CN1634259A - Lotion containing capillary artemisia and wild chrysanthemum flower and its preparing method - Google Patents
Lotion containing capillary artemisia and wild chrysanthemum flower and its preparing method Download PDFInfo
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- CN1634259A CN1634259A CN 200410040957 CN200410040957A CN1634259A CN 1634259 A CN1634259 A CN 1634259A CN 200410040957 CN200410040957 CN 200410040957 CN 200410040957 A CN200410040957 A CN 200410040957A CN 1634259 A CN1634259 A CN 1634259A
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Abstract
The invention provides an oriental wormwood lotion, which is prepared from Chinese medicinal herbs including goldthread root, flavescent sophora root, cnidium fruit, broom cypress fruit, roor of sessile stemona, oriental wormwood, wild chrysanthemum flower, rough gentian, pricklyash peel, mentha, and cape jasmine.
Description
Technical field
The present invention relates to a kind of heat clearing and damp drying, killing parasites for relieving itching of being used for the treatment of.Be applicable to women's profuse leukorrhea, the medicine of diseases such as pudendal pruritus specifically is the washing liquid of feedstock production with the Chinese herbal medicine; The invention still further relates to the preparation method of this washing liquid.
Technical background:
Vaginitis is the commonly encountered diseases and the frequently-occurring disease of gynecological's outpatient service, especially spring, Xia Erji fall ill more, cardinal symptom is a pudendum and vagina is scratched where it itches, redness, pain, leucorrhoea grow in quantity, after the patient is ill, vulva pruritus is on tenterhooks unbearably, influences work and sleep and can infect mutually, fall ill repeatedly, have a strong impact on women's physical and mental health.Similar drug is more in the market, but great majority all contain the sterilization component of Western medicine, and part skin is had serious stimulation.
Technology contents
At problems of the prior art, on the present invention and basis antipruritic, provide a kind of and have no stimulation, Chinese medicine washing liquid safety non-toxic, killing parasites for relieving itching in conjunction with the characteristic of theory of Chinese medical science the hot fiber crops of reusing Pericarpium Zanthoxyli.The present invention prescription is to be guidance with the traditional Chinese medical science " heat clearing and damp drying, wind dispelling are antipruritic, parasite killing, pain relieving " theory.Tradition is thought: pain over the perineum, pudendal pruritus, stranguria with turbid discharge leukorrhagia, skin infection disease such as swell and ache is mainly the heart, spleen, kidney three due to the damp invasion of lower energizer.We on the basis of ancients' medication optional bitter cold, control the heat of all warps.The hot fiber crops of Pericarpium Zanthoxyli are antipruritic, heart channel and the Rhizoma Coptidis of hold concurrently spleen, stomach, liver, gallbladder, large intestine channel is main, and help the merit of heat-clearing and toxic substances removing, be aided with Radix Sophorae Flavescentis, Radix Gentianae with removing pathogen in the heart excess of the liver fire; Assistant is driven heat with Fructus Cnidii, the Fructus Kochiae, the Radix Stemonae, Herba Artemisiae Scopariae etc. with dampness, parasite killing, wind dispelling, and removes the source of scratching where it itches, and removes patient's painful topic.
The present invention's all medicines of writing out a prescription share, heat clearing and damp drying is arranged, the merit that wind dispelling is antipruritic, this medicine is local outer putting on the skin, outer lotion, all medicines affected part of can going directly plays a role, and has more a merit than oral medicine, thereby to reach treatment and prevention men and women's venereal disease infection and by diseases such as caused vaginitis such as mycete, escherichia coli, cervicitis, vulva prurituss.
Another object of the present invention provides the preparation method of this washing liquid.
Solution of the present invention is to be prepared according to aspects such as the physicochemical property of each medicine and main pharmacodynamics.
According to above technical scheme, the mattress flower washing liquid that the present invention relates to is made up of the raw material of following portion rate, wherein:
20～40 parts of Fructus Kochiae 15～30 of 20～40 parts of Fructus Cnidiis of 10～20 parts of Radix Sophorae Flavescentiss of Rhizoma Coptidis
8～20 parts of 5～15 parts of Radix Gentianae of 10～30 parts of Flos Chrysanthemi Indicis of 20～40 portions of Herba Artemisiae Scopariaes of the Radix Stemonae
3～10 parts of 3～10 portions of Fructus Gardeniaes of 3～10 portions of Herba Menthaes of Pericarpium Zanthoxyli
The portion rate of the formula optimization of preparation medicine of the present invention is:
18～25 parts of 25～35 parts of Fructus Kochiae of 25～35 parts of Fructus Cnidiis of 12～18 parts of Radix Sophorae Flavescentiss of Rhizoma Coptidis
10～18 parts of 8～12 parts of Radix Gentianae of 15～25 parts of Flos Chrysanthemi Indicis of 25～35 portions of Herba Artemisiae Scopariaes of the Radix Stemonae
5～8 parts of 5～8 portions of Fructus Gardeniaes of 5～8 portions of Herba Menthaes of Pericarpium Zanthoxyli
The optimum weight umber proportioning of medicine of the present invention is:
30 parts of 20 parts of Radixs Stemonae of 30 parts of Fructus Kochiae of 30 parts of Fructus Cnidiis of 15 parts of Radix Sophorae Flavescentiss of Rhizoma Coptidis
6 parts of 6 portions of Herba Menthaes of 15 portions of Pericarpium Zanthoxylies of 10 parts of Radix Gentianae of 20 parts of Flos Chrysanthemi Indicis of Herba Artemisiae Scopariae
6 parts of Fructus Gardeniaes
The preparation method of the mattress flower washing liquid medicine that the present invention relates to is as follows:
1. Herba Artemisiae Scopariae, Flos Chrysanthemi Indici, Pericarpium Zanthoxyli, Herba Menthae are extracted volatile oil with vapor distillation;
2. distillation back medicinal residues and seven flavors such as medicinal liquid and all the other Rhizoma Coptidis decoct with water 3 times, add 3～8 times of amounts for the first time, decoct 1～3 hour, add 3～6 times of amounts for the second time, decoct 1 hour, add 2～4 times of amounts for the third time, decoct 1 hour;
3. collecting decoction filters, and filtrate is concentrated into the clear paste of relative density 1.05～1.15 (80 ℃), adds equivalent ethanol, stirs evenly, and leaves standstill, and filters filtrate recycling ethanol;
4. filtrate is concentrated into the clear paste that relative density is 1.10～1.30 (80 ℃), adds 1～3 times of amount ethanol again, stirs evenly, and leaves standstill, and filters, and concentrates;
5. add above-mentioned volatile oil.
The specific embodiment
For showing the effect of medicine of the present invention, special from following evidence:
One, to vagina mycete and colibacillary inhibitory action
1. material and method:
Experimental situation: aseptic experiment is indoor to carry out, 18～22 ℃ of room temperatures, relative humidity 60～70%.
For the reagent thing: mattress flower washing liquid is provided by Chongqing Hil'an Pharmaceutical Co., Ltd, and concentration is 100% (being that the 100ml medicinal liquid is equivalent to 100g medical material dry product), is diluted to 1% standby with sterile purified water.PH6.2～6.5。
Culture medium: select the present international M-H agar culture medium of recommending for use.
The antibacterial preparation: mycete is taken from the colpitis mycotica patient who makes a definite diagnosis, and through separating, identifying.Mycete and escherichia coli all are prepared into every milliliter and contain viable bacteria 2 * 10
6Individual (2 * 10
6Individual/ml) standby.
Method: adopt agar dilution.Lotion with 1% adds in the agar culture medium, dilutes with the multiple proportions method, makes " culture medium-medicine " series concentration, pours into then by (25ml/ ware) in the plate that diameter is 9cm, and each drug level prepares the double culture medium.37 ℃ are spent the night, and asepsis growth gets final product each 5 microlitre of inoculating two kinds bacterium liquid in the agar surface of same drug level.24 hours observed results of 37 ℃ of constant temperature culture are MIC with the lowest concentration of drug of complete bacteria growing inhibiting (be less than 3 bacterium colonies for do not grow).
2. result:
Mattress flower washing liquid press the calculating of medical material dry product, is 0.67mg/ml (is 1: 1500 by V/V) to the MIC of vagina mycete; To colibacillary MIC is 0.67mg/ml (is 1: 1500 by V/V).
3. conclusion:
Mattress flower washing liquid has stronger inhibition and killing action to vagina mycete, escherichia coli.
Two, to gonococcal inhibitory action
1. material and method:
Experimental situation: aseptic experiment is indoor to carry out, 10～15 ℃ of room temperatures, relative humidity 60～70%.
For the reagent thing: mattress flower washing liquid is provided by Chongqing Hil'an Pharmaceutical Co., Ltd, and concentration is 100% (being that the 100ml medicinal liquid is equivalent to 100g medical material dry product), is diluted to 1% standby with sterile purified water.PH6.2～6.5。
Culture medium: the GC culture medium of selecting for use U.S. Difco company to produce.
Antibacterial preparation: gonococcus is taken from the gonorrhea patient who makes a definite diagnosis, and through separating, identify, and transferred species counts generation, is prepared into every milliliter and contains viable bacteria 2 * 10
6Individual (2 * 10
6Individual/ml) standby.
Method: adopt agar dilution.Lotion with 1% adds in the GC culture medium, dilutes with the multiple proportions method, makes " culture medium-medicine " series concentration, pours into then by (25ml/ ware) in the plate that diameter is 9cm, and each drug level prepares the double culture medium.37 ℃ are spent the night, and asepsis growth can be inoculated gonococcus liquid 5 microlitres in the media surface with each concentration medicine.36 hours observed results of 37 ℃ of constant temperature culture are with the lowest concentration of drug of complete bacteria growing inhibiting (be less than 3 bacterium colonies for the do not grow) MIC for this lotion.
2. result:
Mattress flower washing liquid is pressed the medical material dry product and is calculated, and is 0.56mg/ml (is 1: 1800 by V/V) to gonococcal MIC.
3. conclusion:
Mattress flower washing liquid has stronger inhibition and killing action to gonococcus.
Three, to the inhibitory action of trichomonas vaginitis
1. material and method:
Experimental situation: aseptic experiment is indoor to carry out, 22～25 ℃ of room temperatures, relative humidity 50～60%.
Supply the reagent thing: mattress flower washing liquid is provided by Chongqing Hil'an Pharmaceutical Co., Ltd, and concentration is 100% (being that the 100ml medicinal liquid is equivalent to 100g medical material dry product), is diluted to 5%, 2.5%, 1.25%, 0.625% serial solution for standby with sterile purified water.PH5.8～6.2。Metronidazole's (positive control medicine), Chongqing the 6th pharmaceutical factory produces.Be diluted to the solution for standby of 40 μ g/ml, 20 μ g/ml, 10 μ g/ml and 5 μ g/ml with sterile purified water.
Culture medium: select for use liver to soak the soup culture medium, by this prepared in laboratory.
Antibacterial preparation: infusorian is taken from the trichomonas vaginitis patient, through separating, and handles with penicillin, streptomycin respectively, removes the roguing bacterium to obtain aseptic culture, and subcultivation is counted generation again, and being prepared into every cubic millimeter, to contain 100 of infusorian standby.
Method: get 18 in 10 * 150 millimeters test tubes, carry out packet numbering.Every Guan Zhongjun adds liver and soaks soup culture fluid 4ml, clog the mouth of pipe with absorbent cotton not, sterilization is 20 minutes under 8 pounds of pressure, be placed in the incubator 37 ℃ 24 hours, prove when aseptic, add aseptic healthy horse serum 1ml in every pipe, add infusorian behind the mixing and prepare liquid 1ml, add medicinal liquid or distilled water 1ml at last, the medicine of each concentration all is prepared into two-tube.Each is managed behind the mixing in 37 ℃ of constant temperature culture 48 hours, takes out back quantitative observation under optical microscope, and each concentration group of medicine and sterile purified water group compare, and obtain protozoon and suppress percentage rate, be minimum but worm concentration with the concentration of 95% above protozoon death.
2. result:
Mattress flower washing liquid press the calculating of medical material dry product, is 1.79mg/ml (is 1: 560 by V/V) to the minimum inhibitory concentration of trichomonas vaginitis.
3. conclusion:
Mattress flower washing liquid has obvious suppression and killing action to trichomonas vaginitis.
To sum up result of the test shows: this washing liquid has obvious suppression and killing action to vagina mycete, escherichia coli, gonococcus and trichomonas vaginitis.
Four, production method embodiment
Embodiment 1.
Take by weighing raw material by following proportioning (by portion rate):
15 parts of 20 parts of Fructus Kochiae of 20 parts of Fructus Cnidiis of 10 parts of Radix Sophorae Flavescentiss of Rhizoma Coptidis
8 parts of 5 parts of Radix Gentianae of 10 parts of Flos Chrysanthemi Indicis of 20 portions of Herba Artemisiae Scopariaes of the Radix Stemonae
3 parts of 3 portions of Fructus Gardeniaes of 3 portions of Herba Menthaes of Pericarpium Zanthoxyli
Production method is as follows:
More than in ten Herba indigoferae Pseudotinctoriae, with Herba Artemisiae Scopariae, Flos Chrysanthemi Indici, Pericarpium Zanthoxyli, Herba Menthae is extracted volatile oil with vapor distillation, and distillation back medicinal residues and seven flavors such as medicinal liquid and all the other Rhizoma Coptidis decoct with water 3 times, for the first time add 3 times of amounts, decocted 1 hour, add 3 times of amounts for the second time, decocted 1 hour, and added 2 times of amounts for the third time, decocted 1 hour, collecting decoction filters, and filtrate is concentrated into the clear paste of relative density 1.08 (80 ℃), add equivalent ethanol, stir evenly, leave standstill, filter, filtrate recycling ethanol, being concentrated into relative density is the clear paste of 1.15 (80 ℃), adds 1.5 times of amount ethanol again, stirs evenly, leave standstill, filter, concentrate, add above-mentioned volatile oil.
Embodiment 2.
Take by weighing raw material by following proportioning (by portion rate):
20 parts of 30 parts of Fructus Kochiae of 30 parts of Fructus Cnidiis of 15 parts of Radix Sophorae Flavescentiss of Rhizoma Coptidis
15 parts of 10 parts of Radix Gentianae of 20 parts of Flos Chrysanthemi Indicis of 30 portions of Herba Artemisiae Scopariaes of the Radix Stemonae
6 parts of 6 portions of Fructus Gardeniaes of 6 portions of Herba Menthaes of Pericarpium Zanthoxyli
Production method is as follows:
More than ten simply, Herba Artemisiae Scopariae, Flos Chrysanthemi Indici, Pericarpium Zanthoxyli, Herba Menthae is extracted volatile oil with vapor distillation, and distillation back medicinal residues and seven flavors such as medicinal liquid and all the other Rhizoma Coptidis decoct with water 3 times, for the first time add 5 times of amounts, decocted 1.5 hours, add 4 times of amounts for the second time, decocted 1 hour, and added 3 times of amounts for the third time, decocted 1 hour, collecting decoction filters, and filtrate is concentrated into the clear paste of relative density 1.08 (80 ℃), add equivalent ethanol, stir evenly, leave standstill, filter, filtrate recycling ethanol, being concentrated into relative density is the clear paste of 1.18 (80 ℃), adds 2 times of amount ethanol again, stirs evenly, leave standstill, filter, concentrate, add above-mentioned volatile oil.
Embodiment 3.
Take by weighing raw material by following proportioning (by portion rate):
30 parts of 40 parts of Fructus Kochiae of 40 parts of Fructus Cnidiis of 20 parts of Radix Sophorae Flavescentiss of Rhizoma Coptidis
20 parts of 15 parts of Radix Gentianae of 30 parts of Flos Chrysanthemi Indicis of 40 portions of Herba Artemisiae Scopariaes of the Radix Stemonae
10 parts of 10 portions of Fructus Gardeniaes of 10 portions of Herba Menthaes of Pericarpium Zanthoxyli
Production method is as follows:
More than ten simply, Herba Artemisiae Scopariae, Flos Chrysanthemi Indici, Pericarpium Zanthoxyli, Herba Menthae is extracted volatile oil with vapor distillation, and distillation back medicinal residues and seven flavors such as medicinal liquid and all the other Rhizoma Coptidis decoct with water 3 times, for the first time add 8 times of amounts, decocted 3 hours, add 6 times of amounts for the second time, decocted 1 hour, and added 4 times of amounts for the third time, decocted 1 hour, collecting decoction filters, and filtrate is concentrated into the clear paste of relative density 1.15 (80 ℃), add equivalent ethanol, stir evenly, leave standstill, filter, filtrate recycling ethanol, being concentrated into relative density is the clear paste of 1.30 (80 ℃), adds 3 times of amount ethanol again, stirs evenly, leave standstill, filter, concentrate, add above-mentioned volatile oil.
Embodiment 4.
Take by weighing raw material by following proportioning (by portion rate):
18 parts of 25 parts of Fructus Kochiae of 25 parts of Fructus Cnidiis of 12 parts of Radix Sophorae Flavescentiss of Rhizoma Coptidis
10 parts of 8 parts of Radix Gentianae of 15 parts of Flos Chrysanthemi Indicis of 25 portions of Herba Artemisiae Scopariaes of the Radix Stemonae
5 parts of 5 portions of Fructus Gardeniaes of 5 portions of Herba Menthaes of Pericarpium Zanthoxyli
Production method is as follows:
More than ten simply, Herba Artemisiae Scopariae, Flos Chrysanthemi Indici, Pericarpium Zanthoxyli, Herba Menthae is extracted volatile oil with vapor distillation, and distillation back medicinal residues and seven flavors such as medicinal liquid and all the other Rhizoma Coptidis decoct with water 3 times, for the first time add 5 times of amounts, decocted 1.5 hours, add 4 times of amounts for the second time, decocted 1 hour, and added 3 times of amounts for the third time, decocted 1 hour, collecting decoction filters, and filtrate is concentrated into the clear paste of relative density 1.08 (80 ℃), add equivalent ethanol, stir evenly, leave standstill, filter, filtrate recycling ethanol, being concentrated into relative density is the clear paste of 1.18 (80 ℃), adds 2 times of amount ethanol again, stirs evenly, leave standstill, filter, concentrate, add above-mentioned volatile oil.
Embodiment 5.
Take by weighing raw material by following proportioning (by portion rate):
25 parts of 35 parts of Fructus Kochiae of 35 parts of Fructus Cnidiis of 18 parts of Radix Sophorae Flavescentiss of Rhizoma Coptidis
18 parts of 12 parts of Radix Gentianae of 25 parts of Flos Chrysanthemi Indicis of 35 portions of Herba Artemisiae Scopariaes of the Radix Stemonae
8 parts of 8 portions of Fructus Gardeniaes of 8 portions of Herba Menthaes of Pericarpium Zanthoxyli
Production method is as follows:
More than ten simply, Herba Artemisiae Scopariae, Flos Chrysanthemi Indici, Pericarpium Zanthoxyli, Herba Menthae is extracted volatile oil with vapor distillation, and distillation back medicinal residues and seven flavors such as medicinal liquid and all the other Rhizoma Coptidis decoct with water 3 times, for the first time add 5 times of amounts, decocted 1.5 hours, add 4 times of amounts for the second time, decocted 1 hour, and added 3 times of amounts for the third time, decocted 1 hour, collecting decoction filters, and filtrate is concentrated into the clear paste of relative density 1.09 (80 ℃), add equivalent ethanol, stir evenly, leave standstill, filter, filtrate recycling ethanol, being concentrated into relative density is the clear paste of 1.19 (80 ℃), adds 3 times of amount ethanol again, stirs evenly, leave standstill, filter, concentrate, add above-mentioned volatile oil.
Claims (4)
1, a kind of mattress flower washing liquid is characterized in that it is the external shampooing agent of being made by the raw material of following portions by weight ratio, wherein:
20～40 parts of Fructus Kochiae 15～30 of 20～40 parts of Fructus Cnidiis of 10～20 parts of Radix Sophorae Flavescentiss of Rhizoma Coptidis
8～20 parts of 5～15 parts of Radix Gentianae of 10～30 parts of Flos Chrysanthemi Indicis of 20～40 portions of Herba Artemisiae Scopariaes of the Radix Stemonae
3～10 parts of 3～10 portions of Fructus Gardeniaes of 3～10 portions of Herba Menthaes of Pericarpium Zanthoxyli.
2, mattress flower washing liquid according to claim 1, wherein the weight proportion of raw material is:
18～25 parts of 25～35 parts of Fructus Kochiae of 25～35 parts of Fructus Cnidiis of 12～18 parts of Radix Sophorae Flavescentiss of Rhizoma Coptidis
10～18 parts of 8～12 parts of Radix Gentianae of 15～25 parts of Flos Chrysanthemi Indicis of 25～35 portions of Herba Artemisiae Scopariaes of the Radix Stemonae
5～8 parts of 5～8 portions of Fructus Gardeniaes of 5～8 portions of Herba Menthaes of Pericarpium Zanthoxyli.
3, mattress flower washing liquid according to claim 1, wherein the weight proportion of raw material is:
30 parts of 20 parts of Radixs Stemonae of 30 parts of Fructus Kochiae of 30 parts of Fructus Cnidiis of 15 parts of Radix Sophorae Flavescentiss of Rhizoma Coptidis
6 parts of 6 portions of Herba Menthaes of 15 portions of Pericarpium Zanthoxylies of 10 parts of Radix Gentianae of 20 parts of Flos Chrysanthemi Indicis of Herba Artemisiae Scopariae
6 parts of Fructus Gardeniaes
4, a kind of preparation method of mattress flower washing liquid according to claim 1 is characterized in that:
(1). Herba Artemisiae Scopariae, Flos Chrysanthemi Indici, Pericarpium Zanthoxyli, Herba Menthae are extracted volatile oil with vapor distillation;
(2). distillation back medicinal residues and seven flavors such as medicinal liquid and all the other Rhizoma Coptidis decoct with water 3 times, add 3～8 times of amounts for the first time, decoct 1～3 hour, add 3～6 times of amounts for the second time, decoct 1 hour, add 2～4 times of amounts for the third time, decoct 1 hour;
(3). collecting decoction, filter, filtrate is concentrated into the clear paste of relative density 1.05～1.15 (80 ℃), adds equivalent ethanol, stirs evenly, and leaves standstill, and filters filtrate recycling ethanol;
(4). filtrate is concentrated into the clear paste that relative density is 1.10～1.30 (80 ℃), adds 1～3 times of amount ethanol again, stirs evenly, and leaves standstill, and filters, and concentrates;
(5). add above-mentioned volatile oil promptly.
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| Application Number | Priority Date | Filing Date | Title |
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| CN 200410040957 CN1289132C (en) | 2004-10-28 | 2004-10-28 | Lotion containing capillary artemisia and wild chrysanthemum flower and its preparing method |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200410040957 CN1289132C (en) | 2004-10-28 | 2004-10-28 | Lotion containing capillary artemisia and wild chrysanthemum flower and its preparing method |
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|---|---|
| CN1634259A true CN1634259A (en) | 2005-07-06 |
| CN1289132C CN1289132C (en) | 2006-12-13 |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101036701B (en) * | 2006-03-17 | 2010-12-29 | 李红梅 | Chinese traditional medicine lotion |
| CN102949647A (en) * | 2012-11-27 | 2013-03-06 | 重庆希尔安药业有限公司 | Medical composition for killing bacteria and relieving itching and preparation method of same |
| CN113082126A (en) * | 2021-04-28 | 2021-07-09 | 四川省通园制药集团有限公司 | Preparation method of dampness-removing itching-relieving lotion |
| CN114272198A (en) * | 2021-12-30 | 2022-04-05 | 重庆希尔安药业有限公司 | Yinhua composition gel liquid and preparation method thereof |
-
2004
- 2004-10-28 CN CN 200410040957 patent/CN1289132C/en active Active
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101036701B (en) * | 2006-03-17 | 2010-12-29 | 李红梅 | Chinese traditional medicine lotion |
| CN102949647A (en) * | 2012-11-27 | 2013-03-06 | 重庆希尔安药业有限公司 | Medical composition for killing bacteria and relieving itching and preparation method of same |
| CN113082126A (en) * | 2021-04-28 | 2021-07-09 | 四川省通园制药集团有限公司 | Preparation method of dampness-removing itching-relieving lotion |
| CN114272198A (en) * | 2021-12-30 | 2022-04-05 | 重庆希尔安药业有限公司 | Yinhua composition gel liquid and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1289132C (en) | 2006-12-13 |
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