CN113402324A - Preparation method and preparation device of gibberellic acid-containing pesticide fertilizer granules - Google Patents
Preparation method and preparation device of gibberellic acid-containing pesticide fertilizer granules Download PDFInfo
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- CN113402324A CN113402324A CN202110794163.1A CN202110794163A CN113402324A CN 113402324 A CN113402324 A CN 113402324A CN 202110794163 A CN202110794163 A CN 202110794163A CN 113402324 A CN113402324 A CN 113402324A
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- kneading
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/12—Powders or granules
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/36—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids
- A01N37/38—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids having at least one oxygen or sulfur atom attached to an aromatic ring system
- A01N37/40—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids having at least one oxygen or sulfur atom attached to an aromatic ring system having at least one carboxylic group or a thio analogue, or a derivative thereof, and one oxygen or sulfur atom attached to the same aromatic ring system
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/06—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom five-membered rings
- A01N43/12—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom five-membered rings condensed with a carbocyclic ring
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/60—Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/10—Solid or semi-solid fertilisers, e.g. powders
- C05G5/12—Granules or flakes
Abstract
The invention discloses a preparation method of gibberellic acid-containing pesticide fertilizer granules, which comprises the following steps: preparing materials, namely taking 0.01 percent by weight of gibberellic acid, 10 percent by weight of urea, 5 percent by weight of monopotassium phosphate, 1 percent by weight of ammonium molybdate, 5 percent by weight of sodium salicylate, 2 percent by weight of adhesive, 1 percent by weight of disintegrant, 1 percent by weight of lubricant and the balance of filler, so that the problem that operators are difficult to operate on the ground due to higher plants in the later period of crops and perform pest control is solved, for example, the problems of corn, sugarcane and other crops are solved by topdressing fertilizers in the earlier period, and the poisoning risk of the operators is reduced; the invention also discloses a preparation device of the gibberellic acid pesticide fertilizer granules, materials can be fully kneaded by matching the screening mechanism with the kneading mechanism, the kneading time is effectively reduced, and the production efficiency of the pesticide fertilizer is improved.
Description
Technical Field
The invention relates to the technical field of pesticides, in particular to a preparation method of gibberellic acid-containing pesticide fertilizer granules, and particularly relates to a preparation device of gibberellic acid-containing pesticide fertilizer granules.
Background
Gibberellic acid is a broad-spectrum plant growth regulator, and can promote the growth and development of crops, make the crops mature in advance, improve the yield and improve the quality; can rapidly break the dormancy of organs such as seeds, tubers and bulbs and promote germination; reduce the falling of buds, flowers, bolls and fruits, improve the fruit bearing rate or form seedless fruits. Certain 2-year-old plants can also flower in the same year;
the urea is a relatively high-efficiency nitrogen fertilizer, has good nitrogen content, good quick action, long lasting period and mild temperament, and is not easy to cause adverse reactions such as seedling burning and the like;
the potassium dihydrogen phosphate is a novel high-concentration phosphorus-potassium two-element compound fertilizer, and contains about 52% of phosphorus pentoxide and about 34% of dipotassium oxide. The monopotassium phosphate has a plurality of excellent effects of remarkably increasing production and income, improving quantity and optimizing quality, resisting lodging, resisting diseases and insect pests, preventing and treating premature senility and the like, and has the effect of overcoming insufficient nutrition caused by the reduction of the aging and absorption capacity of the root system in the later growth stage of crops;
ammonium molybdate is used as a fertilizer, wherein molybdenum is an essential element for crop growth and plays roles in metabolism of nitrogen, phosphorus and carbohydrate, nitrogen fixation of rhizobia, formation of vitamin C, activation and inhibition of certain enzymes and the like;
salicylic acid is named as o-hydroxy benzoic acid, a kind of micromolecular phenolic substance widely existing in plants, is an intermediate product of phenylalanine metabolic pathway, and belongs to a derivative of cinnamic acid. Participating in various physiological and biochemical processes of plant transpiration, seed germination, flowering, fructification, stomatal closure, heat production and the like; inducing plants to generate various physiological characters such as disease resistance, salt resistance, cold resistance and the like, and also participating in the path of cyanogen-resistant respiration and non-phosphorylation of plant cell mitochondria, and improving the metabolic level of jasmonic acid in the plants. The salicylic acid is slightly soluble in water, and as the sodium salt of the salicylic acid, the sodium salicylate is easily soluble in water, so that the salicylic acid is convenient to apply in actual production;
when general crops grow to a certain period, the crops need to be sprayed with the pesticide to prevent the occurrence of plant diseases and insect pests, so that the crop yield is improved, but during the pesticide spraying period, the pesticide spraying is difficult due to the fact that the crops are high, the poisoning risk of operators is increased, meanwhile, due to the fact that the plants are high, the phenomenon that the pesticide is sprayed unevenly occurs, and the crop yield is influenced;
meanwhile, when the existing fertilizer is produced, the superfine powder agent needs to be prepared in advance due to production reasons, the prepared superfine powder agent is stored intensively, but the superfine powder is agglomerated due to moisture and other reasons during storage, so that the superfine powder cannot be dispersed and uniformly mixed quickly during kneading, the kneading work needs a longer time, and the phenomenon not only reduces the production efficiency of the pesticide fertilizer, but also influences the quality of the pesticide fertilizer.
Therefore, a preparation method and a preparation device of the gibberellic acid-containing medical fertilizer granules are provided.
Disclosure of Invention
The technical task of the invention is to provide a preparation method and a preparation device of gibberellic acid-containing medical fertilizer granules to solve the problems.
The technical scheme of the invention is realized as follows:
the invention provides a preparation method of gibberellic acid-containing pesticide fertilizer granules, which comprises the following steps:
s1, preparing materials, namely taking 0.01-0.03 wt% of gibberellic acid, 10-20 wt% of urea, 5-15 wt% of monopotassium phosphate, 1-5 wt% of ammonium molybdate, 5-10 wt% of sodium salicylate, 2-4 wt% of adhesive, 1-3 wt% of disintegrant, 1-3 wt% of lubricant and the balance of filler;
s2, mixing, namely putting the raw materials in the step S1 into a grinder for mixing grinding and crushing to prepare superfine powder;
s3, kneading, namely putting the superfine powder agent prepared in the step S2 into a screening tank of a preparation device containing gibberellic acid medical fertilizer granules for scattering and screening, feeding the scattered superfine powder agent into a kneading tank through a feeding pipe, and simultaneously adding water with the mass of 15-20% of the superfine powder agent into the kneading tank for fully kneading;
s4, granulating and drying, namely putting the kneaded material in the step S3 into a granulator for granulation;
s5, fluidizing, drying and screening, namely fluidizing the particles prepared in the step S4 by a fluidized bed, and then drying and screening to obtain the granules.
S6, checking and packaging; and (5) inspecting the finished product of the granules obtained in the step S5, and packaging to obtain the finished product.
Preferably, the binder in step S1 is selected from any one of starch slurry, ethyl cellulose, and hydroxypropyl cellulose.
Preferably, the binder in step S1 is selected from any one of starch slurry, ethyl cellulose, and hydroxypropyl cellulose.
Preferably, the lubricant in step S1 is selected from any one of stearic acid, calcium stearate, talc, sodium lauryl sulfate and glycine.
The invention also provides a preparation device of the gibberellic acid-containing pesticide fertilizer granules, which comprises a main body mechanism, wherein the main body mechanism comprises a base, and a first support and a second support are fixedly arranged on the upper surface of the base respectively;
the screening mechanism comprises a screening tank, the screening tank is fixedly mounted on the first support, a feeding opening is formed in the top of the screening tank, an annular groove body is fixedly connected to the inside of the screening tank, a screen plate is fixedly mounted on the annular groove body through bolts, a stirring motor is fixedly mounted at the top of the screening tank, a first rotating rod is rotatably arranged in the screening tank, the upper end of the first rotating rod is rotatably mounted outside the screening tank through a bearing, the top of the first rotating rod is fixedly connected with a rotating shaft of the stirring motor, a scattering rod is fixedly connected to the upper end of the first rotating rod and located above the screen plate, and the bottom of the screening tank is communicated with a feeding pipe;
the kneading mechanism comprises a kneading tank, the kneading tank is fixedly mounted on the second support, a feed inlet is formed in the upper end of the kneading tank, one end of the feed pipe is communicated with the feed inlet, a kneading motor is fixedly mounted at the top of the kneading tank, a rotating rod II is rotatably arranged in the kneading tank, the top of the rotating rod II is fixedly connected with a rotating shaft of the kneading motor through a first coupling, and an auxiliary assembly is arranged on the kneading tank; the auxiliary assembly is provided with two, two the auxiliary assembly symmetry sets up the both sides of kneading the motor, the auxiliary assembly includes auxiliary motor and dwang three, auxiliary motor fixed mounting be in knead the top of jar, dwang three passes through the bearing and rotates the installation in knead the inside of jar, the top of dwang three pass through shaft coupling two with auxiliary motor's pivot fixed connection, the surface of dwang two with the equal fixedly connected with helical blade of lower surface of dwang three is one, the upper end intercommunication of kneading the jar has the inlet tube, the bottom intercommunication of kneading the jar has the discharging pipe, fixed mounting has first solenoid valve on the discharging pipe.
Preferably, a scraping plate is fixedly connected to the first rotating rod, bristles are fixedly connected to the bottom of the scraping plate, and the bristles are in contact with the upper surface of the sieve plate.
Preferably, the water inlet pipe is fixedly provided with a second electromagnetic valve, and the water inlet pipe is provided with a flow sensor.
Preferably, a control panel is fixedly mounted on the upper surface of the base, a touch display screen is fixedly embedded on the surface of the control panel, a PLC controller is fixedly mounted inside the control panel, the PLC controller is electrically connected with the touch display screen, the flow sensor is electrically connected with a signal input end of the PLC controller, and a signal output end of the PLC controller is electrically connected with an electric control end of the stirring motor, an electric control end of the kneading motor, an electric control end of the auxiliary motor, an electric control end of the first electromagnetic valve and an electric control end of the second electromagnetic valve respectively.
Preferably, the lower end of the first rotating rod extends into the feeding pipe, and a second helical blade is fixedly connected to the outer wall of the lower end of the first rotating rod.
Preferably, the inner wall of the kneading tank and the surface of the first helical blade are coated with a teflon coating.
Compared with the prior art, the invention has the advantages and positive effects that:
1. the invention provides a method for preparing gibberellic acid-containing pesticide fertilizer granules, which comprises main components such as gibberellic acid, urea, monopotassium phosphate, ammonium molybdate, sodium salicylate and the like, and is used for preventing and controlling plant diseases and insect pests of crops such as corn, sugarcane and the like in the later period due to higher plants, so that the poisoning risk of personnel is reduced;
2. the preparation method of the gibberellic acid-containing pesticide-fertilizer granules provided by the invention has the advantages that pesticide-fertilizer is mutually assisted, and the prevention and the treatment of harmful organisms are beneficial to the health of crops and the absorption of fertilizer nutrients; in turn, nutrient absorption will improve the disease resistance of the crop and the absorption and transmission of endogenous pesticides.
3. According to the preparation device of the gibberellic acid-containing pesticide fertilizer granules, provided by the invention, materials can be sufficiently kneaded by matching the screening mechanism with the kneading mechanism, the kneading time is effectively reduced, the production efficiency of pesticide fertilizers is improved, and the production quality of pesticide fertilizers is improved.
Drawings
In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings needed in the embodiments will be briefly described below, and it is obvious that the drawings in the following description are only some embodiments of the present invention, and it is obvious for those skilled in the art to obtain other drawings without creative efforts.
Fig. 1 is a flow chart of a method for preparing gibberellic acid-containing fertilizer granules according to an embodiment of the present invention;
fig. 2 is a schematic structural diagram of a preparation device for gibberellic acid-containing medicinal fertilizer granules according to an embodiment of the present invention;
fig. 3 is a schematic sectional structure view of a sieving tank of a preparation apparatus for gibberellic acid-containing medicinal fertilizer granules according to an embodiment of the present invention;
FIG. 4 is a schematic structural view of a kneading tank of a device for preparing gibberellic acid-containing fertilizer granules according to an embodiment of the present invention;
FIG. 5 is a schematic sectional view showing the structure of a kneading tank of an apparatus for preparing gibberellic acid-containing fertilizer granules according to an embodiment of the present invention;
FIG. 6 is a schematic view showing a connection structure of a kneading tank and a sieving tank of a manufacturing apparatus for fertilizer granules containing gibberellic acid according to an embodiment of the present invention;
fig. 7 is a schematic view of the structure of an annular groove of a preparation device for gibberellic acid-containing medicinal fertilizer granules according to an embodiment of the present invention;
fig. 8 is a schematic structural view of a scraper of a preparation device containing gibberellic acid fertilizer granules according to an embodiment of the present invention;
fig. 9 is a circuit remote block diagram of a preparation device containing gibberellic acid fertilizer granules according to an embodiment of the present invention.
In the figure: 1. a main body mechanism; 101. a base; 102. a first bracket; 103. a second bracket;
2. a screening mechanism; 201. a screening tank; 202. a stirring motor; 203. rotating the first rod; 204. breaking up the rods; 205. a squeegee; 2051. brushing; 206. a sieve plate; 207. a second helical blade; 208. a feed pipe; 209. an annular groove body; 210. a feed port;
3. a kneading mechanism; 301. a kneading tank; 302. a feed inlet; 303. an auxiliary motor; 304. a kneading motor; 305. a water inlet pipe; 306. a second solenoid valve; 307. a flow sensor; 308. a discharge pipe; 309. a first solenoid valve; 310. a first helical blade; 311. rotating the rod III; 312. rotating the second rod;
4. a control panel; 401. a PLC controller; 402. a display screen is touched.
Detailed Description
In order that the above objects, features and advantages of the present invention can be more clearly understood, the present invention will be further described with reference to the accompanying drawings and examples. It should be noted that the embodiments and features of the embodiments of the present application may be combined with each other without conflict.
The invention is further described with reference to the following figures and specific examples.
Example 1.
As shown in fig. 1, the preparation method of gibberellic acid-containing fertilizer granules provided by the invention comprises the following steps:
s1, preparing materials, namely taking 0.01 wt% of gibberellic acid, 10 wt% of urea, 5 wt% of monopotassium phosphate, 1 wt% of ammonium molybdate, 5 wt% of sodium salicylate, 2 wt% of adhesive, 1 wt% of disintegrant, 1 wt% of lubricant and the balance of filler, wherein the adhesive is selected from any one of starch slurry, ethyl cellulose and hydroxypropyl cellulose, and the lubricant is selected from any one of stearic acid, calcium stearate, talcum powder, sodium dodecyl sulfate and glycine;
s2, mixing, namely putting the raw materials in the step S1 into a grinder for mixing grinding and crushing to prepare superfine powder;
s3, kneading, namely, putting the superfine powder agent prepared in the step S2 into a screening tank 201 of a preparation device containing gibberellic acid medical fertilizer granules for scattering and screening, feeding the scattered superfine powder agent into a kneading tank 301 through a feeding pipe 208, and simultaneously adding water accounting for 15-20% of the weight of the superfine powder agent into the kneading tank 301 for fully kneading;
s4, granulating and drying, namely putting the kneaded material in the step S3 into a granulator for granulation;
s5, fluidizing, drying and screening, namely fluidizing the particles prepared in the step S4 by a fluidized bed, and then drying and screening to obtain the granules.
S6, checking and packaging; and (5) inspecting the finished product of the granules obtained in the step S5, and packaging to obtain the finished product.
Example 2
The difference between this embodiment and embodiment 1 is that, in step S1, a material is prepared, by weight, taking gibberellic acid 0.02% by weight, urea 15% by weight, monopotassium phosphate 10% by weight, ammonium molybdate 2.5% by weight, sodium salicylate 7.5% by weight, a binder 3% by weight, a disintegrant 2% by weight, a lubricant 2% by weight, and a filler in balance, where the binder is any one selected from starch slurry, ethyl cellulose, and hydroxypropyl cellulose, and the lubricant is any one selected from stearic acid, calcium stearate, talc, sodium lauryl sulfate, and glycine;
example 3
The difference between this embodiment and embodiment 2 is that, in step S1, a material is prepared, by weight, including 0.03% of gibberellic acid, 20% of urea, 15% of monopotassium phosphate, 5% of ammonium molybdate, 10% of sodium salicylate, 3% of a binder, 3% of a disintegrant, 3% of a lubricant, and the balance of a filler, where the binder is any one of starch slurry, ethyl cellulose, and hydroxypropyl cellulose, and the lubricant is any one of stearic acid, calcium stearate, talc, sodium lauryl sulfate, and glycine.
Rice growth promotion test:
the test is arranged in the south Henan province, New county, republic of the plain, Korean village, rural plum village, and the test agent is provided by Zhengzhou nongda biochemical products Co., Ltd and contrasts with ternary compound fertilizer (20-10-10) (purchased from city).
Test work: rice (Oryza sativa L.) with improved resistance to stress
Cell area: 20m2
The application method comprises the following steps: spreading in the jointing stage of rice, investigating spike weight and yield
Designing a test scheme:
TABLE 1 design of test Agents
| Treatment of | Medicament | The amount of the fertilizer is spread to each |
|
| 1 | The agent prepared in example 1 of the | 5kg | |
| 2 | The agent prepared in example 2 of the | 5kg | |
| 3 | The agent prepared in example 3 of the | 5kg | |
| 4 | The agent prepared in example 1 of the present invention | 10kg | |
| 5 | The agent prepared in example 2 of the present invention | 10kg | |
| 6 | The agent prepared in example 3 of the present invention | 10kg | |
| 7 | Ternary compound fertilizer (20-10-10) | 20kg | |
| 8 | Control | Not applying fertilizer |
The investigation method comprises the following steps:
according to the five-point sampling method, one hole of rice is taken for each point, and after the rice is mature, the weight gain rate and yield of the rice are measured.
Thousand grain weight gain (%) = (treated area ear thousand grain weight-control area ear thousand grain weight)/control area ear thousand grain weight 100;
yield increase (%) = (treatment zone yield-control zone yield)/control zone yield 100;
TABLE 2 Effect of the products of the invention on thousand kernel weight and yield of rice after treatment
As shown in Table 2, the yield of the product of the present invention was significantly increased after the product was applied to rice, and the plants were grown normally without abnormal physiological changes in the treatments with each application.
After the application, the thousand seed weight of the rice is increased, and the gibberellic acid, urea, monopotassium phosphate, ammonium molybdate and sodium salicylate granules are applied in a broadcast mode with the dosage of 5kg per mu: the thousand seed weight gain rate of the compound fertilizer in example 1, example 2 and example 3 is respectively 8.24%, 9.12% and 9.96% compared with the blank control, and the thousand seed weight gain rate of the compound fertilizer in the three-component compound fertilizer is 7.20% compared with the blank control; the dosage of the granules per mu is 10 kg: the single fruit weight gains of example 1, example 2 and example 3 were 7.72%, 8.72% and 9.56%, respectively, compared with the blank control.
After the application, the rice yield is increased, and the gibberellic acid, urea, monopotassium phosphate, ammonium molybdate and sodium salicylate granules are applied in a broadcast mode with the dosage of 5kg per mu: the yield increase of the compound fertilizer of example 1, example 2 and example 3 is respectively 12.78%, 13.64% and 15.56% compared with the blank control, and the yield increase of the compound fertilizer of three elements is 9.28% compared with the blank control; the dosage of the granules per mu is 10 kg: the yield increase of the blank in example 1, example 2 and example 3 is 10.71%, 12.90% and 10.40%, respectively.
Example 4
Based on the above process, the device for preparing gibberellic acid-containing fertilizer granules according to the embodiments of the present invention, as shown in fig. 2 to 9, comprises a main body mechanism 1, a sieving mechanism 2, and a kneading mechanism 3;
as shown in fig. 2, the main body mechanism 1 is composed of a base 101, a first bracket 102 and a second bracket 103, wherein the first bracket 102 and the second bracket 103 are both fixedly installed on the upper surface of the base 101;
as shown in fig. 2-3 and 6-8, the screening mechanism 2 is composed of a screening tank 201, a stirring motor 202, a screen plate 206, a first rotating rod 203 and a multi-drink scattering rod 204;
the screening tank 201 is fixedly installed on the first support 102, a feeding port 210 is formed in the top of the screening tank 201, an annular groove body 209 is fixedly connected to the inside of the screening tank 201, a screening plate 206 is fixedly installed on the annular groove body 209 through bolts, a stirring motor 202 is fixedly installed at the top of the screening tank 201, a first rotating rod 203 is rotatably arranged inside the screening tank 201, the upper end of the first rotating rod 203 is rotatably installed outside the screening tank 201 through a bearing, the top of the first rotating rod 203 is fixedly connected with a rotating shaft of the stirring motor 202, a plurality of scattering rods 204 are fixedly connected to the upper end of the first rotating rod 203, the scattering rods 204 are located above the screening plate 206, and the bottom of the screening tank 201 is communicated with a feeding pipe 208;
as shown in fig. 2 and fig. 4-6, the kneading mechanism 3 comprises a kneading tank 301, two auxiliary components and a kneading motor 304, the kneading tank 301 is fixedly mounted on a second support 103, a feed inlet 302 is formed at the upper end of the kneading tank 301, one end of the feed pipe 208 is communicated with the feed inlet 302, the kneading motor 304 is fixedly mounted at the top of the kneading tank 301, a second rotating rod 312 is rotatably mounted inside the kneading tank 301, the top of the second rotating rod 312 is fixedly connected with the rotating shaft of the kneading motor 304 through a first coupling, the two auxiliary components are symmetrically arranged at two sides of the kneading motor 304, the auxiliary components comprise an auxiliary motor 303 and a third rotating rod 311, the auxiliary motor 303 is fixedly mounted at the top of the kneading tank 301, the third rotating rod 311 is rotatably mounted inside the kneading tank 301 through a bearing, the top of the third rotating rod 311 is fixedly connected with the rotating shaft of the auxiliary motor 303 through a second coupling, the surface of the second rotating rod 312 and the lower surface of the third rotating rod 311 are both fixedly connected with a first helical blade 310, the upper end of the kneading tank 301 is communicated with a water inlet pipe 305, the bottom of the kneading tank 301 is communicated with a discharge pipe 308, and a first electromagnetic valve 309 is fixedly arranged on the discharge pipe 308;
through adopting above-mentioned technical scheme, through screening mechanism 2 with superfine powder agent stirring, beat and spill, the superfine powder agent after breaking up filters through sieve 206, and the superfine powder that filters passes through conveying pipe 208 and gets into kneading jar 301 in, kneads motor 304 cooperation auxiliary assembly and carries out abundant kneading with the material.
As shown in fig. 3 and 8, the first rotating rod 203 is fixedly connected with the scraper 205, the bottom of the scraper 205 is fixedly connected with the bristles 2051, and the bristles 2051 are in contact with the upper surface of the screen plate 206.
Through adopting above-mentioned technical scheme, dwang one 203 drives the scraper blade 205 and rotates, and the cooperation brush hair 2051 is scraped the surface of brush sieve 206 constantly, avoids the phenomenon of bridging to take place.
As shown in fig. 4, a second electromagnetic valve 306 is fixedly installed on the water inlet pipe 305, and a flow sensor 307 is installed on the water inlet pipe 305.
By adopting the above technical scheme, the water inflow can be monitored in real time conveniently through the flow sensor 307.
As shown in fig. 2 to 9, a control panel 4 is fixedly mounted on the upper surface of the base 101, a touch display screen 402 is fixedly mounted on the surface of the control panel 4 in an embedded manner, a PLC controller 401 is fixedly mounted inside the control panel 4, the PLC controller 401 is electrically connected to the touch display screen 402, the flow sensor 307 is electrically connected to a signal input end of the PLC controller 401, and a signal output end of the PLC controller 401 is electrically connected to an electric control end of the stirring motor 202, an electric control end of the kneading motor 304, an electric control end of the auxiliary motor 303, an electric control end of the first electromagnetic valve 309, and an electric control end of the second electromagnetic valve 306, respectively.
Through adopting above-mentioned technical scheme, the user of being convenient for controls the operation of the relevant electrical apparatus in this preparation facilities that contains the fertile granule of gibberellic acid insecticide.
As shown in fig. 3, the lower end of the rotating rod one 203 extends into the feeding pipe 208, and the outer wall of the lower end of the rotating rod one 203 is fixedly connected with a helical blade two 207.
Through adopting above-mentioned technical scheme, drive two 207 rotations of helical blade through dwang one 203, and then avoid when the ejection of compact, the conveying pipe 208 is plugged up to the material.
The inner wall of the kneading tank 301 and the surface of the first helical blade 310 are coated with a Teflon coating.
By adopting the technical scheme, the kneaded materials are prevented from being adhered to the inner wall of the kneading tank 301 and the surface of the first helical blade 310.
For the convenience of understanding the technical solutions of the present invention, the following detailed description will be made on the working principle or the operation mode of the present invention in the practical process.
In practical application, the ground ultrafine powder is poured into the screening tank 201, the stirring motor 202 is started, the breaking rod 204 breaks up the materials, the broken ultrafine powder is screened to the bottom of the screening tank 201 by matching the scraper 205 with the bristles 2051, the materials enter the kneading tank 301 through the feeding pipe 208, the auxiliary motor 303 and the kneading motor 304 are started to enable the auxiliary motor 303 to rotate clockwise, the kneading motor 304 rotates anticlockwise, the second electromagnetic valve 306 is opened to add water into the kneading tank 301, the first helical blade 310 on the second rotating rod 312 stirs the materials at the bottom of the kneading tank 301, the first helical blade 310 on the third rotating rod 311 extrudes the materials above to the lower part of the kneading tank 301, the kneading and stirring are carried out in a reciprocating manner, meanwhile, the friction and stirring between the rising materials and the materials pressing down can be continued, the kneading efficiency and the kneading quality are effectively improved, so that the materials are quickly and fully kneaded in a short time, after the kneading is finished, the auxiliary motor 303 is closed, the kneading motor 304 is controlled to rotate clockwise, the first electromagnetic valve 309 is opened, and the kneaded materials are led out through the discharge pipe 308.
The present invention can be easily implemented by those skilled in the art from the above detailed description. It should be understood, however, that the intention is not to limit the invention to the particular embodiments described. On the basis of the disclosed embodiments, a person skilled in the art can combine different technical features at will, thereby implementing different technical solutions.
Claims (10)
1. A preparation method of gibberellic acid-containing pesticide fertilizer granules is characterized by comprising the following steps:
s1, preparing materials, namely taking 0.01-0.03 wt% of gibberellic acid, 10-20 wt% of urea, 5-15 wt% of monopotassium phosphate, 1-5 wt% of ammonium molybdate, 5-10 wt% of sodium salicylate, 2-4 wt% of adhesive, 1-3 wt% of disintegrant, 1-3 wt% of lubricant and the balance of filler;
s2, mixing, namely putting the raw materials in the step S1 into a grinder for mixing grinding and crushing to prepare superfine powder;
s3, kneading, namely putting the superfine powder agent prepared in the step S2 into a screening tank (201) of a preparation device containing gibberellic acid medical fertilizer granules for scattering and screening, feeding the scattered superfine powder agent into a kneading tank (301) through a feeding pipe (208), and simultaneously adding water accounting for 15-20% of the mass of the superfine powder agent into the kneading tank (301) for fully kneading;
s4, granulating and drying, namely putting the kneaded material in the step S3 into a granulator for granulation;
s5, fluidizing, drying and screening, namely fluidizing the particles prepared in the step S4 by a fluidized bed, and then drying and screening to obtain the granules.
S6, checking and packaging; and (5) inspecting the finished product of the granules obtained in the step S5, and packaging to obtain the finished product.
2. The method of claim 1, wherein the filler in step S1 is selected from one of starch, lactose, dextrin, sugar, sucrose and glucose.
3. The method of claim 1, wherein the binder in step S1 is selected from one of starch slurry, ethyl cellulose and hydroxypropyl cellulose.
4. The method of claim 1, wherein the lubricant in step S1 is selected from one of stearic acid, calcium stearate, talc, sodium lauryl sulfate, and glycine.
5. An apparatus for preparing gibberellic acid-containing fertilizer granules as set forth in claim 1, comprising:
the main body mechanism (1) comprises a base (101), and a first support (102) and a second support (103) are fixedly mounted on the upper surface of the base (101) respectively;
screening mechanism (2), screening mechanism (2) is including screening jar (201), screening jar (201) fixed mounting is in on support (102), the top of screening jar (201) sets up pay-off mouth (210), the inside fixedly connected with annular cell body (209) of screening jar (201), there is sieve (206) through bolt fixed mounting on annular cell body (209), the top fixed mounting of screening jar (201) has agitator motor (202), the inside rotation of screening jar (201) is provided with dwang one (203), the upper end of dwang one (203) is installed through bearing rotation the outside of screening jar (201), the top of dwang one (203) with the pivot fixed connection of agitator motor (202), the upper end fixedly connected with of dwang one (203) breaks up pole (204), break up pole (204) and is located the top of sieve (206), the bottom of the screening tank (201) is communicated with a feeding pipe (208);
the kneading mechanism (3) comprises a kneading tank (301), the kneading tank (301) is fixedly mounted on the second support (103), a feed inlet (302) is formed in the upper end of the kneading tank (301), one end of the feed pipe (208) is communicated with the feed inlet (302), a kneading motor (304) is fixedly mounted at the top of the kneading tank (301), a rotating rod II (312) is rotatably arranged in the kneading tank (301), the top of the rotating rod II (312) is fixedly connected with the rotating shaft of the kneading motor (304) through a first coupler, and an auxiliary assembly is arranged on the kneading tank (301); the two auxiliary components are symmetrically arranged at two sides of the kneading motor (304), the auxiliary assembly comprises an auxiliary motor (303) and a third rotating rod (311), the auxiliary motor (303) is fixedly arranged at the top of the kneading tank (301), the rotating rod III (311) is rotatably arranged inside the kneading tank (301) through a bearing, the top of the rotating rod III (311) is fixedly connected with the rotating shaft of the auxiliary motor (303) through a coupler II, the surface of the second rotating rod (312) and the lower surface of the third rotating rod (311) are both fixedly connected with a first helical blade (310), the upper end of the kneading tank (301) is communicated with a water inlet pipe (305), the bottom of the kneading tank (301) is communicated with a discharge pipe (308), and a first electromagnetic valve (309) is fixedly mounted on the discharge pipe (308).
6. The apparatus for preparing granules containing gibberellic acid fertilizer according to claim 5, wherein a scraper (205) is fixedly connected to the first rotating rod (203), bristles (2051) are fixedly connected to the bottom of the scraper (205), and the bristles (2051) contact with the upper surface of the sieve plate (206).
7. The apparatus for preparing insecticide-fertilizer granules containing gibberellic acid according to claim 5, wherein a second solenoid valve (306) is fixedly installed on the water inlet pipe (305), and a flow sensor (307) is installed on the water inlet pipe (305).
8. The apparatus for preparing gibberellic acid-containing fertilizer granules of claim 7, a control panel (4) is fixedly arranged on the upper surface of the base (101), a touch display screen (402) is embedded and fixed on the surface of the control panel (4), a PLC controller (401) is fixedly arranged in the control panel (4), the PLC controller (401) is electrically connected with the touch display screen (402), the flow sensor (307) is electrically connected with a signal input end of the PLC controller (401), the signal output end of the PLC (401) is respectively and electrically connected with the electric control end of the stirring motor (202), the electric control end of the kneading motor (304), the electric control end of the auxiliary motor (303), the electric control end of the first electromagnetic valve (309) and the electric control end of the second electromagnetic valve (306).
9. The apparatus for preparing insecticide-fertilizer granules containing gibberellic acid according to claim 5, wherein the lower end of the rotating rod (203) extends into the feeding pipe (208), and a second helical blade (207) is fixedly connected to the outer wall of the lower end of the rotating rod (203).
10. The apparatus for preparing gibberellic acid-containing fertilizer granules of claim 3, wherein the inner wall of the kneading tank (301) and the surface of the first helical blade (310) are coated with Teflon coating.
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Cited By (1)
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| CN114751786A (en) * | 2022-05-13 | 2022-07-15 | 广西首控生物科技股份有限公司 | Gibberellic acid-containing pesticide fertilizer |
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| CN114751786A (en) * | 2022-05-13 | 2022-07-15 | 广西首控生物科技股份有限公司 | Gibberellic acid-containing pesticide fertilizer |
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