CN113234483A - 一种含芳烃变压器油基础油的制备方法 - Google Patents
一种含芳烃变压器油基础油的制备方法 Download PDFInfo
- Publication number
- CN113234483A CN113234483A CN202110516678.5A CN202110516678A CN113234483A CN 113234483 A CN113234483 A CN 113234483A CN 202110516678 A CN202110516678 A CN 202110516678A CN 113234483 A CN113234483 A CN 113234483A
- Authority
- CN
- China
- Prior art keywords
- oil
- preparation
- hydrogen
- reaction
- pressure
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000003921 oil Substances 0.000 title claims abstract description 154
- 239000002199 base oil Substances 0.000 title claims abstract description 54
- 150000004945 aromatic hydrocarbons Chemical class 0.000 title claims abstract description 27
- 238000002360 preparation method Methods 0.000 title claims abstract description 21
- 239000003054 catalyst Substances 0.000 claims abstract description 34
- 238000000034 method Methods 0.000 claims abstract description 27
- 238000005984 hydrogenation reaction Methods 0.000 claims abstract description 22
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 42
- 239000001257 hydrogen Substances 0.000 claims description 42
- 229910052739 hydrogen Inorganic materials 0.000 claims description 42
- 238000006243 chemical reaction Methods 0.000 claims description 39
- 238000006317 isomerization reaction Methods 0.000 claims description 20
- 229910052751 metal Inorganic materials 0.000 claims description 20
- 239000002184 metal Substances 0.000 claims description 20
- 238000002156 mixing Methods 0.000 claims description 20
- 230000009471 action Effects 0.000 claims description 15
- 238000004821 distillation Methods 0.000 claims description 15
- 239000002283 diesel fuel Substances 0.000 claims description 14
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical group [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 10
- DDTIGTPWGISMKL-UHFFFAOYSA-N molybdenum nickel Chemical compound [Ni].[Mo] DDTIGTPWGISMKL-UHFFFAOYSA-N 0.000 claims description 8
- 238000005194 fractionation Methods 0.000 claims description 7
- 239000000203 mixture Substances 0.000 claims description 6
- QZYDAIMOJUSSFT-UHFFFAOYSA-N [Co].[Ni].[Mo] Chemical compound [Co].[Ni].[Mo] QZYDAIMOJUSSFT-UHFFFAOYSA-N 0.000 claims description 5
- LCSNMIIKJKUSFF-UHFFFAOYSA-N [Ni].[Mo].[W] Chemical compound [Ni].[Mo].[W] LCSNMIIKJKUSFF-UHFFFAOYSA-N 0.000 claims description 5
- 229910052759 nickel Inorganic materials 0.000 claims description 5
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 claims description 5
- 229910052721 tungsten Inorganic materials 0.000 claims description 5
- 239000010937 tungsten Substances 0.000 claims description 5
- 239000010779 crude oil Substances 0.000 claims description 4
- FJQPNTGARBKARP-UHFFFAOYSA-N molybdenum nickel tungsten Chemical compound [Ni][W][Mo][W] FJQPNTGARBKARP-UHFFFAOYSA-N 0.000 claims description 4
- 239000002904 solvent Substances 0.000 claims description 4
- 238000003763 carbonization Methods 0.000 claims description 3
- 239000002808 molecular sieve Substances 0.000 claims description 3
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 claims description 3
- 238000005292 vacuum distillation Methods 0.000 claims description 3
- 239000011959 amorphous silica alumina Substances 0.000 claims description 2
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims 1
- 229910052593 corundum Inorganic materials 0.000 claims 1
- 229910001845 yogo sapphire Inorganic materials 0.000 claims 1
- 230000003647 oxidation Effects 0.000 abstract description 15
- 238000007254 oxidation reaction Methods 0.000 abstract description 15
- 230000008569 process Effects 0.000 abstract description 10
- 239000000295 fuel oil Substances 0.000 abstract description 5
- 238000005516 engineering process Methods 0.000 abstract description 4
- 230000004048 modification Effects 0.000 abstract description 3
- 238000012986 modification Methods 0.000 abstract description 3
- 230000009467 reduction Effects 0.000 description 10
- 239000002994 raw material Substances 0.000 description 9
- 239000000047 product Substances 0.000 description 7
- 238000007670 refining Methods 0.000 description 7
- HYBBIBNJHNGZAN-UHFFFAOYSA-N furfural Chemical compound O=CC1=CC=CO1 HYBBIBNJHNGZAN-UHFFFAOYSA-N 0.000 description 6
- 230000000881 depressing effect Effects 0.000 description 4
- 239000000446 fuel Substances 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- 239000004927 clay Substances 0.000 description 3
- 239000007789 gas Substances 0.000 description 3
- PAYRUJLWNCNPSJ-UHFFFAOYSA-N Aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 238000002161 passivation Methods 0.000 description 2
- 229910052717 sulfur Inorganic materials 0.000 description 2
- 239000011593 sulfur Substances 0.000 description 2
- 230000009466 transformation Effects 0.000 description 2
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000003463 adsorbent Substances 0.000 description 1
- CSDREXVUYHZDNP-UHFFFAOYSA-N alumanylidynesilicon Chemical compound [Al].[Si] CSDREXVUYHZDNP-UHFFFAOYSA-N 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000008033 biological extinction Effects 0.000 description 1
- 239000000969 carrier Substances 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000000994 depressogenic effect Effects 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000017525 heat dissipation Effects 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 229910052750 molybdenum Inorganic materials 0.000 description 1
- 239000011733 molybdenum Substances 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 238000013112 stability test Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000005987 sulfurization reaction Methods 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 238000004073 vulcanization Methods 0.000 description 1
- 229910003158 γ-Al2O3 Inorganic materials 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G67/00—Treatment of hydrocarbon oils by at least one hydrotreatment process and at least one process for refining in the absence of hydrogen only
- C10G67/02—Treatment of hydrocarbon oils by at least one hydrotreatment process and at least one process for refining in the absence of hydrogen only plural serial stages only
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
Landscapes
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
Abstract
Description
项目 | 减一线和减二线混合油 |
40℃运动黏度,mm<sup>2</sup>/s | 10.8-11.5 |
密度(20℃),kg/m<sup>3</sup> | 896.0-912.0 |
倾点,℃ | -16~-12 |
硫含量,% | 1.74~1.95 |
氮含量,mg/kg | 472~589 |
C<sub>A</sub>,% | 21~23 |
C<sub>N</sub>,% | 39~44 |
Claims (10)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202110516678.5A CN113234483B (zh) | 2021-05-12 | 2021-05-12 | 一种含芳烃变压器油基础油的制备方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202110516678.5A CN113234483B (zh) | 2021-05-12 | 2021-05-12 | 一种含芳烃变压器油基础油的制备方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN113234483A true CN113234483A (zh) | 2021-08-10 |
CN113234483B CN113234483B (zh) | 2023-05-16 |
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CN202110516678.5A Active CN113234483B (zh) | 2021-05-12 | 2021-05-12 | 一种含芳烃变压器油基础油的制备方法 |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN114410347A (zh) * | 2021-12-13 | 2022-04-29 | 中海油天津化工研究设计院有限公司 | 一种环烷基馏分油中压加氢制低芳变压器油的方法 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20110089080A1 (en) * | 2008-06-17 | 2011-04-21 | Sk Lubricants Co., Ltd. | Process for manufacturing high quality naphthenic base oils |
CN102311785A (zh) * | 2010-07-07 | 2012-01-11 | 中国石油化工股份有限公司 | 一种环烷基馏分油加氢生产润滑油基础油的方法 |
CN110540874A (zh) * | 2018-05-29 | 2019-12-06 | 中国石油化工股份有限公司 | 一种环烷基油的加工工艺 |
-
2021
- 2021-05-12 CN CN202110516678.5A patent/CN113234483B/zh active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20110089080A1 (en) * | 2008-06-17 | 2011-04-21 | Sk Lubricants Co., Ltd. | Process for manufacturing high quality naphthenic base oils |
CN102311785A (zh) * | 2010-07-07 | 2012-01-11 | 中国石油化工股份有限公司 | 一种环烷基馏分油加氢生产润滑油基础油的方法 |
CN110540874A (zh) * | 2018-05-29 | 2019-12-06 | 中国石油化工股份有限公司 | 一种环烷基油的加工工艺 |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN114410347A (zh) * | 2021-12-13 | 2022-04-29 | 中海油天津化工研究设计院有限公司 | 一种环烷基馏分油中压加氢制低芳变压器油的方法 |
Also Published As
Publication number | Publication date |
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CN113234483B (zh) | 2023-05-16 |
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TA01 | Transfer of patent application right |
Effective date of registration: 20230421 Address after: 256500 Boxing Economic Development Zone, Shandong, Binzhou Applicant after: SHANDONG CHAMBROAD PETROCHEMICALS Co.,Ltd. Applicant after: SHANDONG CHAMBROAD NEW ENERGY HOLDINGS DEVELOPMENT Co.,Ltd. Address before: 256500 Boxing Economic Development Zone, Shandong, Binzhou Applicant before: SHANDONG CHAMBROAD PETROCHEMICALS Co.,Ltd. Applicant before: Shandong PetroChina Shengli Petrochemical Co.,Ltd. |
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GR01 | Patent grant | ||
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PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A preparation method for aromatic transformer oil base oil Effective date of registration: 20231201 Granted publication date: 20230516 Pledgee: Boxing Shandong rural commercial bank Limited by Share Ltd. Pledgor: SHANDONG CHAMBROAD NEW ENERGY HOLDINGS DEVELOPMENT Co.,Ltd. Registration number: Y2023980069002 |
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