CN113082126A - Preparation method of dampness-removing itching-relieving lotion - Google Patents
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Abstract
The invention discloses a preparation method of a dehumidifying and itching-relieving lotion, which comprises the following steps: (1) mixing fructus Cnidii, fructus Zanthoxyli and rhizoma Atractylodis to form composition A, adding 16 times of water, distilling to extract aromatic water, and separating residue and liquid to obtain medicinal residue and medicinal liquid A; (2) mixing Coptidis rhizoma, cortex Phellodendri, cortex Dictamni Radicis, radix Sophorae Flavescentis, rhizoma Polygoni Cuspidati, herba Violae, Kochiae fructus, herba Polygoni Avicularis and herba Artemisiae Scopariae to form composition B, decocting the residue and composition B in water for 2 times, mixing decoctions, and filtering to obtain liquid medicine B; (3) mixing the liquid medicine A and the liquid medicine B and then concentrating; filtering the concentrated medicinal liquid, adding aromatic water and Borneolum Syntheticum, stirring, adding citric acid to adjust pH, adding purified water to make the total volume of the liquid 1000 parts, mixing, filtering, packaging, and sterilizing. The dampness removing and itching relieving lotion prepared by the invention is yellow brown liquid, has borneol fragrance, and is used for the adjuvant treatment of acute and subacute eczema syndromes of damp-heat or damp-blocking type.
Description
Technical Field
The invention relates to the technical field of dehumidification and itching relieving, and particularly relates to a preparation method of a dehumidification and itching relieving lotion.
Background
Eczema is caused by various internal and external factors, and is a common allergic, non-infectious and allergic inflammatory skin disease of the epidermis and the superficial dermis of the skin. The eczema is mainly developed in four limbs, has the characteristics of symmetry, exudation, pruritus, polymorphism, recurrence and the like in clinical expression, and is refractory to skin pruritus during the onset of the eczema. The main symptoms of eczema include erythema, papules, blisters, etc., which may cause severe itching, local exudation and erosion after scratching, and infection with suppuration, which may cause recurrent attacks.
The records of traditional Chinese medical science and the clinical practice of traditional Chinese medicine prove that the plant extract with the functions of relieving itching and removing dampness has certain functions of relieving or treating eczema symptoms. Chinese plant resources are rich, the history of herbal medicines is long, the plant medicines for relieving itching and removing dampness comprise phellodendron, rhizoma atractylodis, radix sophorae flavescentis, plantain, fructus cnidii, scutellaria baicalensis and coptis chinensis, the plant medicines have the functions of clearing heat and promoting diuresis and cooling blood, and the volatile oil of the plant medicines comprises mint, chrysanthemum, folium artemisiae argyi, clove, agastache rugosus, lavender, honeysuckle and the like, and has the effects of cooling and relieving itching; therefore, a dehumidifying and itching-relieving lotion containing traditional Chinese medicine components is urgently needed.
In view of this, the present patent is applied.
Disclosure of Invention
The invention aims to provide a preparation method of a dehumidifying and itching-relieving lotion with pure traditional Chinese medicine components, the dehumidifying and itching-relieving lotion prepared by the method is a yellow-brown liquid with borneol fragrance, and is used for the adjuvant treatment of acute and subacute eczema syndromes of damp-heat or damp-block type.
In order to achieve the purpose, the invention adopts the following technical scheme:
a preparation method of a dehumidifying and itching-relieving lotion comprises the following steps:
(1) mixing 45 parts of fructus cnidii, 5 parts of pepper and 10 parts of rhizoma atractylodis according to the parts by weight to form a composition A, adding water which is 16 times of the total mass of the composition A, distilling to extract aromatic water, and performing residue-liquid separation after distillation to obtain medicine residue and medicine liquid A;
(2) mixing 10 parts by weight of coptis chinensis, 10 parts by weight of golden cypress, 15 parts by weight of cortex dictamni, 15 parts by weight of radix sophorae flavescentis, 20 parts by weight of polygonum cuspidatum, 20 parts by weight of philippine violet herb, 25 parts by weight of fructus kochiae, 15 parts by weight of polygonum aviculare and 15 parts by weight of oriental wormwood to form a composition B, adding water into the residue obtained after residue-liquid separation in the step (1) and the composition B, decocting for 2 times, 1 hour each time, 12 times of the amount of the residue added for the first time and 8 times of the amount;
(3) mixing the liquid medicine A obtained after the residue-liquid separation in the step (1) with the liquid medicine B obtained in the step (2), and concentrating the mixture until the relative density is 1.04-1.06; standing for 24h, filtering the concentrated liquid medicine, adding the aromatic water and borneol prepared in the step (1) into the filtered liquid medicine, fully stirring, adding citric acid to adjust the pH value to 5, adding purified water to make the total volume of the liquid be 1000 parts, uniformly mixing, standing for 24h, filtering, subpackaging and sterilizing.
Further, the distillation extraction of aromatic water in the step (1) is specifically operated as follows: firstly soaking the composition A0.5h, then introducing steam with the pipeline pressure of 0.2Mpa, carrying out steam distillation, starting cooling water, distilling and collecting 500 parts by total mass of aromatic water, and then stopping distillation.
Further, the extracted aromatic water is stored in a refrigeration house with the temperature of 2-8 ℃.
Further, in the step (2), the composition B and the decoction dregs in the step (1) are soaked for 0.5h before the first decoction.
Further, the concentration in the step (3) adopts a double-effect concentrator, the pressure in the first-effect concentrator is-0.04 to-0.06 MPa, the temperature is 85 +/-5 ℃, the pressure in the second-effect concentrator is-0.06 to-0.08 MPa, and the temperature is 65 +/-5 ℃.
Further, the borneol solution prepared in the step (3) is prepared by adding 4 parts by mass of borneol into 50 parts by mass of 95% ethanol.
Detailed Description
The preparation method of the dehumidifying and itching-relieving lotion provided by the embodiment comprises the following steps:
(1) 225kg of fructus cnidii, 25kg of pepper and 50kg of rhizoma atractylodis are mixed according to the weight part to form a composition A, namely a distilled composition, drinking water with the total mass 16 times of that of the composition A is added, the composition A is soaked for 0.5 hour, then steam with the pipeline pressure of 0.2Mpa is introduced for steam distillation, the steam pressure is less than or equal to 0.12Mpa, cooling water is started, and the distillation is stopped after the total volume of aromatic water collected by distillation is 2500L; storing the extracted aromatic water in a refrigeration house at the temperature of 2-8 ℃, and performing residue-liquid separation after distillation to obtain medicine residue and medicine liquid A; filtering the liquid medicine A by a sieve of 80 meshes, and then filtering the liquid medicine A by a sieve of 200 meshes for later use;
(2) mixing 50kg of coptis chinensis, 50kg of phellodendron, 75kg of cortex dictamni, 75kg of radix sophorae flavescentis, 100kg of polygonum cuspidatum, 100kg of Chinese violet, 125kg of fructus kochiae, 75kg of polygonum aviculare and 75kg of oriental wormwood according to parts by weight to form a composition B, namely a decoction composition, adding water into the residue obtained after residue-liquid separation in the step (1) and the composition B for decocting for 2 times, adding 12 times of water for soaking for 0.5h each time for 1h, then starting decoction, adding 8 times of water for the second time, combining the decoctions, filtering to obtain a liquid medicine B, filtering the liquid medicine B through a 80-mesh sieve, then filtering through a 200-mesh sieve, adding the liquid medicine A in;
(3) mixing the liquid medicine B obtained in the step (2) and the liquid medicine A obtained in the step (1), pumping the mixture into a double-effect concentrator to concentrate the mixture until the relative density is 1.04-1.06, the pressure in a first-effect concentrator is-0.04-0.06 MPa, the temperature is 85 +/-5 ℃, the pressure in a second-effect concentrator is-0.06-0.08 MPa, the temperature is 65 +/-5 ℃, and the extract yield after detection and concentration is 65.0-75.0%; standing for 24h, filtering the concentrated liquid medicine, adding 2500L of aromatic water and 50L of borneol in the step (1) into the filtered liquid medicine, fully stirring, adding 0.5kg of citric acid to adjust the pH value to 5, adding purified water to make the total volume of the liquid be 1000 parts, uniformly mixing, standing for 24h, filtering, subpackaging and sterilizing.
The borneol preparation liquid in the step (3) is prepared by adding 50L of 95% ethanol into 4kg of borneol in parts by mass.
The dehumidifying and itching-relieving lotion prepared in the embodiment is a yellow-brown liquid with borneol fragrance; clear heat, remove dampness, dispel wind and relieve itching. Can be used for the adjuvant treatment of acute and subacute eczema due to damp-heat or damp obstruction. The use method comprises the following steps: the external preparation is applied to the affected part 3-4 times a day; or diluting with water by 10 times and bathing.
The above description is only a preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any modification and replacement based on the technical solution and inventive concept provided by the present invention should be covered within the scope of the present invention.
Claims (6)
1. A preparation method of a dehumidifying and itching-relieving lotion is characterized by comprising the following steps:
(1) mixing 45 parts of fructus cnidii, 5 parts of pepper and 10 parts of rhizoma atractylodis according to the parts by weight to form a composition A, adding water which is 16 times of the total mass of the composition A, distilling to extract aromatic water, and performing residue-liquid separation after distillation to obtain medicine residue and medicine liquid A;
(2) mixing 10 parts by weight of coptis chinensis, 10 parts by weight of golden cypress, 15 parts by weight of cortex dictamni, 15 parts by weight of radix sophorae flavescentis, 20 parts by weight of polygonum cuspidatum, 20 parts by weight of philippine violet herb, 25 parts by weight of fructus kochiae, 15 parts by weight of polygonum aviculare and 15 parts by weight of oriental wormwood to form a composition B, adding water into the residue obtained after residue-liquid separation in the step (1) and the composition B, decocting for 2 times, 1 hour each time, 12 times of the amount of the residue added for the first time and 8 times of the amount;
(3) mixing the liquid medicine A obtained after the residue-liquid separation in the step (1) with the liquid medicine B obtained in the step (2), and concentrating the mixture until the relative density is 1.04-1.06; standing for 24h, filtering the concentrated liquid medicine, adding the aromatic water and borneol prepared in the step (1) into the filtered liquid medicine, fully stirring, adding citric acid to adjust the pH value to 5, adding purified water to make the total volume of the liquid be 1000 parts, uniformly mixing, standing for 24h, filtering, subpackaging and sterilizing.
2. The method for preparing a dehumidifying itching-relieving lotion according to claim 1, wherein: the operation of distilling and extracting the aromatic water in the step (1) is as follows: firstly soaking the composition A0.5h, then introducing steam with the pipeline pressure of 0.2Mpa, carrying out steam distillation, starting cooling water, distilling and collecting 500 parts by total mass of aromatic water, and then stopping distillation.
3. The method for preparing a dehumidifying itching-relieving lotion according to claim 1 or 2, characterized in that: the extracted aromatic water is stored in a refrigeration house with the temperature of 2-8 ℃.
4. The method for preparing a dehumidifying itching-relieving lotion according to claim 1, wherein: soaking the composition B and the decoction dregs in the step (1) for 0.5h before the first decoction in the step (2).
5. The method for preparing a dehumidifying itching-relieving lotion according to claim 1, wherein: and (3) concentrating by adopting a double-effect concentrator, wherein the pressure in the first-effect concentrator is-0.04 to-0.06 MPa, the temperature is 85 +/-5 ℃, the pressure in the second-effect concentrator is-0.06 to-0.08 MPa, and the temperature is 65 +/-5 ℃.
6. The method for preparing a dehumidifying itching-relieving lotion according to claim 1, wherein: the borneol preparation liquid in the step (3) is prepared by adding 4 parts by mass of borneol into 50 parts by mass of 95% ethanol.
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Cited By (1)
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CN114099623A (en) * | 2021-10-14 | 2022-03-01 | 辽宁中医药大学 | Dehumidifying and itching-relieving ointment and preparation method thereof |
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CN1634259A (en) * | 2004-10-28 | 2005-07-06 | 重庆希尔安药业有限公司 | Lotion containing capillary artemisia and wild chrysanthemum flower and its preparing method |
CN1768812A (en) * | 2005-10-24 | 2006-05-10 | 高欲林 | Medicinal composition for removing dampness to relieve itching and its preparation method and uses |
CN101862400A (en) * | 2010-04-09 | 2010-10-20 | 成都天宇联盟医药科技有限责任公司 | Dehumidifying itching-relieving gels and preparation method thereof |
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