and the agilawood seeds in example 1 are collected from the same tree.
Comparative example 2
An agilawood tea powder is prepared from agilawood blocks containing resin. The preparation method of the agilawood tea powder is the same as that of the example 1, and the agilawood blocks containing the resin and the agilawood seeds of the example 1 are collected from the same tree.
Comparative example 3
An agilawood tea powder, wherein the raw material of the agilawood tea powder is agilawood flowers. The preparation method of the agilawood tea powder is the same as that of the example 1, and the agilawood blocks containing the resin and the agilawood seeds of the example 1 are collected from the same tree.
Tea powder sensory evaluation test
According to the GB/T23776-2018 tea sensory evaluation method, evaluation personnel comprehensively analyze and evaluate the appearance, liquor color, aroma and taste of the agilawood tea powder as tea powder. The evaluation personnel, the water for evaluation, the environment for evaluation, the operation method for evaluation and the like are all carried out according to GB/T23776-2018.
TABLE 1 sensory evaluation chart of Chenxiang tea powder
As is clear from Table 1, examples 1 to 8 are better in the overall evaluation (93 points or more) of appearance, liquor color, aroma and taste than comparative examples 1 to 3. The single eaglewood leaves are light in smell and green and astringent in taste; the single agilawood has light fragrance and taste; the smell and taste of the single resin-containing eaglewood block are too strong; the agilawood tea powder prepared by taking the agilawood seeds as the raw materials is higher than the agilawood tea powder prepared by single agilawood leaves, agilawood flowers or resin-containing agilawood blocks in overall comprehensive quality.
Physicochemical index of tea powder
According to the NY/T2672-2015 tea powder standard, the physicochemical indexes of the samples 1-6 are measured as shown in the following table 2, the particle sizes are all less than or equal to 75um, the water content is less than or equal to 6.0 percent, and the ash content is less than or equal to 7.0 percent, which meet the NY/T2672-2015 tea powder standard.
TABLE 2
Content determination of tea powder linaloe oil
By using supercritical CO2The fluid extraction method is to compare the content of the linaloe oil in the powder (or mixed powder) before fermentation with the content of the finished tea powder after constant-temperature drying after fermentation. Specific supercritical CO2The fluid extraction method comprises the following process conditions: soaking the powder before and after fermentation in water for 83h, air drying, adding entrainer ethyl acetate (material-liquid ratio 1: 1.2), extracting at 28MPa and 46 ℃ for 2h, collecting the extract every 0.5h, concentrating with a rotary evaporator after completely collecting, and calculating the extraction rate. Y (%) (W1/W2) × 100%, wherein: w1-weight of extracted oil (g); w2-weight of powder before extraction (g).
The results of measuring the contents of eaglewood powder and eaglewood oil according to the tea powders of examples 1 to 8 are shown in Table 3, and it can be seen from Table 3 that the powders (mixed powders) before fermentation of examples 1 to 8 are not only the powder of single ingredient of eaglewood seed, but also the powder of mixture of eaglewood seed and eaglewood leaf/eaglewood flower, or the powder of mixture of three of eaglewood seed, eaglewood leaf and eaglewood piece containing resin, or the powder of mixture of three of eaglewood seed, eaglewood leaf, eaglewood flower and eaglewood piece containing resin, and the supercritical CO is used2The extraction rate of the obtained linaloe oil by a fluid extraction method is between 24.8 and 45.6 percent.
As can be seen from the tea powder prepared by drying the fermented and constant-temperature tea powder of the embodiments 1 to 8, the supercritical CO is utilized to prepare the single-component agilawood seed powder, the mixed powder of the agilawood seed and the agilawood leaf/agilawood flower, the mixed powder of the agilawood seed, the agilawood leaf and the agilawood block containing the resin, or the mixed powder of the agilawood seed, the agilawood leaf, the agilawood flower and the agilawood block containing the resin2The fluid extraction method has the advantages that the extraction rate of the obtained linaloe oil is 30.6-54.5%, and the extraction rate after fermentation is higher than that before fermentation, which proves that the oil content of the linaloe powder is higher after fermentation, namely the fermentation promotes the secondary conversion of the linaloe substances.
As can be seen from the comparison of the examples 1 and 2, the comparison of the examples 3 and 4, and the comparison of the examples 5 and 6, the extraction rate of the artificial fermentation is higher than that of the natural fermentation, and the fermentation bacteria provided by the artificial fermentation can better ensure the secondary conversion of the agilawood substance, so that the content of the agilawood oil in the tea powder is increased. And the artificial fermentation will take less time than the natural fermentation.
TABLE 3
It was confirmed according to example 1 and comparative examples 1 to 3 that four agilawood seeds, agilawood leaves, agilawood flowers and agilawood blocks containing resin utilize supercritical CO under the same conditions2Fluid extraction method to obtain Chinese eaglewood oil with different contents, wherein the Chinese eaglewood oil block containing resin has the highest Chinese eaglewood oil content (related to selection of Chinese eaglewood block), the Chinese eaglewood seed has the next lowest Chinese eaglewood flower; and the oil content of the agilawood in the finished tea powder after fermentation and constant-temperature drying is higher than that before fermentation, because the fermentation promotes the secondary conversion of the agilawood substance, see table 4.
TABLE 4
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents, improvements and the like that fall within the spirit and principle of the present invention are intended to be included therein.
Claims (10)
1. The agilawood tea powder is characterized in that: the raw material of the agilawood tea powder comprises agilawood seeds.
2. The agilawood tea powder according to claim 1, wherein: the raw materials of the agilawood tea powder also comprise a second raw material, wherein the second raw material is one or more of agilawood leaves, agilawood flowers and agilawood blocks containing resin which are mixed in any proportion.
3. The agilawood tea powder according to claim 2, wherein: the weight ratio of the agilawood seeds to the second raw material is 1: 0.2-0.8.
4. A method for preparing the agilawood tea powder as claimed in any one of claims 1 to 3, which is characterized in that: drying, crushing and mixing the raw materials at low temperature in sequence to prepare mixed powder; fermenting the mixed powder, and drying at constant temperature to obtain agilawood tea powder; the low-temperature drying is to dry the raw materials for 12 to 24 hours at the low temperature of between 10 ℃ below zero and 4 ℃; the constant-temperature drying is constant-temperature drying at the temperature of 40-60 ℃ for 6-12 h.
5. The preparation method of the agilawood tea powder according to claim 4, characterized by comprising the following steps: the fermentation is natural stacking fermentation for 5-10 days.
6. The preparation method of the agilawood tea powder according to claim 4, characterized by comprising the following steps: the fermentation is artificial fermentation, and the artificial fermentation is carried out by mixing the mixed powder with zymophyte and then fermenting for 12-48h under the conditions of the temperature of 35-38 ℃ and the humidity of 60-80%.
7. The preparation method of the agilawood tea powder according to claim 6, characterized in that: the fermentation bacteria are one or more of the following components of the cacao trichoderma, the staphylotrichum, the cacao globisporus, the brick red fusarium, the aspergillus, the mucor, the penicillium, the trichoderma, the schizophyllum, the cephalosporium and the fusarium in any proportion.
8. The preparation method of the agilawood tea powder according to claim 6, characterized in that: the weight ratio of the mixed powder to the zymocyte is as follows: 1:0.015-0.03.
9. The preparation method of the agilawood tea powder according to claim 4, characterized by comprising the following steps: the pulverization is ultramicro pulverization, and the raw materials are pulverized into powder with the granularity of more than 400 meshes.
10. Use of the eaglewood tea powder according to any one of claims 1 to 3 or 5 to 9, wherein: the agilawood tea powder is applied to tea drinking and baking.
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