CN113331219A - Spraying vital qi and preparation method thereof - Google Patents

Spraying vital qi and preparation method thereof Download PDF

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Publication number
CN113331219A
CN113331219A CN202110610412.7A CN202110610412A CN113331219A CN 113331219 A CN113331219 A CN 113331219A CN 202110610412 A CN202110610412 A CN 202110610412A CN 113331219 A CN113331219 A CN 113331219A
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Prior art keywords
parts
extract
raw material
spray
good
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CN202110610412.7A
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林义清
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    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/08—Alkali metal chlorides; Alkaline earth metal chlorides
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N63/00—Biocides, pest repellants or attractants, or plant growth regulators containing microorganisms, viruses, microbial fungi, animals or substances produced by, or obtained from, microorganisms, viruses, microbial fungi or animals, e.g. enzymes or fermentates
    • A01N63/10—Animals; Substances produced thereby or obtained therefrom
    • A01N63/14—Insects
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08—Magnoliopsida [dicotyledons]
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08—Magnoliopsida [dicotyledons]
    • A01N65/32—Ranunculaceae [Buttercup family], e.g. hepatica, hydrastis or goldenseal
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40—Liliopsida [monocotyledons]
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40—Liliopsida [monocotyledons]
    • A01N65/42—Aloeaceae [Aloe family] or Liliaceae [Lily family], e.g. aloe, veratrum, onion, garlic or chives
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40—Liliopsida [monocotyledons]
    • A01N65/44—Poaceae or Gramineae [Grass family], e.g. bamboo, lemon grass or citronella grass
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K33/00—Medicinal preparations containing inorganic active ingredients
    • A61K33/14—Alkali metal chlorides; Alkaline earth metal chlorides
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K35/00—Medicinal preparations containing materials or reaction products thereof with undetermined constitution
    • A61K35/56—Materials from animals other than mammals
    • A61K35/63—Arthropods
    • A61K35/64—Insects, e.g. bees, wasps or fleas
    • A61K35/644—Beeswax; Propolis; Royal jelly; Honey
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/06—Fungi, e.g. yeasts
    • A61K36/07—Basidiomycota, e.g. Cryptococcus
    • A61K36/076—Poria
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
    • A61K36/284—Atractylodes
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/32—Burseraceae (Frankincense family)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/65—Paeoniaceae (Peony family), e.g. Chinese peony
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/71—Ranunculaceae (Buttercup family), e.g. larkspur, hepatica, hydrastis, columbine or goldenseal
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/80—Scrophulariaceae (Figwort family)
    • A61K36/804—Rehmannia
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/88—Liliopsida (monocotyledons)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/88—Liliopsida (monocotyledons)
    • A61K36/884—Alismataceae (Water-plantain family)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/88—Liliopsida (monocotyledons)
    • A61K36/894—Dioscoreaceae (Yam family)
    • A61K36/8945—Dioscorea, e.g. yam, Chinese yam or water yam
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/88—Liliopsida (monocotyledons)
    • A61K36/896—Liliaceae (Lily family), e.g. daylily, plantain lily, Hyacinth or narcissus
    • A61K36/8962—Allium, e.g. garden onion, leek, garlic or chives
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/88—Liliopsida (monocotyledons)
    • A61K36/899—Poaceae or Gramineae (Grass family), e.g. bamboo, corn or sugar cane
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K9/00—Medicinal preparations characterised by special physical form
    • A61K9/10—Dispersions; Emulsions
    • A61K9/12—Aerosols; Foams
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P31/00—Antiinfectives, i.e. antibiotics, antiseptics, chemotherapeutics
    • A61P31/12—Antivirals

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Microbiology (AREA)
  • Chemical & Material Sciences (AREA)
  • Biotechnology (AREA)
  • Mycology (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Medicinal Chemistry (AREA)
  • Animal Behavior & Ethology (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Epidemiology (AREA)
  • Medical Informatics (AREA)
  • Botany (AREA)
  • Alternative & Traditional Medicine (AREA)
  • Zoology (AREA)
  • Agronomy & Crop Science (AREA)
  • Wood Science & Technology (AREA)
  • Plant Pathology (AREA)
  • Environmental Sciences (AREA)
  • Dentistry (AREA)
  • Insects & Arthropods (AREA)
  • Dispersion Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Pest Control & Pesticides (AREA)
  • Virology (AREA)
  • Oncology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Communicable Diseases (AREA)
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  • Medicines Containing Plant Substances (AREA)

Abstract

The invention relates to a spray vital qi and a preparation method thereof, and specifically comprises the following steps: 1) weighing the following raw materials in parts by weight: 1-10 parts of sorghum, 0.01-1 part of olive extract, 0.03-3 parts of yellow yam, 0.01-1 part of prepared rhizome of rehmannia, 3-10 parts of wheat extract, 1-10 parts of garlic extract, 1-10 parts of dragon whiskers extract, 0.01-1 part of rhizoma alismatis extract, 0.01-8 parts of poria cocos, 0.01-3 parts of moutan bark, 0.01-5 parts of honey and 0.01-5 parts of deep sea salt; 2) soaking the raw material extracts in the step 1) for 1 year, and collecting liquid as a raw material for spraying healthy atmosphere. The invention has the advantages that: the raw material proportion is reasonable in design, convenient to manufacture, free of toxicity and good in disinfection effect due to the adoption of a pure natural principle, and has good popularization prospect and value. The invention has the advantages that: the raw material proportion is reasonable in design, convenient to manufacture, free of toxicity and good in disinfection effect due to the adoption of a pure natural principle, and has good popularization prospect and value.

Description

Spraying vital qi and preparation method thereof
Technical Field
The invention relates to the technical field of Chinese character food, in particular to a spray healthy atmosphere and a preparation method thereof.
Background
At present, viruses run across the world, but no gas can expel invisible viruses from invisible air in the world, and no nontoxic spray with good sterilization and disinfection effects exists.
Disclosure of Invention
The present invention aims to provide a spraying healthy atmosphere and a manufacturing method thereof to solve the problems in the background art.
In order to solve the technical problems, the technical scheme provided by the invention is as follows: a preparation method of a spray healthy atmosphere comprises the following steps:
1) weighing the following raw materials in parts by weight: 1-10 parts of sorghum, 0.01-1 part of olive extract, 0.03-3 parts of yellow yam, 0.01-1 part of prepared rhizome of rehmannia, 3-10 parts of wheat extract, 1-10 parts of garlic extract, 1-10 parts of dragon whiskers extract, 0.01-1 part of rhizoma alismatis extract, 0.01-8 parts of poria cocos, 0.01-3 parts of moutan bark, 0.01-5 parts of honey and 0.01-5 parts of deep sea salt;
2) soaking the raw material extracts in the step 1) for 1 year, and collecting liquid as a raw material for spraying healthy atmosphere.
A spray vital qi is prepared by the above preparation method.
The invention has the advantages that: the raw material proportion is reasonable in design, convenient to manufacture, free of toxicity and good in disinfection effect due to the adoption of a pure natural principle, and has good popularization prospect and value.
Detailed Description
The invention is illustrated below by means of specific examples, without being restricted thereto.
Example 1
A preparation method of a spray healthy atmosphere comprises the following steps:
1) weighing the following raw materials in parts by weight: 1 part of sorghum, 1 part of olive extract, 0.03 part of yellow yam, 1 part of prepared rhizome of rehmannia, 3 parts of wheat extract, 10 parts of garlic extract, 1 part of dragon whiskers extract, 1 part of rhizoma alismatis extract, 0.01 part of poria with cocklebur, 3 parts of moutan bark, 0.01 part of honey and 5 parts of deep sea salt;
2) soaking the raw material extracts in the step 1) for 1 year, and collecting liquid as a raw material for spraying healthy atmosphere.
A spray vital qi is prepared by the above preparation method.
Example 2
A preparation method of a spray healthy atmosphere comprises the following steps:
1) weighing the following raw materials in parts by weight: 10 parts of sorghum, 0.01 part of olive extract, 3 parts of yellow yam, 0.01 part of prepared rhizome of rehmannia, 10 parts of wheat extract, 1 part of garlic extract, 10 parts of dragon whisker extract, 0.01 part of rhizoma alismatis extract, 8 parts of poria cocos, 0.01 part of tree peony bark, 5 parts of honey and 0.01 part of deep sea salt;
2) soaking the raw material extracts in the step 1) for 1 year, and collecting liquid as a raw material for spraying healthy atmosphere.
A spray vital qi is prepared by the above preparation method.
Example 3
A preparation method of a spray healthy atmosphere comprises the following steps:
1) weighing the following raw materials in parts by weight: 5 parts of sorghum, 0.5 part of olive extract, 1.5 parts of dioscorea panthaica, 0.5 part of prepared rhizome of rehmannia, 6 parts of wheat extract, 6 parts of garlic extract, 5 parts of dragon whisker extract, 0.5 part of rhizoma alismatis extract, 4 parts of poria with cocklebur, 1.6 parts of moutan bark, 2.5 parts of honey and 2.6 parts of deep sea salt;
2) soaking the raw material extracts in the step 1) for 1 year, and collecting liquid as a raw material for spraying healthy atmosphere.
A spray vital qi is prepared by the above preparation method.
The principle of the invention is as follows: the camphor wood cabinet is free of insects, namely the camphor wood can exert vital energy to keep away from the insects. The gas generated by the invention enters the five sense organs for internal circulation, kills the inflammation virus of the five sense organs for seconds, and the external circulation enters the air space to kill and expel the invisible virus in the air.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.

Claims (2)

1. The preparation method of the spray vital qi is characterized by comprising the following steps:
1) weighing the following raw materials in parts by weight: 1-10 parts of sorghum, 0.01-1 part of olive extract, 0.03-3 parts of yellow yam, 0.01-1 part of prepared rhizome of rehmannia, 3-10 parts of wheat extract, 1-10 parts of garlic extract, 1-10 parts of dragon whiskers extract, 0.01-1 part of rhizoma alismatis extract, 0.01-8 parts of poria cocos, 0.01-3 parts of moutan bark, 0.01-5 parts of honey and 0.01-5 parts of deep sea salt;
2) soaking the raw material extracts in the step 1) for 1 year, and collecting liquid as a raw material for spraying healthy atmosphere.
2. A spray healthy atmosphere, which is produced by the production method according to claim 1.
CN202110610412.7A 2021-06-01 2021-06-01 Spraying vital qi and preparation method thereof Pending CN113331219A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202110610412.7A CN113331219A (en) 2021-06-01 2021-06-01 Spraying vital qi and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202110610412.7A CN113331219A (en) 2021-06-01 2021-06-01 Spraying vital qi and preparation method thereof

Publications (1)

Publication Number Publication Date
CN113331219A true CN113331219A (en) 2021-09-03

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Country Status (1)

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102792976A (en) * 2012-08-16 2012-11-28 张宜东 Herbal disinfectant for space spray disinfection
CN106508897A (en) * 2016-09-06 2017-03-22 广东康绿宝科技实业有限公司 Plant source sterilization aerosol
CN109092037A (en) * 2018-09-21 2018-12-28 湖北煜韩环境科技有限公司 A kind of antibacterial preparation and preparation method thereof that eliminates the unusual smell
CN111249370A (en) * 2020-03-25 2020-06-09 广州依侬化妆品有限公司 Traditional Chinese medicine bacteriostatic spray

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102792976A (en) * 2012-08-16 2012-11-28 张宜东 Herbal disinfectant for space spray disinfection
CN106508897A (en) * 2016-09-06 2017-03-22 广东康绿宝科技实业有限公司 Plant source sterilization aerosol
CN109092037A (en) * 2018-09-21 2018-12-28 湖北煜韩环境科技有限公司 A kind of antibacterial preparation and preparation method thereof that eliminates the unusual smell
CN111249370A (en) * 2020-03-25 2020-06-09 广州依侬化妆品有限公司 Traditional Chinese medicine bacteriostatic spray

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RJ01 Rejection of invention patent application after publication

Application publication date: 20210903

RJ01 Rejection of invention patent application after publication